ANAMA Package & Container Testing Services, Inc.

Transcription

1 ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY Tel: (914) Fax: (914) DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING CERTIFICATION Page 1 of 62 Testing Performed by: ANAMA Package & Container Testing Services, Inc. (+CM) Approval 607 Fayette Avenue Mamaroneck, NY (914) Testing Performed for: County Road 1000 Godley, TX Mr. Matt Holzer (817) matt.holzer@corelab.com 4G Design Qualification Testing 350# DW Fibrebord Box With: Iteration 1: Grams; Grams & Kg Average Gross Weight Articles (B CUT ) Iteration 2: Kg Average Gross Weight Barrier Bags (D JEC) Iteration 3: Kg Average Gross Weight Barrier Bags (E KOD) Iteration 4: Kg Average Gross Weight Inner Boxes (C ACE) Iteration 5: Grams Average Gross Weight Anti-Stat Bags (G COR) u n 4G / Y 22.8 / S / ** USA / +CM0471 ** insert year the packaging is manufactured Anton Cotaj, Certification Officer

2 ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY Tel:(914) Fax: (914) Page 2 of 62 SECTION 1 - CERTIFICATION 4G Design Qualification Testing of the, Godley, TX 350# DW Fibrebord Box With: Iteration 1: Grams; Grams & Kg Average Gross Weight Articles (B CUT ) Iteration 2: Kg Average Gross Weight Barrier Bags (D JEC) Iteration 3: Kg Average Gross Weight Barrier Bags (E KOD) Iteration 4: Kg Average Gross Weight Inner Boxes (C ACE) Iteration 5: Grams Average Gross Weight Anti-Stat Bags (G COR) Requesting Party: Tel: (817) County Road 1000, PO Box matt.holzer@corelab.com Godley, TX Attn: Mr. Matt Holzer ANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under and certifies that the, Godley, TX packaging prepared as for transport, referenced above and tested in September & October 2017 has passed the Standards of the US Department of Transportation, Title 49CFR, Performance Oriented Packaging Standards; Section 178. This package is also certified under IMDG and UN Recommendations of the Committee of Experts on the Transportation of Dangerous Goods. It is the responsibility of the shipper / end user to ensure appropriate use. The use of other packaging methods or components other than those documented in this report may render this report invalid. SUMMARY OF PERFORMANCE TESTS Test Specification Test Level Time Results Drop 49 CFR m N/A Pass Stacking 49 CFR kg 24 Hours Pass Cobb 49 CFR gr/m² 30 Minutes Pass Vibration 49 CFR CPM 60 Minutes Pass Test Report #0471 UN Marking (49 CFR ) 4G / Y 22.8 / S / ** USA / +CM0471 Package Identification Code 4G - Fibreboard Box (49 CFR ) Performance Standard Y - Packaging meets Packing Group II and III Tests Authorized Gross Mass 22.8 kg (50.16 lbs) "S" Designation Denotes Inner Packaging Year of Manufacture ** Insert year the packaging is manufactured Country Authorizing The Mark USA DOT UN Third-Party Certification Agency (+CM) ANAMA Package & Container Testing Services, Inc. Approval Third Party Packaging Identification Number +CM0471 Anton Cotaj, Certification Officer

3 Page 3 of 62 SECTION 2 - Description of The Tested Package Iteration 1 (Box B CUT ): Forty-Eight (48) 90.8 grams average gross weight each small spiral wound fiberboard tube rings filled with Copper Innerts, placed in 2 layers, 24 tubes per layer; three (3) 22.5 grams average gross weight each solid product filled foil/plastic laminate bags each folded and placed into three (3) larger spiral wound fiberboard tube rings, one (1) ring on each corner of the cutter primary inner packagings and one (1) 15.7 kg gross weight casing cutter assembly secondary inner packaging, all installed within a center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard top and bottom pads and fibreboard/honeycomb side fillers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #1-1 - Reference Section 8 for drawings Small Fiberboard Tube Rings Count (per outer packaging) 48 Style Spiral wound fiberboard Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN2.125 X 1.25 Part # TUBE (2.125 x 1.25 x.555) Material 26 Plies of High Density Paperboard Laminated with PVOH Adhesive Size (mm, OD) 69.3 x 52.5 Size (mm, ID) 42.4 x 52.5 Caliper 13.2 mm Tare Weight 80.1 grams each Average Gross Weight 90.8 grams Average Net Weight 10.7 grams Notes Arranged 4 X 6 in two (2) layers within the box INNERT MATERIAL Count 18 Style/Description Trapezoidal Shaped Copper Frame Manufacturer Owen Oil Tools, Godley, TX Size (mm, OD) 31.9 x 25.8 x 44.2 Caliper 1.66 mm Tare Weight 40.0 grams each Average Gross Weight (as tested) 64.2 grams Average Net Weight (as tested) 24.3 grams Test Material Putty Notes These innerts were placed within the small fibre tubes INNERT TEST MATERIAL Count 18 Description White putty material Average Net Weight (as tested) 24.3 grams Notes This material was placed within copper frame

4 Page 4 of 62 INNER PACKAGING DETAIL #1-2 (Barrier Bag) Reference Section 8 for drawings Type Barrier Bag Count 3 Style/Description Laminated watervaporproof, greaseproof, flexible barrier bag with heat-sealed bottom and sides Type MIL-PRF-131J, Type 1, Class 1, Style 1 Manufacturer Ludlow Coated Products, Inc., Columbus, GA Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S Owen Part # BAG-0305-F100 3 X 5 Foil Bag Material of Construction Plastic/foil/plastic laminate, 5 Mil nominal gauge Minimum Thickness mm (0.0045") Nominal Thickness mm (0.005") Bursting Strength 65 lbs/inch² Dimension (mm, OD), W X L, flat 128 x 130 Dimension (mm, ID), W X L, flat 90 x 110 Bottom Seam Width, mm 18.4 mm Side Seam Width, mm 18.4 mm Tare Weight 4.4 grams Average Gross Weight (as tested) 22.5 grams Average Net Weight (as tested) 18.1 grams Print INNERT Each bag was filled with solid product (putty). Top of bags was left open to Method of Closure place the putty, bag was then folded and placed individually in the center of each large fibreboard tube ring (Refer to Section 7.2) INNERT TEST MATERIAL Count 3 Description White putty material Average Net Weight (as tested) 18.1 grams Notes This material was placed inside each barrier bag INNER PACKAGING DETAIL #1-3 - Reference Section 8 for drawings Large Fiberboard Tube Rings Count (per outer packaging) 3 Style Spiral wound fiberboard Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN3.45 X 1.25 Part # TUBE (3.45 x1.25 x.555) Material 26 Plies of High Density Paperboard Laminated with PVOH Adhesive Size (mm, OD) x 31.7 Size (mm, ID) 89.6 x 31.7 Caliper 12.0 mm Tare Weight 91.2 grams each Average Gross Weight grams Average Net Weight 22.5 grams Notes These tubes were placed next to the three cutter corners. Each tube contains one (1) solid product filled folded barrier bag

5 Page 5 of 62 INNER PACKAGING DETAIL #1-4 Reference Section 8 for drawings Type Large Casing Cutter Count 1 Style/Description Machined steel cylindrical shape with steel cover Manufacturer Owen Oil Tools, Godley, TX Nominal Thickness 1.35 mm Dimension (mm, OD) x 74.7 (without lid) Dimension (mm, OD) x 44.5 (without lid) Dimension (mm, ID) x 90.4 (with lid) Print/Label CUT R3; Gross Weight (as tested) kg with lid Lid Dimension (mm, OD) x 38.5 Gross Weight (as tested) 5.94 kg Lid Screws Count 4 Style Allen screws Dimension (mm, OD) 7.9 x 17.0, 4.75 mm diameter body Weight 2.7 grams each Note This article was placed on the bottom of shipper Overall Inner Packaging Gross Weight (OIP1GW) kg

6 Page 6 of 62 Iteration 2 (Box D JEC): Ten (10) 1.27 kg average gross solid product filled metal-in film laminate bags, inner packagings installed sideways 2 layers high within the center special slotted fibreboard container (International Box Code 0204) outer packaging backfilled with bubble sheets void space fillers and honeycomb top and bottom pads. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #2-1 (ESD Shielding Bag) Reference Section 8 for drawings Type Metal-in Film Laminate Bag Count 10 Style/Description Lead free RoHs Compliant, Stat Shielding bag with heat-sealed bottom and sides Type RoHs Compliant 0217/617 Desco Part # Owen Part # BAG-0715-F100 7 X 15 Foil Bag Manufacturer Desco Industries, Chino, CA Material of Construction Metal-in film laminate, 3 Mil nominal gauge Minimum Thickness mm Nominal Thickness mm Dimension (mm, OD), W X L, flat 197 x 375 Dimension (mm, ID), W X L, flat 175 x 327 Bottom Seam Width, mm 8.1 mm Side Seam Width, mm 8.1 mm Top Seam Width, mm 4.2 mm, 40 mm away from top edge Tare Weight 11.5 grams Average Gross Weight (as tested) 1272 grams Print EMI/STATIC SHIELD Test material was inserted into bag. Air was expelled from bag, then bag was Method of Closure heat-sealed. Each bag contains 1 sand filled steel tube with plastic caps and 2 Desiccant bags. PRODUCT/ARTICLES - TEST MATERIAL DETAIL #2-1-1 Reference Section 8 for drawings Type Metal cylinder with plastic plugs Count 10 Style/Description Machined metal halo cylinder Material of Construction Steel Manufacturer Owen Oil Tools, Godley, TX Nominal Thickness 1.65 mm Dimension (mm, OD) 57.5 x Dimension (mm, ID) 52.9 x Average Tare Weight 442 grams Average Gross Weight 1210 grams Plastic Plugs Count 2 Material of Construction Red plastic Manufacturer/Supplier Caplugs, Inc., Buffalo, NY Nominal Thickness 1.20 mm Dimension (mm, OD) 59.2 x 23.3 Tare Weight 6.3 grams each Test Material Sand Note These articles were inserted individually within the barrier bags

7 Page 7 of 62 INNER PACKAGING DETAIL # Reference Section 8 for drawings Desiccant Bag Count 20 (2 per bag) Manufacturer Desiccare, Inc., Reno, NV Material Silica Gel, Indicating Silica Gel, Clay, Molecular Sieve and Carbon Owen Part # PAK Dimension (mm, OD), D X H 59.6 x 11.5 x 88.7 Weight 22.0 grams each Notes 2 desiccant bags were placed inside each barrier bag PRODUCT/ARTICLES ADDITIONAL WEIGHT TEST MATERIAL DETAIL #2-2 Type Metal Blocks Count 8 Style/Description Solid steel block 1 X 76 x 76 x 4.6, grams 2 X 76 x 76 x 3.35, grams each Dimension (mm, OD), D X H 3 X 76 x 76 x 9.4, grams each 2 X 76 x kg each Overall Gross Weight 9.41 kg Note These steel blocks and cylinders were placed on both sides of the barrier bags (to reach the desired weight) Overall Inner Packaging Gross Weight (OIP2GW) kg

8 Page 8 of 62 Iteration 3 (Box E KOD): Nine (9) 2.38 kg average gross solid product filled metal-in film laminate bags, inner packagings installed upright 3 X 3 within the center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard partition system and fibreboard and honeycomb top and bottom pads. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #3-1 (ESD Shielding Bag) Reference Section 8 for drawings Type Metal-in Film Laminate Bag Count 9 Style/Description Lead free RoHs Compliant, Stat Shielding bag with heat-sealed side seams Type RoHs Compliant 0217/617 Desco Part # Owen Part # BAG-0715-F100 7 X 15 Foil Bag Manufacturer Desco Industries, Chino, CA Material of Construction Metal-in film laminate, 3 Mil nominal gauge Minimum Thickness mm Nominal Thickness mm Dimension (mm, OD), W X L, flat 200 x 315 Dimension (mm, ID), W X L, flat 178 x 185 Side Seam Width, mm 9.5 mm Top Seam Width, mm 4.0 mm, 22 mm away from top edge Tare Weight 9.6 grams Average Gross Weight (as tested) 2.38 kg Print EMI/STATIC SHIELD Test material was inserted into bag. Air was expelled from bag, then bag was Method of Closure heat-sealed. Each bag contains 1 steel cylinder filled fibre tube with plastic caps

9 Page 9 of 62 PRODUCT/ARTICLES - TEST MATERIAL DETAIL #3-1-1 Reference Section 8 for drawings Style Spiral wound fiberboard Count 9 Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN3.45 X 1.25 Owen Part # TUBE ( x1.25 x.555) Material 26 Plies of High Density Paperboard Laminated with PVOH Adhesive Size (mm, OD) 66.7 x Size (mm, ID) 54.2 x Caliper 6.2 mm Tare Weight grams each Average Gross Weight 2320 grams Average Net Weight grams Plastic Plugs Count 2 Owen Part # CAP-A-1875A Material of Construction Blue plastic Manufacturer/Supplier Alliance Plastics Company, Erie, PA Nominal Thickness 0.98 mm Dimension (mm, OD) 68.3 x 26.4 Tare Weight 8.2 grams each Test Material 50.4 x (mm, OD), grams steel cylinder Note These tubes were inserted individually within the Metal-in Film Laminate Bags TUBE SEALING TAPE Count 2 (per tube) Description 3M Scotch brand Supper 33+ vinyl electrical tape Width 19 mm Length 930 mm Thickness 0.16 mm Tare Weight 3.2 grams Notes This tape was used to seal plastic caps around to the fibre tube PRODUCT/ARTICLES - TEST MATERIAL DETAIL # Reference Section 8 for drawings Fibre Tube Pads Count 36 (4 per tube) Manufacturer DanHil Containers, LTD, Temple, TX Material 200# DW BC-flute corrugate Owen Part # DIV Dimension (mm, OD), D X H 47.0 x 45.6 Thickness 4.62 mm Weight 1.72 grams each Notes 2 pads were placed over and 2 below the steel cylinder inside each tube Overall Inner Packaging Gross Weight (OIP3GW) kg

10 Page 10 of 62 Iteration 4 (Box C ACE): Five (5) 4.38 kg average gross solid product filled DW fibreboard boxes, inner packagings installed sideways 2 layers high within the center special slotted fibreboard container (International Box Code 0204) outer packaging backfilled with bubble sheets void space fillers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #4-1 (Inner Box) Reference Section 8 for drawings Type Fiberboard Box Count 5 Style Center Special Slotted Container (CSSC), FEDCO Style: 0204 Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # File # 9551 DanHil # XXx Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA Dimension (mm, OD), L X W X H 113 x 113 x 253 Dimension (mm, ID), L X W X H 100 x 100 x 229 Number of Walls - Flute Type Double-Wall BC-Flute BMC (Box Marked Certification) 275# (42/26/26/26/42) Tare Weight grams Tested Basis Weight (lbs/1000ft²) ( ) Tested Caliper 6.53 mm Method of Joining Panels Folded inside and stitched with seven (7) 12.5 mm wide staples Mfr's Joint Flap Size 42 mm Mfr's Joint Location 5-2 corner as per the ASTM diagram Top Flap Gap/Meet Inner: Meet Outer: Meet Bottom Flap Gap/Meet Inner: Meet Outer: Meet Print None Tare Weight grams Average Gross Weight 4.38 kg Closure Method (Refer to Section 7 for Closing Instruction and Section 8 for Specs) Closure 3/4" C34 Stick Staples S-1396 Uline Description 18 mm (3/4") long, 31 mm (1-1/4") crown galvanized metal staples Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S-1396 Owen Part # STA S Top Closure Two (2) 0.8 grams each staples along the flap seam, 38 mm (1-1/2") away from boxes outside edges, 38 mm (1-1/2") apart Bottom Closure Two (2) 0.8 grams each staples along the flap seam, 38 mm (1-1/2") away from boxes outside edges, 38 mm (1-1/2") apart Note These boxes were placed sideways, 3 on bottom layer and 2 on top layer

11 Page 11 of 62 PRODUCT/ARTICLES ADDITIONAL WEIGHT TEST MATERIAL DETAIL #4-1-1 Type Metal Blocks Count 11 Style/Description Solid steel block Dimension (mm, OD), D X H 2 X 76 x 76 x 3.2, 155 grams each 9 X 76 x 76 x 9.4, 431 grams each Overall Gross Weight 4.18 kg Note These steel blocks and cylinders were placed on both sides of the barrier bags (to reach the desired weight) INNER PACKAGING DETAIL #4-1-2 Reference Section 8 for drawings Type Bubble Wrap Count 3 Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16") Dimension (mm, OD) flat 305 x 1120 Tare Weight 15.3 grams Note These bubble sheets were folded and placed over, below and around the inner articles Overall Inner Packaging Gross Weight (OIP4GW) 21.9 kg

12 Page 12 of 62 Iteration 5 (Box G COR): Fifty (50) 400 grams average gross solid product filled zip-locked anti-stat bags, inner packagings installed 5 x 5 2-layers high within the center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard partition systems and fibreboard and honeycomb top and bottom pads and dividers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #5-1 (ESD Shielding Bag) Reference Section 8 for drawings Type Anti-Stat Zip-Lock Bag Count 50 Style/Description Zip-lock bag with heat-sealed side seams Uline Part # S-3701 Owen Part # BAG Manufacturer Uline, Inc., Waukegan, IL Material of Construction Pink anti-stat LDPE, 3 Mil nominal gauge Minimum Thickness mm Nominal Thickness mm Dimension (mm, OD), W X L, flat x Dimension (mm, ID), W X L, flat 98.6 x Side Seam Width, mm 1.5 mm Top Seam Width, mm 3.5 mm, 22 mm away from top edge Tare Weight 5.1 grams Average Gross Weight (as tested) grams Print None Method of Closure Test material was inserted into bag, then bag was press-and-seal closed. Each bag contains 1 steel cylinder and 1 Desiccant bag PRODUCT/ARTICLES - TEST MATERIAL DETAIL #5-2 Type Metal cylinder Count 50 Style/Description Machined metal halo cylinder Material of Construction Steel Manufacturer Owen Oil Tools, Godley, TX Dimension (mm, OD) 50.7 x 25.2 Average Gross Weight grams Note These articles were inserted individually within the zip-locked bags INNER PACKAGING DETAIL #5-3 - Reference Section 8 for drawings Desiccant Bag Count 50 (1 per bag) Manufacturer Desiccare, Inc., Reno, NV Material Silica Gel, Indicating Silica Gel, Clay, Molecular Sieve and Carbon Dimension (mm, OD), D X H 16.8 x 2.8 x 25.5 Weight 0.43 grams each Notes 1 desiccant bag was placed inside each barrier bag Overall Inner Packaging Gross Weight (OIP5GW) kg

13 Page 13 of 62 OUTER PACKAGING - UN 4G (Reference Section 8 for drawings) Type Fiberboard Box Style Center Special Slotted Container (CSSC), FEDCO Style: 0204 Manufacturer/Supplier All Star Corrugated, Fort Worth TX Part # WHS-350 BC Spec. # Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA Dimension (mm, OD), L X W X H 354 x 354 x 267 Dimension (mm, ID), L X W X H 344 x 344 x 253 Stacking Height (mm) 267 Number of Walls - Flute Type Double-Wall BC-Flute Tare Weight grams BMC (Box Marked Certification) 350# ( ) ( ) CUT ( ) JEC Tested Basis Weight (lbs/1000ft²) ( ) KOD ( ) ACE ( ) COR Tested Burst Strength (lbs/inch²) Minimum Tested Caliper 6.94 mm Method of Joining Panels Stitched withy at least seven (7) 12.5 mm wide staples Mfr's Joint Flap Size 35 mm Mfr's Joint Location 5-2 corner as per the ASTM diagram Top Flap Gap/Meet Inner: Meet Outer: Meet Bottom Flap Gap/Meet Inner: Meet Outer: Meet Print None Closure Method (Refer to Section 7 for Closing Instruction and Section 8 for Specs) Closure 3/4" C34 Stick Staples S-1396 Uline Description 18 mm (3/4") long, 31 mm (1-1/4") crown galvanized metal staples Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S-1396 Owen Part # STA S Four (4) staples along the flap seam, 38 mm (1-1/2") away from boxes outside Top Closure edges, 38 mm (1-1/2") apart on both sides & 178 mm (7") apart on center, 0.8 grams each Four (4) staples along the flap seam, 38 mm (1-1/2") away from boxes outside Bottom Closure edges, 38 mm (1-1/2") apart on both sides & 178 mm (7") apart on center, 0.8 grams each Method of Closure See Section 7.2

14 Page 14 of 62 OUTER PACKAGING DETAIL #1 - Reference Section 8 for drawings Plain Corrugated Pad Iteration 1: 7 Iteration 2: 0 Count Iteration 3: 3 Iteration 4: 0 Iteration 5: 4 Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Corrugate Manufacturer/Supplier All Star Corrugated, Fort Worth TX Part # WHS Spec. # Size (mm, OD) 343 x 338 Caliper 7.25 mm Weight grams each Iteration 1: 1 top, 2 under each tube layer and 2 bottom Iteration 3: 2 pads sandwich the honeycomb pad on top, 1 pad was placed Pad Location directly under partition system Iteration 5: 2 pads are placed on top and 2 pads are placed on bottom OUTER PACKAGING DETAIL #2 - Reference Section 8 for drawings Large Honeycomb Pad Iteration 1: 0 Iteration 2: 4 Count Iteration 3: 2 Iteration 4: 0 Iteration 5: 4 Material Hexacomb Core Type 4 35# facing Manufacturer/Supplier Pregis Hexacomb Corporation Supplier All Star Corrugated, Fort Worth TX Spec # H Owen Part # PAD-HEX-100 Size (mm, OD) 343 x 343 Caliper 25.4 mm Weight 129 grams each Iteration 2: 2 over and 2 bellow Metal-in Film Laminate Bags Iteration 3: 1 pad is sandwiched between 2 BC flute top pads, 1 pad was placed Pad Location on the bottom of box Iteration 5: 2 pads are placed on top under flat pads, 1 pad was placed between layers and 1 pad was placed on the bottom over the flat pads

15 Page 15 of 62 OUTER PACKAGING DETAIL #3 - Reference Section 8 for drawings Small Honeycomb Filler Iteration 1: 13 Iteration 2: 0 Count Iteration 3: 0 Iteration 4: 0 Iteration 5: 0 Material Hexacomb Core Type 4 35# facing Manufacturer/Supplier Pregis Hexacomb Corporation Supplier All Star Corrugated, Fort Worth TX Spec # H Owen Part # PAD-HEX-1X2 Size (mm, OD) 48.8 x 272 Caliper 25.4 mm Weight 12 grams each Pad Location Iteration 1: These honeycomb fillers were placed around the cutter casing OUTER PACKAGING DETAIL #4 - Reference Section 8 for drawings 9-Cell Partition System Iteration 1: 0 Iteration 2: 0 Count Iteration 3: 1 Iteration 4: 0 Iteration 5: 0 Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Corrugate Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # PTN File # 7045 Size (mm, OD) 330 x 330 x 150 Cell Size (mm, OD) 85 x 85 x 150 Caliper 6.46 mm Weight grams Partition Location Iteration 3: 8 die-cut sheets interlocked with each other forming a 3 X 3 closed cell partition system OUTER PACKAGING DETAIL #5 - Reference Section 8 for drawings 25-Cell Partition System Iteration 1: 0 Iteration 2: 0 Count Iteration 3: 0 Iteration 4: 0 Iteration 5: 2 Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Corrugate Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # DIV File # 5797 Size (mm, OD) 330 x 330 x 150 Caliper 6.46 mm Weight grams Iteration 5: 8 die-cut sheets interlocked with each other forming a 5 X 5 open Partition Location cell partition system

16 Page 16 of 62 OUTER PACKAGING DETAIL #6 - Reference Section 8 for drawings Corrugated Tray Iteration 1: 0 Iteration 2: 0 Count Iteration 3: 0 Iteration 4: 0 Iteration 5: 2 Material 200# (42/26/42) Kraft/Kraft B-Flute Corrugate Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # 1313-TRAY File # Size (mm, OD) 340 x 337 x 46 Size (mm, _D) 325 x 325 x 45 Caliper 2.78 mm Weight grams each Partition Location Iteration 5: These trays were placed 2 layers high. Each contains 50 bags within the partition system cells OUTER PACKAGING DETAIL #7 Reference Section 8 for drawings Bubble Sheet Iteration 1: 0 Iteration 2: 2 Count Iteration 3: 0 Iteration 4: 2 Iteration 5: 0 Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16") Iteration 2: 300 x 1520 Dimension (mm, OD) flat Iteration 3: 305 x 5690 & 305 x 3845 Iteration 2: 19 grams Tare Weight Iteration 4: 74 grams & 50 grams respectively Iteration 2: These bubble sheet were placed over and around the Metal-in Film Laminate Bags Sheet Location Iteration 4: larger bubble sheet fills void space ob top layer, smaller sheet fills the void space on bottom layer Overall Outer Package Tare Weight (OPTW) Iteration 1: grams Iteration 2: grams Iteration 3: grams Iteration 4: grams Iteration 5: grams

17 Page 17 of 62 SECTION 3 - Test Description and Test Results Drop Test 49 CFR Test Specimen/Contents Characteristics Number of Packages Tested 25 (5 per iteration) Packing Group Number PG II State Solid Dummy Load (Solid) Steel disks or blocks Drop Height Multiplier 0.67 for PG III; 1 for PG II & 1.5 for PG I Drop Height 1.2 m Conditioning Temperature & Duration, 49 CFR (c) F & 50 % R.H. Content (Dummy Load) Test Temperature 73 F Drop Test Method: The inner packagings were filled to 98% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 7). Twenty-five (25) assembled packages, 5 packages for each iteration, were subjected to a free fall drop test from a height of 1.2 meters onto a solid steel plated concrete floor as described below. Drops were conducted within 60 seconds of removal of the outer packagings from the conditioning chamber. Drop Test Results Iteration 1 Test Sample # Weight (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance

18 Page 18 of 62 Drop Test Results Iteration 2 Sample Test Weight # (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance Drop Test Results Iteration 3 Sample Test Weight # (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance

19 Page 19 of 62 Drop Test Results Iteration 4 Sample Test Weight # (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance Drop Test Results Iteration 5 Sample Test Weight # (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance

20 Page 20 of 62 Pass/Fail Criteria - A package is considered to successfully pass the drop tests if for each sample tested: For packaging containing liquid, there is no leakage of the filling substance from the inner packaging. There is no damage to the outer packaging likely to adversely affect safety during transport. Inner receptacles, inner packagings or articles must remain completely within the outer packaging. Any discharge from a closure is slight and ceases immediately after impact or pressure equalization with no further leakage. No rupture is permitted in packagings for materials in Class 1 which would permit spillage of loose explosive substances or articles from the outer packaging. Stacking Test - 49 CFR (See Section 5.2 for Calculation) Test Specimen/Contents Characteristics Number of Packages Tested Product State Dummy Load (Solid) Conditioning of Outer Packaging - 49 CFR (d) Test Temperature Test Method Test Duration Minimum calculated stacking test weight Actual stacking test weight Test Duration 25 (3 per iteration) Solid Steel disks or blocks F & 50 % R.H. 73 F & 50 % R.H. Free standing, static (dead weight) test 24 hours kg ( lbs) per package kg (565 lbs) per package 24 hours Stacking Test Method: The inner packagings were filled to 98% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 7). Stacking test load (dead weight) of kg was applied individually to the top of the three (3) assembled packages for each iteration using wood load spreaders and the weight was maintained for 24 hours. Stacking Test Results - Iteration 1 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance

21 Page 21 of 62 Stacking Test Results - Iteration 2 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance Stacking Test Results - Iteration 3 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance Stacking Test Results - Iteration 3 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance

22 Page 22 of 62 Stacking Test Results - Iteration 5 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance Pass/Fail Criteria - A package is considered to successfully pass the stack tests if for each sample tested: No test sample shows any deterioration or distortion that could adversely affect safety during transport causing instability in stacks of packages, or cause damage to inner packagings that is likely to reduce safety in transport. There no leakage of the filling substance from the inner receptacle, or inner packaging

23 Page 23 of 62 Vibration Test - 49 CFR Test Specimen/Contents Characteristics Number of Packages Tested Product State Dummy Load (Solid) Conditioning of Outer Packaging - 49 CFR (d) Test Temperature Test Method Test Duration Test Frequency 25 (3 simultaneously, 3 per iteration) same samples used for stacking test Solid Steel disks or blocks F & 50 % R.H. Ambient ASTM D Rotary Motion Vibration 60 minutes 235 CPM Vibration Test Method: The inner packagings were filled to 98% overflow capacity with dummy load. The packages were re-assembled as per closing instruction (Reference Section 7). Three (3) assembled packages, for each iteration were simultaneously placed on a rotary vibration table platform having 25.4 mm peak-to-peak displacement and vibrated in normal shipping orientation for one (1) hour at 235 CPM such that a 1.6 mm thickness could be passed between the bottom of the samples and the platform. Immediately thereafter, the packages were removed from the platform and turned on its side for examination. Vibration Test Results - Iteration 1 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance Vibration Test Results - Iteration 2 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance

24 Page 24 of 62 Vibration Test Results - Iteration 3 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance Vibration Test Results - Iteration 4 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance Vibration Test Results - Iteration 5 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance Pass/Fail Criteria - A package is considered to successfully pass the vibration test, if for each sample tested after it was immediately removed from table platform and turned on its side: There is no leakage or rupture from any of the packaging. No test sample shows any deterioration which could adversely affect safety or container strength, during transport liable to reduce packaging strength.

25 Page 25 of 62 Cobb (Water Absorption) Test - 49 CFR [ISO International Standard (E)] Test Specimen/Contents Characteristics Number of Samples Tested 5 Test Duration 30 Minutes Test Intensity 100 ml Distilled Water Conditioning of Test Samples F & 50 % R.H. Test Method ISO 535, Cobb Method Cobb Test Results Sample # #1 #2 #3 #4 #5 Average Results grams/m² Pass Pass/Fail Criteria An increase in mass of greater than 155 grams/m² over the 30 minute duration of the tests represents an unacceptable level of water absorption. SECTION 4 - Shippers Responsibility It is the responsibility of the end shipper to determine authorization for use under these regulations. It is the shippers responsibility to determine if the packaging is compatible for products to be shipped. Use of the marking of this certification for any variations without further testing as allowed under US DOT 49 CFR Section will be at complete responsibility of the shipper. By continuing to place the UN Markings on Packagings, the packaging manufacturer or shipper is certifying that each packaging is constructed in the same manner as the originally tested and certified packaging, and that each packaging is capable of withstanding the prescribed performance tests. According to 49 CFR Section (1) Variation 1 - variations are permitted in inner packaging of a tested combination packaging without further testing of the package, provided an equivalent level of performance is maintained as described in (1) Variation 4 (i),(a),(b),(c),(d),(e) and (F) and (ii). According to US DOT 49 CFR Section (e), the packaging manufacturer shall achieve successful test results for the periodic retesting at intervals established by the manufacturer of sufficient frequency to ensure that each packaging produced by manufacturer is capable of passing the design qualification test. Changes in retest frequency are subject to the approval of the Associate Administrator for Hazardous Materials Safety. For combination packaging, the periodic retest must be conducted at least once every 24 months.

26 Page 26 of 62 SECTION 5 - Calculations 5.1 Certified Package Gross Mass Calculations Based on Test Level Iteration 1: kg Iteration 2: kg Overall Inner Package Gross Weight (OIPGW) Iteration 3: kg Iteration 4: kg Iteration 5: kg Iteration 1: grams Iteration 2: grams Overall Outer Package Tare Weight (OPTW) Iteration 3: grams Iteration 4: grams Iteration 5: grams Test Material Specific Gravity (TMSG) - Packing Group Number II Iteration 1: kg Iteration 2: kg Minimum Package Weight as Tested (PGW) Iteration 3: kg Iteration 4: kg Iteration 5: kg Packing Group Multiplication Factor (PMF) 1.0 Formula for Calculating Certified Gross Mass (CGW) Certified Package Marking CGW = Minimum PGW CGW = Minimum PGW = kg CGW = 22.8 kg (50.16 lbs) Y = 22.8 (50.16 lbs) 5.2 Stacking Strength Test Calculations Test Load (TL) Overall Stacking Height of Packages (SH) Overall Stacking Height of Package (PH) TL (Static) TL = [(SH - PH) - 1] x CGW (static) TL = [(SH - PH) - 1] x CGW x 1.5 (dynamic) 3000 mm (10 feet) 267 mm TL = [(3000/267) - 1] x 22.8 = 14 (rounded up) x 22.8 TL = kg ( lbs) Rounded up to at kg (565 lbs) per package for test purposes

27 Page 27 of 62 Regulatory Standard References: Test Appendix A Regulatory & Industry Standard References CFR UN Regulation IMDG ICAO IATA Drop Test Stacking Test Hydrostatic Pressure (c) Cobb Test Vibration Test United States Code of Federal Regulations (CFR), Title 49, Transportation, Parts The United Nations Recommendations on The Transport of Dangerous Goods Model Regulations (Orange Book) 3. International Maritime Dangerous Goods Code (IMDG) 4. Technical Instructions for the Safe Transport of Dangerous Goods by Air (ICAO) 5. International Air Transport Association (IATA), Dangerous Goods Regulations Industry Standard References: Drop Test ASTM D5276 Standard Test Method for Drop Test of Loaded Containers by Free Fall Stacking Test ASTM D4577 Standard Test Method for Compression Resistance of a Container Under Constant Load Hydrostatic Standard Guide for Conducting Internal Pressure Tests on United Nations ASTM D7660 Pressure (UN) Packagings Cobb Test ISO 535 Paper and Board Determination of Water Absorption Cobb Method Vibration Test ASTM D999 Standard Test Method for Vibration Testing of Shipping Containers American Society for Testing and Materials (ASTM) International Organization for Standardization (ISO)

28 Page 28 of 62 Appendix B Test Equipment & Instrumentation No. Test Machine, Model # and Serial # Capacity Calibration Date Re-Calibration Date 1. Drop Table, Lansmont Corporation: Model #PDT-56-ED; Serial #M " 72" 2/27/2017 2/27/ Drop Table, Gaynes Eng. Inc., Serial #G " 120" 2/27/2017 2/27/ Vibration Table, Gaynes Eng. Inc.: Model #6000V 3000 lbs 2/27/2017 2/27/ Compression Machine, TechLab Systems: Model #Validator; S/N # T lbs 2/27/2017 2/27/ Digital Thermometer, Mannix: Model #DT721 (for Conditioning, Freezer), F 2/23/2017 2/23/ Paperless Temperature & Humidity Recorder, Dickson: Model #TH660 (for Cold Chamber) F 2/23/2017 2/23/ Paperless Temperature & Humidity Recorder, F, Dickson: Model #TH635 (for Hot Chamber) 0% 95% RH 2/23/2017 2/23/ Thermometer & Hygrometer, F, Omega Engineering: Model #RH520 10% 95% RH (for Conditioning Room) 2/23/2017 2/23/ Bench Scale, SeiKo Scale Division: Model #WA200001XP; S/N# mg 20 kg 5/16/2017 5/16/ Bench Scale, Mettler Toledo: Model #ICS4x9-1; S/N# mg 30 kg 5/16/2017 5/16/ Analytical Balance, PCA, Germany: Model #AB200; S/N # mg 200 g 5/16/2017 5/16/ Bench Scale, Ohaus: Serial # XZ lbm 5/16/2017 5/16/ Caliper, General Tools & Instruments: Model # , S/N: 81PCS " 5/16/2017 5/16/ Caliper, Fowler: Model # " 5/16/2017 5/16/ Electronic Torque-Meter, Kaps-All: Model #EB-650; S/N # inch-lbs 12/19/ /19/ Toque Wrench, CDI, Model No. 301LDIN 0 30 inch-lbs 5/17/2017 5/17/ General Purpose Digital Pressure Gauge, Omega Engineering: Model #DPG psi 5/15/2017 5/15/ General Purpose Digital Pressure Gauge, Omega Engineering: Model #DPG V psi 5/15/2017 5/15/ Winters Pressure Gauge, WG psi 5/15/2017 5/15/ Ashcrof Pressure Gauge, V/300 Psi Part # ; S/N: The Mullen Tester, B.F Perkins and Son: Serial # ECT Tester, Testing Machines, Inc.: S/N 5852X Measuring Tape, Ultra-Touch: ANAMA TM1 & TM2 Measuring Tape, Stanley Power Lock, ; ANAMA TM3 Measuring Tape, Made In China; ANAMA TM4 Presto Dart Impact Tester, Model No. PCN-230; S/N: psi 10/21/ /21/ psi 5/18/2017 5/18/ lbs 5/18/2017 5/18/ Feet 5/16/2017 5/16/ Feet 5/16/2017 5/16/ Feet 5/16/2017 5/16/ " 1.7 feet 2/28/2017 2/28/2018

29 Page 29 of 62 SECTION 6 Inner & Outer Packaging Photographs Primary Inner Packaging Components Iteration 1

30 Page 30 of 62 Primary Inner Packaging Details - Iteration 2

31 Page 31 of 62 Primary Inner Packaging Details - Iteration 3

32 Page 32 of 62 Primary Inner Packaging Details - Iteration 4

33 Page 33 of 62 Primary Inner Packaging Details - Iteration 5

34 Page 34 of 62 Outer Packaging Components All 5 Iterations: Outer Packaging Details

35 Page 35 of 62 SECTION 7 - Packaging Assembly (Closing) Instruction) Note: Packages were re-assembled same way as received. Step-by-Step Packaging Assembly Demonstration - Iteration 1

36 Page 36 of 62 Step-by-Step Packaging Assembly Demonstration - Iteration 2

37 Page 37 of 62 Step-by-Step Packaging Assembly Demonstration - Iteration 3

38 Page 38 of 62 Step-by-Step Packaging Assembly Demonstration - Iteration 4

39 Page 39 of 62 Step-by-Step Packaging Assembly Demonstration - Iteration 5

40 Page 40 of 62 Manufacturer s Closing Instructions: Iteration 1:

41 Page 41 of 62 Iteration 2:

42 Page 42 of 62 Iteration 3:

43 Page 43 of 62 Iteration 4:

44 Page 44 of 62 Iteration 5:

45 Page 45 of 62 SECTION 8 - Package Specifications & Drawings Fibre Tube for CUT-8250 Iteration 1

46 Page 46 of 62 Fibre Tube for CUT-8250 Iteration 1

47 Page 47 of 62 Barrier Bag Iteration 1

48 Page 48 of 62 Barrier Bag Specifications Iteration 1

49 Page 49 of 62 Barrier Bag Iteration 3

50 Page 50 of 62 Fibre Tube Iteration 3

51 Page 51 of 62 Desiccant Bag

52 Page 52 of 62 Inner Box Drawing & Specifications Iteration 4

53 Page 53 of 62 Anti-Stat Bag Iteration 5

54 Page 54 of 62 Outer Box Drawing & Specifications

55 Page 55 of 62 Plain Pad Drawing & Specifications

56 Page 56 of 62 Honeycomb Pad Drawing & Specification

57 Page 57 of 62 Honeycomb Pad Drawing & Specification

58 Page 58 of 62 9-Cell Partition Drawing & Specification

59 Page 59 of Slot Partition Drawing & Specification

60 Page 60 of 62 Corrugated Tray Drawing & Specification

61 Page 61 of 62 Anti-Static Sheet Specifications

62 Page 62 of 62 Carton Sealing Staples Specification