Hexcel 8552 AS4 Unidirectional Prepreg at 190 gsm & 35% RC Qualification Material Property Data Report

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1 NATIONAL INSTITUTE FOR AVIATION RESEARCH Wichita State University CAM-RP-- April 4, Revision N/C Hexcel 855 AS4 Unidirectional Prepreg at 9 gsm & 5% RC Qualification Material Property Data Report FAA Special Project Number SP464WI-Q NCAMP Test Report Number: CAM-RP-- N/C April 4, Prepared by: Kristin Marlett Reviewed by: Yeow Ng and John Tomblin Approved By: Ed Hooper (FAA DER) Accepted By: Wichita FAA ACO Office (pending) Page of 78

2 NATIONAL INSTITUTE FOR AVIATION RESEARCH Wichita State University CAM-RP-- April 4, Revision N/C Testing Facility: National Institute for Aviation Research Wichita State University 845 N. Fairmount Wichita, KS REVISIONS: Rev By Date Rev App By Pages Revised or Added N/C Kristin Marlett 4/4/ Yeow Ng ILT Values Updated. Test Summary for UNC, UNC and UNC updated. Raw data for UNC updated. Section FSBS deleted. N/C Kristin Marlett 7// Yeow Ng Processing changed on lamina/laminate sheet; updated CAI individual test chart. Update template section.5.8 N/C Kristin Marlett 8// Yeow Ng Stress Strain/values changed and edits made to Introduction (material spec release date) and other minor chart updates N/C Kristin Marlett 8// Yeow Ng DMA results chart modi fied to on ly include qualification data. Change in Tg also reflected in lamina/laminate sheets. N/C Kristin Marlett 8/6/ Yeow Ng SBS Conditioning Chart added. N/C Kristin Marlett 8/8/ Yeow Ng OHT RTD value edited based on outlier and physical testing values changed for OHT N/C Kristin Marlett 8// Yeow Ng Wet TMA values added N/C Kristin Marlett /7/ Yeow Ng Minor lamina chart template change N/C Kristin Marlett // Yeow Ng Modified SBS Conditioning Chart added. Page of 78

3 TABLE OF CONTENTS. Introduction Scope Symbols Used... 9 Acronyms and Definitions.... NIAR Hexcel Specimen Naming Format....4 References....5 Methodology Process Definition Specimen & Testing Details Tabbing Specimen Dimensions & Test Configuration Test Matrix Physical Testing Environmental Conditioning Non-ambient Testing Normalization Procedures Conformity Material Pedigree Information Test Results Lamina Level Test Summary.... Laminate Level Test Summary.... Individual Test Summaries..... Longitudinal Tension Properties..... Transverse Tension Properties..... Longitudinal Compression Properties Transverse Compression Properties Unnotched Compression Properties Unnotched Tension Properties In-Plane Shear Properties Lamina Short Beam Strength Properties... 9 Page of 78

4 ..9 Unnotched Tension Properties Unnotched Tension Properties Unnotched Tension Properties Unnotched Compression Properties Unnotched Compression Properties Unnotched Compression Properties Laminate Short Beam Strength Properties Open Hole Tension Properties Open Hole Tension Properties Open Hole Tension Properties Filled-Hole Tension Properties Filled-Hole Tension Properties Filled-Hole Tension Properties Open Hole Compression Properties Open Hole Compression Properties Open Hole Compression Properties Filled-Hole Compression Properties Filled-Hole Compression Properties Filled-Hole Compression Properties Single Shear Bearing Properties Single Shear Bearing Properties Single Shear Bearing Properties Compression After Impact Properties Interlaminar Tension Properties Individual Test Charts Longitudinal Tension Properties Transverse Tension Properties Longitudinal Compression Properties Transverse Compression Properties Unnotched Compression Properties Unnotched Tension Properties Lamina Short Beam Strength Properties In-Plane Shear Properties... 7 Page 4 of 78

5 .9 Unnotched Tension Properties Unnotched Tension Properties Unnotched Tension Properties Unnotched Compression Properties Unnotched Compression Properties Unnotched Compression Properties Laminate Short Beam Strength Properties Open Hole Tension Properties Open Hole Tension Properties Open Hole Tension Properties Filled-Hole Tension Properties Filled-Hole Tension Properties Filled-Hole Tension Properties Open Hole Compression Properties Open Hole Compression Properties Open Hole Compression Properties Filled Hole Compression Properties Filled Hole Compression Properties Filled Hole Compression Properties Single Shear Bearing Strength Properties Single Shear Bearing Strength Properties Single Shear Bearing Properties Compression Strength After Impact Properties Interlaminar Tension Properties Raw Data Longitudinal Tension Properties Transverse Tension Properties Longitudinal Compression Properties Transverse Compression Properties Unnotched Compression Properties Unnotched Tension Properties In-Plane Shear Properties Lamina Short Beam Shear Properties Page 5 of 78

6 4.9 Unnotched Tension Properties Unnotched Tension Properties Unnotched Tension Properties Unnotched Compression Properties Unnotched Compression Properties Unnotched Compression Properties Laminate Short Beam Strength Properties Open Hole Tension Properties Open Hole Tension Properties Open Hole Tension Properties Filled-Hole Tension Properties Filled-Hole Tension Properties Filled-Hole Tension Properties Open Hole Compression Properties Open Hole Compression Properties Open Hole Compression Properties Filled-Hole Compression Properties Filled-Hole Compression Properties Filled-Hole Compression Properties Single Shear Bearing Properties Single Shear Bearing Properties Single Shear Bearing Properties Compression Strength After Impact Properties Interlaminar Tension Properties Shear Stress vs. Shear Strain, RTD FLUID SENSITIVITY COMPARISON MOISTURE CONDITIONING CHARTS Longitudinal Tension Thinnest Panel Short Beam Strength- Thickest Panel DMA Results DMA Wet Batch A DMA Dry Batch A TMA Results... 7 Page 6 of 78

7 9. TMA Dry Batch A Results TMA Wet Batch A Results Physical Test Results Deviations List of Tables Table -: Lamina Level Test Matrix... 9 Table -: Laminate Level Test Matrix... Table -: Physical Testing Matrix... Table -: Lamina Summary Data... Table -: Laminate Summary Data... Table 8-: DMA Wet Results Table 8-: DMA Dry Results Table 9-: Dry TMA Results... 7 Table 9-: Wet TMA Results List of Figures Figure -: Specimen Selection Methodology... 4 Figure -: Specimen Traceability Line... 5 Page 7 of 78

8 . Introduction. Scope The test methods and results described in this document are intended to provide basic composite properties essential to most methods of analysis and are consistent with MIL-HDBK-7-F Composite Materials Handbook for Polymer Matrix Composites. This report contains material property data of common usefulness to wide range of projects. The lamina and laminate material property data have been generated with FAA oversight through FAA Special Project Number SP464WI-Q and also meet the requirements of NCAMP Standard Operating Procedure NSP ; the test panels, test specimens, and test setups have been conformed by the FAA and the testing has been witnessed by the FAA. However, the data may not fulfill all the needs of any specific company's programs. Specific properties, environments, laminate architecture, and loading situations that individual companies may require additional testing. The use of NCAMP material and process specifications do not guarantee material or structural performance. Material users should be actively involved in evaluating material performance and quality including, but not limited to, performing regular purchaser quality control tests, performing periodic equivalency/additional testing, participating in material change management activities, conducting statistical process control, and conducting regular supplier audits. The applicability of NCAMP material property data, material allowables, and specifications must be evaluated on caseby-case basis by aircraft companies and certifying agencies. NCAMP assumes no liability whatsoever, expressed or implied, related to the use of the material property data, material allowables, and specifications. This report contains material property data only. Statistical analysis of the data including the calculations of b-basis values is given in a separate report Hexcel 855 AS4 Unidirectional Qualification Statistical Analysis Report panels were fabricated by Cessna Aircraft Company, 58 E Pawnee, Wichita, KS 678. The qualification material was procured to NCAMP Material Specification NMS 8/ Rev - Initial Release February 6, 7. The qualification test panels were cured in accordance with Baseline Cure Cycle (M) of NCAMP Process Specification NPS 88 Rev A Cure Cycle M. The NCAMP Test Plan NTP 8Q was used for this qualification program. Part fabricators that wish to utilize the material property data, allowables, and specifications may be able to do so by demonstrating the capability to reproduce the original material properties; a process known as equivalency. More information about this equivalency process including the test statistics and its limitations can be found in Section 6 of Page 8 of 78

9 DOT/FAA/AR-/9 and Section 8.4. of MIL-HDBK-7-F. The applicability of equivalency process must be evaluated on program-by-program basis by the applicant and certifying agency. The applicant and certifying agency must agree that the equivalency test plan along with the equivalency process described in Section 6 of DOT/FAA/AR-/9 and Section 8.4. of MIL-HDBK-7-F are adequate for the given program. Aircraft companies should not use the data published in this report without specifying NCAMP Material Specification NMS 8/. NMS 8/ have additional requirements that are listed in its prepreg process control document (PCD), fiber specification, fiber PCD, and other raw material specifications and PCDs which impose essential quality controls on the raw materials and raw material manufacturing equipment and processes. Aircraft companies and certifying agencies should assume that the material property data published in this report is not applicable when the material is not procured to NMS 8/. NMS 8/ is a free, publicly available, non-proprietary aerospace industry material specification. The data contained in this report is intended for general distribution to the public, either freely or at a price that does not exceed the cost of reproduction (e.g. printing) and distribution (e.g. postage). Data that is subject to export control regulations, if any, will be made available on a case by case basis through written request to NCAMP.. Symbols Used major Poisson s ratio, tension µε micro-strain c E compressive modulus, Warp / Longitudinal direction t E tensile modulus, Warp / Longitudinal direction c E compressive modulus, Transverse / Fill direction t E tensile modulus, Transverse / Fill direction cu F ultimate compressive strength, Warp / Longitudinal direction tu F ultimate tensile strength, Warp / Longitudinal direction cu F ultimate compressive strength, Transverse / Fill direction tu F ultimate tensile strength, Transverse / Fill direction SBS short beam strength c ν major Poisson s Ratio, compression c ν minor Poisson s Ratio, compression ν t Page 9 of 78

10 s5% strain F s.% F s G in-plane shear strength at 5% strain in-plane shear strength at.% offset in-plane shear modulus Superscripts c cu s su t tu compression compression ultimate shear shear ultimate tension tension ultimate Subscripts axis; Warp / Longitudinal direction (parallel to Warp direction of reinforcement) axis; Transverse / Fill direction (parallel to Fill direction of reinforcement) ; in-plane Acronyms and Definitions ASTM B Basis CV CTD CPT ETD ETW Gr/Ep norm RTD SACMA SRM American Society for Testing and Materials 95% lower confidence limit on the tenth population percentile Coefficient of variation cold temperature dry cured ply thickness elevated temperature dry elevated temperature wet graphite/epoxy normalized room temperature dry Suppliers of Advanced Composite Materials Association SACMA Recommended Method Page of 78

11 Tply thickness divided by the number of plies provides the average ply thickness of the specimen wet specimen with an equilibrium moisture content T, RH temperature, relative humidity Page of 78

12 . NIAR Hexcel Specimen Naming Format NIAR NCAMP HEXCEL SPECIMEN NAMING FORMAT PREPREG LOT #/ BATCH # SUB-PANEL # HPJAA SPECIMEN # CODE M M 5 AH 6 AH 8 AL 9 AL CURE CYCLE CODE CONDITIONING A RTD (7± F) B CTD (-65 F) C ETD (5 F) D ETW (5 F) CODE FSBS Fluid (7 F, 5 F) a, Low Lead b, SAE AMS 69 c, MIL-PRF-566 d,4 MIL-PRF-88 e,5 MIL-PRF-788 f,6 MIL-PRF-699 g,7 Salt Water h,8 Skydrol LD-4 i,9 5% Water w/ 5% Skydrol j,m MEK washing fluid k,n Polypropylene Glycol Deicer l,p Isopropyl Alcohol Deicing r,s Distilled Water A,C Dry t,d 85% Relative Humidity CODE COMPANY CODE MATERIAL SYSTEM CODE TEST METHOD CODE TEST METHOD HO HT HB HE HF HG HW HU HY HJ HL HN HP Hexcel ATK Space Systems Bell Helicopter Boeing Helicopters Cessna Aircraft Company General Atomics Goodrich Gulfstream Aerospace Hawker Beechcraft Israel Aircraft Industries Lockheed Martin Aeronautics Northrop Grumman Spirit AeroSystems P I U (H) AS4 PW Fab Prepreg 8%RC-68 (H) IM7 Uni Prepreg 8% RC-88 (H) AS4 Uni Prepreg 5% RC-8Q J (WT) Warp Tension/ (LT) Longitudinal Tension (D9) Q (SBS) Short Beam Shear (D44) U (FT) Fill Tension/ (TT) Transverse Tension (D9) q (SBS) Laminate Short Beam Shear L (WC) Warp Compression/ (LC) Longitudinal Compression (D664) Z (FC) Fill Compression/ (TC) Transverse Compression (D664) N (IPS) In Plane Shear (D58) A (UNT) Un-notched Tension Layup (D9) (SSB) Single Shear Pin Bearing Layup (D596) B (UNT) Un-notched Tension Layup (D9) (SSB) Single Shear Pin Bearing Layup (D596) C (UNT) Un-notched Tension Layup (D9) (SSB) Single Shear Pin Bearing Layup (D596) W (UNC) Un-notched Compression Layup (D664) P (UNT) Un-notched Tension /9 (D9) X (UNC) Un-notched Compression Layup (D664) R (UNC) Un-notched Compression /9 (D664) Y (UNC) Un-notched Compression Layup (D664) D (OHT) Open Hole Tension Layup (D5766) 4 (FHT) Filled Hole Tension Layup (D674) E (OHT) Open Hole Tension Layup (D5766) 5 (FHT) Filled Hole Tension Layup (D674) F (OHT) Open Hole Tension Layup (D5766) 6 (FHT) Filled Hole Tension Layup (D674) G (OHC) Open Hole Compression (D6484) 7 (FHC) Filled Hole Compression Layup (D6484) H (OHC) Open Hole Compression (D6484) 8 (FHC) Filled Hole Compression Layup (D6484) I (OHC) Open Hole Compression (D6484) 9 (FHC) Filled Hole Compression Layup (D6484) K M T V (CAI) Compression After Impact Layup (SRM-R) (ILT) Interlaminar Tension Layup (D645) (MOL) Material Operating Limit Short Beam Shear (D44) (MOLC) Material Operating Limit Open Hole Compression (D44) Page of 78

13 .4 References ASTM Standards All testing was in accordance with nationally recognized standards, methods and procedures. Specific mechanical property test methods applicable to the test program in this document include: ASTM D44/D44M-(6) Standard Test Method for Short-Beam Strength of Polymer Matrix Composite Materials and Their Laminates ASTM D9/D9M-(6) Standard Test Method for Tensile Properties of Polymer Matrix Composite Materials ASTM D58/D58M-94(7) Standard Test Method for In-Plane Shear Response of Polymer Matrix Composite Materials by Tensile Test of a ± 45º Laminate In-Plane Shear Strength and Modulus ASTM D5766/D5766M-a Standard Test Method for Open Hole Tensile Strength of Polymer Matrix Composite Laminates ASTM D596/D596M-5e Standard Test Method for Bearing Response of Polymer Matrix Composite Laminates ASTM D645-6ae Standard Test Method for Measuring the Curved Beam Strength of a Fiber-Reinforced Polymer-Matrix Composite ASTM D6484/D6484M-4 Standard Test Method for Open-Hole Compressive Strength of Polymer Matrix Composite Laminates ASTM D664/D664M-e Standard Test Method for Determining the Compressive Properties of Polymer Matrix Composite Laminates Using a Combined Loading Compression (CLC) Test Fixture ASTM D674/D674M- Standard Practice for Filled-Hole Tension and Compression Testing of Polymer Matrix Composite Laminates ASTM D76/D76M-5e Standard Test Method for Measuring the Damage Resistance of a Fiber- Reinforced Polymer Matrix Composite to a Drop-Weight Impact Event ASTM D77/D77M-5e Standard Test Method for Compressive Residual Strength Properties of Damaged Polymer Matrix Composite Plates Page of 78

14 .5 Methodology.5. Process Definition For each combination of test, batch and condition, the specimens were selected from minimum two separate panels cured separately as shown in Figure - unless otherwise specified. PER ENVIRONMENTAL CONDITION AND TEST METHOD Material Batch BATCH BATCH BATCH Panel Manufacturing & Independent Cure Process PANEL PANEL PANEL PANEL 4 PANEL 5 PANEL 6 Number of Specimens Required per Test Method & Environment spec. spec. spec. spec. spec. spec. 8 SPECIMENS TOTAL Figure -: Specimen Selection Methodology All panels were fabricated in accordance with NCAMP Process Specification NPS 88 Cure Cycle M. In order to facilitate individual specimen trace ability, individual specimen numbering and/or skewed lines were written or drawn across each sub-panel as shown in Figure -. Page 4 of 78

15 Figure -: Specimen Traceability Line For the single shear bearing tests, the ASTM D596 was used with one of the pairs of specimens replaced by a steel fixture. The configuration is shown in Figure - below. Page 5 of 78

16 Specimen Extensometer shim same thickness as specimen Shim of similar stiffness and equal thickness to specimen. One shim per panel. Shim is held in place with grip pressure only Figure -: Modified ASTM D596 (Single Shear Bearing) Specimen and Loading Arrangement Page 6 of 78

17 .5. Specimen & Testing Details.5.. Tabbing Tabs were used on LT specimens..5.. Specimen Dimensions & Test Configuration For filled-hole and bearing tests, the hole diameter was.5 in in. For filled-hole tension tests, the fasteners were installed to 85±5 in-lb. For filled-hole compression and bearing tests, the fasteners were installed to ±5 in-lb. Fasteners were installed after moisture conditioning. Unless otherwise specified, a tolerance of ±5 F applied to all temperature conditions specified in this document. For filled-hole and bearing tests, the hole diameter was.5 in in. The following fasteners were used: ) NASM 97-4 bolts with MS 84 nuts and MS6 washers for FHT and FHC ) NASM 97-4 bolts with MS 84 nuts and MS6 washers for SSB Page 7 of 78

18 .5. Test Matrix The tables below show the lay-ups and test matrices used for lamina and laminate level testing. Layup Test Type and Direction Property [] 6 [] 4 [9] [9] 4 [/9] S [9//9] 5 [45/-45] S [] 4 ASTM D9 Tension ASTM D664 Compression (Note ) ASTM D9 9 Tension ASTM D664 9 Compression (Note ) ASTM D9 Tension (see Note ) ASTM D664 Compression (see Note & ) ASTM D58 In-Plane Shear ASTM D44 Short Beam Strength, Modulus and Poisson s Ratio Number of Batches x No. of Panels x No. of Specimens Test Temperature/Moisture Condition CTD RTD ETD ETW xx xx xx Modulus xx xx xx xx Strength and Modulus Strength and Modulus Strength and Modulus Strength and Modulus Strength and Modulus xx xx xx xx xx xx xx xx xx xx xx xx xx xx xx xx Strength xx xx xx xx Page 8 of 78

19 Note : Back-to-back strain gages are needed on the first two specimens of each environment. If no buckling is observed, the remaining modulus specimens will require a strain gage on one side of the specimens only. An appropriate extensometer may be used in place of strain gage. u Note : Derive the lamina tensile or compressive strength F as follows plies u F = plies BF P f wh BF = E[ V E + ( V ) E] ( ν E) [ VE + ( V ) E][ V E + ( V ) E] ( ν E) Where BF = Back-out factor obtained using linear classical lamination theory P f = Peak load carried by the test specimen (usually at failure) w = specimen gage width, mm [in.] h = specimen gage thickness, mm [in.] V = fraction of plies in the cross-ply laminate (/ for [/9]ns and / for [9//9]s) E = axial tensile or compressive stiffness of plies, from an average of all batches E = transverse tensile or compressive stiffness of plies, from an average of all ν = major Poisson s ratio of plies, from an average of all batches batches Table -: Lamina Level Test Matrix Table - below summarizes the laminate level tests carried out. The layup angles º, 45º, -45º, and 9º refer to the orientation of the Warp/longitudinal fiber direction. The laminate stacking sequences in this program are not specific to any design. Therefore, careful consideration should be given to the validity of properties derived from this program based on the design specific laminates in a structure to be certified. Page 9 of 78

20 Table - also emphasizes those properties and test condition combinations believed to constitute the worst case, which in general is cold dry for tension and hot wet for compression and other matrix dominated properties. Page of 78

21 (%º/%±45º/%9º) Actual Test Type Test Type and Layup (5) Property Number of Batches x Number of Panels x Number of Test Specimens Test Temperature/Moisture Condition CTD RTD ETW (5/5/5 - QI) ASTM D9 Un-notched Tension Strength & UNT [45//-45/9]S modulus xx xx xx (/8/) ASTM D9 Un-notched Tension Strength & UNT [45/-45//45/-45/9/45/-45/45/-45]S modulus xx xx xx (5/4/) ASTM D9 Un-notched Tension Strength & UNT [/45//9//-45//45//-45]S modulus xx xx xx (5/5/5 - QI) ASTM D664 Un-notched Compression (4) Strength & UNC [45//-45/9]S modulus xx xx (/8/) ASTM D664 Un-notched Compression (4) Strength & UNC [45/-45//45/-45/9/45/-45/45/-45]S modulus xx xx (5/4/) ASTM D664 Un-notched Compression (4) Strength & UNC [45//9//-45//45//-45/]S modulus xx xx ASTM D44 Short Beam (5/5/5 - QI) (specimens may be taken from panels SBS designed for (5/5/5 - QI) CAI) Strength xx xx (5/5/5 - QI) ASTM D5766 Open Hole Tension () OHT [45//-45/9]S Strength xx xx xx (/8/) ASTM D5766 Open Hole Tension () OHT [45/-45//45/-45/9/45/-45/45/-45]S Strength xx xx xx (5/4/) ASTM D5766 Open Hole Tension () OHT [/45//9//-45//45//-45]S Strength xx xx xx (5/5/5 - QI) ASTM D674 Filled Hole Tension () FHT [45//-45/9]S Strength xx xx xx (/8/) ASTM D674 Filled Hole Tension () FHT [45/-45//45/-45/9/45/-45/45/-45]S Strength xx xx xx (5/4/) ASTM D674 Filled Hole Tension () FHT [/45//9//-45//45//-45]S Strength xx xx xx (5/5/5 - QI) ASTM D6484 Open Hole Compression ()(4) OHC [45//-45/9]S Strength xx xx (/8/) ASTM D6484 Open Hole Compression ()(4) OHC [45/-45//45/-45/9/45/-45/45/-45]S Strength xx xx (5/4/) ASTM D6484 Open Hole Compression ()(4) OHC [/45//9//-45//45//-45]S Strength xx xx (5/5/5 - QI) ASTM D6484 Filled Hole Compression () Strength xx xx Page of 78

22 FHC [45//-45/9]S (/8/) ASTM D6484 Filled Hole Compression () FHC [45/-45//45/-45/9/45/-45/45/-45]S Strength xx xx (5/4/) ASTM D6484 Filled Hole Compression () FHC [/45//9//-45//45//-45]S Strength xx xx (5/5/5 - QI) ASTM D596 Single Shear Bearing () (6) Strength & SSB [45//-45/9]S Deformation xx xx (/8/) ASTM D596 Single Shear Bearing () (6) Strength & SSB [45/-45//45/-45/9/45/-45/45/-45]S Deformation xx xx (5/4/) ASTM D596 Single Shear Bearing () (6) Strength & SSB [/45//9//-45//45//-45]S Deformation xx xx (//) ASTM D645 Interlaminar Tension ILT [] Strength xx6 xx6 xx6 ASTM D76 & D77 Compression After (5/5/5 - QI) Impact (5 in.lb/in) (4) CAI [45//-45/9]S Strength xx6 () Open-hole configuration:.5 hole diameter,.5 inch width. () Filled-hole test configuration:.5 diameter, protruding head see section for fastener callout,.5 width. () Single shear bearing test configuration:.5: hole diameter,.5 width, see section for fastener callout, e/d= (4) Back-to-back strain gages needed on the first two specimens of each environment. If no buckling is observed, the remaining modulus specimens will require strain gage on one side of the specimens only. Appropriate extensometer may be used in place of the strain gage. (5) Loading direction is generally along the -degree direction (6) Use modified ASTM D596 per Figure (Note that the layup numbers, and correspond to those designated as quasi isotropic, soft and hard respectively. In addition, the /9 cross-plied laminates used for the unidirectional materials only are designated Layup ). Table -: Laminate Level Test Matrix Page of 78

23 .5.4 Physical Testing The properties in Table - were determined for each panel used for test coupons with the exception of Tg by DMA which were conducted on one laminate per batch from each oven cure conducted where that batch is present. The tests were performed by the National Institute for Aviation Research (NIAR) Composites Laboratory under the supervision of NCAMP. Property Condition/Method (Note ) Min Replicates per panel Cured Ply Thickness ASTM D7-6 All data from mechanical test specimens Laminate Density ASTM D79- Fiber Volume, % by Volume ASTM D7-6 (Note ) Resin Content, % by Weight ASTM D7-6(Note ) Ultrasonic Through Transmission, C-Scan Glass Transition Temperature, Tg by DMA or RDA MIL-HDBK-787A (Note ) Dry and Wet SACMA SRM 8R-94 Dry, Wet (Note 4) Notes : Where the applicable standard allows variations in specimen form or test method, the specific parameters used were specified in the PMC Data Collection Template.. : Method II, except for laminates of materials where actual fiber weight is not known accurately prior to impregnation, as in the case for unidirectional materials. For these materials, in order to verify Method II is accurate, a minimum of samples per batch were tested by Method I, Procedure B. : Five MHz was used for solid laminates. Panels with anomaly were segregated. Microscopy images may have been taken from questionable areas. NCAMP was involved in the review of all the C-scans. 4: Minimum total of 4 dry and 4 wet for each material system. Table -: Physical Testing Matrix Page of 78

24 .5.5 Environmental Conditioning The following tests were performed by the NIAR Composites Laboratory under the supervision of NCAMP. CTD = -65±5 F, dry RTD = 7± F, room temperature dry ETD = 5±5 F, dry ETW = 5±5 F, wet (equilibrium moisture content) Within each test method and test environment, the failure mode was evaluated immediately after each test by an FAA DER. All tested specimens were digitally photographed after each test in order to pictorially document failure modes. Representative photos are included in the CD accompanying this report. For dry testing, specimens were dried at 6 F±5 F for to hours. After drying, specimens were kept in a desiccator until mechanical testing. Alternatively, the specimens may have been left ambient laboratory condition for a maximum of 4 days until mechanical testing (no drying was required if specimens were tested within 4 days from the date they were cured). Ambient laboratory condition is defined as 7 F± F. Since moisture absorption and desorption rate for epoxy is very slow at ambient temperature, there was no requirement to maintain relative humidity levels. For wet conditioning, specimens were dried at 6 F±5 F for to hours before being conditioned to equilibrium at 6 F±5 F and 85% ± 5%. Effective moisture equilibrium was achieved when the average moisture content of the traveler specimen changed by less than.5% for three consecutive readings which are 7 ±.5 days apart and may be expressed by: W i -W i W b where: W i = weight at current time W i = weight at previous time W b = baseline weight prior to conditioning - <.5 Page 4 of 78

25 When representative specimens could not be measured to determine the moisture content (due to size, fastener and tab effects), traveler coupons of at least by by specimen thickness and weighing at least 5 grams were used to establish weight gain measurements. If the specimens or traveler coupons pass the criteria for three consecutive readings which are 7 ±.5 days apart, the specimens were kept in the environmental chamber for up to an additional 6 days. Alternatively, the specimens may have been removed from the environmental chamber and placed in a sealed plastic bag along with a moist cotton towel for a maximum of 4 days until mechanical testing. Strain-gaged specimens were removed from the controlled environment for a maximum of hours for application of gages in ambient laboratory conditions. Page 5 of 78

26 .5.6 Non-ambient Testing The chamber was of adequate size so that all test fixtures and load frame grips were contained within the chamber. For elevated temperature testing, the temperature chamber, test fixture, and grips were preheated to the specified temperature. Each specimen was heated to the required test temperature as verified by a thermocouple in direct contact with and taped to the specimen gage section. The heat-up time of the specimen did not exceed 5 minutes, + minutes after the specimen unless otherwise specified in individual test summary sheets. The test was started reached the test temperature. During the test, the temperature, as measured on the specimen, was within ±5 F of the required test temperature. For subzero temperature testing, each specimen was cooled to the required test temperature as verified by a 5 thermocouple in direct contact with and taped to the specimen gage section. The test started + minutes after the specimen reached the test temperature. During the test, the temperature, as measured on the specimen, was within ±5 F of the required test temperature. Page 6 of 78

27 .5.7 Normalization Procedures Most lamina level tension and compression strength and modulus properties, and all laminate level properties were normalized according to nominal cured ply thickness. Lamina level properties that were not normalized include 9º tensile strength and modulus (unidirectional only), 9º compressive strength and modulus (unidirectional only), in-plane shear strength and modulus, Poisson s ratio, SBS, and ILT. After normalizing, data scatter reduced or remained the same. If data scatter increased significantly after normalizing, the reason was investigated. Wherever properties are normalized, both measured and normalized data were reported. For unidirectional materials the fiber areal weight cannot be measured in advance of impregnation, hence Method I of ASTM D7, utilizing acid digestion, will be used to verify the CPT method in accordance with note () of Table -. Method I Fiber Volume (%vol) is and Method Fiber Volume (%vol) is By comparing Fiber Volume values obtained from Method I and Method II, the values are deemed close enough therefore the FAW is close to the nominal of ~9 gsm. Based on the FAW data from Hexcel (Avg ~9 gsm) and our Method I Phys test data (Avg. void content ~ % except for a panel where it is close to 4%) it is appropriate to use the CPT Method for normalization. The average cured ply thickness of.74 inch has been used as the nominal cured ply thickness (CPT) for normalization purpose. The following normalization formula was used: Normalized Value = Measured Value x Measured CPT / Nominal CPT. Page 7 of 78

28 .5.8 Conformity The -batch qualification panels have been fabricated according to the requirements of the test plan and conformed by the FAA. The test specimens and test setups have also been conformed by the FAA. Testing was witnessed by the FAA. Witnessing was delegated to a DER. Mechanical testing was carried out at the National Institute for Aviation Research, Wichita State University. The test setup and procedures were reviewed by NCAMP IAB and NCAMP staff during a facility audit. FAA conformity inspection records and approvals are included in the CD accompanying this report..5.9 Material Pedigree Information The PMC Data Collection Template includes the material pedigree information required, such as material and batch information, as well as panel fabrication record, environmental conditioning, test equipment, and test procedures. This template in Microsoft Excel file format is included on the CD provided with this report. Page 8 of 78

29 . Test Results Page 9 of 78

30 . Lamina Level Test Summary Prepreg Material: Hexcel Corporation - Hexcel 855 AS4 Unidirectional NMS 8/ Material Specification Fiber: AS4 Unidirectional Resin: Hexcel 855 Hexcel 855 AS4 Unidirectional Tape Lamina Properties Summary Tg(dry): 4.7 F Tg(wet):.4 F Tg METHOD: DMA (SRM 8-94) PROCESSING: NPS 88 Cure Cycle "M" Lot Lot Lot Date of fiber manufacture /4/7 /7/6 //7 Date of testing //9 to 4/6/ Date of resin manufacture /6/7 /5/7 //7 Date of data submittal 4/8/ Date of prepreg manufacture /6/7 /5/7 //7 Date of composite manufacture //7 to //7 LAMINA MECHANICAL PROPERTY SUMMARY Data reported as: Normalized & Measured (Normalized by CPT=.74 inch) CTD Mean RTD Mean ETD Mean ETW Mean Normalized Measured Normalized Measured Normalized Measured Normalized Measured tu F (ksi) from LT from UNT t E (Msi) of LT E (Msi) of UNT ν t F tu (ksi) t E (Msi) of TT F cu (ksi) from UNC c E (Msi) of LC E (Msi) of UNC ν c cu F (ksi) of TC E c (Msi) of TC c ν of TC ν of UNC s5%strain F (ksi) F s.% (ksi) s G (Msi) SBS (ksi) * Derived from cross-ply using back-out factor Table -: Lamina Summary Data Page of 78

31 . Laminate Level Test Summary Prepreg Material: Hexcel Corporation - Hexcel 855 AS4 Unidirectional NMS 8/ Material Specification Fiber: AS4 Unidirectional Resin Hexcel 855 Hexcel 855 AS4 Unitape Laminate Properties Summary Tg(dry): 4.7 F Tg(wet):.4 F Tg METHOD: DMA (SRM 8-94) PROCESSING: NPS88 Cure Cycle "M" Lot Lot Lot Date of fiber manufacture /4/7 /7/6 //7 Date of testing //9 to 4/6/ Date of resin manufacture /6/7 /5/7 //7 Date of data submittal 4/8/ Date of prepreg manufacture /6/7 /5/7 //7 Date of composite manufacture //7 to //7 LAMINATE MECHANICAL PROPERTY SUMMARY Data reported as: Normalized & Measured (Normalized by CPT=.74 inch) Layup: 5/5/5 /8/ 5/4/ Test Condition Normalized Measured Normalized Measured Normalized Measured OHT CTD Strength (ksi) RTD ETW OHC RTD Strength (ksi) ETW UNT CTD Strength (ksi) RTD ETW CTD Modulus (Msi) RTD ETW UNC RTD Strength (ksi) ETW Modulus (Msi) RTD ETW νunc RTD ETW FHT CTD Strength (ksi) RTD ETW FHC RTD Strength (ksi) ETW LSBS RTD Strength (ksi) ETW SSB % offset RTD Strength (ksi) ETW ILT CTD Strength (ksi) RTD ETW CAI Strength (ksi) RTD Table -: Laminate Summary Data Page of 78

32 . Individual Test Summaries.. Longitudinal Tension Properties Material: Hexcel AS4 UNI Resin content:.8 % w eight Comp. density:.59 [g/cc] Fiber volume: % vol Ply count: 6 Tension, -axis Gr/ Ep Hexcel AS4 UNI []6 Test method: ASTM D9- Modulus calculation: to microstrain Normalized by:.74 in. CPT Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code F tu (ksi) E t (Msi) ν 6 F,85% Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum C.V.(%) No. Specimens No. Prepreg Lots 9 4 Mean Minimum Maximum C.V.(%) No. Specimens No. Prepreg Lots Mean No. Specimens No. Prepreg Lots CTD RTD ETW HFUJXXXXB HFUJXXXXA HFUJXXXXD Page of 78

33 .. Transverse Tension Properties Material: Hexcel AS4 UNI Resin content: 4. % w eight Comp. density:.58 [g/cc] Fiber volume: 58.7 % vol Ply count: Tension, -axis Gr/ Ep Hexcel AS4 UNI [9] Test method: ASTM D9- Modulus calculation: to microstrain Normalized by: NA CTD RTD ETW Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code HFUUXXXXB HFUUXXXXA 6 F,85% HFUUXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum F tu E t C.V.(%) (ksi) No. Specimens No. Prepreg Lots Mean Minimum Maximum C.V.(%) (Msi) No. Specimens No. Prepreg Lots Page of 78

34 .. Longitudinal Compression Properties Material: Hexcel AS4 UNI Resin content:.4 % w eight Comp. density.6 [g/cc] Fiber volume: 6.76 % vol Ply count: 4 Compression, -axis Gr/ Ep Hexcel AS4 UNI []4 Test method: ASTM D664- E Modulus calculation: to microstrain Normalized by:.74 in. CPT CTD RTD ETD ETW Test Temperature [ F] Moisture Conditioning dry dry dry equilibrium Equilibrium at T, RH Source code HFULXXXXB HFULXXXXA HFULXXXXC 6 F,85% HFULXXXXD E c ν Normalized Measured Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum C.V.(%) (Msi) No. Specimens No. Prepreg Lots Mean No. Specimens 9 9 No. Prepreg Lots.86 Page 4 of 78

35 ..4 Transverse Compression Properties Material: Hexcel AS4 UNI Resin content:.95 % w eight Comp. density.58 [g/cc] Fiber volume: 6.48 % vol Ply count: 4 Compression, -axis Gr/ Ep Hexcel AS4 UNI [9]4 Test method: ASTM D664- E Modulus calculation: to microstrain Normalized by: NA CTD RTD ETW Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code -65 dry HFUZXXXXB 75 dry HFUZXXXXA 5 equilibrium 6 F,85% HFUZXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum F cu (ksi) E c (Msi) ν c C.V.(%) No. Specimens No. Prepreg Lots 9 9 Mean Minimum Maximum C.V.(%) No. Specimens No. Prepreg Lots Mean No. Specimens No. Prepreg Lots Page 5 of 78

36 ..5 Unnotched Compression Properties Material: Hexcel 855 AS4 Uni Prepreg Resin content:.5 % w eight Comp. density:.59 [g/cc] Fiber volume: 6.8 % vol Ply count: 5 Unnotched Compression Gr/ Ep Hexcel 855 AS4 Uni Prepreg [9//9]5 Test method: ASTM D664- E Modulus calculation: to microstrain Normalized by:.74 in. CPT CTD RTD ETD ETW Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code -65 dry HFURXXXXB 75 F dry HFURXXXXA 5 F dry HFURXXXXC 5 F equilibrium 6 F,85% HFURXXXXD Normalized Measured Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum UNC C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots 5 8 Mean Minimum Maximum UNC C.V.(%) Modulus (Msi) No. Specimens No. Prepreg Lots Mean νunc No. Specimens No. Prepreg Lots Page 6 of 78

37 ..6 Unnotched Tension Properties Material: Hexcel AS4 UNI Resin content: 4.5 % w eight Comp. density:.58 [g/cc] Fiber volume: 58.4 % vol Ply count: 8 Unnotched Tension Gr/ Ep Hexcel AS4 UNI [,9]S Test method: ASTM D9- Modulus calculation: to microstrain Normalized by:.74 in. CPT CTD RTD ETW Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code HFUPXXXXB HFUPXXXXA 6 F,85% HFUPXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum UNT C.V.(%) Strength (ksi) No. Specimens 9 9 No. Prepreg Lots Mean Minimum Maximum UNT C.V.(%) Modulus (Msi) No. Specimens 9 9 No. Prepreg Lots Page 7 of 78

38 ..7 In-Plane Shear Properties Material: Hexcel AS4 UNI Resin content:.7 % w eight Comp. density:.58 [g/cc] Fiber volume: Ply count: % vol Test method: ASTM D58-94 Normalized by: N/A Modulus calculation: to 6 microstrain Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code F s5% strain (ksi) F s.% (ksi) G s (Msi) CTD RTD ETW HFUNXXXXB HFUNXXXXA 6 F,85% HFUNXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum C.V.(%) No. Specimens No. Prepreg Lots 6 9 Mean Minimum Maximum C.V.(%) No. Specimens No. Prepreg Lots 9 Mean Minimum Maximum C.V.(%) No. Specimens No. Prepreg Lots 9 Note: ALL CTD SPECIMENS FAILED BEFORE IT REACHED 5% STRAIN. In-Plane Shear Gr/ Ep Hexcel AS4 UNI [45/-45]s Page 8 of 78

39 ..8 Lamina Short Beam Strength Properties Material: Hexcel AS4 UNI Resin content: 5.65 % w eight Comp. density.58 [g/cc] Fiber volume: 57.8 % vol Ply count: 4 Short Beam Strength Gr/ Ep Hexcel AS4 UNI []4 Test method: ASTM D44- E Normalized by: NA CTD RTD ETD ETW Test Temperature [ F] Moisture Conditioning dry dry dry equilibrium Equilibrium at T, RH 6 F,85% Source code HFUQXXXXB HFUQXXXXA HFUQXXXXC HFUQXXXXD Normalized Measured Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum SBS C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots Page 9 of 78

40 ..9 Unnotched Tension Properties Material: Hexcel AS4 UNI Resin content: 5. % w eight Comp. density:.57 [g/cc] Fiber volume: 57. % vol Ply count: 6 Unnotched Tension Gr/ Ep Hexcel AS4 UNI [45//-45/9]s Test method: ASTM D9- Modulus calculation: to microstrain Normalized by:.74 in. CPT Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code 6 F,85% Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum UNT C.V.(%) Strength (ksi) No. Specimens CTD HFUAXXXXB No. Prepreg Lots Mean Minimum Maximum UNT C.V.(%) Modulus (Msi) No. Specimens No. Prepreg Lots 9 9 RTD HFUAXXXXA ETW HFUAXXXXD 9 9 Page 4 of 78

41 .. Unnotched Tension Properties Material: Hexcel AS4 UNI Resin content: 5.58 % w eight Comp. density:.57 [g/cc] Fiber volume: % vol Ply count: Unnotched Tension Gr/ Ep Hexcel AS4 UNI [45/-45//45/-45/9/45/-45/45/-45]s Test method: ASTM D9- Modulus calculation: to microstrain Normalized by:.74 in. CPT Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code 6 F,85% Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum UNT C.V.(%) Strength (ksi) CTD HFUBXXXXB No. Specimens No. Prepreg Lots Mean Minimum Maximum UNT C.V.(%) Modulus (Msi) No. Specimens No. Prepreg Lots RTD HFUBXXXXA ETW HFUBXXXXD Page 4 of 78

42 .. Unnotched Tension Properties Material: Hexcel AS4 UNI Resin content: 5.65 % w eight Comp. density:.57 [g/cc] Fiber volume: % vol Ply count: Unnotched Tension Gr/ Ep Hexcel AS4 UNI [/45//9//-45//45//-45]s Test method: ASTM D9- Modulus calculation: to microstrain Normalized by:.74 in. CPT Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH Source code 6 F,85% Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum UNT C.V.(%) Strength (ksi) CTD HFUCXXXXB No. Specimens No. Prepreg Lots 8 9 Mean Minimum Maximum UNT C.V.(%) Modulus (Msi) No. Specimens No. Prepreg Lots 9 RTD HFUCXXXXA ETW HFUCXXXXD Page 4 of 78

43 .. Unnotched Compression Properties Material: Hexcel AS4 UNI Resin content: 4.4 % w eight Comp. density:.59 [g/cc] Fiber volume: 58.4 % vol Ply count: 6 Unnotched Compression Gr/ Ep Hexcel AS4 UNI [45//-45/9]S Test method: ASTM D664- E Modulus calculation to microstrain Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code 75 F HFUWXXXXA 5 F equilibrium 6 F,85% HFUWXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum UNC C.V.(%) Strength (ksi) No. Specimens 9 No. Prepreg Lots Mean Minimum Maximum UNC C.V.(%) Modulus (Msi) No. Specimens 9 9 No. Prepreg Lots Mean..4 νunc No. Specimens No. Prepreg Lots 9 8 Page 4 of 78

44 .. Unnotched Compression Properties Material: Hexcel AS4 UNI Resin content: 5.7 % w eight Comp. density:.58 [g/cc] Fiber volume: % vol Ply count: Unnotched Compression Gr/ Ep Hexcel AS4 UNI [45/-45//45/-45/9/45/-45/45/-45]s Test method: ASTM D664- E Modulus calculation: to microstrain Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code 75 F dry HFUXXXXXA 5 F equilibrium 6 F,85% HFUXXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum UNC C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots 9 Mean Minimum Maximum UNC C.V.(%) Modulus (Msi) No. Specimens No. Prepreg Lots Mean νunc No. Specimens No. Prepreg Lots 9 9 Page 44 of 78

45 ..4 Unnotched Compression Properties Material: Hexcel AS4 UNI Resin content: 4.96 % w eight Comp. density:.58 [g/cc] Fiber volume: % vol Ply count: Unnotched Compression Gr/ Ep Hexcel AS4 UNI [45//9//-45//45//-45/]s Test method: ASTM D664- E Modulus calculation: to microstrain Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] 7 F 5 F Moisture Conditioning Equilibrium at T, RH Source code dry HFUYXXXXA equilibrium 6 F,85% HFUYXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum UNC C.V.(%) Strength (ksi) No. Specimens 9 No. Prepreg Lots Mean Minimum Maximum UNC C.V.(%) Modulus (Msi) No. Specimens 9 9 No. Prepreg Lots Mean.4.45 νunc No. Specimens 9 9 No. Prepreg Lots Page 45 of 78

46 ..5 Laminate Short Beam Strength Properties Material: Hexcel AS4 UNI Resin content: See FHC Comp. density: See FHC Fiber volume: See FHC Ply count: 4 Laminate Short Beam Strength Gr/ Ep Hexcel AS4 UNI [45//-45/9]s Test method: ASTM D44- E Normalized by: NA Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code RTD 7 F dry HFUqXXXXA ETW 5 F equilibrium 6 F,85% HFUqXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum LSBS C.V.(%) (ksi) No. Specimens 9 9 No. Prepreg Lots Page 46 of 78

47 ..6 Open Hole Tension Properties Material: Hexcel AS4 UNI Resin content: 5.79 % w eight Comp. density:.57 [g/cc] Fiber volume: % vol Ply count: 6 Open Hole Tension Gr/ Ep Hexcel AS4 UNI [45//-45/9]S Test method: ASTM D5766-a Normalized by:.74 in. CPT CTD RTD ETW Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH 6 F,85% Source code HFUDXXXXB HFUDXXXXA HFUDXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum OHT C.V.(%) Strength (ksi) No. Specimens 9 No. Prepreg Lots Page 47 of 78

48 ..7 Open Hole Tension Properties Material: Hexcel AS4 UNI Resin content:.84 % w eight Comp. density:.59 [g/cc] Fiber volume: % vol Ply count: Open Hole Tension Gr/ Ep Hexcel AS4 UNI [45/-45//45/-45/9/45/-45/45/-45]s Test method: ASTM D5766-a Normalized by:.74 in. CPT CTD RTD ETW Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH 6 F,85% Source code HFUEXXXXB HFUEXXXXA HFUEXXXXD Normalized Measured Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum OHT C.V.(%) Strength (ksi) No. Specimens 9 8 No. Prepreg Lots Page 48 of 78

49 ..8 Open Hole Tension Properties Material: Hexcel AS4 UNI Resin content:. % w eight Comp. density:.58 [g/cc] Fiber volume: 6.4 % vol Ply count: Open Hole Tension Gr/ Ep Hexcel AS4 UNI [/45//9//-45//45//-45]S Test method: ASTM D5766-a Normalized by:.74 in. CPT CTD RTD ETW Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH 6 F,85% Source code HFUFXXXXB HFUFXXXXA HFUFXXXXD Normalized Measured Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum OHT C.V.(%) Strength (ksi) No. Specimens 9 9 No. Prepreg Lots Page 49 of 78

50 ..9 Filled-Hole Tension Properties Material: Hexcel AS4 UNI Resin content: 4.9 % w eight Comp. density:.58 [g/cc] Fiber volume: 58.8 % vol Ply count: 6 Filled Hole Tension Gr/ Ep Hexcel AS4 UNI [45//-45/9]S Test method: ASTM D674- Normalized by:.74 in. CPT CTD RTD ETW Test Temperature [ F] Moisture Conditioning dry dry equilibrium Equilibrium at T, RH 6 F,85% Source code HFU4XXXXB HFU4XXXXA HFU4XXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum FHT C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots Page 5 of 78

51 .. Filled-Hole Tension Properties Material: Hexcel AS4 UNI Resin content:.84 % w eight Comp. density:.58 g/cc Fiber volume: % vol Ply count: Filled Hole Tension Gr/ Ep Hexcel AS4 UNI [45/-45//45/-45/9/45/-45/45/- 45]S Test method: ASTM D674- Normalized by:.74 in. CPT Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code equilibrium 6 F,85% Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum FHT C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots CTD dry HFU5XXXXB RTD dry HFU5XXXXA 9 8 ETW HFU5XXXXD Page 5 of 78

52 .. Filled-Hole Tension Properties Material: Hexcel AS4 UNI Resin content:.69 % w eight Comp. density:.58 [g/cc] Fiber volume: 59.8 % vol Ply count: Filled Hole Tension Gr/ Ep Hexcel AS4 UNI [/45//9//-45//45//-45]S Test method: ASTM D674- Normalized by:.74 in. CPT Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code equilibrium 6 F,85% Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum FHT C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots CTD dry HFU6XXXXB RTD dry HFU6XXXXA 9 9 ETW HFU6XXXXD 9 Page 5 of 78

53 .. Open Hole Compression Properties Material: Hexcel AS4 UNI Resin content: 5.58 % w eight Comp. density.57 [g/cc] Fiber volume: % vol Ply count: 4 Open Hole Compression Gr/ Ep Hexcel AS4 UNI [45//-45/9]s Test method: ASTM D Normalized by:.74 in. CPT Test Temperature [ F] RTD 75 ETW 5 Moisture Conditioning dry equilibrium Equilibrium at T, RH Source code HFUGXXXXA 6 F,85% HFUGXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum OHC C.V.(%) Strength (ksi) No. Specimens 9 No. Prepreg Lots Page 5 of 78

54 .. Open Hole Compression Properties Material: Hexcel AS4 UNI Resin content:.9 % w eight Comp. density.58 [g/cc] Fiber volume: 59.7 % vol Ply count: Open Hole Compression Gr/ Ep Hexcel AS4 UNI [45/-45//45/-45/9/45/-45/45/-45]s Test method: ASTM D Normalized by:.74 in. CPT Test Temperature [ F] RTD 7 ETW 5 Moisture Conditioning dry equilibrium Equilibrium at T, RH Source code HFUHXXXXA 6 F,85% HFUHXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum OHC C.V.(%) Strength (ksi) No. Specimens 9 9 No. Prepreg Lots Page 54 of 78

55 ..4 Open Hole Compression Properties Material: Hexcel AS4 UNI Resin content:.75 % w eight Comp. density.58 [g/cc] Fiber volume: 58.8 % vol Ply count: Open Hole Compression Gr/ Ep Hexcel AS4 UNI [/45//9//-45//45//-45]S Test method: ASTM D Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] 7 5 Moisture Conditioning dry equilibrium Equilibrium at T, RH Source code HFUIXXXXA 6 F,85% HFUIXXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum OHC C.V.(%) Strength (ksi) No. Specimens 9 9 No. Prepreg Lots Page 55 of 78

56 ..5 Filled-Hole Compression Properties Material: Hexcel 855-AS4 Uni Resin content:.4 % w eight Comp. density:.59 [g/cc] Fiber volume: 59.9 % vol Ply count: 4 Filled Hole Compression Gr/ Ep HEXCEL 855-AS4 UNI [45//-45/9]S Test method: ASTM D674- Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] 75 5 Moisture Conditioning Equilibrium at T, RH Source code dry HFU7XXXXA equilibrium 6 F,85% HFU7XXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum FHC C.V.(%) Strength (ksi) No. Specimens 9 9 No. Prepreg Lots Page 56 of 78

57 ..6 Filled-Hole Compression Properties Material: Hexcel 855-AS4 Unidrectional Resin content:.86 % w eight Comp. density:.59 [g/cc] Fiber volume: 6.74 % vol Ply count: Filled Hole Compression Gr/ Ep HEXCEL 855 AS4 UNI [45/-45,,45,-45/9/45/-45/45/-45]S Test method: ASTM D674- Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code 75 dry HFU8XXXXA 5 equilibrium 6 F,85% HFU8XXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum FHC C.V.(%) Strength (ksi) No. Specimens 9 No. Prepreg Lots Page 57 of 78

58 ..7 Filled-Hole Compression Properties Material: HEXCEL 855-AS4 Uni Resin content:.4 % w eight Comp. density:.58 [g/cc] Fiber volume: 6. % vol Ply count: Filled Hole Compression Gr/ Ep HEXCEL 855-AS4 Uni [/45//9//-45//45//-45]S Test method: ASTM D674- Normalized by:.74 in. CPT RTD ETW Test Temperature [ F] 7 5 Moisture Conditioning Equilibrium at T, RH Source code dry HFU9XXXXA equilibrium 6 F,85% HFU9XXXXD Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum FHC C.V.(%) Strength (ksi) No. Specimens 9 No. Prepreg Lots Page 58 of 78

59 ..8 Single Shear Bearing Properties Material: Hexcel AS4 UNI Resin content: 5.66 % w eight Comp. density:.58 [g/cc] Fiber volume: 57. % vol Ply count: 6 Test method: ASTM D596-5 Single Shear Bearing Gr/ Ep Hexcel AS4 UNI [45//-45/9]S Normalized by:.74 RTD ETW Test Temperature [ F] Moisture Conditioning 75 dry 5 equilibrium Equilibrium at T, RH Source code HFUXXXXA 6 F,85% HFUXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum SSB C.V.(%) % offset Strength (ksi) No. Specimens 9 No. Prepreg Lots Physical testing results only available from one batch and cure cycle. Page 59 of 78

60 ..9 Single Shear Bearing Properties Material: Hexcel AS4 UNI Resin content: 4.9 % vol Comp. density:.58 [g/cc] Fiber volume: 58.9 % vol Ply count: Test method: ASTM D596-5 Single Shear Bearing Gr/ Ep Hexcel AS4 UNI [45/-45//45/-45/9/45/-45/45/-45]S Normalized by:.74 RTD ETW Test Temperature [ F] Moisture Conditioning 75 dry 5 equilibrium Equilibrium at T, RH Source code HFUXXXXA 6 F,85% HFUXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum SSB C.V.(%) % offset Strength (ksi) No. Specimens 9 5 No. Prepreg Lots Page 6 of 78

61 .. Single Shear Bearing Properties Material: Hexcel AS4 UNI Resin content: 4.94 % vol Comp. density:.58 [g/cc] Fiber volume: 58.6 % vol Ply count: Test method: ASTM D596-5 Single Shear Bearing Gr/ Ep Hexcel AS4 UNI [/45//9//-45//45//-45]S Normalized by:.74 RTD ETW Test Temperature [ F] Moisture Conditioning 75 dry 5 equilibrium Equilibrium at T, RH Source code HFUXXXXA 6 F,85% HFUXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum SSB C.V.(%) % offset Strength (ksi) No. Specimens 9 No. Prepreg Lots Page 6 of 78

62 .. Compression After Impact Properties Material: Hexcel 855-AS4 Unidrectional Resin content: 5.9 % w eight Comp. density:.57 [g/cc] Fiber volume: % vol Ply count: 4 Compression After Impact Gr/ Ep Hexcel 855-AS4 Uni [45,,-45,9]s Test method: ASTM D76 & D77 Normalized by:.74 in. CPT RTD Test Temperature [ F] Moisture Conditioning 75 dry Equilibrium at T, RH Source code HFUKXXXXA Normalized Measured Normalized Measured Normalized Measured Mean Minimum Maximum CAI C.V.(%).57.5 Strength (ksi) No. Specimens No. Prepreg Lots 7 Page 6 of 78

63 .. Interlaminar Tension Properties Material: Hexcel AS4 UNI Resin content: 6.8 % w eight Comp. density:.58 [g/cc] Fiber volume: 56.5 % vol Ply count: Interlaminar Tension Gr/ Ep Hexcel AS4 UNI [] Test method: ASTM D E Normalized by: NA CTD RTD ETW Test Temperature [ F] Moisture Conditioning Equilibrium at T, RH Source code dry HFUMXXXXB dry HFUMXXXXA equilibrium 6 F,85% HFUMXXXXD Normalized Measured Normalized Measured Mean Minimum Maximum ILT C.V.(%) Strength (ksi) No. Specimens No. Prepreg Lots Physical testing w as not conducted on ILT Page 6 of 78

64

65 . Individual Test Charts These charts combine all three batches of data and plot the minimum and maximum modulus and strength range based on the test temperature. Page 65 of 78

66 . Longitudinal Tension Properties Longitudinal Tension Strength(LT) -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 4 Strength (ksi) Temperature ( F) 5. Longitudinal Tension Modulus(LT) -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet. Modulus (Msi) Temperature ( F) Page 66 of 78

67 . Transverse Tension Properties Transverse Tension Strength(TT) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F).5 Transverse Tension Modulus(TT) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet. Modulus (Msi) Temperature ( F) Page 67 of 78

68 . Longitudinal Compression Properties Longitudinal Compression Modulus(LC) -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 5.. Modulus (Msi) Temperature ( F) Page 68 of 78

69 .4 Transverse Compression Properties 6 Transverse Compression Strength (TC) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet 4 Strength (ksi) Temperature ( F).5 Transverse Compression Modulus (TC) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet. Modulus (Msi) Temperature ( F) Page 69 of 78

70 .5 Unnotched Compression Properties Laminate Unnotched Compression (UNC) Strength -- Normalized HEXCEL AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Laminate Unnotched Compression (UNC) Modulus -- Normalized HEXCEL AS4 UNI Conditioning X Dry O Wet 5 Modulus (Msi) Temperature ( F) Page 7 of 78

71 .6 Unnotched Tension Properties Laminate Unnotched Tension (UNT) Strength -- Normalized 8 HEXCEL AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F). Laminate Unnotched Tension (UNT) Modulus -- Normalized HEXCEL AS4 UNI Conditioning X Dry O Wet. Modulus (Msi) Temperature ( F) Page 7 of 78

72 .7 Lamina Short Beam Strength Properties 5. Lamina Short Beam Strength (SBS) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet. Strength (ksi) Temperature ( F) Page 7 of 78

73 .8 In-Plane Shear Properties In-Plane Shear (IPS) Strength -- Measured At 5% Strain Hexcel AS4 UNI 5. Conditioning X Dry O Wet Temperature ( F). In-Plane Shear (IPS) Modulus -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet Modulus (Msi) Strength (ksi) Temperature ( F) Page 7 of 78

74 .9 Unnotched Tension Properties Laminate Unnotched Tension (UNT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Laminate Unnotched Tension (UNT) Modulus -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Modulus (Msi) Temperature ( F) Page 74 of 78

75 . Unnotched Tension Properties Laminate Unnotched Tension (UNT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Laminate Unnotched Tension (UNT) Modulus -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Modulus (Msi) Temperature ( F) Page 75 of 78

76 . Unnotched Tension Properties Laminate Unnotched Tension (UNT) Strength -- Normalized Hexcel AS4 UNI 8 Conditioning X Dry O Wet 6 4 Strength (ksi) Temperature ( F) Laminate Unnotched Tension (UNT) Modulus -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 4.. Modulus (Msi) Temperature ( F) Page 76 of 78

77 . Unnotched Compression Properties Laminate Unnotched Compression (UNC) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 Strength (ksi) Temperature ( F) Laminate Unnotched Compression (UNC) Modulus -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 Modulus (Msi) Temperature ( F) Page 77 of 78

78 . Unnotched Compression Properties Laminate Unnotched Compression (UNC) Strength -- Normalized Hexcel AS4 UNI 8 Strength (ksi) 6 4 Conditioning X Dry O Wet Temperature ( F) Laminate Unnotched Compression (UNC) Modulus -- Normalized Hexcel AS4 UNI 8 Modulus (Msi) 5 Conditioning X Dry O Wet Temperature ( F) Page 78 of 78

79 .4 Unnotched Compression Properties 6 Laminate Unnotched Compression (UNC) Strength -- Normalized Hexcel AS4 UNI 4 Strength (ksi) Conditioning X Dry O Wet Temperature ( F) Laminate Unnotched Compression (UNC) Modulus -- Normalized Hexcel AS4 UNI Modulus (Msi) 8 5 Conditioning X Dry O Wet Temperature ( F) Page 79 of 78

80 .5 Laminate Short Beam Strength Properties 4... Laminate Short Beam Strength (LSBS) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 8 of 78

81 .6 Open Hole Tension Properties Open Hole Tension (OHT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 6 Strength (ksi) Temperature ( F) Page 8 of 78

82 .7 Open Hole Tension Properties 8 Open Hole Tension (OHT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 6 Strength (ksi) Temperature ( F) Page 8 of 78

83 .8 Open Hole Tension Properties Open Hole Tension (OHT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 Strength (ksi) Temperature ( F) Page 8 of 78

84 .9 Filled-Hole Tension Properties Filled Hole Tension (FHT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 6 Strength (ksi) Temperature ( F) Page 84 of 78

85 . Filled-Hole Tension Properties Filled Hole Tension (FHT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 8 6 Strength (ksi) Temperature ( F) Page 85 of 78

86 . Filled-Hole Tension Properties Filled Hole Tension (FHT) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 86 of 78

87 . Open Hole Compression Properties Open Hole Compression (OHC) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 6 5 Strength (ksi) Temperature ( F) Page 87 of 78

88 . Open Hole Compression Properties Open Hole Compression (OHC) Strength -- Normalized Hexcel AS4 UNI 6 Conditioning X Dry O Wet 5 Strength (ksi) Temperature ( F) Page 88 of 78

89 .4 Open Hole Compression Properties Open Hole Compression (OHC) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 89 of 78

90 .5 Filled Hole Compression Properties Filled Hole Compression (FHC) Strength -- Normalized HEXCEL 855 AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 9 of 78

91 .6 Filled Hole Compression Properties 8 Filled Hole Compression (FHC) Strength -- Normalized HEXCEL 855 AS4 UNI Conditioning X Dry O Wet 6 Strength (ksi) Temperature ( F) Page 9 of 78

92 .7 Filled Hole Compression Properties Filled Hole Compression (FHC) Strength -- Normalized HEXCEL 855-AS4 Uni Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 9 of 78

93 .8 Single Shear Bearing Strength Properties Single Shear Bearing Strength (SSB), % Offset -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 4 Strength (ksi) Temperature ( F) Page 9 of 78

94 .9 Single Shear Bearing Strength Properties Single Shear Bearing Strength (SSB), % Offset -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 94 of 78

95 . Single Shear Bearing Properties Single Shear Bearing Strength (SSB), % Offset -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet Strength (ksi) Temperature ( F) Page 95 of 78

96 . Compression Strength After Impact Properties Compression After Impact (CAI) Strength -- Normalized Hexcel AS4 UNI Conditioning X Dry O Wet 5 Strength (ksi) Temperature ( F) Page 96 of 78

97 . Interlaminar Tension Properties Laminate Curved Beam Strength (CBS) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet CBS (lb) Temperature ( F) 4. Laminate Interlaminar Tension Strength (ILT) -- Measured Hexcel AS4 UNI Conditioning X Dry O Wet Interlaminar Tension Strength (ksi) Temperature ( F) Page 97 of 78

98 4. Raw Data 4. Longitudinal Tension Properties Longitudinal Tension Properties (LT) -- (CTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUJA6B A M SGM HFUJA7B A M SGM HFUJA8B A M XGM HFUJA9B A M XGM HFUJA6B A M SGM HFUJA7B A M SGM HFUJA8B A M XGM HFUJB6B B M SGM HFUJB7B B M XGM HFUJB8B B M XGM HFUJB6B B M SGM HFUJB7B B M SGM HFUJB8B B M XGM HFUJC6B C M SGM HFUJC7B C M XGM HFUJC8B C M XGM HFUJC6B C M XGM HFUJC7B C M SGM HFUJC8B C M XGM Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec Number of Spec. 9 9 Page 98 of 78

99 Longitudinal Tension Properties (LT) -- (CTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Longitudinal Tension Strength [ksi] Longitudinal Tension Properties (LT) -- (CTD) Normalized Modulus Hexcel AS4 UNI Longitudinal Tension Modulus [Msi] Page 99 of 78

100 LogitudinalTension Properties (LT) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUJAA A M SGM HFUJAA A M SGM/LGM HFUJAA A M XGM HFUJA4A A M SGM HFUJAA A M SGM HFUJAA A M SGM HFUJA4A A M SGM HFUJBA B M SGM HFUJBA B M XGM HFUJB4A B M XGM HFUJBA B M SGM HFUJBA B M SGM/LGM HFUJBA B M SGM HFUJB4A B M XGM HFUJCA C M SGM HFUJCA C M SGM HFUJCA C M SGM HFUJC4A C M SGM HFUJCA C M SGM HFUJCA C M LGM/SGM HFUJCA C M SGM Average Average norm Standard Dev ` Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. Number of Spec. Page of 78

101 Longitudinal Tension Properties (LT) -- (RTD) Normalized Strength Hexcel AS4 UNI Longitudinal Tension Strength [ksi] Longitudinal Tension Properties (LT) -- (RTD) Normalized Modulus Hexcel AS4 UNI Longitudinal Tension Modulus [Msi] Page of 78

102 Longitudinal Tension Properties (LT) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUJABD A M SGM HFUJACD A M SGM HFUJADD A M SGM HFUJAED A M SGM HFUJABD A M SGM HFUJACD A M SGM HFUJADD A M SGM HFUJBBD B M SGM HFUJBCD B M SGM HFUJBDD B M SGM HFUJBED B M SGM HFUJBFD B M SGM HFUJBBD B M SGM HFUJBCD B M SGM HFUJBDD B M SGM HFUJBED B M SGM HFUJBFD B M SGM HFUJCBD C M SGM HFUJCCD C M SGM HFUJCDD C M SGM HFUJCED C M SGM HFUJCBD C M SGM HFUJCCD C M SGM HFUJCDD C M SGM Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm.6. Min Min Max Max Number of Spec Number of Spec. 4 4 Page of 78

103 Longitudinal Tension Properties (LT) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Longitudinal Tension Strength [ksi] Longitudinal Tension Properties (LT) -- (ETW) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Longitudinal Tension Modulus [Msi] Page of 78

104 4. Transverse Tension Properties Transverse Tension Properties (TT) -- (CTD) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] HFUUA6B A M LAT/LAB.7 HFUUA7B A M LAT/LAB.7 HFUUA8B A M LGM.7 HFUUA9B A M LGM.7 HFUUAAB A M LGM.7 HFUUA6B A M LAB.7 HFUUA7B A M LAT.74 HFUUA8B A M LAT.74 HFUUB6B B M LAT.7 HFUUB7B B M LAB.7 HFUUB8B B M LAB.7 HFUUB6B B M LAT.7 HFUUB7B B M LAB.7 HFUUB8B B M LAT.7 HFUUA5A A M LGM.7 HFUUA4A A M LAT.7 HFUUA5A A M LAT.7 HFUUB4A B M LAB.7 Batch C specimens were removed due to deep scratches on the specimens * Last four specimens were originally from RTD but were tested as CTD Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec Page 4 of 78

105 Transverse Tension Properties (TT) -- (CTD) Measured Strength Hexcel AS4 UNI Transverse Tension Strength [ksi] Transverse Tension Properties (TT) -- (CTD) Measured Modulus Hexcel AS4 UNI Transverse Tension Modulus [Msi] Page 5 of 78

106 Transverse Tension Properties (TT) -- (RTD) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] HFUUAA A M LGM.7 HFUUAA A M LGM.7 HFUUAA A M LAT.7 HFUUA4A A M LWB.7 HFUUAA A M LWB.7 HFUUAA A M LAB.74 HFUUAA A M LAB.7 HFUUBA B M LGM.69 HFUUBA B M LAB.7 HFUUBA B M LAB.7 HFUUBA B M LGM.68 HFUUBA B M LAB.7 HFUUBA B M LAB.74 HFUUB4B B M LGM.7 HFUUB5B B M LAT.7 HFUUB9B B M LAB.7 HFUUBAB B M LAB.67 Batch C specimens were removed due to deep scratches on the specimens Last four specimens were originally designated for CTD but were tested in RTD. Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec Page 6 of 78

107 Transverse Tension Properties (TT) -- (RTD) Measured Strength Hexcel AS4 UNI 4 Transverse Tension Strength [ksi] Transverse Tension Properties (TT) -- (RTD) Measured Modulus Hexcel AS4 UNI Transverse Tension Modulus [Msi] Page 7 of 78

108 Transverse Tension Properties (TT) -- (ETW) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] HFUUABD A M LGM.7 HFUUACD A M LGM.7 HFUUADD A M LGM.79 HFUUAED A M LGM.79 HFUUABD A M LGM.79 HFUUACD A M LGM.78 HFUUADD A M LGM.75 HFUUBBD B M LGM.78 HFUUBCD B M LGM.79 HFUUBDD B M LGM.77 HFUUBBD B M LGM.77 HFUUBCD B M LGM.76 HFUUBDD B M LGM.7 HFUUCBD C M LGM.667 HFUUCCD C M LGM.78 HFUUCDD C M LGM.7 HFUUCBD C M LGM.79 HFUUCCD C M LGM.748 HFUUCDD C M LGM.74 Average Standard Dev...6 Coeff. of Var. [%] Min Max Number of Spec Page 8 of 78

109 Transverse Tension Properties (TT) -- (ETW) Measured Strength Hexcel AS4 UNI Transverse Tension Strength [ksi] Transverse Tension Properties (TT) -- (ETW) Measured Modulus Hexcel AS4 UNI Transverse Tension Modulus [Msi] Page 9 of 78

110 4. Longitudinal Compression Properties Longitudinal Compression Properties (LC) -- (CTD) Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Modulus norm Number Batch # Cycle Lot # # [Msi] Ratio Thickn. [in] Laminate Mode [in] [Msi] HFULA6B A M NO FAILURE HFULA7B A M NO FAILURE HFULA8B A M NO FAILURE HFULA9B A M NO FAILURE.74.5 HFULAAB A M NO FAILURE HFULA5B A M NO FAILURE HFULA6B A M NO FAILURE HFULA7B A M NO FAILURE HFULB5B B M NO FAILURE HFULB6B B M NO FAILURE HFULB7B B M NO FAILURE.7.47 HFULB5B B M NO FAILURE HFULB6B B M NO FAILURE.7 4. HFULB7B B M NO FAILURE.7 5. HFULC5B C M NO FAILURE HFULC6B C M NO FAILURE HFULC7B C M NO FAILURE.7 6. HFULC5B C M NO FAILURE HFULC6B C M NO FAILURE HFULC7B C M NO FAILURE Average Average norm Standard Dev Standard Dev. norm.44 Coeff. of Var. [%] Coeff. of Var. [%] norm 9. Min Min Max Max Number of Spec. Number of Spec. Page of 78

111 Longitudinal Compression Properties (LC) -- (CTD) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Longitudinal Compression Modulus [Msi] Page of 78

112 Longitudinal Compression Properties (LC) -- (RTD) Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Modulus norm Number Batch # Cycle Lot # # [Msi] Ratio Thickn. [in] Laminate Mode [in] [Msi] HFULAA A M NO FAILURE HFULAA A M NO FAILURE HFULA4A A M NO FAILURE HFULA5A A M NO FAILURE HFULAA A M NO FAILURE HFULAA A M NO FAILURE HFULAA A M NO FAILURE HFULBA B M NO FAILURE HFULBA B M NO FAILURE HFULB4A B M NO FAILURE HFULBA B M NO FAILURE HFULBA B M NO FAILURE HFULBA B M NO FAILURE HFULCA C M NO FAILURE HFULCA C M NO FAILURE HFULCA C M NO FAILURE HFULCA C M NO FAILURE HFULCA C M NO FAILURE HFULCA C M NO FAILURE Average Average norm Standard Dev..4.4 Standard Dev. norm.84 Coeff. of Var. [%].58. Coeff. of Var. [%] norm 5. Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 Page of 78

113 Longitudinal Compression Properties (LC) -- (RTD) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Longitudinal Compression Modulus [Msi] Page of 78

114 Longitudinal Compression Properties (LC) -- (ETD) Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Modulus norm Number Batch # Cycle Lot # # [Msi] Ratio Thickn. [in] Laminate Mode [in] [Msi] HFULABC A M NO FAILURE HFULACC A M NO FAILURE HFULADC A M NO FAILURE HFULAEC A M NO FAILURE HFULA9C A M NO FAILURE HFULAAC A M NO FAILURE HFULABC A M NO FAILURE HFULB9C B M NO FAILURE HFULBAC B M NO FAILURE HFULBBC B M NO FAILURE HFULB9C B M NO FAILURE.7 6. HFULBAC B M NO FAILURE HFULBBC B M NO FAILURE HFULC9C C M NO FAILURE.7 6. HFULCAC C M NO FAILURE HFULCBC C M NO FAILURE HFULC9C C M NO FAILURE HFULCAC C M NO FAILURE HFULCBC C M NO FAILURE Average Average norm Standard Dev Standard Dev. norm.5 Coeff. of Var. [%] Coeff. of Var. [%] norm.9 Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 Page 4 of 78

115 Longitudinal Compression Properties (LC) -- (ETD) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Longitudinal Compression Modulus [Msi] Page 5 of 78

116 Longitudinal Compression Properties (LC) -- (ETW) Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Modulus norm Number Batch # Cycle Lot # # [Msi] Ratio Thickn. [in] Laminate Mode [in] [Msi] HFULAGD A M NO FAILURE HFULAHD A M NO FAILURE HFULAID A M NO FAILURE HFULAJD A M NO FAILURE HFULAED A M NO FAILURE HFULAFD A M NO FAILURE HFULAGD A M NO FAILURE HFULBED B M NO FAILURE HFULBFD B M NO FAILURE HFULBGD B M NO FAILURE HFULBID B M NO FAILURE HFULBED B M NO FAILURE HFULBFD B M NO FAILURE HFULBGD B M NO FAILURE HFULCCD C M NO FAILURE HFULCED C M NO FAILURE HFULCFD C M NO FAILURE HFULCGD C M NO FAILURE HFULCED C M NO FAILURE HFULCFD C M NO FAILURE HFULCGD C M NO FAILURE Average Average norm Standard Dev Standard Dev. norm.578 Coeff. of Var. [%] Coeff. of Var. [%] norm.47 Min Min Max Max Number of Spec. Number of Spec. Page 6 of 78

117 Longitudinal Compression Properties (LC) -- (ETW) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Longitudinal Compression Modulus [Msi] Page 7 of 78

118 4.4 Transverse Compression Properties Transverse Compression Properties (TC) -- (CTD) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] HFUZA6B A M HGM.74 HFUZA7B A M HGM.74 HFUZA8B A M HGM.74 HFUZA9B A M HGM.74 HFUZAAB A M HGM.75 HFUZA6B A M HGM.74 HFUZA7B A M HGM.74 HFUZA8B A M HGM.74 HFUZB6B B M HGM.7 HFUZB7B B M HAT.7 HFUZB8B B M HAT.7 HFUZB6B B M HAT.7 HFUZB7B B M HAT.7 HFUZB8B B M HAT.7 HFUZC6B C M HGM.74 HFUZC7B C M HGM.74 HFUZC8B C M HGM.74 HFUZC6B C M HGM.7 HFUZC7B C M HGM.7 HFUZC8B C M HGM.7 Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec. Page 8 of 78

119 Transverse Compression Properties (TC) -- (CTD) Measured Strength Hexcel AS4 UNI Transverse Compression Strength [ksi] Transverse Compression Properties (TC) -- (CTD) Measured Modulus Hexcel AS4 UNI Transverse Compression Modulus [Msi] Page 9 of 78

120 Transverse Compression Properties (TC) -- (RTD) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] HFUZAA A M HGM.7 HFUZAA A M HGM.74 HFUZA4A A M HGM.74 HFUZA5A A M HGM.74 HFUZAA A M HGM.7 HFUZAA A M HGM.7 HFUZAA A M HGM.74 HFUZBA B M HAB.68 HFUZBA B M HAB.7 HFUZBA B M HAB.7 HFUZBA B M HGM.67 HFUZBA B M HGM.7 HFUZBA B M HGM.7 HFUZCA C M HGM.68 HFUZCA C M HGM.7 HFUZCA C M HGM.7 HFUZCA C M HAB.69 HFUZCA C M HAB.7 HFUZCA C M HAB.7 Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec Page of 78

121 Transverse Compression Properties (TC) -- (RTD) Measured Strength Hexcel AS4 UNI Cure Cycl e # Transverse Compression Strength [ksi] Transverse Compression Properties (TC) -- (RTD) Measured Modulus Hexcel AS4 UNI Cure Cycl e # Transverse Compression Modulus [Msi] Page of 78

122 Transverse CompressionProperties (TC) -- (ETW) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] HFUZAD* A M HGM.7 HFUZABD* A M HGM.74 HFUZACD* A M HGM.74 HFUZADD A M HGM/HAT.74 HFUZAED A M HGM.74 HFUZAFD A M HAT.75 HFUZA4D A M HGM.74 HFUZA5D A M HAT/HGM.74 HFUZA9D A M HAB/HGM.74 HFUZABD* A M... 4 HGM.74 HFUZACD* A M HGM.74 HFUZADD* A M HGM.74 HFUZAED* A M HGM.74 HFUZAFD A M HGM.74 HFUZB4D B M HGM.7 HFUZBBD* B M HGM.7 HFUZBCD* B M HGM/HAB.7 HFUZBDD* B M.. 4 HGM.7 HFUZBED B M HGM/HAT.7 HFUZBFD B M HGM.7 HFUZB5D B M HGM.7 HFUZBBD* B M HGM.7 HFUZBCD* B M HGM.7 HFUZBDD* B M HGM.7 HFUZBED B M HGM.7 HFUZBFD B M HGM.7 HFUZC4D C M HGM.74 HFUZCBD* C M HGM.74 HFUZCCD* C M HGM.74 HFUZCDD* C M HGM.74 HFUZCED C M HGM.74 HFUZCFD C M HGM.7 HFUZC4D C M.. 4 HGM.7 HFUZCBD* C M HGM.7 HFUZCCD* C M HGM.74 HFUZCDD* C M HGM.7 HFUZCED C M.4. 4 HGM.74 HFUZCFD C M HGM.7 *Strength removed on ETW data that had protective coating over gage Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec Page of 78

123 Transverse Compression Properties (TC) -- (ETW) Measured Strength Hexcel AS4 UNI Transverse Compression Strength [ksi] Transverse Compression Properties (TC) -- (ETW) Measured Modulus Hexcel AS4 UNI Transverse Compression Modulus [Msi] Page of 78

124 4.5 Unnotched Compression Properties Laminate Unnotched Compression Properties (UNC) -- (CTD) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # Batch # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFURA6B A M BAT HFURA7B A M BGM HFURA8B A M BAT HFURA9B A M BGM HFURA5B* A M BGM / CIT HFURA6B* A M BGM / CIT.7 6. HFURA7B A M BGM HFURB5B B M BGM HFURB6B B M HAT/BAB HFURB7B B M BAB HFURB5B B M BAB HFURB6B B M BGM HFURB7B B M BGM/HAT HFURC5B* C M CIT HFURC6B* C M CIT HFURC7B C M BAT HFURC5B C M BAT HFURC6B C M BGM HFURC7B C M BGM Note : * Strength values were not reported due to bad failure mode Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec Number of Spec. 5 9 Page 4 of 78

125 Laminate Unnotched Compression Properties (UNC) -- (CTD) Normalized Strength Hexcel 855 AS4 Uni Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (CTD) Normalized Modulus Hexcel 855 AS4 Uni Laminate Compression Modulus (UNC) [Msi] Page 5 of 78

126 Laminate Unnotched Compression Properties (UNC) -- (RTD) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # Batch # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFURAA A M BAT HFURAA A M BGM HFURAA A M BGM HFURA4A A M BAT HFURAA A M BAT HFURAA A M BAT HFURAA A M BAT HFURBA B M BGM HFURBA B M BGM HFURBA B M BGM HFURB4A B M BAT HFURBA B M HAT HFURBA B M BAB HFURBA B M BAT HFURCA C M BAB HFURCA C M BAT HFURCA C M BGM HFURCA C M BGM HFURCA C M BAT HFURCA C M BAT Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. Number of Spec. Page 6 of 78

127 Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Strength Hexcel 855 AS4 Uni Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Modulus Hexcel 855 AS4 Uni Laminate Compression Modulus (UNC) [Msi] Page 7 of 78

128 Laminate Unnotched Compression Properties (UNC) -- (ETD) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFURABC A M BAT / HAT HFURACC * A M ENDCRUSH HFURADC A M BAB / HAB HFURAEC A M BAB / HAB HFURA9C A M HAB / HAT HFURAAC A M HAT HFURABC A M HAT HFURB9C B M BGM HFURBAC B M BAT / HAT HFURBBC B M BGM HFURB9C B M HAT / BGM HFURBAC B M BGM HFURBBC B M HAB / BGM HFURC9C C M BAB HFURCAC C M BAT HFURCBC C M BGM HFURC9C C M BGM HFURCAC C M BAT HFURCBC C M BAT * Strength value was removed due to bad failure mode. Average Average norm Standard Dev Standard Dev. norm.76.6 Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec Number of Spec. 8 9 Page 8 of 78

129 Laminate Unnotched Compression Properties (UNC) -- (ETD) Normalized Strength Hexcel 855 AS4 Uni Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (ETD) Normalized Modulus Hexcel 855 AS4 Uni Laminate Compression Modulus (UNC) [Msi] Page 9 of 78

130 Laminate Unnotched Compression Properties (UNC) -- (ETW) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFURAGD* A M BGM HFURAHD* A M BAT HFURAID* A M BGM HFURAJD* A M BAT HFURAKD A M BAT HFURA5D A M BAB HFURAAD A M BAB HFURAFD A M BAT HFURAED* A M BAT HFURAFD* A M BGM.7 5. HFURAGD A M BAT HFURAHD A M BAT HFURAID A M BAT HFURADD A M BGM.7 6. HFURBED* B M BAT HFURBFD* B M BAB/HGM HFURBGD B M BAT HFURBHD B M BGM HFURBID B M BAT HFURB8D B M BAB HFURBDD B M BAT HFURBED* B M BGM HFURBFD* B M BGM HFURBGD B M BGM HFURBHD B M BAT HFURBID B M BGM HFURBDD B M BAT/HIT HFURCDD* C M BGM HFURCED* C M HGM HFURCFD* C M BGM/HIB HFURCGD C M BGM HFURCHD C M BAT HFURCID C M BAT HFURC8D C M BGM HFURC8D C M BGM.7 5. HFURCDD C M BAT HFURCED* C M BAT HFURCFD* C M BAB HFURCGD* C M BAT HFURCID C M BAT HFURBDD: STRENGTH REMOVED DUE TO AN UNACCEPTABLE FAILURE MODE HFURCFD: STRENGTH REMOVED DUE TO AN UNACCEPTABLE FAILURE *Strength removed on ETW data that had protective coating over gage Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 Page of 78

131 Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Strength Hexcel 855 AS4 Uni Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Modulus Hexcel 855 AS4 Uni Laminate Compression Modulus (UNC) [Msi] Page of 78

132 4.6 Unnotched Tension Properties Laminate Unnotched Tension Properties (UNT) -- (CTD) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUPA6B A M LGM HFUPA7B A M LWT HFUPA8B A M LGM HFUPA9B A M LGM HFUPA6B A M LGM HFUPA7B A M LGM HFUPA8B A M LGM HFUPB6B B M LGM HFUPB7B B M LGM HFUPB8B B M LWB HFUPB6B B M LGM HFUPB7B B M LGM HFUPB8B B M LGM HFUPC6B C M LGM HFUPC7B C M LGM HFUPC8B C M LGM HFUPC6B C M LGM HFUPC7B C M LGM HFUPC8B C M LGM Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page of 78

133 Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Strength Hexcel 855 AS4 Uni LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Modulus Hexcel 855 AS4 Uni 4 Cure Cycl e # Laminate Tension Modulus (UNT) [Msi] Page of 78

134 Laminate Unnotched Tension Properties (UNT) -- (RTD) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUPAA A M LAT HFUPAA A M LWB HFUPAA A M LAB HFUPA4A A M LWB HFUPAA A M LGM HFUPAA A M LAT HFUPAA A M LAB HFUPBA B M LWB HFUPBA B M LGM HFUPBA B M LAT HFUPBA B M LGM HFUPBA B M LWB HFUPBA B M LGM HFUPCA C M LGM HFUPCA C M LGM HFUPCA C M LGM HFUPCA C M LAB HFUPCA C M LAB HFUPCA C M LAT Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page 4 of 78

135 Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Strength Hexcel 855 AS4 Uni 4 Cure Cycl e # Laminate Tension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Modulus Hexcel 855 AS4 Uni 4 Cure Cycl e # Laminate Tension Modulus (UNT) [Msi] Page 5 of 78

136 Laminate Unnotched Tension Properties (UNT) -- (ETW) Strength & Modulus Hexcel 855 AS4 Uni normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUPABD A M LGM/LAB HFUPACD A M LWT HFUPADD A M LWT/LGM HFUPAED A M LWT HFUPABD A M LWB HFUPACD A M LGM HFUPADD A M LGM HFUPBBD B M LAB HFUPBCD B M LAT HFUPBDD B M LIB HFUPBED B M LAT/LAB HFUPBCD B M LGM HFUPBDD B M LAT/LAB HFUPBED B M LAT HFUPCBD C M LWT HFUPCCD C M LGM HFUPCDD C M LWT HFUPCBD C M LGM HFUPCCD C M LGM HFUPCDD C M LGM Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm.7.88 Min Min Max Max Number of Spec. Number of Spec. Page 6 of 78

137 Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Strength Hexcel 855 AS4 Uni LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Modulus Hexcel 855 AS4 Uni Laminate Tension Modulus (UNT) [Msi] Page 7 of 78

138 4.7 In-Plane Shear Properties In-Plane Shear Properties (IPS) -- (CTD) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle.% Offset Modulus Avg. Specimen # Plies in Avg. tply Number Batch # Cycle Lot # # Strength [ksi] [Msi] Thickn. [in] Laminate [in] HFUNA6B A M HFUNA7B A M HFUNA8B A M HFUNA9B A M HFUNAAB A M HFUNA6B A M HFUNA7B A M HFUNA8B A M HFUNB6B B M HFUNB7B B M HFUNB8B B M HFUNB6B B M HFUNB7B B M HFUNB8B B M HFUNC8B C M HFUNC9B C M HFUNCAB C M HFUNC6B C M HFUNC7B C M HFUNC9B C M Note: ALL CTD SPECIMENS FAILED BEFORE IT REACHED 5% STRAIN. Average.7.89 Average.7 Standard Dev Standard Dev. Coeff. of Var. [%].4.7 Coeff. of Var. [%] Min Min..67 Max Max..74 Number of Spec. Number of Spec. Page 8 of 78

139 In-Plane Shear Properties (IPS) -- (CTD) Measured Modulus Hexcel AS4 UNI 4 Cure Cycl e # Prepeg Lot # In-Plane Shear Modulus (IPS) [Msi] Page 9 of 78

140 In-Plane Shear Properties (IPS) -- (RTD) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength at.% Offset Modulus Avg. Specimen # Plies in Avg. tply Number Batch # Cycle Lot # # 5% Strain [ksi] Strength [ksi] [Msi] Thickn. [in] Laminate [in] HFUNAA A M HFUNAA A M HFUNAA A M HFUNA4A A M HFUNAA A M HFUNAA A M HFUNAA A M HFUNBA B M * HFUNBA B M HFUNBA B M HFUNB4A B M HFUNBA B M HFUNBA B M HFUNBA B M HFUNC5A C M HFUNC6A C M HFUNC7A C M HFUNCA C M * HFUNCA C M * HFUNCA C M * HFUNC4A C M * HFUNC5A C M * Note: * SPECIMENS FAILED BEFORE IT REACHED 5% STRAIN. Average Average.7 Standard Dev Standard Dev. Coeff. of Var. [%] Coeff. of Var. [%] Min Min..67 Max Max..74 Number of Spec. 6 Number of Spec. Page 4 of 78

141 In-Plane Shear Properties (IPS) -- (RTD) Measured Strength Hexcel AS4 UNI 4 Cure Cycl e # Prepeg Lot # 5 5 In-Plane Shear Strength at 5% Strain (IPS) [ksi] In-Plane Shear Properties (IPS) -- (RTD) Measured Modulus Hexcel AS4 UNI Cure Cycl e # 4 Prepeg Lot # In-Plane Shear Modulus (IPS) [Msi] Page 4 of 78

142 In-Plane Shear Properties (IPS) -- (ETW) Strength & Modulus Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength at.% Offset Modulus Avg. Specimen # Plies in Avg. tply Number Batch # Cycle Lot # # 5% Strain [ksi] Strength [ksi] [Msi] Thickn. [in] Laminate [in] HFUNABD A M HFUNACD A M HFUNADD A M HFUNAED A M HFUNABD A M HFUNACD A M HFUNADD A M HFUNBBD B M HFUNBCD B M HFUNBDD B M HFUNBCD B M HFUNBDD B M HFUNBED B M HFUNCCD C M HFUNCDD C M HFUNCED C M HFUNCBD C M HFUNCCD C M HFUNCDD C M Average Average.7 Standard Dev Standard Dev. Coeff. of Var. [%] Coeff. of Var. [%] Min Min..67 Max Max..78 Number of Spec Number of Spec. 9 Page 4 of 78

143 In-Plane Shear Properties (IPS) -- (ETW) Measured Strength Hexcel AS4 UNI Cure Cycl e # 4 4 Prepeg Lot # In-Plane Shear Strength at 5% Strain (IPS) [ksi] - In-Plane Shear Properties (IPS) -- (ETW) Measured Modulus Hexcel AS4 UNI 4 Cure Cycl e # Prepeg Lot # In-Plane Shear Modulus (IPS) [Msi] Page 4 of 78

144 4.8 Lamina Short Beam Shear Properties Short Beam Strength Properties (SBS) -- (CTD) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Avg. tply Failure Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate [in] Mode HFUQA6B A M INTERLAMINAR SHEAR HFUQA7B A M INTERLAMINAR SHEAR HFUQA8B A M INTERLAMINAR SHEAR HFUQA9B A M INTERLAMINAR SHEAR HFUQA6B A M INTERLAMINAR SHEAR HFUQA7B A M INTERLAMINAR SHEAR HFUQA8B A M INTERLAMINAR SHEAR HFUQA9B A M INTERLAMINAR SHEAR HFUQB6B B M INTERLAMINAR SHEAR HFUQB7B B M INTERLAMINAR SHEAR HFUQB8B B M INTERLAMINAR SHEAR HFUQB9B B M INTERLAMINAR SHEAR HFUQB6B B M INTERLAMINAR SHEAR HFUQB7B B M INTERLAMINAR SHEAR HFUQB8B B M INTERLAMINAR SHEAR HFUQB9B B M INTERLAMINAR SHEAR HFUQC6B C M INTERLAMINAR SHEAR HFUQC7B C M INTERLAMINAR SHEAR HFUQC8B C M INTERLAMINAR SHEAR HFUQC9B C M INTERLAMINAR SHEAR HFUQC6B C M INTERLAMINAR SHEAR HFUQC7B C M INTERLAMINAR SHEAR HFUQC8B C M INTERLAMINAR SHEAR HFUQC9B C M INTERLAMINAR SHEAR Average.866 Average.7 Standard Dev..588 Standard Dev. Coeff. of Var. [%].87 Coeff. of Var. [%] Min. 9.6 Min..59 Max..87 Max..75 Number of Spec. 4 Number of Spec. 4 Page 44 of 78

145 Short Beam Strength Properties (SBS) -- (CTD) Measured Strength Hexcel AS4 UNI Cure Cycl e # Short Beam Strength (SBS) [ksi] Page 45 of 78

146 Short Beam Strength Properties (SBS) -- (RTD) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Avg. tply Failure Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate [in] Mode HFUQAA A M COMPRESSION / ILS HFUQAA A M ILS / COMPRESSION / TENSION HFUQA4A A M COMPRESSION / ILS / TENSION HFUQA5A A M ILS / COMPRESSION / TENSION HFUQAA A M COMPRESSION / ILS LEFT HFUQA4A A M COMPRESSION / ILS LEFT RIGHT HFUQA5A A M COMPRESSION / ILS RIGHT HFUQBA B M COMPRESSION / ILS / TENSION HFUQB4A B M COMPRESSION / ILS / TENSION HFUQB5A B M ILS / COMPRESSION / TENSION HFUQBA B M COMPRESSION / ILS LEFT HFUQB4A B M COMPRESSION / ILS LEFT HFUQB5A B M COMPRESSION / ILS / TENSION HFUQCA C M COMPRESSION / ILS HFUQC4A C M COMPRESSION / ILS HFUQC5A C M COMPRESSION / ILS HFUQCA C M COMPRESSION / ILS HFUQC4A C M COMPRESSION / ILS HFUQC5A C M COMPRESSION / ILS Average 6.6 Average.7 Standard Dev..8 Standard Dev. Coeff. of Var. [%].68 Coeff. of Var. [%] Min. 6. Min..7 Max. 7.6 Max..75 Number of Spec. 9 Number of Spec. 9 Page 46 of 78

147 Short Beam Strength Properties (SBS) -- (RTD) Measured Strength Hexcel AS4 UNI Cure Cycl e # Short Beam Strength (SBS) [ksi] Page 47 of 78

148 Short Beam Strength Properties (SBS) -- (ETD) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Avg. tply Failure Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate [in] Mode HFUQAAC A M ILS HFUQABC A M ILS HFUQACC A M ILS HFUQADC A M ILS HFUQAAC A M ILS HFUQABC A M ILS HFUQACC A M ILS HFUQBAC B M ILS HFUQBBC B M ILS HFUQBCC B M ILS HFUQBAC B M ILS HFUQBBC B M ILS HFUQBCC B M ILS HFUQCAC C M ILS HFUQCBC C M ILS HFUQCCC C M ILS HFUQCAC C M ILS HFUQCBC C M ILS HFUQCDC C M ILS Average.95 Average.74 Standard Dev..74 Standard Dev. Coeff. of Var. [%].54 Coeff. of Var. [%] Min..599 Min..69 Max..676 Max..76 Number of Spec. 9 Number of Spec. 9 Page 48 of 78

149 Short Beam Strength Properties (SBS) -- (ETD) Measured Strength Hexcel AS4 UNI Cure Cycl e # Short Beam Strength (SBS) [ksi] Page 49 of 78

150 Short Beam Strength Properties (SBS) -- (ETW) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Avg. tply Failure Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate [in] Mode HFUQAED A M COMPRESSION / INTERLAMINAR SHEAR HFUQAFD A M COMPRESSION / INTERLAMINAR SHEAR HFUQAGD A M COMPRESSION HFUQAID A M COMPRESSION HFUQAED A M COMPRESSION HFUQAFD A M COMPRESSION / INTERLAMINAR SHEAR HFUQAHD A M COMPRESSION / INTERLAMINAR SHEAR HFUQBED B M COMPRESSION / INTERLAMINAR SHEAR HFUQBFD B M COMPRESSION / INTERLAMINAR SHEAR HFUQBHD B M COMPRESSION / INTERLAMINAR SHEAR HFUQBED B M COMPRESSION / INTERLAMINAR SHEAR HFUQBGD B M COMPRESSION / INTERLAMINAR SHEAR HFUQBHD B M COMPRESSION / INTERLAMINAR SHEAR HFUQCED C M COMPRESSION / INTERLAMINAR SHEAR HFUQCFD C M COMPRESSION HFUQCGD C M COMPRESSION / INTERLAMINAR SHEAR HFUQCED C M COMPRESSION / INTERLAMINAR SHEAR HFUQCFD C M COMPRESSION / INTERLAMINAR SHEAR HFUQCGD C M COMPRESSION / INTERLAMINAR SHEAR Average 8.46 Average.7 Standard Dev..9 Standard Dev. Coeff. of Var. [%].5 Coeff. of Var. [%] Min Min..68 Max Max..76 Number of Spec. 9 Number of Spec. 9 Page 5 of 78

151 Short Beam Strength Properties (SBS) -- (ETW) Measured Strength Hexcel AS4 UNI Cure Cycl e # Short Beam Strength (SBS) [ksi] Page 5 of 78

152 4.9 Unnotched Tension Properties Laminate Unnotched Tension Properties (UNT) -- (CTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUAA6B A M MGM HFUAA7B A M MGM HFUAA8B A M MWB HFUAA9B A M MWT HFUAA6B A M MGM HFUAA7B A M MGM HFUAA8B A M MGM HFUAB6B B M MGM HFUAB7B B M MGM HFUAB8B B M MGM HFUAB6B B M MGM HFUAB7B B M MGM HFUAB8B B M MGM HFUAC6B C M MGM HFUAC7B C M MGM HFUAC8B C M MWB HFUAC6B C M MWT HFUAC7B C M MWT HFUAC8B C M MGM Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%].7.6 Coeff. of Var. [%] norm.4. Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page 5 of 78

153 4 Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Strength Hexcel AS4 UNI LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Modulus Hexcel AS4 UNI Laminate Tension Modulus (UNT) [Msi] Page 5 of 78

154 Laminate Unnotched Tension Properties (UNT) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUAAA A M MGM HFUAAA A M MGM HFUAAA A M MWB HFUAA4A A M MGM HFUAAA A M MGM HFUAAA A M MGM HFUAAA A M MGM HFUABA B M MGM HFUABA B M MWT HFUABA B M MGM HFUABA B M MWT HFUABA B M MGM HFUABA B M MWB HFUACA C M MGM HFUACA C M MGM HFUAC4A C M MGM HFUACA C M MWB HFUACA C M MWT HFUACA C M MWB Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page 54 of 78

155 Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Tension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Modulus Hexcel AS4 UNI Laminate Tension Modulus (UNT) [Msi] Page 55 of 78

156 Laminate Unnotched Tension Properties (UNT) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUAABD A M MGM HFUAACD A M MGM HFUAADD A M LWB HFUAAED A M MGM HFUAABD A M MGM HFUAACD A M LGM/AGM HFUAADD A M MGM HFUABBD B M MGM HFUABCD B M LAT HFUABDD B M MGM HFUABBD B M MGM HFUABCD B M MGM HFUABDD B M MGM HFUACBD C M MGM HFUACDD C M MGM HFUACED C M MGM HFUACFD C M MGM HFUACBD C M MGM HFUACCD C M MGM HFUACDD C M MGM Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm.8.8 Min Min Max Max Number of Spec. Number of Spec. Page 56 of 78

157 Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Strength Hexcel AS4 UNI LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Modulus Hexcel AS4 UNI Laminate Tension Modulus (UNT) [Msi] Page 57 of 78

158 4. Unnotched Tension Properties Laminate Unnotched Tension Properties (UNT) -- (CTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUBA6B A M MGM HFUBA7B A M MWT HFUBA8B A M MWT HFUBA9B A M MGM HFUBA7B A M MGM HFUBA8B A M MGM HFUBA9B A M MGM HFUBB6B B M MWT HFUBB7B B M MGM HFUBB8B B M MWT HFUBB6B B M MGM HFUBB7B B M MWT HFUBB8B B M MGM HFUBC6B C M MWB HFUBC7B C M MWB HFUBC8B C M MGM HFUBC6B C M MGM HFUBC7B C M MGM HFUBC8B C M MGM Average Average norm Standard Dev Standard Dev. norm..9 Coeff. of Var. [%] Coeff. of Var. [%] norm..95 Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page 58 of 78

159 Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Laminate Tension Modulus (UNT) [Msi] Page 59 of 78

160 Laminate Unnotched Tension Properties (UNT) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUBAA A M DWT HFUBAA A M DGM HFUBA4A A M DWT HFUBA5A A M DGM HFUBAA A M DGM HFUBAA A M DGM HFUBA4A A M DGM HFUBBA B M MGM HFUBBA B M MGM HFUBBA B M MGM HFUBBA B M MGM HFUBBA B M MGM HFUBBA B M MGM HFUBCA C M DGM HFUBCA C M DGM HFUBC4A C M DGM HFUBCA C M DGM HFUBCA C M DGM HFUBCA C M DGM Average Average norm Standard Dev...9 Standard Dev. norm.4.95 Coeff. of Var. [%] Coeff. of Var. [%] norm.95. Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page 6 of 78

161 Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Tension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Laminate Tension Modulus (UNT) [Msi] Page 6 of 78

162 Laminate Unnotched Tension Properties (UNT) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUBABD A M MGM HFUBACD A M MGM HFUBADD A M MGM HFUBAED A M MGM HFUBABD A M MGM HFUBACD A M MGM HFUBADD A M MGM HFUBBBD B M MGM HFUBBCD B M MGM HFUBBDD B M MGM HFUBBBD B M AGM HFUBBCD B M MGM HFUBBDD B M MGM HFUBCBD C M MGM HFUBCCD C M MGM HFUBCDD C M MGM HFUBCBD C M MGM HFUBCCD C M MGM HFUBCDD C M MGM Average Average norm Standard Dev Standard Dev. norm.84.8 Coeff. of Var. [%].964. Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 9 Page 6 of 78

163 Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Laminate Tension Modulus (UNT) [Msi] Page 6 of 78

164 4. Unnotched Tension Properties Laminate Unnotched Tension Properties (UNT) -- (CTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUCA6B A M MWB HFUCA7B A M MWB HFUCA8B A M MAB HFUCA9B A M MAB HFUCA6B A M MAT HFUCA7B A M MAT/MWB HFUCA8B A M MGM HFUCB6B B M MAB HFUCB7B B M MAT/MWB HFUCB8B B M MWT/MAB HFUCB6B B M MWT HFUCB7B B M MAB/MWT HFUCB8B B M MWB HFUCC6B C M MAB HFUCC7B C M MAT HFUCC8B C M MGM HFUCC6B C M MGM HFUCC7B C M MGM HFUCC8B C M MGM HFUCC9B C M MGM HFUCCAB C M MAB Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. Number of Spec. Page 64 of 78

165 Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Strength Hexcel AS4 UNI Laminate Tension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (CTD) Normalized Modulus Hexcel AS4 UNI Laminate Tension Modulus (UNT) [Msi] Page 65 of 78

166 Laminate Unnotched Tension Properties (UNT) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUCAA A M LAT HFUCAA A M LAB HFUCAA A M LAB HFUCA4A A M LAT HFUCA5A A M AWT HFUCAAA A M LAB HFUCAA A M LWT, LAB HFUCAA* A M LIB HFUCAA A M LGM HFUCA4A A M LAB HFUCA5A A M MGM HFUCA9A A M LAT HFUCAAA A M AAT HFUCBA B M MAT HFUCBA B M MWT HFUCBA B M AWB HFUCB4A B M LWT,LIB HFUCB5A B M MAB HFUCB9A B M LWT HFUCBAA B M LAB HFUCBA B M MAT HFUCBA B M MWT HFUCBA B M MWB HFUCB4A B M LWB, MWT HFUCB5A B M MWB,LWT HFUCB9A B M LAT HFUCBAA B M MWT HFUCCA C M MWB,LWT HFUCCA C M MWT HFUCCA C M LWT HFUCC4A C M MWB HFUCC5A C M LWT,LWB HFUCC9A C M MGM HFUCCAA C M MWT HFUCCA C M MWB HFUCCA C M LAB HFUCCA C M LAB HFUCC4A C M MWB HFUCC5A C M MWT/LWB *Strength removed due to bad failure mode obtained Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%]..74 Coeff. of Var. [%] norm.8.66 Min Min Max Max Number of Spec. 8 9 Number of Spec. 8 9 Page 66 of 78

167 Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Strength Hexcel AS4 UNI LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (RTD) Normalized Modulus Hexcel AS4 UNI Laminate Tension Modulus (UNT) [Msi] Page 67 of 78

168 Laminate Unnotched Tension Properties (UNT) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUCABD A M MAB HFUCACD A M LWT HFUCADD A M LAB/LWT HFUCAED A M LAB/LWT HFUCABD A M MAB HFUCACD A M LWB HFUCADD A M LWT/LAB/DGM HFUCBBD B M MWB HFUCBCD* B M LWB/LIT.7.8 HFUCBDD B M LWT/LAB HFUCBED B M MGM HFUCBBD B M LAB/LWT HFUCBCD B M LAB/LWT HFUCBDD B M LAB/LWT HFUCCBD C M LWT/MAB HFUCCCD C M MAB HFUCCDD C M MAB HFUCCBD C M LAT/LWB HFUCCCD C M LWT/MAB HFUCCDD C M MWT *Specimen had strength removed due to bad failure during test. Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm.87.7 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page 68 of 78

169 Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Strength Hexcel AS4 UNI LaminateTension Strength (UNT) [ksi] Laminate Unnotched Tension Properties (UNT) -- (ETW) Normalized Modulus Hexcel AS4 UNI Laminate Tension Modulus (UNT) [Msi] Page 69 of 78

170 4. Unnotched Compression Properties Laminate Unnotched Compression Properties (UNC) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # Batch # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUWAA A M BGM HFUWAA A M BGM HFUWAA A M BGM HFUWA4A A M BGM HFUWAA A M BGM HFUWAA A M BGM HFUWAA A M BGM HFUWBA B M BGM HFUWBA B M BGM HFUWBA B M BGM/HAT HFUWBA B M BGM HFUWBA B M BGM HFUWBA B M BGM HFUWCA C M BGM HFUWCA C M BGM HFUWC4A C M BGM HFUWCA C M BGM HFUWCA C M BGM HFUWCA C M HAT Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec Number of Spec. 9 9 Page 7 of 78

171 Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Modulus Hexcel AS4 UNI Laminate Compression Modulus (UNC) [Msi] Page 7 of 78

172 Laminate Unnotched Compression Properties (UNC) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUWA7D* A M BGM HFUWA8D* A M BGM HFUWA9D* A M BGM HFUWAAD* A M BGM HFUWABD A M HAB HFUWACD A M HAB / BGM HFUWA5D A M BGM HFUWA6D A M BGM HFUWA6D* A M BGM HFUWA7D* A M BGM HFUWA8D* A M BGM HFUWA9D A M BGM HFUWAAD A M BGM HFUWA5D A M BGM HFUWB6D* B M BGM HFUWB7D* B M BGM HFUWB8D* B M BGM HFUWB9D B M BGM HFUWBAD B M BGM HFUWB4D B M BGM HFUWB5D B M BGM HFUWB6D* B M BGM HFUWB7D* B M BGM HFUWB8D* B M BGM HFUWB9D B M BGM HFUWBAD B M BGM HFUWB4D B M BGM HFUWB5D B M BGM HFUWCD C M BGM HFUWC5D C M BGM HFUWC6D* C M BAT HFUWC7D* C M BAB.7 6. HFUWC8D* C M BGM HFUWC9D C M BAT HFUWCAD C M BGM HFUWC4D C M BGM HFUWC5D C M BGM HFUWC6D* C M BGM HFUWC7D* C M BGM HFUWC8D* C M BGM HFUWC9D C M BGM HFUWCAD C M BGM *Strength removed on ETW data that had protective coating over gage Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 8 Number of Spec. 9 Page 7 of 78

173 Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Modulus Hexcel AS4 UNI Laminate Compression Modulus (UNC) [Msi] Page 7 of 78

174 4. Unnotched Compression Properties Laminate Unnotched Compression Properties (UNC) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # Batch # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUXAA A M BGM HFUXAA A M BGM HFUXAA A M BGM HFUXA4A A M BGM HFUXAA A M BGM HFUXAA A M BGM HFUXAA A M BGM HFUXBA B M BGM HFUXBA B M BGM HFUXBA B M BGM HFUXBA B M BGM HFUXBA B M BGM HFUXB4A B M BGM HFUXCA C M BGM HFUXCA C M BGM HFUXCA C M BGM HFUXCA C M BGM HFUXCA C M BGM HFUXCA C M BGM Average Average norm Standard Dev Standard Dev. norm.6. Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec Number of Spec. 9 9 Page 74 of 78

175 Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Modulus Hexcel AS4 UNI Laminate Compression Modulus (UNC) [Msi] Page 75 of 78

176 Laminate Unnotched Compression Properties (UNC) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUXA7D* A M BGM HFUXA8D* A M BGM HFUXA9D* A M BGM / END CRUSHED.7.7 HFUXAAD* A M BGM HFUXABD A M BGM.7 5. HFUXACD A M BGM HFUXA5D A M BGM HFUXA6D A M BGM HFUXA6D* A M BGM.74.9 HFUXA7D* A M BGM.7.87 HFUXA8D* A M BGM.7.9 HFUXA9D A M BGM HFUXAAD A M BGM.7 4. HFUXA5D A M BGM HFUXA4D A M BGM HFUXB6D* B M BGM.7.74 HFUXB7D* B M BGM.7.8 HFUXB8D* B M BGM.7.84 HFUXB9D B M BGM HFUXBAD B M BGM HFUXB4D B M BGM HFUXB5D B M BGM HFUXB6D* B M BGM HFUXB7D* B M BGM HFUXB8D* B M BGM HFUXB9D B M BGM HFUXBAD B M BGM HFUXB5D B M BGM HFUXC6D* C M BGM.7 4. HFUXC7D* C M BGM HFUXC8D* C M BGM HFUXC9D C M BGM HFUXCAD C M BGM HFUXC4D C M BGM HFUXC5D C M BGM HFUXC6D* C M BGM HFUXC7D* C M BGM HFUXC8D* C M BGM HFUXC9D C M BGM HFUXCAD C M BGM HFUXC5D C M BGM *Strength removed on ETW data that had protective coating over gage Average Average norm Standard Dev Standard Dev. norm.49. Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 Page 76 of 78

177 Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Compression Strength (UNC) [ksi] - Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Laminate Compression Modulus (UNC) [Msi] Page 77 of 78

178 4.4 Unnotched Compression Properties Laminate Unnotched Compression Properties (UNC) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # Batch # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUYAA A M BGM HFUYAA A M BGM HFUYAA A M BGM HFUYA4A A M BGM HFUYAA A M BGM HFUYAA A M BGM HFUYAA* A M BGM / HIB HFUYA4A A M BGM HFUYBA B M BGM HFUYBA B M BGM HFUYBA B M BGM HFUYBA B M BGM HFUYBA B M BGM HFUYBA B M BGM HFUYCA C M BGM HFUYCA C M BAT HFUYCA C M HAT HFUYCA C M BGM HFUYCA C M BGM HFUYCA C M BGM * Strength not reported due to improper failure mode Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec Number of Spec. 9 9 Page 78 of 78

179 Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (RTD) Normalized Modulus Hexcel AS4 UNI Laminate Compression Modulus (UNC) [Msi] Page 79 of 78

180 Laminate Unnotched Compression Properties (UNC) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Modulus Poisson's Avg. Specimen # Plies in Failure Avg. t ply Strength norm Modulus norm Number Batch # Cycle Lot # # [ksi] [Msi] Ratio Thickn. [in] Laminate Mode [in] [ksi] [Msi] HFUYA8D* A M HFUYA9D* A M HFUYAAD A M.7.49 BAT.74.9 HFUYABD A M BAB HFUYACD A M BGM HFUYADD A M BAT HFUYA5A* A M HFUYA7D* A M BAT HFUYA6D A M HFUYA7D A M HFUYA8D A M HFUYAAD A M BAT HFUYABD A M BAT HFUYACD A M BAB HFUYB7D B M HFUYB9D B M BAB HFUYBBD B M BGM HFUYBCD B M BGM HFUYB5D B M HFUYB6D B M HFUYB5D B M HFUYB6D B M HFUYB7D* B M HFUYB8D B M BAT HFUYB9D B M BGM HFUYBCD B M BAB HFUYC7D C M HFUYC8D C M BAB HFUYCBD C M BGM.7 8. HFUYCCD C M BGM HFUYC5D* C M HFUYC6D C M HFUYC7D C M HFUYC8D C M HFUYC9D* C M HFUYCAD C M BAT HFUYCBD C M BAT HFUYCCD C M BAB HFUYC5D C M BAT HFUYC6D C M BAB *Strength removed on ETW data that had protective coating over gage Average Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min Max Max Number of Spec. 9 9 Number of Spec. 9 Page 8 of 78

181 Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Compression Strength (UNC) [ksi] Laminate Unnotched Compression Properties (UNC) -- (ETW) Normalized Modulus Hexcel AS4 UNI Cure Cycl e # Laminate Compression Modulus (UNC) [Msi] Page 8 of 78

182 4.5 Laminate Short Beam Strength Properties Laminate Short Beam Strength Properties (LSBS) -- (RTD) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Avg. tply Failure Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate [in] Mode HFUqA7A A M ILS HFUqA7A A M ILS HFUqA7A A M ILS HFUqA74A A M ILS HFUqA7A A M ILS HFUqA7A A M ILS HFUqA7A A M ILS HFUqB7A B M ILS HFUqB7A B M ILS HFUqB74A B M ILS HFUqB7A B M ILS HFUqB7A B M ILS HFUqB74A B M ILS HFUqC7A C M ILS LEFT HFUqC7A C M ILS LEFT HFUqC74A C M ILS LEFT, CENTER HFUqC7A C M ILS LEFT HFUqC7A C M ILS LEFT HFUqC74A C M ILS RIGHT Average.94 Average.7 Standard Dev..679 Standard Dev. Coeff. of Var. [%] Coeff. of Var. [%] Min..5 Min..68 Max..97 Max..75 Number of Spec. 9 Number of Spec. 9 Page 8 of 78

183 Laminate Short Beam Strength Properties (LSBS) -- (RTD) Measured Strength Hexcel AS4 UNI Laminate Short Beam Strength (LSBS) [ksi] Page 8 of 78

184 Laminate Short Beam Strength Properties (LSBS) -- (ETW) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Avg. tply Failure Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate [in] Mode HFUqA77D A M ILS HFUqA78D A M ILS HFUqA79D A M ILS HFUqA7AD A M ILS HFUqA76D A M ILS HFUqA77D A M ILS HFUqA79D A M ILS HFUqB76D B M ILS HFUqB77D B M ILS HFUqB78D B M ILS HFUqB76D B M ILS HFUqB77D B M ILS HFUqB78D B M ILS HFUqC76D C M ILS HFUqC77D C M ILS HFUqC78D C M ILS HFUqC78D C M ILS HFUqC79D C M ILS HFUqC7AD C M ILS Average 6.8 Average.74 Standard Dev..8 Standard Dev. Coeff. of Var. [%].58 Coeff. of Var. [%] Min Min..7 Max. 7.6 Max..74 Number of Spec. 9 Number of Spec. 9 Page 84 of 78

185 Laminate Short Beam Strength Properties (LSBS) -- (ETW) Measured Strength Hexcel AS4 UNI Laminate Short Beam Strength (LSBS) [ksi] Page 85 of 78

186 4.6 Open Hole Tension Properties Laminate Open Hole Tension Properties (OHT) -- (CTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUDA6B A M LGM/AGM HFUDA7B A M LGM/AGM HFUDA8B A M LGM/AGM HFUDA9B A M LGM/AGM HFUDA5B A M LGM/AGM HFUDA6B A M LGM/AGM HFUDA7B A M LGM/AGM HFUDA9B A M LGM/AGM HFUDB6B B M LGM/AGM HFUDB7B B M LGM/AGM HFUDB8B B M LGM/AGM HFUDB6B B M LGM/AGM HFUDB7B B M LGM/AGM HFUDB8B B M LGM/AGM HFUDC6B C M LGM/AGM HFUDC7B C M LGM/AGM HFUDC8B C M LGM/AGM HFUDC6B C M LGM/AGM HFUDC7B C M LGM/AGM HFUDC8B C M LGM/AGM Average Average norm Standard Dev..5 Standard Dev. norm. Coeff. of Var. [%].765 Coeff. of Var. [%] norm.75 Min. 4.4 Min Max Max Number of Spec. Number of Spec. Page 86 of 78

187 Laminate Open Hole Tension Properties (OHT) -- (CTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Open Hole Tension Strength [ksi] Page 87 of 78

188 Laminate Open Hole Tension Properties (OHT) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUDAA A M MGM HFUDAA A M MGM HFUDA4A A M MGM HFUDA5A A M MGM HFUDAA A M MGM HFUDAA A M MGM HFUDAA A M MGM HFUDBA B M MGM HFUDBA B M MGM HFUDBA B M MGM HFUDBA B M MGM HFUDBA B M MGM HFUDBA B M MGM HFUDCA C M MGM HFUDCA C M MGM HFUDC4A C M MGM HFUDCA C M MGM HFUDCA C M MGM HFUDC4A C M MGM Average Average norm Standard Dev..454 Standard Dev. norm.8 Coeff. of Var. [%].4 Coeff. of Var. [%] norm.788 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page 88 of 78

189 Laminate Open Hole Tension Properties (OHT) -- (RTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Open Hole Tension Strength [ksi] Page 89 of 78

190 Laminate Open Hole Tension Properties (OHT) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUDAAD A M LGM HFUDABD A M LGM HFUDACD A M LGM HFUDADD A M LGM HFUDAAD A M LGM HFUDABD A M LGM HFUDACD A M LGM HFUDADD A M LGM HFUDBAD B M LGM HFUDBBD B M LGM HFUDBCD B M LGM HFUDBDD B M LGM HFUDBAD B M LGM HFUDBBD B M LGM HFUDBCD B M LGM HFUDCAD C M LGM HFUDCBD C M LGM HFUDCCD C M LGM HFUDCDD C M LGM HFUDCAD C M LGM HFUDCBD C M LGM HFUDCCD C M LGM Average Average Average norm Standard Dev..84 Standard Dev. norm.685 Coeff. of Var. [%].48 Coeff. of Var. [%] norm.6 Min Min. Min Max Max. Max Number of Spec. Number of Spec. Page 9 of 78

191 Laminate Open Hole Tension Properties (OHT) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Open Hole Tension Strength [ksi] Page 9 of 78

192 4.7 Open Hole Tension Properties Laminate Open Hole Tension Properties (OHT) -- (CTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUEA6B A M AGM HFUEA7B A M AGM / LGM HFUEA8B A M AGM HFUEA6B A M AGM / LGM HFUEA7B A M AGM HFUEA8B A M AGM / LGM HFUEA9B A M AGM / LGM HFUEB6B B M AGM HFUEB7B B M MGM HFUEB8B B M LGM HFUEB6B B M LGM HFUEB7B B M LGM HFUEB8B B M 4..4 AGM HFUEC6B C M AGM / LGM HFUEC7B C M AGM HFUEC8B C M AGM HFUEC6B C M AGM.7 4. HFUEC7B C M MGM HFUEC8B C M AGM / MGM Average 4.5 Average norm Standard Dev..689 Standard Dev. norm.88 Coeff. of Var. [%].67 Coeff. of Var. [%] norm.6 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page 9 of 78

193 Laminate Open Hole Tension Properties (OHT) -- (CTD) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Tension Strength [ksi] Page 9 of 78

194 Laminate Open Hole Tension Properties (OHT) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUEAA A M MGM HFUEAA A M LGM HFUEAA A M LGM HFUEA4A A M LGM HFUEAA A M LGM HFUEAA A M LGM HFUEAA A M LGM HFUEBA B M LGM HFUEBA B M LGM HFUEBA B M LGM HFUEBA B M 4..4 LGM HFUEBA B M LGM HFUEBA B M LGM HFUECA C M LGM HFUECA C M LGM HFUECA C M LGM HFUECA* C M HFUECA C M LGM HFUECA C M LGM *Specimen has uneven grip marks due to thickness taper Average 4. Average norm Standard Dev..595 Standard Dev. norm.845 Coeff. of Var. [%].48 Coeff. of Var. [%] norm.57 Min Min Max. 4. Max Number of Spec. 8 Number of Spec. 8 Page 94 of 78

195 Laminate Open Hole Tension Properties (OHT) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Tension Strength [ksi] Page 95 of 78

196 Laminate Open Hole Tension Properties (OHT) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUEAAD A M..46 DGM.7.84 HFUEABD A M DGM.7. HFUEACD A M DGM HFUEADD A M DGM.7.6 HFUEAAD A M DGM HFUEABD A M DGM.7.77 HFUEACD A M..46 DGM.7.9 HFUEBAD B M.6.46 DGM.7.6 HFUEBBD B M.9.45 MGM HFUEBCD B M DGM.7.7 HFUEBDD B M.9.45 DGM.7.59 HFUEBAD B M AGM HFUEBBD B M.7.46 DGM.7.77 HFUEBCD B M DGM.7.8 HFUEBDD B M.8.46 MGM.7.84 HFUECAD C M.5.45 DGM.7.9 HFUECBD C M DGM.7.7 HFUECCD C M DGM.7.6 HFUECDD C M DGM.7. HFUECAD C M..45 DGM HFUECBD C M DGM.7.96 HFUECCD C M.6.46 DGM.7.64 Average.548 Average norm Standard Dev..589 Standard Dev. norm.544 Coeff. of Var. [%].89 Coeff. of Var. [%] norm.695 Min..554 Min Max..68 Max Number of Spec. Number of Spec. Page 96 of 78

197 Laminate Open Hole Tension Properties (OHT) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Tension Strength [ksi] Page 97 of 78

198 4.8 Open Hole Tension Properties Laminate Open Hole Tension Properties (OHT) -- (CTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUFA6B A M LGM HFUFA7B A M LGM HFUFA8B A M LGM HFUFA6B A M LGM HFUFA7B A M LGM HFUFA8B A M LGM HFUFA9B A M LGM HFUFB6B B M LGM HFUFB7B B M LGM HFUFB8B B M LGM HFUFB6B B M LGM HFUFB7B B M LGM HFUFB8B B M LGM HFUFC6B C M LGM HFUFC7B C M LGM HFUFC8B C M LGM HFUFC6B C M LGM HFUFC7B C M LGM HFUFC8B C M LGM Average 6.95 Average Average norm Standard Dev..474 Standard Dev. norm.45 Coeff. of Var. [%].868 Coeff. of Var. [%] norm.99 Min Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page 98 of 78

199 Laminate Open Hole Tension Properties (OHT) -- (CTD) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Tension Strength [ksi] Page 99 of 78

200 Laminate Open Hole Tension Properties (OHT) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUFAA A M LGM HFUFAA A M LGM HFUFAA A M LGM.7 7. HFUFA4A A M LGM HFUFAA A M 7..8 LGM HFUFAA A M LGM HFUFAA A M LGM HFUFBA B M LGM HFUFBA B M LGM HFUFBA B M LGM HFUFBA B M LGM HFUFBA B M LGM HFUFBA B M LGM HFUFCA C M LGM HFUFCA C M LGM HFUFC4A C M LGM HFUFCA C M LGM HFUFCA C M LGM HFUFCA C M LGM Average Average Average norm Standard Dev Standard Dev. norm.8 Coeff. of Var. [%] Coeff. of Var. [%] norm Min Min. Min Max Max. Max Number of Spec. 9 9 Number of Spec. 9 Page of 78

201 Laminate Open Hole Tension Properties (OHT) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Tension Strength [ksi] Page of 78

202 Laminate Open Hole Tension Properties (OHT) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUFAAD A M LGM HFUFABD A M LGM HFUFACD A M LGM HFUFADD A M LGM HFUFAAD A M LGM HFUFABD A M LGM HFUFACD A M LGM HFUFADD A M LGM HFUFBAD B M LGM HFUFBBD B M LGM HFUFBCD B M LGM HFUFBDD B M LGM HFUFBAD B M LGM HFUFBBD B M LGM HFUFBCD B M LGM HFUFBDD B M LGM HFUFCAD C M LGM HFUFCBD C M LGM HFUFCCD C M LGM HFUFCAD C M LGM HFUFCBD C M LGM HFUFCCD C M LGM Average 8.8 Average Average norm Standard Dev..456 Standard Dev. norm.587 Coeff. of Var. [%].56 Coeff. of Var. [%] norm.7 Min. 75. Min. Min Max Max. Max Number of Spec. Number of Spec. Page of 78

203 Laminate Open Hole Tension Properties (OHT) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Open Hole Tension Strength [ksi] Page of 78

204 4.9 Filled-Hole Tension Properties Laminate Filled Hole Tension Properties (FHT) -- (CTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU4A5B A M LGM HFU4A6B A M LGM HFU4A7B A M LGM HFU4A9B A M LGM HFU4A5B A M LGM HFU4A6B A M LGM HFU4A7B A M LGM HFU4B7B B M LGM HFU4B8B B M LGM HFU4B9B B M LGM HFU4B7B B M LGM HFU4B8B B M LGM HFU4B9B B M LGM HFU4C5B C M LGM.7 5. HFU4C6B C M LGM/MGM HFU4C7B C M LGM HFU4C5B C M LGM HFU4C6B C M LGM HFU4C7B C M LGM/MGM Average Average Average norm Standard Dev..9 Standard Dev. norm.95 Coeff. of Var. [%].964 Coeff. of Var. [%] norm.698 Min Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page 4 of 78

205 Laminate Filled Hole Tension Properties (FHT) -- (CTD) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page 5 of 78

206 Laminate Filled Hole Tension Properties (FHT) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU4AA A M LGM HFU4AA A M LGM HFU4AA A M LGM HFU4A4A A M LGM HFU4AA A M LGM.7 5. HFU4AA A M LGM HFU4AA A M LGM HFU4BA B M LGM HFU4BA B M LGM HFU4BA B M LGM HFU4BA B M LGM HFU4BA B M LGM HFU4BA B M LGM HFU4CA C M LGM HFU4CA C M LGM HFU4CA C M LGM HFU4CA C M LGM HFU4CA C M LGM HFU4CA C M LGM Average 54.6 Average Average norm Standard Dev..647 Standard Dev. norm.644 Coeff. of Var. [%].6 Coeff. of Var. [%] norm.8 Min. 5. Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page 6 of 78

207 Laminate Filled Hole Tension Properties (FHT) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page 7 of 78

208 Laminate Filled Hole Tension Properties (FHT) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU4AAD A M MGM HFU4ABD A M MGM HFU4ACD A M MGM HFU4AED A M MGM HFU4AAD A M MGM HFU4ABD A M MGM HFU4AED A M MGM HFU4BAD B M MGM HFU4BBD B M MGM HFU4BCD B M MGM HFU4BAD B M MGM HFU4BBD B M MGM HFU4BCD B M MGM HFU4CAD C M MGM HFU4CCD C M MGM HFU4CDD C M MGM HFU4CAD C M MGM HFU4CBD C M MGM HFU4CCD C M MGM Average Average Average norm Standard Dev..7 Standard Dev. norm.65 Coeff. of Var. [%].7 Coeff. of Var. [%] norm.965 Min. 5.8 Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page 8 of 78

209 Laminate Filled Hole Tension Properties (FHT) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page 9 of 78

210 4. Filled-Hole Tension Properties Laminate Filled Hole Tension Properties (FHT) -- (CTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU5A5B A M LGM HFU5A6B A M AGM/LGM HFU5A7B A M MGM HFU5A8B A M MGM HFU5A5B A M LGM HFU5A6B A M LGM HFU5A9B A M LGM HFU5B5B B M LGM HFU5B6B B M LGM HFU5B9B B M LGM HFU5B5B B M LGM HFU5B6B B M LGM HFU5B7B B M LGM HFU5C5B C M LGM HFU5C6B C M LGM HFU5C9B C M LGM HFU5C5B C M LGM HFU5C6B C M LGM HFU5C7B C M LGM Average 46.7 Average Average norm Standard Dev..659 Standard Dev. norm.854 Coeff. of Var. [%].4 Coeff. of Var. [%] norm.86 Min Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page of 78

211 Laminate Filled Hole Tension Properties (FHT) -- (CTD) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page of 78

212 Laminate Filled Hole Tension Properties (FHT) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU5AA A M AGM HFU5AA A M AGM HFU5A4A A M AGM HFU5AA A M AGM HFU5AA A M AGM HFU5A4A A M AGM HFU5BA B M AGM HFU5BA B M AGM HFU5BA B M AGM HFU5BA B M AGM HFU5BA B M AGM HFU5B4A B M AGM HFU5CA C M AGM HFU5CA C M AGM HFU5C4A C M AGM HFU5CA C M AGM HFU5CA C M AGM HFU5C4A C M AGM Average Average Average norm Standard Dev..855 Standard Dev. norm.8 Coeff. of Var. [%].95 Coeff. of Var. [%] norm.86 Min Min. Min Max Max. Max Number of Spec. 8 Number of Spec. 8 Page of 78

213 Laminate Filled Hole Tension Properties (FHT) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page of 78

214 Laminate Filled Hole Tension Properties (FHT) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU5AAD A M MGM/ HFU5ABD A M MGM HFU5ACD A M MGM HFU5ADD A M MGM HFU5AAD A M MGM HFU5ABD A M MGM HFU5AED A M MGM HFU5BAD B M MGM HFU5BBD B M MGM.7 5. HFU5BCD B M MGM HFU5BDD B M MGM HFU5BAD B M MGM.7 6. HFU5BBD B M MGM HFU5BCD B M MGM HFU5CAD C M MGM HFU5CBD C M MGM HFU5CCD C M MGM HFU5CAD C M MGM HFU5CBD C M MGM HFU5CCD C M MGM Average Average Average norm Standard Dev..689 Standard Dev. norm.689 Coeff. of Var. [%].889 Coeff. of Var. [%] norm.96 Min Min. Min Max. 7.4 Max. Max Number of Spec. Number of Spec. Page 4 of 78

215 Laminate Filled Hole Tension Properties (FHT) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page 5 of 78

216 4. Filled-Hole Tension Properties Laminate Filled Hole Tension Properties (FHT) -- (CTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU6A6B A M LGM/AGM HFU6A7B A M LGM HFU6A8B A M LGM HFU6A9B A M LGM/AGM HFU6A7B A M LGM HFU6A8B A M LGM HFU6A9B A M LGM HFU6B5B B M LGM HFU6B6B B M LGM HFU6B7B B M LGM HFU6B5B B M LGM HFU6B7B B M LGM HFU6B8B B M LGM HFU6C7B C M LGM HFU6C8B C M LGM HFU6C9B C M LGM HFU6C5B C M LGM HFU6C6B C M LGM HFU6C8B C M LGM Average Average Average norm Standard Dev..497 Standard Dev. norm.66 Coeff. of Var. [%].684 Coeff. of Var. [%] norm 4.6 Min. 6.4 Min. Min Max. 7.5 Max. Max Number of Spec. 9 Number of Spec. 9 Page 6 of 78

217 Laminate Filled Hole Tension Properties (FHT) -- (CTD) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page 7 of 78

218 Laminate Filled Hole Tension Properties (FHT) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU6AA A M AGM HFU6AA A M AGM HFU6AA A M AGM HFU6A4A A M AGM HFU6AA A M AGM HFU6AA A M AGM HFU6A4A A M AGM HFU6BA B M AGM HFU6BA B M AGM HFU6B4A B M AGM HFU6BA B M AGM HFU6BA B M AGM HFU6B4A B M AGM HFU6CA C M AGM HFU6CA C M AGM HFU6C4A C M AGM HFU6CA C M AGM HFU6CA C M AGM HFU6C4A C M AGM Average Average Average norm Standard Dev..694 Standard Dev. norm.944 Coeff. of Var. [%].579 Coeff. of Var. [%] norm.978 Min Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page 8 of 78

219 Laminate Filled Hole Tension Properties (FHT) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page 9 of 78

220 Laminate Filled Hole Tension Properties (FHT) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen HEXCEL Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU6AAD A M LGM HFU6ABD A M LGM HFU6ACD A M LGM HFU6AAD A M LGM HFU6ABD A M LGM HFU6ACD A M LGM HFU6ADD A M LGM HFU6BAD B M LGM HFU6BBD B M LGM HFU6BCD B M LGM HFU6BAD B M LGM HFU6BBD B M LGM HFU6BCD B M LGM HFU6CAD C M LGM HFU6CBD C M LGM HFU6CCD C M LGM HFU6C9D C M LGM HFU6CAD C M LGM HFU6CCD C M LGM Average 79.7 Average Average norm Standard Dev..75 Standard Dev. norm.66 Coeff. of Var. [%].86 Coeff. of Var. [%] norm. Min Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page of 78

221 Laminate Filled Hole Tension Properties (FHT) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Filled Hole Tension Strength [ksi] Page of 78

222 4. Open Hole Compression Properties Laminate Open Hole Compression Properties (OHC) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUGAA A M LGM HFUGAA A M LGM HFUGAA A M LGM HFUGA4A A M LGM HFUGAA A M LGM HFUGAA A M LGM HFUGAA A M LGM HFUGBA B M LGM HFUGBA B M LGM HFUGB4A B M LGM HFUGBA B M LGM HFUGBA B M LGM HFUGB4A B M LGM HFUGCA C M LGM HFUGCA C M LGM HFUGC4A C M LGM HFUGCA C M LGM HFUGCA C M LGM HFUGC4A C M LGM Average Average Average norm Standard Dev..957 Standard Dev. norm.8 Coeff. of Var. [%]. Coeff. of Var. [%] norm.77 Min Min. Min Max Max. Max Number of Spec. 9 Number of Spec. 9 Page of 78

223 Laminate Open Hole Compression Properties (OHC) -- (RTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Open Hole Compression Strength [ksi] Page of 78

224 Laminate Open Hole Compression Properties (OHC) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUGA7D A M LGM.7.4 HFUGA8D A M LGM.74.9 HFUGA9D A M LGM.74.6 HFUGAAD A M LGM.74.6 HFUGA7D A M LGM.7.4 HFUGA8D A M LGM HFUGA9D A M LGM HFUGB6D B M LGM HFUGB7D B M LGM HFUGB8D B M LGM.7.5 HFUGBAD B M LGM.7.78 HFUGB6D B M LGM.7.8 HFUGB7D B M LGM HFUGB8D B M LGM.7.46 HFUGC6D C M LGM HFUGC7D C M LGM HFUGC8D C M LGM.7.77 HFUGC9D C M LGM.7.98 HFUGC6D C M LGM.7 4. HFUGC7D C M LGM HFUGC8D C M LGM Average.456 Average Average norm.7.9 Standard Dev..97 Standard Dev. norm.75 Coeff. of Var. [%].98 Coeff. of Var. [%] norm.9 Min..54 Min. Min Max Max. Max Number of Spec. Number of Spec. Page 4 of 78

225 Laminate Open Hole Compression Properties (OHC) -- (ETW) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Open Hole Compression Strength [ksi] Page 5 of 78

226 4. Open Hole Compression Properties Laminate Open Hole Compression Properties (OHC) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUHAA A M 4..4 MGM HFUHAA A M MGM HFUHAA A M MGM HFUHA4A A M MGM HFUHAA A M LGM HFUHAA A M LGM HFUHAA A M LGM HFUHBA B M LGM HFUHBA B M LGM HFUHBA B M LGM HFUHBA B M LGM HFUHBA B M LGM HFUHBA B M LGM HFUHCA C M LGM HFUHCA C M LGM HFUHC4A C M LGM HFUHCA C M LGM HFUHCA C M LGM HFUHCA C M LGM.7 4. Average 4.78 Average norm Standard Dev..547 Standard Dev. norm. Coeff. of Var. [%].7 Coeff. of Var. [%] norm 5.7 Min. 9.6 Min Max Max Number of Spec. 9 Number of Spec. 9 Page 6 of 78

227 Laminate Open Hole Compression Properties (OHC) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Compression Strength [ksi] Page 7 of 78

228 Laminate Open Hole Compression Properties (OHC) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUHA7D A M LGM HFUHA8D A M LGM HFUHA9D A M LGM HFUHAAD A M LGM HFUHA6D A M LGM HFUHA7D A M MGM HFUHA8D A M MGM.7 6. HFUHB6D B M LGM HFUHB7D B M LGM HFUHB8D B M MGM HFUHB7D B M LGM HFUHB8D B M 6..7 LGM HFUHB9D B M LGM HFUHC6D C M LGM HFUHC7D C M LGM.7 6. HFUHC8D C M LGM HFUHC6D C M LGM HFUHC7D C M LGM HFUHC8D C M LGM Average 7. Average norm Standard Dev..98 Standard Dev. norm.4 Coeff. of Var. [%].44 Coeff. of Var. [%] norm 4.65 Min. 5.7 Min Max Max Number of Spec. 9 Number of Spec. 9 Page 8 of 78

229 Laminate Open Hole Compression Properties (OHC) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Compression Strength [ksi] Page 9 of 78

230 4.4 Open Hole Compression Properties Laminate Open Hole Compression Properties (OHC) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUIAA A M AGM HFUIAA A M AGM HFUIAA A M AGM HFUIA4A A M LGM HFUIAA A M LGM HFUIAA A M LGM HFUIAA A M LGM HFUIBA B M LGM HFUIBA B M LGM HFUIBA B M LGM HFUIBA B M LGM HFUIBA B M LGM HFUIBA B M LGM HFUICA C M LGM HFUICA C M LGM HFUICA C M LGM HFUICA C M LGM HFUICA C M LGM HFUICA C M LGM Average 64.9 Average norm Standard Dev..49 Standard Dev. norm.4 Coeff. of Var. [%].59 Coeff. of Var. [%] norm.78 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page of 78

231 Laminate Open Hole Compression Properties (OHC) -- (RTD) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Compression Strength [ksi] Page of 78

232 Laminate Open Hole Compression Properties (OHC) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Modes [in] [ksi] HFUIA7D A M LGM HFUIA8D A M LGM HFUIAAD A M LGM HFUIABD A M LGM HFUIA6D A M LGM HFUIA7D A M 5..4 LGM HFUIA8D A M LGM HFUIB6D B M LGM HFUIB7D B M LGM HFUIB8D B M LGM HFUIB6D B M LGM HFUIB7D B M LGM HFUIB8D B M LGM HFUIC6D C M LGM HFUIC7D C M LGM HFUIC8D C M LGM HFUIC6D C M LGM HFUIC7D C M LGM HFUIC8D C M LGM Average 49. Average norm Standard Dev..45 Standard Dev. norm.757 Coeff. of Var. [%] Coeff. of Var. [%] norm 5.7 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page of 78

233 Laminate Open Hole Compression Properties (OHC) -- (ETW) Normalized Strength Hexcel AS4 UNI Laminate Open Hole Compression Strength [ksi] Page of 78

234 4.5 Filled-Hole Compression Properties Laminate Filled Hole Compression Properties (FHC) -- (RTD) Strength HEXCEL 855 AS4 UNI normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU7AA A M MGM HFU7AA A M MGM HFU7AA A M MGM HFU7A4A A M MGM HFU7AA A M MGM HFU7AA A M MGM HFU7A4A A M MGM HFU7BA B M MGM HFU7BA B M MGM HFU7BA B M MGM HFU7BA B M MGM HFU7BA B M MGM HFU7B5A B M MGM HFU7CA C M LGF HFU7CA C M MGM HFU7C5A C M MGM HFU7CA C M MGM HFU7CA C M MGM HFU7CA C M MGM Average 78.8 Average norm Standard Dev..59 Standard Dev. norm.75 Coeff. of Var. [%].98 Coeff. of Var. [%] norm 4.45 Min. 7.9 Min Max Max Number of Spec. 9 Number of Spec. 9 Page 4 of 78

235 Laminate Filled Hole Compression Properties (FHC) -- (RTD) Normalized Strength HEXCEL 855 AS4 UNI Laminate Filled Hole Compression Strength [ksi] Page 5 of 78

236 Laminate Filled Hole Compression Properties (FHC) -- (ETW) Strength HEXCEL 855 AS4 UNI normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU7A7D A M LGF HFU7A8D A M LGF HFU7A9D A M LGF HFU7AAD A M MGF HFU7A6D A M LGF HFU7A7D A M LGF HFU7AAD A M LGF HFU7B6D B M MGF HFU7B7D B M LGF HFU7B8D B M LGF HFU7B6D B M LGF HFU7B7D B M LGF HFU7B8D B M LGF HFU7C6D C M MGF HFU7C7D C M LGM HFU7C8D C M MGF HFU7C6D C M LGM HFU7C7D C M LGF HFU7C8D C M LGF Average 56.4 Average norm Standard Dev..8 Standard Dev. norm. Coeff. of Var. [%].4 Coeff. of Var. [%] norm.848 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page 6 of 78

237 Laminate Filled Hole Compression Properties (FHC) -- (ETW) Normalized Strength HEXCEL 855 AS4 UNI Laminate Filled Hole Compression Strength [ksi] Page 7 of 78

238 4.6 Filled-Hole Compression Properties Laminate Filled Hole Compression Properties (FHC) -- (RTD) Strength HEXCEL 855 AS4 UNI normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU8AA A M MGF HFU8AA A M MGF HFU8AA A M MGF HFU8A6A A M MGF HFU8AA A M LGO HFU8A4A A M LGO HFU8A5A A M LGO HFU8BA B M LGO HFU8BA B M LGO HFU8BA B M MGO HFU8B4A B M LGO HFU8BA B M MGO HFU8BA B M MGO HFU8BA B M LGO HFU8CA C M LGO HFU8CA C M LGO HFU8CA C M LGO HFU8CA C M LGO HFU8CA C M LGO HFU8CA C M LGO Average Average norm Standard Dev..99 Standard Dev. norm.86 Coeff. of Var. [%].65 Coeff. of Var. [%] norm.67 Min Min Max. 64. Max Number of Spec. Number of Spec. Page 8 of 78

239 Laminate Filled Hole Compression Properties (FHC) -- (RTD) Normalized Strength HEXCEL 855 AS4 UNI Cure Cycl e # Laminate Filled Hole Compression Strength [ksi] Page 9 of 78

240 Laminate Filled Hole Compression Properties (FHC) -- (ETW) Strength HEXCEL 855 AS4 UNI normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU8A7D A M LGF HFU8A8D A M LGF HFU8A9D A M LGF HFU8ABD A M LGF HFU8A6D A M LGF HFU8A7D A M LGF HFU8A9D A M LGF HFU8B6D B M LGF.7 4. HFU8B7D B M LGF HFU8B8D B M LGF HFU8B6D B M LGF HFU8B7D B M LGF HFU8B8D B M MGF HFU8C6D C M LGF HFU8C7D C M MGF HFU8C8D C M LGF HFU8C6D C M LGF HFU8C7D C M LGF HFU8C8D C M LGF Average 9.94 Average norm Standard Dev.. Standard Dev. norm.46 Coeff. of Var. [%] Coeff. of Var. [%] norm 5.7 Min Min Max Max Number of Spec. 9 Number of Spec. 9 Page 4 of 78

241 4.7 Filled-Hole Compression Properties Laminate Filled Hole Compression Properties (FHC) -- (RTD) Strength HEXCEL 855-AS4 Uni normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU9AA A M 5..4 MGM HFU9AA A M MGM HFU9A5A A M AGM.7.98 HFU9A6A A M AGM HFU9AA A M.6.45 LGM,AGM HFU9A4A A M LGF,LGM.7.8 HFU9A5A A M AGM.7.4 HFU9BA B M LGM,AGM HFU9BA B M LGM.7.8 HFU9B4A B M.6.46 LGM HFU9B5A B M LGM,AGM HFU9BA B M LGM,LGF HFU9B4A B M LGM HFU9B5A B M LGM HFU9CA C M LGM.7.89 HFU9C4A C M LGM,LGF.7.6 HFU9C5A C M LGM,LGF HFU9CA C M.58.4 LGF HFU9CA C M LGM,LGF HFU9CA C M LGM,LGF Average.97 Average norm.7.46 Standard Dev Standard Dev. norm 4.6 Coeff. of Var. [%] 4.59 Coeff. of Var. [%] norm 4.64 Min. 88. Min Max..66 Max Number of Spec. Number of Spec. Page 4 of 78

242 Laminate Filled Hole Compression Properties (FHC) -- (RTD) Normalized Strength HEXCEL 855-AS4 Uni Cure Cycl e # Laminate Filled Hole Compression Strength [ksi] Page 4 of 78

243 Laminate Filled Hole Compression Properties (FHC) -- (ETW) Strength HEXCEL 855-AS4 Uni normalizing t ply [in].74 Specimen HEXCEL HEXCEL Cure Prepreg Cure Cycle Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFU9A7D A M LGF HFU9A8D A M LGO HFU9AAD A M LGF HFU9ACD A M LGO HFU9A6D A M LGF HFU9A7D A M LGF.7 8. HFU9A9D A M LGF HFU9B6D B M MGF HFU9B7D B M MGF HFU9B9D B M MGF HFU9B6D B M LGF HFU9B7D B M LGF HFU9B8D B M LGF HFU9C6D C M LGO HFU9C7D C M LGF HFU9C8D C M LGF HFU9C6D C M LGO HFU9C7D C M LGO HFU9C8D C M LGF Average 76.9 Average norm Standard Dev Standard Dev. norm Coeff. of Var. [%] 6.6 Coeff. of Var. [%] norm 6.86 Min. 67. Min Max Max Number of Spec. 9 Number of Spec. 9 Page 4 of 78

244 Laminate Filled Hole Compression Properties (FHC) -- (ETW) Normalized Strength HEXCEL 855-AS4 Uni Cure Cycl e # Laminate Filled Hole Compression Strength [ksi] Page 44 of 78

245 4.8 Single Shear Bearing Properties Laminate Single Shear Bearing Properties (SSB) -- (RTD) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg % Offset Avg. Specimen # Plies in Comments Avg. t ply % Offset Strength norm Number Batch # Cycle Lot # Strength [ksi] Thickn. [in] Laminate [in] [ksi] HFUAA A M BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS* HFUA4A A M BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS*.7.4 HFUAA A M.8. 6 BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS*.7.9 HFUBA B M.7. 6 BI / % OFFSET FOR UBS*.7 4. HFUBA B M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS*.7.9 HFUBA B M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS*.7. HFUCA C M BI / % OFFSET FOR UBS*.7.7 HFUCA C M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS*.7.96 Ultimate Bearing Strength / BI: B:Bearing, :first hole, I: Inapplicable (not on bolt, nut or head side) Average 7.49 Average.7.4 Standard Dev. 6.8 Standard Dev Coeff. of Var. [%] 6.4 Coeff. of Var. [%] 7.4 Min Min Max Max..75. Number of Spec. 9 Number of Spec. 9 9 Page 45 of 78

246 Laminate Single Shear Bearing Properties (SSB) -- (RTD) Strength & Modulus Hexcel AS4 UNI Laminate Bearing Strength [ksi] - Page 46 of 78

247 Laminate Single Shear Bearing Properties (SSB) -- (ETW) Strength & Modulus Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg % Offset Avg. Specimen # Plies in Comments Avg. t ply % Offset Strength norm Number Batch # Cycle Lot # Strength [ksi] Thickn. [in] Laminate [in] [ksi] HFUA6D A M BI / % OFFSET FOR UBS* HFUA7D A M BI / % OFFSET FOR UBS*.7 6. HFUA8D A M BI / % OFFSET FOR UBS* HFUA9D A M.4. 6 BI / % OFFSET FOR UBS* HFUA6D A M BI / % OFFSET FOR UBS* HFUA7D A M BI / % OFFSET FOR UBS* HFUA8D A M..5 6 BI / % OFFSET FOR UBS* HFUB6D B M BI / % OFFSET FOR UBS* HFUB7D B M BI / % OFFSET FOR UBS* HFUB8D B M.6. 6 BI / % OFFSET FOR UBS* HFUB9D B M BI / % OFFSET FOR UBS* HFUB6D B M BI / % OFFSET FOR UBS*.7.46 HFUB7D B M.4. 6 BI / % OFFSET FOR UBS* HFUB8D B M BI / % OFFSET FOR UBS* HFUC6D C M BI / % OFFSET FOR UBS* HFUC7D C M BI / % OFFSET FOR UBS*.7.97 HFUC8D C M BI / % OFFSET FOR UBS*.7.6 HFUC6D C M BI / % OFFSET FOR UBS* HFUC7D C M BI / % OFFSET FOR UBS* HFUC8D C M BI / % OFFSET FOR UBS* Ultimate Bearing Strength / BI: B:Bearing, :first hole, I: Inapplicable (not on bolt, nut or head side) Average.97 Average Standard Dev. 8. Standard Dev. 7.6 Coeff. of Var. [%] 8.8 Coeff. of Var. [%] 7.8 Min. 89. Min Max..46 Max Number of Spec. Number of Spec. Page 47 of 78

248 Laminate Single Shear Bearing Properties (SSB) -- (ETW) % Offset Strength Hexcel AS4 UNI Laminate Bearing Strength [ksi] Page 48 of 78

249 4.9 Single Shear Bearing Properties Laminate Single Shear Bearing Properties (SSB) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg % Offset Avg. Specimen # Plies in Comments Avg. t ply % Offset Strength norm Number Batch # Cycle Lot # Strength [ksi] Thickn. [in] Laminate [in] [ksi] HFUAA A M BI / % OFFSET FOR UBS* HFUAA A M.95.4 BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS* HFUA4A A M 5..4 BI / % OFFSET FOR UBS*.7.7 HFUAA A M BI / % OFFSET FOR UBS*.7.96 HFUAA A M BI / % OFFSET FOR UBS*.74.6 HFUAA A M BI / % OFFSET FOR UBS* HFUBA B M..5 BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUCA C M 7.9. BI / % OFFSET FOR UBS* HFUCA C M.65.5 BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS*.7.6 Ultimate Bearing Strength / BI: B:Bearing, :first hole, I: Inapplicable (not on bolt, nut or head side) Average. Average Standard Dev. 4.4 Standard Dev. 5.4 Coeff. of Var. [%] 4. Coeff. of Var. [%] 5.66 Min Min Max. 8. Max Number of Spec. 9 Number of Spec. 9 9 Page 49 of 78

250 Laminate Single Shear Bearing Properties (SSB) -- (RTD) Strength & Modulus Hexcel AS4 UNI Laminate Bearing Strength [ksi] Page 5 of 78

251 Laminate Single Shear Bearing Properties (SSB) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg % Offset Avg. Specimen # Plies in Comments Avg. t ply % Offset Strength norm Number Batch # Cycle Lot # Strength [ksi] Thickn. [in] Laminate [in] [ksi] HFUA6D A M.45.4 BI / % OFFSET FOR UBS* HFUA7D A M BI / % OFFSET FOR UBS* HFUA8D A M BI / % OFFSET FOR UBS* HFUA9D A M BI / % OFFSET FOR UBS* HFUAAD A M BI / % OFFSET FOR UBS* HFUA6D A M BI / % OFFSET FOR UBS* HFUA7D A M BI / % OFFSET FOR UBS* HFUA8D A M BI / % OFFSET FOR UBS* HFUAAD A M BI / % OFFSET FOR UBS* HFUB6D B M BI / % OFFSET FOR UBS* HFUB7D B M 9.9. BI / % OFFSET FOR UBS* HFUB8D B M BI / % OFFSET FOR UBS* HFUB9D B M BI / % OFFSET FOR UBS* HFUB6D B M BI / % OFFSET FOR UBS* HFUB7D B M BI / % OFFSET FOR UBS* HFUB8D B M BI / % OFFSET FOR UBS* HFUB9D B M BI / % OFFSET FOR UBS* HFUC6D C M BI / % OFFSET FOR UBS* HFUC7D C M BI / % OFFSET FOR UBS* HFUC8D C M BI / % OFFSET FOR UBS* HFUC9D C M BI / % OFFSET FOR UBS* HFUC6D C M BI / % OFFSET FOR UBS* HFUC7D C M BI / % OFFSET FOR UBS* HFUC8D C M BI / % OFFSET FOR UBS* HFUC9D C M BI / % OFFSET FOR UBS* Ultimate Bearing Strength / BI: B:Bearing, :first hole, I: Inapplicable (not on bolt, nut or head side) Average Average Standard Dev Standard Dev Coeff. of Var. [%] 9.88 Coeff. of Var. [%].44 Min Min Max..45 Max Number of Spec. 5 Number of Spec. 5 5 Page 5 of 78

252 Laminate Single Shear Bearing Properties (SSB) -- (ETW) % Offset Strength Hexcel AS4 UNI Laminate Bearing Strength ksi] Page 5 of 78

253 4. Single Shear Bearing Properties Laminate Single Shear Bearing Properties (SSB) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg % Offset Avg. Specimen # Plies in Comments Avg. t ply % Offset Strength norm Number Batch # Cycle Lot # Strength [ksi] Thickn. [in] Laminate [in] [ksi] HFUAA A M BI / % OFFSET FOR UBS*.7.49 HFUAA A M BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS* HFUA4A A M BI / % OFFSET FOR UBS*.7.97 HFUAA A M BI / % OFFSET FOR UBS* HFUAA A M.8.45 BI / % OFFSET FOR UBS* HFUAA A M BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS*.7.68 HFUBA B M BI / % OFFSET FOR UBS* HFUB4A B M.8.45 BI / % OFFSET FOR UBS*.7.88 HFUBA B M BI / % OFFSET FOR UBS*.69.6 HFUBA B M.4.44 BI / % OFFSET FOR UBS* HFUBA B M BI / % OFFSET FOR UBS* HFUCA C M BI / % OFFSET FOR UBS*.7.48 HFUCA C M BI / % OFFSET FOR UBS*.7.48 HFUC4A C M..4 BI / % OFFSET FOR UBS* HFUCA C M.9.4 BI / % OFFSET FOR UBS* HFUCA C M.7.4 BI / % OFFSET FOR UBS* HFUC4A C M.58.4 BI / % OFFSET FOR UBS* Ultimate Bearing Strength / BI: B:Bearing, :first hole, I: Inapplicable (not on bolt, nut or head side) Average 8.76 Average Standard Dev Standard Dev. 6. Coeff. of Var. [%] 6.9 Coeff. of Var. [%] 6. Min. 9.4 Min Max Max..7.5 Number of Spec. 9 Number of Spec. 9 9 Page 5 of 78

254 Laminate Single Shear Bearing Properties (SSB) -- (RTD) % OffsetStrength Hexcel AS4 UNI Cure Cycl e # Laminate Bearing Strength [ksi] Page 54 of 78

255 Laminate Single Shear Bearing Properties (SSB) -- (ETW) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg % Offset Avg. Specimen # Plies in Comments Avg. t ply % Offset Strength norm Number Batch # Cycle Lot # Strength [ksi] Thickn. [in] Laminate [in] [ksi] HFUA6D A M BI / % OFFSET FOR UBS* HFUA7D A M BI / % OFFSET FOR UBS* HFUA8D A M BI / % OFFSET FOR UBS* HFUA9D A M BI / % OFFSET FOR UBS* HFUAAD A M BI / % OFFSET FOR UBS* HFUA6D A M BI / % OFFSET FOR UBS* HFUA7D A M BI / % OFFSET FOR UBS* HFUA8D A M BI / % OFFSET FOR UBS* HFUB6D B M BI / % OFFSET FOR UBS* HFUB7D B M BI / % OFFSET FOR UBS* HFUB8D B M BI / % OFFSET FOR UBS* HFUB9D B M BI / % OFFSET FOR UBS* HFUB7D B M BI / % OFFSET FOR UBS* HFUB8D B M BI / % OFFSET FOR UBS* HFUB9D B M BI / % OFFSET FOR UBS* HFUC6D C M BI / % OFFSET FOR UBS* HFUC7D C M BI / % OFFSET FOR UBS* HFUC8D C M BI / % OFFSET FOR UBS* HFUC9D C M BI / % OFFSET FOR UBS* HFUC6D C M BI / % OFFSET FOR UBS* HFUC7D C M BI / % OFFSET FOR UBS* HFUC8D C M BI / % OFFSET FOR UBS* Ultimate Bearing Strength / BI: B:Bearing, :first hole, I: Inapplicable (not on bolt, nut or head side) Average 87. Average Standard Dev Standard Dev Coeff. of Var. [%] 7.78 Coeff. of Var. [%] 7.89 Min. 67. Min Max Max Number of Spec. Number of Spec. Page 55 of 78

256 Laminate Single Shear Bearing Properties (SSB) -- (ETW) % Offset Strength Hexcel AS4 UNI Cure Cycl e # Laminate Bearing Strength [ksi] Page 56 of 78

257 4. Compression Strength After Impact Properties Laminate Compression After Impact Properties (CAI) -- (RTD) Strength Hexcel AS4 UNI normalizing t ply [in].74 Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Measured Impact Strength Avg. Specimen # Plies in Failure Avg. t ply Strength norm Number Batch # Cycle Lot # # Energy (in-lbf) [ksi] Thickn. [in] Laminate Mode [in] [ksi] HFUKAA A M LDM HFUKAA A M LDM HFUKAA A M LDM HFUKA4A A M LDM HFUKA5A A M LDM HFUKA6A A M LDM HFUKA7A A M LDM Average Average norm Standard Dev..54 Standard Dev. norm.4 Coeff. of Var. [%].49 Coeff. of Var. [%] norm.565 Min Min Max Max Number of Spec. 7 Number of Spec. 7 Page 57 of 78

258 Laminate Compression After Impact Properties (CAI) -- (RTD) Normalized Strength Hexcel AS4 UNI Cure Cycl e # Laminate Compression After Impact Strength (CAI) [ksi] Page 58 of 78

259 4. Interlaminar Tension Properties Laminate Interlaminar Tension Strength Properties (ILT) -- (CTD) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Curved Beam Interlaminar Tension Avg. Specimen # Plies in Number Batch # Cycle Lot # # Strength [lb] Strength [ksi] Thickn. [in] Laminate HFUMA9B A M HFUMAAB A M HFUMABB A M HFUMACB A M HFUMADB A M HFUMAEB A M HFUMAFB A M HFUMAGB A M Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec. 8 8 Page 59 of 78

260 Laminate Curved Beam Strength Properties (CBS) -- (CTD) Measured Strength Hexcel AS4 UNI Laminate Curved Beam Strength (CBS) [lb] Laminate Interlaminar Tension Strength (ILT) -- (CTD) Measured Strength Hexcel AS4 UNI Laminate Interlaminar Tension Strength (ILT) [ksi] Page 6 of 78

261 Laminate Interlaminar Tension Strength Properties (ILT) -- (RTD) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Curved Beam Interlaminar Tension Avg. Specimen # Plies in Number Batch # Cycle Lot # # Strength [lb] Strength [ksi] Thickn. [in] Laminate HFUMAA A M HFUMAA A M HFUMAA A M HFUMA4A A M HFUMA5A A M HFUMA6A A M Average Standard Dev Coeff. of Var. [%] Min Max Number of Spec. 6 6 Page 6 of 78

262 Laminate Curved Beam Strength Properties (CBS) -- (RTD) Measured Strength Hexcel AS4 UNI Laminate Curved Beam Strength (CBS) [lb] Laminate Interlaminar Tension Strength (ILT) -- (RTD) Measured Strength Hexcel AS4 UNI Laminate Interlaminar Tension Strength (ILT) [ksi] Page 6 of 78

263 Laminate InterlaminarTension Strength Properties (ILT) -- (ETW) Strength Hexcel AS4 UNI Specimen Hexcel Hexcel Cure Prepreg Cure Cycle Curved Beam Interlaminar Tension Avg. Specimen # Plies in Number Batch # Cycle Lot # # Strength [lb] Strength [ksi] Thickn. [in] Laminate HFUMAHD A M HFUMAID A M HFUMAJD A M HFUMAKD A M HFUMALD A M HFUMAMD A M Average Standard Dev Coeff. of Var. [%].94.4 Min..7.8 Max Number of Spec. 6 6 Page 6 of 78

264 Laminate Curved Beam Strength Properties (CBS) -- (ETW) Measured Strength Hexcel AS4 UNI Laminate Curved Beam Strength (CBS) lb] Laminate Interlaminar Tension Strength (ILT) -- (ETW) Measured Strength Hexcel AS4 UNI 4 6 Laminate Interlaminar Tension Strength (ILT) [ksi] Page 64 of 78

265 5. Shear Stress vs. Shear Strain, RTD Shear Stress vs Shear Strain Shear Stress (psi) Shear Strain (micro in/in) 6. FLUID SENSITIVITY COMPARISON Fluid Sensitivity was not performed on this reinforcement. It was performed on Hexcel 855 IM7 and AS4 Plain Weave. Page 65 of 78

266 7. MOISTURE CONDITIONING CHARTS 7. Longitudinal Tension Thinnest Panel NCAMP Hexcel AS4 Uni..9.8 % Weight Gain (Total) HFUJA Time (days) Page 66 of 78

267 7. Short Beam Strength- Thickest Panel.5 Hexcel - SBS - ETW Chart. % Weight Gain (Total).5. HFUQA Time (days) The chart above is missing two readings due to a chamber malfunction, but specimens remained in the chamber and were conditioned to equilibrium. The rest of the curves can be found on the CD that accompanies this report. Page 67 of 78

268 8. DMA Results DMA Results Summary Hexcel / Cessna HXUDX XX Wet Onset Storage Modulus Peak of Tangent Delta Sample # Average Average Tg [ C] Tg [ F] Tg [ C] Tg [ F] HFUDA W HFUDA W HFUDA X HFUDA X HFUDB W HFUDB W HFUDB X HFUDB X HFUDC W HFUDC W HFUDC X HFUDC X Average.4 Table 8-: DMA Wet Results Page 68 of 78

269 DMA Results Summary Hexcel / Cessna HXUDX XX Dry Onset Storage Modulus Peak of Tangent Delta Sample # Average Average Tg [ C] Tg [ F] Tg [ C] Tg [ F] HFUDA W HFUDA W HFUDA X HFUDA X HFUDB W HFUDB W HFUDB X HFUDB X HFUDC W HFUDC W HFUDC X HFUDC X Average 4.7 Table 8-: DMA Dry Results Page 69 of 78

270 8. DMA Wet Batch A The charts below are only examples. The remaining files can be obtained from the CD provided with this report. Page 7 of 78

271 8. DMA Dry Batch A Page 7 of 78

272 9. TMA Results The TMA results were tested at Hexcel. Specimens were taken from the same panels as DMA and wet and dry testing was tested concurrently. NCAMP and Hexcel investigated the close numbers between the dry and wet TMA but no determination was made as to the cause. Below is the discussion that took place at Hexcel. NCAMP is open to further discussion. From Bill Gillam: I do know that drying will occur to some degree during testing and would be dependent on thickness; however in my experience even TMA specimens should still show a knock-down in Tg for wet conditioning. Typically a requirement for the wet conditioned specimens is to keep them submerged in solution right up until the time of sample prep/testing. [NCAMP: Specimens were conditioned and then sent overnight to Hexcel in a sealed plastic bag with a moist towel]. Obviously a thick DMA specimen would retain moisture in the matrix to a higher degree during testing than a thin TMA sliver. I would expect the delta between wet and dry to be greater with DMA than TMA however I would always expect the wet knock-down, even with TMA. Regards, Bill From: Bolke, Robert Sent: Tuesday, June 8, : AM To: Kristin (Strole) Marlett; Gleason, Michael; Lallas, George Cc: Wu, Joy; Gillam, William R. Subject: RE: Dry TMA results Kristin- I put together the TMA scans from March 9 when we tested the Dry specimens and October 9 when we tested the Wet specimens. I agree that it is surprising that the TG for the Wet specimens is higher than for the Dry specimens. I am trying to think of anything that may have caused this. Do you know if the only difference between the samples that were sent to Salt Lake is the Wet conditioning? [Yes that is the only difference]. Do you know if the Wet samples were dried with the Dry samples before they were conditioned? [I am not sure of this but they were dried under the same parameters per the test plan]. Additionally I wonder if the size of sample may have an effect on the difference between the DMA and TMA results. When we do TMA the sample is only a small sliver. It may be possible that the samples was dried during testing while the oven ramped to temperature. The DMA samples are also a lot bigger than the TMA sample and may possibly hold in the moisture better. Rob Bolke Hexcel Corp. robert.bolke@hexcel.com office: Page 7 of 78

273 Table 9-: Dry TMA Results Page 7 of 78

274 Table 9-: Wet TMA Results Page 74 of 78

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