Novares and ruetasolv. for the Coatings Industry

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1 Novares and ruetasolv for the Coatings Industry 1

2 Content Novares and ruetasolv : Paint and Varnishes Civil Engineering Heavy-duty Corrosion Protection Cavity Protection Pigment Pastes Application Advantages - Novares and Ruetasolv in EP-Systems - Influence on Potlife, Nonylphenol Replacement - Migration Tendency, Water Repellency - Flexibility Water borne Epoxy Resins Benzylalcohol Replacement Novares and Ruetasolv in PUR Systems - Hardness Development - Water Repellency Company Profile The RÜTGERS group with it s eight international production sites is a global market leader in the field of aromatic chemicals. The company s success is based on flexibility and innovation along with partnership-based cooperation with clients. With some 15 years experience the RÜTGERS group is a competent and reliable partner for all kinds of applications, particularly when it comes to developing innovative products for new challenges.

3 3 on track for Durable surface Protection Our Products Novares resins are thermoplastic hydrocarbon resins based on petrochemical and carbon feedstock. With innovative product solutions and logistical concepts and a high level of flexibility we can adapt to a large range of individual customer needs. Our clients can choose from a broad selection of different resins with a wide range of viscosities and softening points. We can provide these products tailor-made to special requirements. Ruetasolv products are non-reactive modifiers based on naphthalene or biphenyl and are suitable for coatings, casting resins, reactive- and water-borne systems. Delivery Forms solid resins in pastilles supplied in paper bags and big bags molten resin in heatable tankcontainer liquid resins in drums, IBCs or by tanktruck solid resins dissolved in solvents. Our production processes, application technology and marketing system are of course certified according to DIN EN ISO 91, EN ISO 51 and DIN EN ISO 141 quality and environmental standards. CH CH 2 CH 2 CH CH 2 CH 3 C9 Resins Isopropylnaphthalenes Isopropylbiphenyls CH 3 CH 3

4 4 Paints and varnishes Paints and varnishes have a broad range of requirements to cover, with their main purpose being to protect surfaces and provide them with a decorative design. The type of basic binder to be used will depend on the particular application and usage. Using Novares resins as co-binders means that the required technical properties of the coating system can be adjusted and improved to suit your preferences. The practical benefits of Novares resins include: - reduced drying time - improved adhesion - increased solid content - reduced solvent content - increased film durability - improved moisture resistance. Selected Novares resins for paints and varnishes Application Alkyds Acrylates Vinyls Corrosion protection, TD 1 - TD 12 Industrial application, TL 1 - TL 12 Primer TT 1 - TT 12 LF 22, 1 LF 22, 115 Wood protection TK 1 Metal protection CA 8 TNA 8 Road markings, Top coats TM 9 Alkyd Compatibility Novares TD 1 TD 12 TT 1 TT 12 Resin content (%) Fatty acid modified alkyd, Short oil, Low viscosity P P P P P P P P P P P P Fatty acid modified alkyd, Short oil, Air drying P P P P P P P P P P P P Soya bean oil alkyd, Short-/medium oil, Air drying P P P P P P P P P P P P Soya bean oil alkyd, Medium oil, Air drying P P P P P P P P P P P P Linseed oil-/tall oil alkyd, Resin modified P P P P P P P P P P P P Soya bean oil fatty alkyd, Medium oil, Fast drying P P P P P P P P P P P P Fatty acid modified alky, Urethane modified, Air drying P P P P P P P P P P P P Fatty acid modified alkyd (vegetable oil), Short oil, Air- and heat drying P P P P P P P P P P P P P compatible P partially compatible P incompatible

5 5 Civil engineering In the civil engineering industry Novares resins and Ruetasolv products are used in many different applications based on a wide range of reactive resin systems. The scope of uses extends from floor coverings and sealing systems to formulations for roof coatings, wind generator construction, casting resins and pottings for electrical and electronic equipment. Novares resins and Ruetasolv products offer the following advantages in this particular area: - improved resistance to moisture and aqueous media - improved adhesion to substrate - improved intercoat adhesion - reduced brittleness/improved flexibility - rheology control - enhanced wetting of pigments and fillers - increased solid content / reduced solvent content. Selected Novares resins and Ruetasolv products for civil engineering Application Epoxy 2K PUR 1K PUR Polysulfide Silanterm. PUR Floorings, EPX-L, EPX-L5 Ruetasolv L 1 EPX-L EPX-L2 Membranes, LA 3, LA 7 L 8 L 1 L 1 Sealants LC 2, LC 4 Ruetasolv LA 7 TL 1 Ruetasolv LC 25 Roadmarking, Roadconstruction, LA 12 LA 12 Jointing compounds HA 21 HA 21 Sealing systems for EPX-L EPX-L2 L 1 waterproof membranes, LA 7 C 1 L 8 Resin injection LS 5 L 8 Ruetasolv Ruetasolv Ruetasolv Mortars EPX-L2 HA 3 Ruetasolv

6 6 Heavy-duty Corrosion Protection Expensive capital equipment such as industrial facilities, ships and pipelines need reliable protection from corrosion. Anti-corrosion coatings based on reactive resins play a key role in preserving the value and operational reliability of facilities of this type. Novares resins and Ruetasolv make a major contribution to the performance and effectiveness of such coatings. Novares resins and Ruetasolv products help to provide the following technological benefits: - water-repellency and resistance to aqueous media - improved adhesion to substrate - improved intercoat adhesion - reduced brittleness/improved flexibility - rheology management - enhanced pigment and filler wetting. Selected Novares resins and Ruetasolv products for heavy-duty corrosion protection Application Epoxy 2K PUR 1K PUR Target: Hydrophobicity / Flexibility LA 3, LA 7 LA 7 C 1 Marine paints, Off shore, EPX-L, EPX-L5 LA 12 L 1 Industrial corrosion protection LC 15, LC 2, LC4 EPX-L L 8 (pipelines) TL 1 Ruetasolv TL 1 Ruetasolv Ruetasolv Target: Hydrophobicity / Fast physical drying CA 8-1 TL 1 Marine paints, Off shore, TD 1-12 TM 9 Industrial corrosion protection TL 1-12 (pipelines) TN 11 TT 1 TM 9 Corrosion protection, Steel construction for HA 11, HA 21 L 8 L 1 hydraulic engineering LA 7 LA 12 L 8 EPX-L Ruetasolv Ruetasolv TL 1 Ruetasolv

7 7 Cavity Protection In the automotive industry the protection of the bodywork and undersealing plays a key role in extending vehicle life. Applying noise-reducing coatings provide a more pleasant ride. Novares resins provide outstanding properties to the overall system: - high heat resistance - improved resistance to water - high film durability - reduced moisture absorption - high abrasion resistance - reduced noise transmission over a wide range of temperatures and vibration levels. Selected Novares resins for cavity protection Application Recommendation Cavity preservation NL 85 - NL 1 TA 1 TD 1 - TD 11 TT 1 Temporary corrosion protection TK 1 Quenching oils TK 1 Noise insulation LF 22, 1 NL 1 TD 9 TD 12

8 8 Pigment Pastes The excellent wetting properties of Novares special liquid resins and Ruetasolv products make them ideally suited for the preparation of pigment formulations. These liquid resins and modifiers are solvent free and are therefore especially suitable for the formulation of low-voc and VOC-free systems. The low product viscosities also mean that high pigment concentrations are possible. Advantages of using Novares and Ruetasolv in pigment pastes: - good compatibility with epoxy resins, PUR and acrylates - high pigment concentrations - excellent material flow and pumpability - fewer/zero solvents required. Selcted Novares resins and Ruetasolv Products for pigment pastes Application Recommendation Pigment pastes for 1K PUR L 1 L 8 Ruetasolv Pigment pastes for PVC L 1 L 8 Pigment pastes for 2K PUR and EP-systems L 1 EPX-L2 LA 3 / EPX-L5 Ruetasolv

9 9 application advantages Novares and Ruetasolv in epoxy resin systems Epoxy resins are an important product category in corrosionprotection and civil engineering applications. Novares resins and Ruetasolv products are often used in combination with epoxy resins in order to achieve the desired product characteristics. The product properties that can be adjusted by using Novares and Ruetasolv in EP systems are described in detail below. Viscosity reduction Low viscosity modifiers enable the adjustment of requiered processing and product viscosity. Reduce product viscosity improves the surface wetting and the adhesion properties of the coating. viscosity in epoxy resin systems 25 2 [mpa*s / 25 C] unmodified + 2% Ruetasolv DI + 2% Novares L 1 + 2% Novares LA 3 / EPX-L5 Pot life Nonpolar modifiers such as Ruetasolv and Novares L 1 will extend the pot life of the system because of the dilution of the reactive components. The polar OH group has an impact on the pot life - as has been determined by using Novares LA 3. In general an increase in the OH content of the liquid resin results in a reduced pot life of the EP system. The pot life is defined as the period of time from the mixing of the components until the formulation achieves twice the initial viscosity level. Pot life [min] unmodified + 2% Ruetasolv DI + 2% Novares L 1 + 2% Novares LA 3 / EPX-L5

10 1 Pot life as a function of polarity The following graph illustrates how the polarity of the liquid resin, as mentioned above, affects the curing of the epoxy system. 25 Pot life 2 15 [min] 1 5 unmodified LC 5 LC 15 LC 4 LC 6 LS 5 An increase in the OH content of the liquid resin leads to a reduction in pot life. (LC 5 =,5% OH; LC 6 = 6, % OH) Substitute for nonylphenol Novares liquid resin LS 5 has the highest polarity and when used in the EP system it displays a similar accelerative effect during the curing reaction as nonylphenol. Novares LS 5 is therefore recommended as a possible substitute product. The following graphic compares nonylphenol and Novares in terms of their effect on the pot life of the system [min] LS 5 Nonylphenol LA 7 / EPX-L LC 4 N unmodified N + 5 % Modifier N + 1 % Modifier N + 15 % Modifier N + 2 % Modifier

11 11 Migration properties of Novares and Ruetasolv Novares liquid resins and Ruetasolv products are not chemically bound into the epoxy resin structure. When compared directly, polar Novares resins have a lower tendency of migration from the EP system. This can be attributed, among other things, to the OH groups that are attached via hydrogen bridge bonding to the nitrogen from the hardener structure. The following graph compares the migration characteristics of Novares and Ruetasolv. Here the weight loss was measured after 22 days storage of the samples at room temperature. Migration property 1,6 1,4 1,2 1, [%],8,6,4,2 unmodified + 2% Ruetasolv DI + 2% Novares L 1 + 2% Novares LA 3 / EPX-L5 Water repellency and chemical resistance Novares resins and Ruetasolv products have a very hydrophobic, aromatic structure that significantly increases the resistance of civil engineering and corrosion-protection systems to moisture and aqueous media. After 6 months storage in a range of aqueous media the Novares-modified EP system exhibited a much lower weight increase than the unmodified reference system. This means that the modified expoxy systems are showing a much better performance under heavy environmental conditions, e.g. offshore sector, compared with unmodified formulations. Because of their positive characteristics the modifiers generally help extend the life-span of the formulation and also provide increased surface protection. Hydrophobicity 25 2 weight increase [%] 15 1 unmodified N 2% Novares LA 3 / EPX-L5 N 5 Destilled Sulfuric- Acetic- Lactic- Sodium Potassium Ammonia Ethanol Water acid acid acid carbonate hydroxide 1% 1% 1% 1% 1% 2% 1%

12 12 Improved flexibility/plasticisation Novares modifiers and Ruetasolv products reduce the brittleness and hardness of EP systems. The low glass transition temperatures of the modifiers reduce the tensile strength in the system and increase the elongation. The coatings become more flexible and the impact resistance of the formulation is significantly improved. 6 Mechanical properties 5 [MPa] / [%] unmodified 2% Ruetasolv DI 2% Novares L 1 2% Novares LS 5 N Tensile strength [MPa] N Elongation [%]

13 13 Novares in waterborne epoxies During the recent year s waterborne epoxies expanding steadily their market share in civil engineering and corrosion protection application. The main target for this health and environmental friendly development is to avoid solvents without losing the technical performance of the coatings. The liquid resins showing good storage stability after incorporated in the waterborne amine part. Like in conventional epoxy coatings Novares liquid resins are improving also the performance of waterborne epoxy systems. The wide polarity range of the Novares liquid resins offers the possibility to be used in a broad range of different amine systems. Novares liquid resins are clearly improving the chemical resistance of water based epoxies without having a big influence on the hardness of the coating as shown below. Chemical resistance Sulfuric Acid 1% 2% LA 3 1% LS 5 1% L 1 2% LC 4 unmodified Acetic Acid 1% 1% LS 5 unmodified no impact slight irritation 1 first damage 2 blisters 3 big blisters 4 destroyed 5 Ethanol 1% Ammonia 1% 1% LC 4 1% L 1 1% LS 5 unmodified 2% LA 3 2% LC 4 1% L 1 unmodified Buchholz hardness [mm -1 ] without H 2 [mm -1 ] N +1% H 2 [mm -1 ] N +2% H 2 [mm -1 ] N 2 1 un- 1% 2% 1% 2% 1% 2% 1% 2% modified LC 4 L 1 LA 3 LS 5 Modifier

14 14 Benzyl alcohol replacement by ruetasolv products In conventional epoxy systems benzyl alcohol is widely used to reduce the viscosity of the epoxy coating. Due to its relative low boiling point benzyl alcohol has to be counted as a VOC and migrate comparable fast out of the epoxy system into the ambient air. In addition benzyl alcohol tends also to migrate into the water phase if it is used in pipe coatings, off shore- and marine paint application and in this case can contribute to blister forming and reduced corrosion protection. To reduce the migration tendency and improve the water repellency of epoxy coatings we recommend Ruetasolv DI. Depending on the customers or application request the curing speed can be adjusted by Novares LS 5. 3,5 evaporation losses 3, 2,5 weight loss [%] 2, 1,5 1,,5 BZA R DI +1% R DI +3% R DI +1% R DI +5% LS 5 LS 5 LS 5 LS 5 N 1 h 1 C N 2 h 1 C N 3 h 1 C 3 Hardness development viscosity in mpa*s time [min] 3 BZA 3 R-DI +3 % LS 5 3 R-DI +1 % LS 5 3 R-DI +5 % LS 5

15 15 Ruetasolv modified hardeners show a similar viscosity range as the conventionally with benzyl alcohol formulated products. With an increasing amount of Novares LS 5 in Ruetasolv, the viscosity of the hardener will increase accordingly. viscosity 3 25 viscosity in mpa*s / 25 C BZA R DI R DI +1% R DI +3% R DI +1% R DI +5% LS 5 LS 5 LS 5 LS 5

16 16 Novares and ruetasolv in Pur-systems As well as epoxy resins, polyurethanes also are an important reactive resin group with a wide range of applications, including civil engineering and corrosion-protection. The following shows how Novares liquid resins and Ruetasolv products affect a PUR system comprising a polyether polyol cross-linked with an aromatic polyisocyanate based on diphenylmethane diisocyanate. Viscosity reduction Nonpolare modifiers such as Ruetasolv and Novares L 1 will reduce the viscosity, depending on the concentration level, while a rise in the viscosity of the formulation can be observed as the polarity of the liquid resin increases. [mpa*s / 25 C] Ruetasolv DI Novares L 1 Novares LA 3 / Novares LC 4 EPX-L5 viscosity N unmodified N + 18% Modifier N + 33% Modifier Impact on curing time Novares resins and Ruetasolv products dilute the reactive components of the formulation. This will increase the curing time of the systems. 8 Curing time [h] Ruetasolv DI Novares L 1 Novares LA 3 / Novares LC 4 EPX-L5 N unmodified N + 1% Modifier N + 2% Modifier

17 17 Impact on hardness development The unmodified PUR system exhibits the lowest hardness development (König pendulum hardness). The reaction of polyol with isocyanate produces a build-up of molecular structures that increase the viscosity of the system and consequently restrict the mobility of the remaining reactants. By introducing Novares and Ruetasolv the reaction partners remain mobile and a more uniform structure with a higher level of cross-linkage (higher hardness level) is able to develop. Hardness development (polyether polyol) unmodified 3 2% Ruetasolv DI 3 2% Novares L 1 3 2% Novares LA 3 / EPX-L5 3 2% Novares LC 4 3 pendulum hardness König [s] d 2 d 3 d 4 d 5 d 6 d 7 d This behaviour applies specifically to the named reactants and may vary when other polyols are used. In the following graph the polyether polyol has been replaced by a polyester polyol and the impact of the modifier on the curing process can be clearly seen. Hardness development (polyester polyol) Shore D 4 3 unmodified 3 1% Novares L 1 3 1% Novares LA 3 / EPX-L d 3 d 7 d 14 d

18 18 Water repellency and resistance to aqueous media The basic aromatic structure of Novares resins will improve the hydrophobicity both during and after the curing of the PUR system. Test specimens of modified and unmodified PUR systems were stored for 6 months in the below mentioned media and their weight increases were determined. The positive effect of the Novares resins can be clearly seen in the graphs below. The modified systems exhibit a much lower increase in weight than the unmodified reference system. Using Novares modifiers in PUR provides reliable, long-term surface protection. 4,5 4 Weight increase 3,5 3 [%] 2,5 2 1,5 1,5 Dest. Water Sulfuric acid 1% Acetic acid 1% Lactic acid 1% N unmodified N + 2% Novares L 1 N + 2% Novares LA 3 / EPX-L [%] Potassiumhydroxide Sodium carbonate Ammonia Ethanol 1% 1% hydroxid 1% 1% N unmodified N + 2% Novares L 1 N + 2% Novares LA 3 / EPX-L5

19 This information is based on the present level of knowledge. Due to the fact that the individual conditions are beyond our control, no warranty or product liability can be given. Please note that for the time being the EPXL liquid resins are not available in the USA, in Canada and Mexico. The solid resins (LF- types, NL types, Colle, AD) are available in Europe only. 19

20 2 3/213 RÜTGERS Novares GmbH Varziner Strasse 49 D Duisburg Tel Fax

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