In this Standard the comma has been adopted as the decimal sign. INDEX SECTION TITLE PAGE 1. SCOPE CLASSIFICATION... 3

Transcription

1 In this Standard the comma has been adopted as the decimal sign. INDEX SECTION TITLE PAGE 1. SCOPE CLASSIFICATION MATERIAL - CHARACTERISTICS AND PROPERTIES APPLICABLE DOCUMENTS DEFINITIONS LOT SHELF LIFE QUALITY ASSURANCE REQUIREMENTS QUALIFICATION Tests/Inspections for the Material Qualification Requalification Plans Notification and Tests Monitoring Test Equipment Test/Inspection Methods Evaluation Samples Availability of the Tested Material Reports/Results of Tests/Inspections SUPPLYING CONDITIONS FOR LOTS SUBSEQUENT TO QUALIFICATION Tests/Inspections to be performed by the Manufacturer Conformity Certification Package Transportation... 9 continue LIST OF EFFECTIVE PAGES st ISSUE: 27 Jun 02 PAG PAG PAG PAG ALL G THIS DOCUMENT CAN NOT BE USED, PUBLISHED NOR COMMUNICATED TO THIRD PARTIES OR REPRODUCED WITHOUT AUTHORIZATION OF THE ISSUING COMPANY. ISION REPORT RR_MEP10-075G WATER BASE PRIMER FOR COMPOSITE AND PLASTIC PARTS PAGE 1 of 10

2 continued INDEX SECTION TITLE PAGE 6.3 RECEIVING Tests/Inspections Rejection STORAGE PURCHASE ORDER...10 ANNEX 1 QUALIFIED PRODUCTS LIST- QPL...1 of A1 PAGE 2

3 1. SCOPE This Standard establishes the requirements for water base primer, two components, to be applied in composite and plastic parts as base to water base topcoat. 2. CLASSIFICATION 2.1 TYPES TYPE I: Conventional primer (VOC 300 g/l). TYPE II: Low VOC/high solids primer (VOC 70 g/l). 3. MATERIAL - CHARACTERISTICS AND PROPERTIES Material: water-reducible, two component primer, polyurethane base. TABLE 1: CHARACTERISTICS AND PROPERTIES ITEM CHARACTERISTIC AND PROPERTY 1 APPEARANCE 2 ODOR AND TOXICITY 3 STORAGE STABILITY MIXING RATIO SOLIDS CONTENT SPECIFIC GRAVITY SPECIFIED VALUE TYPE I TYPE II HOMOGENEOUS LIQUID, NO CAKING, FREE OF SKINS, GELLED PARTICLES WHEN VIEWED ON GLASS PLATE MATERIALS SHALL BE HEALTH SAFE DURING MIXING, APPLICATION AND CURE SHALL MEET ALL REQUIREMENTS AFTER 12 MONTHS STORAGE IN UNOPENED CONTAINERS AT 4 C TO 38 C (40 TO 100) F. STORAGE SHALL START AT DATE OF MANUFACTURING BASE HARDENER WATER BASE HARDENER MIXED BASE 1,30 ± 0,05 1,65 ± 0,05 HARDENER 1,01 ± 0,05 1,01 ± 0,05 MIXED 1,22 ± 0,05 1,39 ± 0,05 VOLATILE ORGANIC COMPOUND (VOC), MIXED (MAX) UNIT TEST/INSPECTION METHOD - VISUAL - - MONTH - g - % BY WEIGHT Kg/l ASTM D2369 ASTM D g/l - 8 POT LIFE (±20 C) 3 2,5 h ASTM D FLASH POINT (MIN) 10 VISCOSITY AT 20ºC (DIN CUP 4) 11 SPRAYING PROPERTIES BASE: NOT FLAMMABLE HARDENER: 43 MAX 10% WATER TO OBTAIN SPRAYED AND DRIED FILM ON ALUMINUM SHALL BE FREE OF DEFECTS C - s - - FED-STD-141 METHOD PAGE 3 continue

4 continued ITEM 12 TABLE 1: CHARACTERISTICS AND PROPERTIES CHARACTERISTIC AND SPECIFIED VALUE PROPERTY BASE HARDENER DRYING TIME, AT 21 C ± 2 C UNIT SET TO TOUCH 8 8 TACK FREE DRY HARD min DRY THROUGH FULL CURE 7 7 d TEST/INSPECTION METHOD ASTM D THEORETICAL COVERAGE (MIXED) 8 10 m 2 /l - RECOMMENDED DRY FILM ONE COAT 20 TO THICKNESS μm ASTM D1400 AS REFERENCE (1) TWO COATS 40 TO 60 NO LOSS OF ADHESION TO 15 DRY ADHESION SUBSTRATE NOR OF ENAMEL - ASTM D3359 TO PRIMER 16 WATER RESISTANCE NO FLAKING, BLISTERING OR LOSS OF ADHESION AFTER 24 HOURS IMMERSION, SHALL MEET - - THE REQUIREMENTS OF ADHESION TEST BURN LENGTH (MAX) 6 in 17 FLAMMABILITY SELF RBHA/14CFR PART 25 VERTICAL BURN EXTINGUISHING 15 sec APP. F, PART I (b), (4), (60 sec) TIME AMENDMENT 111 DRIPPING FLAME TIME 3 sec HEAT RELEASE TEST SMOKE DENSITY TEST AVERAGE PEAK HEAT RELEASE RATE AT 5 MINUTES (MAX) AVERAGE TOTAL HEAT RELEASED DURING FIRST 2 MINUTES (MAX) AVERAGE SPECIFIC OPTICAL SMOKE DENSITY AT 4 MINUTES (MAX) 25 kw/m 2 25 kw.min/m 2 50 OSD RBHA/14CFR PART 25 APP. F, PART IV, AMENDMENT 61 AND 66 RBHA/14CFR PART 25 APP. F, PART V, AMENDMENT 66 HAZARDOUSNESS SEE QPL SHELF LIFE (STORED IN THE CONDITIONS OF ITEM 6) BASE : 12 HARDENER: 6 MONTH - (1) On aluminum test panel. PAGE 4

5 4. APPLICABLE DOCUMENTS Embraer Standard MEP Polycarbonate Sheet Texturized. MEP Glass Fabrics Preimpregnated with Epoxy Resin, 121 C (250 F) Curing. NE Hazardous Materials - Classification and Identification. NE Aluminum and its Alloys Chemical - Conversion. NE Metallic Parts - Cleaning. Foreign Standards ASTM - American Society for Testing and Materials (USA) D Standard Test Method for Nondestructive Measurement of Dry Film Thickness of Nonconductive Coatings Applied to a Nonferrous Metal Base. D Standard Test Method for Density of Liquid Coatings, Inks, and Related Products. D Standard test Method for Drying, Curing, or Film Formation of Organic Coatings at Room Temperature. D Standard test Method for Volatile Content of Coatings. D Standard test Method for Gel Time and Peak Exothermic Temperature of Reacting Thermosetting Resins. D Standard Test Methods for Measuring Adhesion by Tape Test. D Standard Practice for Determining Volatile Organic Compound (V.O.C.) Content of Paint, and Related Coatings. FAA - Federal Airworthiness Administration FAR 25 - Airworthiness Standard - Transport Category Airplanes Section Interior Compartment. Federal Specification Standards (DoD - USA) FED-STD Paint, Varnish, Lacquer and Related Materials, Methods of Inspection, Sampling and Testing. ISO - International Organization for Standardization ISO Quality Assurance Requirements for Measuring Equipment. Part 1: Metrological Confirmation System for Measuring Equipment. 5. DEFINITIONS 5.1 LOT It is all material manufactured during a single and continuous manufacturing operation. 5.2 SHELF LIFE It is the period of time from it s manufacturing (synthesis, manufacturing, etc), in which the packed and stored material under some specific conditions keeps its physical and chemical properties adequate for use. PAGE 5

6 6. QUALITY ASSURANCE REQUIREMENTS 6.1 QUALIFICATION The manufacturer/supplier shall demonstrate to Embraer that the material meets all the requirements of this Standard TESTS/INSPECTIONS FOR THE MATERIAL QUALIFICATION The manufacturer is responsible for performing and documenting all the tests/inspections for the qualification of his product, as indicated on Table 1. NOTE The exemption of tests/inspections may be proposed to Embraer for analysis, always followed by technical evidences which justify such exemption. Embraer reserves the right to accept or not the manufacturer s proposal REQUALIFICATION The manufacturer/supplier shall inform Embraer of any change in the manufacturing method, area, or change of the equipments for the analysis of the necessity of the product requalification. The manufacturer/supplier may request the partial or total exemption of the requalification for the analysis by Embraer PLANS NOTIFICATION AND TESTS MONITORING The manufacturer/supplier shall allow the access of Embraer representatives to the tests areas. A plan indicating the test date and place shall be sent to Embraer, whenever required TEST EQUIPMENT The manufacturer shall use the calibrated equipments according to ISO When required, the laboratory shall be qualified by Embraer TEST/INSPECTION METHODS The test methods no covered by specific Standard shall be performed as follows: TEST PANEL PREPARATION Dimensions, material type and quantity of panels shall be according to Table 2. PAGE 6

7 ITEM OF TABLE 1 TABLE 2: TEST PANELS PREPARATION TEST TEST PANEL DIMENSION (mm) MATERIAL AND CONDITION 15 DRY ADHESION 75 x 150 IA, IB OR IC 16 WATER RESISTANCE 75 x 150 IC 17 FLAMMABILITY: VERTICAL BURN NECESSARY QUANTITY x 305 IC HEAT RELEASE TEST (150 x 150)+0-1,5 IC SMOKE DENSITY (73 x 73) ±1,5 IC 03 I) MATERIAL AND CONDITION OF TEST PANELS A: Compression Molded Epoxy Fiberglass 3 plies in accordance with MEP Style B: Polycarbonate according to MEP C: 2024 Aluminum Alloy, Clad, 0,5 mm thickness, treated with colored chemical conversion according to NE and primed according to this MEP material. II) CLEANING OF TEST PANELS The test panels ( ) shall be cleaned with solution according to NE prior to painting. III) PAINTING OF TEST PANELS - Mix the coating according to manufacturer s instructions. - Apply two coats to a total dry film thickness of (40 to 60)μm. - Flash off time is ± 30 minutes at 20 C before curing. - Allow to dry 168 hours minimum at 21 C to 26 C (75 ± 5 F) before testing. IV) TEST CONDITIONS Unless otherwise specified in section , test conditions shall be 21 C to 26 C (75 ± 5 F) and (30 to 60)% of relative humidity EVALUATION SAMPLING SAMPLES Whenever requested, the manufacturer/supplier shall send to Embraer samples of the material for evaluation along with the qualification test report informing the following: a) material quantity; b) PN, material designation and classification; c) lot number; and d) manufacturing date. PAGE 7

8 6.1.7 AVAILABILITY OF THE TESTED MATERIAL All sample of material used in the tests/inspections shall be separated from the lot, identified and allowed at the disposition of Embraer for a period of 1 year, minimum REPORTS/RESULTS OF TESTS/INSPECTIONS Records, reports, results and other documents regarding qualification shall be subject to approval by Embraer. Besides the information concerning the qualification test, these documents shall present the test methodology and information allowing the traceability of the qualified item, such as: - test date/place; - item PN; - lot number; - manufacturing date; and - Standards applicable to test instrumentation gauging, etc. Copy of these documents shall be filed and available at the manufacturer/supplier and at Embraer during at least 7 years. 6.2 SUPPLYING CONDITIONS FOR LOTS SUBSEQUENT TO QUALIFICATION TESTS/INSPECTIONS TO BE PERFORMED BY THE MANUFACTURER The manufacturer shall perform tests/inspections in each lot so as to guarantee the material with conformity the requirements of this Standard CONFORMITY CERTIFICATION In order to certify the material conformity with the requirements of this Standard, the manufacturer/supplier shall send for each lot the following documents: a) Conformity Certificate, containing: - PN, material designation and classification, - lot number and manufacturing date, - number of this Standard and revision letter, - number of Embraer Purchase Order, - number of lot analysis report (approval result); - text certifying the material conformity, signed by the quality responsible; and - statement confirming compliance with REACH (Registration, Evaluation, Authorization and Restrictions of Chemicals) updated legislation. PAGE 8

9 b) Test Report, containing: - lot number, - inspection level used, and - characteristics and properties, test/inspection methods, specified values, obtained values and measurement units. NOTE These documents shall be kept on file and available at the manufacturer/supplier and at Embraer during at least 7 years PACKAGE The package, hermetically sealed, without damages and infringement marks shall protect the material against mechanical, chemical and physical damages. The material shall be packed in metallic containers. NOTE Futher information on the material preservation shall be provided by the manufacturer/supplier. The original package of the material, besides other markings required by law, shall be identified with: a) PN, material designation and classification; b) number of this Standard and revision letter; c) manufacturer/supplier s name; d) lot number; e) net weight; f) manufacturing date and/or validity; g) usage, handling, and storage conditions; and h) Purchase Order number. NOTE A supplementary package is allowed provided that the quantity of original packages is informed and the identification requirements are met TRANSPORTATION The material shall be transported accordingly packed, identified and at storage conditions defined in item 7, so as to maintain its characteristics and properties. PAGE 9

10 6.3 RECEIVING TESTS/INSPECTIONS Embraer reserves the right to perform some or all the tests/inspections indicated in Table 1, and observe the limit of the elapsed shelf life (20% MAX), to verify the material conformity with the requirements specified in this Standard. The performance of these tests/inspections by Embraer does not release the manufacturer/supplier from the responsibility for the material conformance REJECTION All material lot which does not meet the requirements of this Standard shall be rejected. 7. STORAGE The material, in its original package, shall be stored: a) in an environment at temperature of (4 to 38) C ;90 % (MAX) % of relative humidity; b) in areas away from thermic sources, direct sunlight, dust, oxidants and other deterioration sources. 8. PURCHASE ORDER The following data, at least, shall be in the Purchase Order: a) PN, material designation and classification; b) number of this Standard and revision letter; c) required quantity; d) supplying conditions for lots subsequent to qualification (see 6.2); and e) request for a statement confirming compliance with REACH (Registration, Evaluation, Authorization and Restrictions of Chemicals) updated legislation /ANNEX 1 PAGE 10

11 ANNEX 1 QUALIFIED PRODUCTS LIST THE PRODUCTS LISTED BELOW HAVE BEEN QUALIFIED IN ACCORDANCE WITH THIS MEP. THE INCLUSION OF A PRODUCT IN THIS STANDARD DOES NOT RELEASE THE MANUFACTURER/SUPPLIER FROM COMPLIANCE WITH THE SPECIFICATION REQUIREMENTS. EMBRAER CODE (1) E E E E E E MATERIAL DESIGNATION, PN AND DIMENSION PRIMER,WATER BASE, WHITE- FOR COMPOSITES PARTS, TYPE I PN: INTERPLAN 1100B PRIMER DIM: CAN OF 3,6 kg PRIMER, WATER BASE, WHITE- FOR COMPOSITES PARTS, TIPE II PN: INTERPLAN 1200B DIM: CAN OF 5kg CATALYST FOR PAINT IP1083, PRIMER IP1100 AND IP1200, WATER BASED PN: IP1041 DIM: CAN OF 1,2 kg PRIMER, WATER BASE, GRAY FS , FOR COMPOSITE, TYPE II PN: INTERPLAN 1200B DIM: CAN OF 5 kg WATER BASE PRIMER FOR COMPOSITE ALEXIT-FST, BEIGE, TYPE II PN: ALEXIT-FST DIM: CAN OF 5 kg HARDENER FOR ALEXIT PRIMER PN: ALEXIT HARDENER DIM: CAN OF 1 kg HAZARDOUSNESS ONU NUMBER: NR GHS CLASS: H303, H305, H317 AND H335 ONU NUMBER: NR GHS CLASS: NR MANUFACTURER/ SUPPLIER (2) NOTES HSH AEROSPACE (I) --- MANKIEWICZ (II) TECHNICAL REPORT 170MAO025 (1) For the verification of other Embraer codes of qualified products in accordance with this Specification, refer to Embraer Material List -RME. (2) Manufacturer/Supplier s name and address: (I) HSH AEROSPACE FINISH NV Research Park Zone 1 De Haak, 3 B-1731 Zellik Belgium Phone: (II) MANKIEWICZ GEBR & CO Georg Wilhelm Strasse, 189 D Hamburg Germany Phone: 49 (0) Total of pages: 01 =============== MEP QPL PAGE 1 of A1