ANALYTICAL REPORT. Attn: Richard Boelter

Transcription

1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Community Drive Suite South Burlington, VT 00 Tel: (0)0- TestAmerica Job ID: 00-- TestAmerica Sample Delivery Group: 00- Client Revision: For: ARCADIS U.S. Inc Massena Facility, Route East Chevrolet Road Massena, New York Attn: Richard Boelter Authorized for release by: /0/0 :0: PM Kathryn Kelly Project Manager I kathryn.kelly@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

2 Client: ARCADIS U.S. Inc Table of Contents TestAmerica Job ID: 00-- SDG: 00- Cover Page Table of Contents Definitions/Glossary Case Narrative Detection Summary Client Sample Results Surrogate Summary QC Sample Results QC Association Summary Lab Chronicle Certification Summary Method Summary Sample Summary Chain of Custody Field Data Sheets Receipt Checklists Page of /0/0

3 Client: ARCADIS U.S. Inc Qualifiers Air - GC Semi VOA Qualifier Qualifier Description U Indicates the analyte was analyzed for but not detected. * Recovery or RPD exceeds control limits X Surrogate is outside control limits Glossary Definitions/Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample EDL Estimated Detection Limit EPA United States Environmental Protection Agency MDL Method Detection Limit ML Minimum Level (Dioxin) ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RL Reporting Limit RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Job ID: 00-- SDG: 00- Page of /0/0

4 Case Narrative Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Job ID: 00-- Laboratory: Narrative CASE NARRATIVE Client: ARCADIS U.S. Inc Project: RACER - Central Foundry Massena NY Report Number: 00-- With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. Calculations are performed before rounding to avoid round-off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. This report has been revised to reflect the correct sample identifications for the samples in this sample set. The laboratory incorrectly identified the samples in the sample set as AIRB-, AIRA- and AIR-. The sample ID's have been updated to AIRB-(), AIRA-() and AIR-(). In addition to this the chain of custody was not included in the original report. RECEIPT The samples were received on //0; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was. C. PCB IN AIR Samples AIRB-, AIRA- and AIR- were analyzed for PCB in Air in accordance with TO-A. The samples were prepared on //0 and analyzed on //0. DCB Decachlorobiphenyl failed the surrogate recovery criteria low for AIR-. Refer to the QC report for details. Aroclor 0 failed the recovery criteria low for LCS 00-0/-B. Refer to the QC report for details. No other difficulties were encountered during the TO-A analyses. All other quality control parameters were within the acceptance limits. Page of /0/0

5 Detection Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Client Sample ID: AIRB-() Lab Sample ID: 00-- Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Aroclor ug/m PUF TO-A Client Sample ID: AIRA-() Lab Sample ID: 00-- Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Aroclor ug/m PUF TO-A Client Sample ID: AIR-() Lab Sample ID: 00-- Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Aroclor ug/m PUF TO-A Page of /0/0

6 Client: ARCADIS U.S. Inc Client Sample ID: AIRB-() Date Collected: // : Date Received: // :0 Sample Container: PUF/XAD Method: TO-A - Pesticides and PCBs in Ambient Air Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID: 00-- Analyzed Aroclor U ug/m PUF // : // :0 Aroclor U Aroclor U Aroclor 0.00 Aroclor U Aroclor U Aroclor U * Aroclor U Aroclor U Surrogate %Recovery Qualifier Unit D Dil Fac ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // :0 Limits Analyzed DCB Decachlorobiphenyl - // : // :0 Tetrachloro-m-xylene 0-0 // : // :0 Client Sample ID: AIRA-() Date Collected: // :0 Date Received: // :0 Sample Container: PUF/XAD Method: TO-A - Pesticides and PCBs in Ambient Air Analyte Result Qualifier RL MDL Dil Fac Lab Sample ID: 00-- Analyzed Aroclor U ug/m PUF // : // : Aroclor U Aroclor U Aroclor 0.00 Aroclor U Aroclor U Aroclor U * Aroclor U Aroclor U Unit D Dil Fac ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : Surrogate %Recovery Qualifier Limits Analyzed DCB Decachlorobiphenyl - // : // : Tetrachloro-m-xylene 0-0 // : // : Dil Fac Client Sample ID: AIR-() Date Collected: // : Date Received: // :0 Sample Container: PUF/XAD Lab Sample ID: 00-- Method: TO-A - Pesticides and PCBs in Ambient Air Analyte Result Qualifier RL Aroclor U ug/m PUF // : // : Aroclor U Aroclor U Aroclor 0.00 Aroclor U Aroclor U Aroclor U * Aroclor U Aroclor U MDL Unit D Analyzed Dil Fac ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : ug/m PUF // : // : Page of /0/0

7 Client: ARCADIS U.S. Inc Client Sample ID: AIR-() Date Collected: // : Date Received: // :0 Sample Container: PUF/XAD Surrogate %Recovery Client Sample Results Qualifier Limits TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID: 00-- Analyzed DCB Decachlorobiphenyl X - // : // : Tetrachloro-m-xylene 0-0 // : // : Dil Fac Page of /0/0

8 Surrogate Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Method: TO-A - Pesticides and PCBs in Ambient Air Prep Type: Percent Surrogate Recovery (Acceptance Limits) DCB DCB TCX TCX Lab Sample ID Client Sample ID (-) (-) (0-0) (0-0) 00-- AIRB-() 00-- AIRA-() 00-- AIR-() X X LCS 00-0/-B Lab Control Sample MB 00-0/-B Method Blank Surrogate Legend DCB = DCB Decachlorobiphenyl TCX = Tetrachloro-m-xylene Page of /0/0

9 Client: ARCADIS U.S. Inc Method: TO-A - Pesticides and PCBs in Ambient Air QC Sample Results TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID: MB 00-0/-B Client Sample ID: Method Blank Prep Type: Analysis : 0 Prep : MB MB Analyte Result Qualifier RL Aroclor- 0. U ug/m PUF // : // :0 Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor 0 Aroclor Aroclor Surrogate MDL Unit D Analyzed Dil Fac 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 0. U ug/m PUF // : // :0 MB %Recovery MB Qualifier Limits Analyzed DCB Decachlorobiphenyl - // : // :0 Tetrachloro-m-xylene 0-0 // : // :0 Lab Sample ID: LCS 00-0/-B Client Sample ID: Lab Control Sample Prep Type: Analysis : 0 Prep : Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Aroclor ug/m PUF - Aroclor * ug/m PUF - Surrogate LCS %Recovery LCS Qualifier Limits DCB Decachlorobiphenyl - Tetrachloro-m-xylene 0-0 Limits Dil Fac Page of /0/0

10 QC Association Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Air - GC Semi VOA Prep : Lab Sample ID Client Sample ID Prep Type Matrix Method Prep 00-- AIRB-() Air 0C 00-- AIRA-() Air 0C 00-- AIR-() Air 0C LCS 00-0/-B Lab Control Sample Air 0C MB 00-0/-B Method Blank Air 0C Analysis : 0 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep 00-- AIRB-() Air TO-A 00-- AIRA-() Air TO-A 00-- AIR-() Air TO-A LCS 00-0/-B Lab Control Sample Air TO-A MB 00-0/-B Method Blank Air TO-A Page of /0/0

11 Lab Chronicle Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Client Sample ID: AIRB-() Lab Sample ID: 00-- Date Collected: // : Date Received: // :0 Prep Type Type Method Run Dilution Factor or Analyzed Analyst Prep 0C // : MLT TAL BUR Number Analysis TO-A 0 // :0 SLD TAL BUR Client Sample ID: AIRA-() Lab Sample ID: 00-- Date Collected: // :0 Date Received: // :0 Prep Type Type Method Run Dilution Factor or Analyzed Analyst Prep 0C // : MLT TAL BUR Number Analysis TO-A 0 // : SLD TAL BUR Client Sample ID: AIR-() Lab Sample ID: 00-- Date Collected: // : Date Received: // :0 Prep Type Laboratory References: Type Method Run Dilution Factor or Analyzed Analyst Prep 0C // : MLT TAL BUR Number Analysis TO-A 0 // : SLD TAL BUR TAL BUR =, 0 Community Drive, Suite, South Burlington, VT 00, TEL (0)0- Lab Lab Lab Page of /0/0

12 Certification Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Laboratory: All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification ID Expiration Date Connecticut State Program PH DE Haz. Subst. Cleanup Act (HSCA) State Program NA 0-- Florida NELAC E 0-0- Louisiana NELAC 0-0- Maine State Program VT Minnesota NELAC New Hampshire NELAC New Jersey NELAC VT 0-0- New York NELAC 0-0- Pennsylvania NELAC Rhode Island State Program LAO00-0- USDA Federal P Vermont State Program VT Virginia NELAC Page of /0/0

13 Client: ARCADIS U.S. Inc Method Summary TestAmerica Job ID: 00-- SDG: 00- Method Method Description Protocol Laboratory TO-A Pesticides and PCBs in Ambient Air EPA TAL BUR Protocol References: EPA = US Environmental Protection Agency Laboratory References: TAL BUR =, 0 Community Drive, Suite, South Burlington, VT 00, TEL (0)0- Page of /0/0

14 Client: ARCADIS U.S. Inc Sample Summary TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID Client Sample ID Matrix Collected Received 00-- AIRB-() Air // : // : AIRA-() Air // :0 // : AIR-() Air // : // :0 Page of /0/0

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17 Login Sample Receipt Checklist Client: ARCADIS U.S. Inc Job Number: 00-- Login Number: List Number: Creator: Marion, Greg T Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact., Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. N/A N/A N/A N/A N/A N/A N/A SDG Number: 00- List Source: Lab does not accept radioactive samples..ºc IR GUN ID /CF=0. Page of /0/0