Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 1 of 17

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1 Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 1 of 17

2 TABLE OF CONTENTS 1.SCOPE DEFINITIONS REFERENCES CONTRACTOR RESPONSIBILITIES GENERAL SPECIFICATION MANUFACTURING PRE QUALIFICATION TESTING...13 APPENDIX A: APPENDIX B: APPENDIX C: SUMMARY OF TEST REQUIREMENTS CONTRACTOR DATA REQUIREMENTS LIST INSPECTION MATRIX Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 2 of 17

3 1. SCOPE This specification covers materials, surface preparation, application, quality control and repairs of external abrasion resistant coating of line pipe for a flow line bundle casing. The purpose of the coating system is to protect the casing s corrosion resistant undercoating of fusion bonded epoxy during a 400 mile bottom tow of the flowline bundle from the make up site to its permanent location. Materials which have not been subjected to or passed the tests required herein; and Materials which, if used, will result in a nonconformity; and Documents or software that do not meet the requirements herein 2.1 CONTRACTOR REPRESENTATIVE 2. DEFINITIONS COMPANY CONTRACTOR The company that contracts to apply coating according to this specification. CONTRACT The entire written procurement agreement between CONTRACTOR and COMPANY. NONCONFORMITY An instance of failure to meet contractual requirements, including physical, procedural or performance deficiencies. STANDARDS Industry codes, standards, and recommended practices referenced herein. WORKS The location(s) at which manufacturing, inspection and testing are performed. NONCONFORMING MATERIALS Materials which do not meet requirements set out herein; CONTRACTOR shall designate in writing to COMPANY an authorized representative to serve as liaison with COMPANY on matters associated with this Specification and on the Purchase Order or Contract referencing this Specification. This representative shall be designated prior to the performance of services associated with this Specification and the Purchase Order or Contract referencing this Specification. 2.2 DOCUMENT PRECEDENCE In the event of conflict between documents, the priority shall be as follows: a) Purchase Order or Contract b) This Specification c) Referenced Standards However, conflicts shall be reviewed and resolved with COMPANY's Representative prior to initiation or continuation of the services to be performed in association with the Purchase Order or Contract. Materials not documented according to the requirements herein; Materials which were not processed according to the requirements herein; 3. REFERENCES Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 3 of 17

4 The appropriate sections and supplements of the latest versions of the following codes and standards are incorporated in this specification by reference, as they apply in the context of this specification. a) Steel Structures Painting Council SSPC SP 1 Solvent Cleaning b) American Society for Testing and Materials: ASTM D 1002 Test Method for Strength Properties of Adhesives in Shear by Tension Loading (Metal to Metal) ASTM G 14 Impact Resistance of Pipeline Coatings by Falling Weight Method c) International Organization for Standardization: ISO 1519 Paints and Varnishes Bend Test (Cylindrical Mandrel) d) COMPANY Specifications Specification for Steel Line Pipe for Bundle Casing Specification for Handling, Transporting and Storing of Line Pipe External Fusion Bonded Epoxy Coating for Steel Line Pipe Handling, Transporting and Storing of Line Pipe 4. CONTRACTOR RESPONSIBILITIES 4.1 GENERAL CONTRACTOR shall provide all labor, materials, tools and equipment and shall undertake all inspection, handling, reporting, storage and shipping necessary to do the work required in this specification and the CONTRACT. If CONTRACTOR believes that this specification conflicts with other terms of the CONTRACT, CONTRACTOR shall inform COMPANY and resolve the conflict by the terms of the CONTRACT. 4.2 SUBCONTRACTORS CONTRACTOR shall be responsible for the actions and performance of subcontractors, including those hired for handling and transportation. 4.3 REPORTING AND APPROVALS Work Plan Forty five (45) days before work begins, CONTRACTOR shall submit and receive approval for a work plan and procedures for carrying out the work required by this specification and the CONTRACT. The work plan shall include: a) CONTRACTOR s Quality Plan detailing inspections to be performed during the coating process. b) Procedures for surface preparation and for coating application; c) A description of the equipment to be used, including the film thickness gauge, the abrasive cleaning equipment and the coating application equipment; d) Abrasive cleaning and coating materials to be used; e) Inspection Procedure. CONTRACTOR will submit for approval as proposed, including, but not limited to activities listed in Appendix C. f) Testing procedures; g) Coating repair procedures; h) Procedures for transportation, storage and handling, according to SP 051; and i) Location on coating yard where work is to be performed including a description of facilities and CONTRACTOR s equipment specifications. j) CONTRACTOR s data per Appendix B. Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 4 of 17

5 k) Procedures for identifying, documenting, and segregating or disposing of nonconforming materials Disposition of Nonconforming Materials During the work materials contractor shall submit to COMPANY a summary report of all nonconformities and their disposition. Dispositions of nonconforming materials should be categorized as "scrap," "rework," or "use as is." The report also should include a full description of the condition that caused the nonconformity. If a nonconformity cannot be eliminated by replacement or by a procedure set out herein, then immediately upon its occurrence or discovery, CONTRACTOR shall inform COMPANY and propose a disposition. Dispositions must be approved in writing by a COMPANY representative whose authority CONTRACTOR has established by the terms of the CONTRACT. COMPANY may reject coating that does not conform to these specifications. CONTRACTOR shall not let repairs or replacements delay the delivery schedule or increase costs to COMPANY. 4.4 RECORDS CONTRACTOR shall keep up to date records adequate to confirm that the work has been carried out to this specification. These records shall be indexed and legibly recorded in enough detail that they can be accessed and understood by a qualified, independent third party. In absence of other instructions, CONTRACTOR shall keep these records available to COMPANY for inspection or photocopying for ten years. The records should include: a) When and where the coating was applied; b) A description of each test or inspection and its results, with a reference to the paragraph number of the test requirement in this specification; c) The time, date and place each test or inspection was done; d) The name and qualifications or authority of the inspector or reviewer and his employer; e) Evidence of calibrations; and f) Pertinent information about nonconforming materials or test failures, including: Material condition that caused rejection Method of detection Number of items involved, if more than one Proposed and actual disposition Preventive action taken Corrective action taken 4.5 INTERACTIONS BETWEEN CONTRACTOR AND COMPANY CONTRACTOR shall allow COMPANY access to his facilities and processes for the purposes of monitoring, surveillance and inspection, including but not limited to: a) Review of adequacy of facilities and equipment; b) Review of personnel qualifications; c) Performing or witnessing inspections, tests and analyses COMPANY deems necessary to confirm compliance with requirements. Manufacturer shall give COMPANY notice of the production start up and all tests and inspections required herein. The number of days notice shall be according to the requirements of the CONTRACT. CONTRACTOR shall provide all reasonable facilities to COMPANY for the above purposes. 5. GENERAL SPECIFICATION 5.1 MATERIALS Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 5 of 17

6 The coating material shall be Sigma Coatings Colturiet Armour Compound 7490, Carboline C Gaurd, as specified in the CONTRACT or COMPANY approved equal Carboline C Gaurd. Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 6 of 17

7 5.2 AREA TO BE COATED The coating density (120 lbs./ft) and thickness shall be controlled so that the coating weight on any joint All pipe specified in the CONTRACT shall be coated over approximately half of the circumference of the pipe to within a "cutback" of 4 inches from each end. The longitudinal center of the area to be coated shall be offset approximately 150 degrees from the seam weld on the pipe. The area to be coated is also shown in Figure 1. The exposed surfaces of the casing pipe and the "cutback" areas and bevels shall be free of coating and overspray. 5.3 COATING THICKNESS The finished coating shall be uniformly applied to a nominal thickness of 105 mils over 120 o of the outer circumference of the pipe, and feathered down over the adjacent 30 o to zero thickness as shown in Figure 1. The 30 degree feathered zone shall decrease in thickness more or less continuously to no less than half the nominal abrasion resistant coating thickness (in addition to the thickness of the FBE) at 15 degrees beyond the full thickness area. The minimum thickness shall be 90 mils and the maximum, 120 mils. No abrasion resistant coating is required on the remaining half of the pipe. 5.4 WEIGHT FIGURE 1 is not less than the theoretical weight, calculated using the thickness limits specified in Section 5.3 and in the CONTRACT. The theoretical weight of abrasion coating per unit length of abrasion coating is as follows: Coating ThicknessWeight (mils)(lbs./ft) 30" Riser Casing 38" Bundle Casing Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 7 of

8 nominal MANUFACTURING < with clean, dry lint free rags using hydrocarbon solvents (xylol mineral spirits) Bevel Protectors and End Caps Bevel protectors shall be removed from the joint ends and be replaced by suitable caps to prevent coating material entering the bore. The end caps shall be installed in such a manner that they do not cause damage to the pipe markings inside the bore Masking 6.1 TRANSPORTING, HANDLING AND STORING OF LINE PIPE CONTRACTOR shall be responsible for the safe transportation, handling and storage of the pipe according to COMPANY specification number SP 051. Care should be taken not to damage or obscure the markings inside the pipe. The pipe shall not be racked in more than three tiers. If CONTRACTOR intends to move the pipe before the coating is cured, then the reasons for this, the time between coating and the move and procedures for handling shall be included in CONTRACTOR's work plan. 6.2 UNDERCOATING AND PREPARATION FBE Undercoat The abrasion resistant coating shall be applied to pipes which have been coated with fusion bonded epoxy according to COMPANY specification Inspection and Cleaning If the pipes are moved or handled between coats, then they shall be visually examined for dents, laps, defective bevels, damage to the coating and other obvious defects in order to avoid coating unusable pipe. CONTRACTOR shall record the pipe numbers of the defective pipes, mark the pipes and remove them from the stack to be coated. Salts and dirt shall be removed. Organic contaminants shall be removed Anodes, bevels and "cutback" areas described in Section 5.2 shall be masked to prevent overspray. Any coating or overspray which is inadvertently deposited on these areas must be removed Abrasive Cleaning The fusion bonded epoxy coating shall be roughened by light sweep blasting over the area to be coated with the abrasion resistant coating. Before sweep blasting, each joint of pipe shall be uniformly dried to completely remove all moisture and to prevent any condensation of moisture on the pipe. FBE coated pipe temperatures shall be at least 5º F above the dew point. Ends of the pipe shall be protected with plugs that prevent entry of abrasive into the pipe interior during blasting. Any abrasive entering the pipe shall be removed prior to coating. The blasting shall be done with a virgin abrasive mix described in CONTRACTOR's approved work plan. To remove all dirt, mill scale, rust, corrosion products, oxides, paint and other foreign matters. The surface shall have a uniform appearance; very light shadows, streaks or discolorations may be considered acceptable; however, at least 95% of the surface shall have a uniform light cleaned non lustrous surface. The compressed air for blasting shall be free of water and oil. Adequate separators, filters, or traps shall be provided. The blasting media working mix shall be selected to produce an anchor pattern profile of not less than 2.0 mils nor more than 4.0 mils. This blasting shall not remove more than 4 mils from the area to be coated with the anti abrasion coating and shall not remove any significant amount of coating Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 8 of 17

9 from the half of the pipe which is left exposed. The blast shall be directed more or less in the direction of the center of the 120 degree arc of the pipe that will receive the full thickness, leaving the 15 degrees on both sides as a transition area. CONTRACTOR shall remove any abrasive remains left in the pipe after blasting. For consistent surface finish and anchor pattern a stabilized abrasive working mix shall be maintained by frequent small additions of new grit (dry sand or steel) commensurate with abrasive consumption. Infrequent large additions shall be avoided. The abrasive working mix shall be maintained clear of contaminants by continuous effective operation of blasting machine scalping and air wash separators. Anchor patterns will be verified by the CONTRACTOR by taking anchor patterns on both ends of the first ten (10) joints blasted. Thereafter, tests will be conducted on both ends of every twenty fifth (25) joints. The test must be conducted with Istex Presso Film or equivalent and measured with the appropriate gauge. The COMPANY Representative shall maintain the test results and include them with inspection reports Final Surface Preparation The area where the pipe leaves the cleaning station after sweep blasting shall be well illuminated (500 lux) to permit visual inspection of the condition of the cleaned surfaces to locate defects. The blastcleaned surface shall not be contaminated with dirt, dust, metal particles, oil, water, or any other foreign matter from any source, nor shall the anchor pattern be destroyed or burnished by pipe transport systems, processing equipment, tools, or follow up cleaning with abrasive sanders. Following abrasive cleaning and prior to coating application, all dust, or other loose contaminants remaining on the surface or entering the interior of the pipe shall be blown off with clean, dry, oil free compressed air in a manner not affecting the other clean pipe or pipe to be coated. When compressed air cleaning facilities are not available, vacuum cleaning or other suitable methods may be used. Any pipe not coated within two hours after blasting, if the dew point is less than 50º F, shall be reblasted. In addition, any pipe not coated within 30 minutes after blasting, if the dew point is greater than or equal to 50º F, shall be reblasted. An anchor pattern removed by excessive grinding, will be reblasted before coating. Determination of what constitutes excessive grinding is to be made by COMPANY s authorized representative. Typically any continuous ground area of more than 0.5 square feet or a total ground area of more than 2 square feet per joint will be considered excessive. If the anchor pattern is destroyed, the ground areas shall be checked by ultrasonic testing to ensure that the remaining thickness exceeds the minimum required in accordance with COMPANY specification PS The surface condition of the material shall be approved by the COMPANY s Representative prior to the application of the coating. Pipe surfaces not acceptable by the COMPANY s Representative for coating will be recleaned at no extra cost to the COMPANY. When required by the COMPANY, the material will be subjected to an external acid wash after blasting but prior to coating. Prior to the commencement of the coating, the CONTRACTOR shall furnish the COMPANY, for review and approval, detailed procedures and specifications regarding the actual acid wash operations the CONTRACTOR proposes to utilize for the job. 6.3 COATING APPLICATION General CONTRACTOR shall be familiar with and strictly follow the coating manufacturer s specifications and recommendations for the application, curing Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 9 of 17

10 temperatures and curing time for the fusion bonded epoxy system used. If required by COMPANY, CONTRACTOR shall work with the manufacturer and/or his representative to eliminate any difficulties that might arise in the application of the coating. The coating shall be sprayed to the nominal thickness in Section 5.3 and CONTRACTOR's approved work plan described in Section The CONTRACTOR shall give particular care and attention to keeping the pipe and the coating dry during application Equipment CONTRACTOR shall provide spare equipment (pumps, nozzles, etc.) to ensure production is continuous and no breakdowns occur due to equipment cleaning or repairing. Coating shall be applied with equipment which conforms to the coating manufacturer's recommendations for humidity, and dew point temperature and CONTRACTOR's approved work plan described in Section Multiple Coats The CONTRACTOR shall not allow more than the coating manufacturers recommended maximum time to lapse between coats. CONTRACTOR shall cover or shelter the pipes to prevent rain or mist from settling between coats. If more time does lapse, the COMPANY may, at COMPANY's option require CONTRACTOR to remove the coating or to sweep blast the surface according to Section Curing The coating shall be cured according to the manufacturer's recommendation. It will be the responsibility of the coating applicator to take immediate corrective measures when conditions exist which adversely affect the external coating operation with respect to cleaning, application or material performance. NOTE: Temperature at the coating station and post application curing time shall be closely monitored to comply with the limits set by the coating manufacturer. A best temperature and cure time can usually be determined after the first few joints are coated Marking If the paint stenciled pipe markings applied at the pipe mill are removed in the coating process, CONTRACTOR shall record the markings and paint stencil them on the inside surface of the pipe after coating. Paint markings shall be weather and sunlight resistant End Caps/Bevel Protectors If bevel protectors were removed to install pipe caps, CONTRACTOR shall re install them before shipping or storing the pipe. 6.4 IN PROCESS INSPECTION AND TESTING COMPANY Inspection COMPANY shall have full and free access to every part of the coating yard and the on/off loading facilities of CONTRACTOR to inspect the coating materials, equipment, and CONTRACTOR s work. CONTRACTOR shall provide reasonable assistance to COMPANY at every stage of inspection. COMPANY reserves the right to inspect the work but is in no manner obligated to supervise the work CONTRACTOR Inspection and Testing CONTRACTOR shall furnish all material, equipment, and qualified personnel to perform the examinations and testing specified herein. Inspection provided by COMPANY shall not relieve CONTRACTOR of his responsibility to ensure quality control Visual Inspection Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 10 of 17

11 CONTRACTOR shall visually inspect each pipe joint for any damage and shall report such damage immediately to COMPANY s Representative. CONTRACTOR shall visually inspect the integrity and uniformity of all of the coating on each pipe. Discontinuities or abnormalities shall be circled with a waterproof marker. Markings shall be far enough from the imperfection or damaged area to allow surface preparation and patching to take place without obliterating the markings. The area shall be repaired using a method described in CONTRACTOR's approved work plan (see Section 4.3.1) Thickness Measurements Dry coating thickness shall be measured with a properly calibrated Mikrotest magnetic film thickness gauge, or equivalent, to ensure finished coated pipe has a minimum dry film thickness of 100 mils including FBE coating. The film thickness gauge shall be calibrated at a minimum of once every four hours against the coated substrate standard for 100 mils thickness, as defined by the U.S. Department of Commerce, National Bureau of Standards, Certified Coating Thickness Calibration Standards for Non Magnetic Coating of Steel. Six measurements of the dry film thickness shall be made on each pipe using a coating thickness gauge described in CONTRACTOR's approved work plan of Section Two measurements shall be taken within three feet of each end and two shall be taken within three feet of the center of the pipe. Measurements shall include one measurement on the center of coated when full thickness and one measurement approximately 1/8 of the pipe circumference beyond this area. If the coating thickness varies enough to be visually detected, then each pair of measurements shall include one at a high spot and one at a low spot in the coating. The measurements shall confirm that the combined thickness of both layers is within allowable limits determined as follows. Minimum Thickness: 100 mils (including FBE) Maximum Thickness: 150 mils (including FBE) Holiday Detector CONTRACTOR shall furnish, maintain, and operate a high voltage holiday detector of a type acceptable to COMPANY and shall locate and repair all holidays and damaged spots. The entire coated surface area shall be checked for holidays. CONTRACTOR shall furnish COMPANY a certification from the manufacturer of the holiday detector or from a testing agency acceptable to COMPANY that the unit has been properly adjusted and the voltage set within that range which is necessary for the detection of holidays in the type coating applied in accordance with this Specification. The adjusting mechanism shall be sealed. The holiday detector shall be checked and recalibrated, if necessary, every four (4) hours with an accurate D.C. voltage meter furnished by CONTRACTOR and by use on a control coated pipe with known holidays The search electrode shall be steel spring, wet sponge or conductive rubber CONTRACTOR shall test all coating applications immediately after coating for holidays, pinholes and discontinuities. Testing for coating flaws shall be in accordance with the latest edition of NACE RP 02. Minimum voltage shall never be less than 125 volts per mil of coating thickness All holidays and other coating defects shall be marked with non grease type markers and the number and types of holidays recorded for each pipe joint Any joint of pipe with unacceptable, unbonded, or non adherent coating and pipe with excessive damaged coating and/or holidays in excess of 10 per 40 feet joint length, shall be rejected and reblasted and recoated. Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 11 of 17

12 Patching repair limits will be based on 1 holiday per each foot of length with a maximum of 10 holidays for an average 40 foot joint and 13 holidays for an average 60 foot joint. Repetitious holiday counts near maximum shall be cause for rejection. In all cases, COMPANY s authorized representative, shall make the final acceptance/rejections determination In the event the specified dry mil average is not of sufficient thickness to prevent more than the maximum allowable holidays per 40 foot joint of pipe, then it will be the responsibility of the coating applicator to increase the thickness sufficiently to meet the specified maximum allowable holiday requirement. This increase in coating thickness and extra expense will be done only with authorization of the COMPANY s Representative Coated pipe requiring closer inspection of cured coating film by COMPANY s Representative shall be set aside at no additional cost Laboratory analysis of coating materials shall be conducted for each batch (or lot) at the COMPANY s discretion When requested, applicator shall furnish sufficient amount of cured coating to allow the COMPANY to perform infra red scans and/or Differential Scanning Calorimeter (DSC) to determine conformance with manufacturer s specifications Ring Samples A coated sample 12 in length shall be cut from the end of a joint of pipe, labeled by coating date, joint number, and batch number. The cleaning, heating, and application history shall also be included. Ring samples may be selected from pipe as requested by the COMPANY s authorized representative Weighing General CONTRACTOR shall weigh every joint of pipe before and after being coated, and record these weights for submittal to COMPANY with all other required documentation Weigh Scales and Calculation The pipes shall be weighed with a 20,000 pound scale which is certified to be accurate within ten pounds based on calibration with weights traceable to the weights at the National Bureau of Standards, the scale shall be calibrated before and after used to weigh pipe. The CONTRACTOR shall furnish calibration certificates showing that the scale was calibrated no more than 30 days before weighing. Before coating begins, the CONTRACTOR shall weigh twenty one randomly selected FBE coated pipes. The first pipe weighed shall be set aside and used as a reference to be used to check the scale calibration each day before any weighing is done Weighing Procedure CONTRACTOR shall prepare a submerged weight procedure to be presented with its work plan for COMPANY approval. CONTRACTOR shall supply facilities to weigh coated pipe in water. The water temperature and density shall be measured and recorded before and after weighing and water samples collected and labeled daily. Twenty percent (20%) of all the coated casing pipes shall be fully submerged for weighing. CONTRACTOR will temporarily cap both ends of joint to be weighed so that it is completely watertight during immersion. Watertight night caps of known weight, such as those made by CRC pipeline equipment, or COMPANY approved equal; shall be Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 12 of 17

13 affixed to edge of each end of the pipe. CONTRACTOR shall weigh these caps before and after weighing each joint of pipe to an accuracy of ± 0.1 lb. CONTRACTOR shall ballast the pipe as required to fully submerged pipe. The ballast shall be equally distributed along the casing joint to be weighed. The added ballast required will be between 275 lbs. and 300 lbs. shall also be weighed to an accuracy of ± 0.1 lb. before and after each joint is weighed. 6.5 REPAIRS CONTRACTOR shall repair coating which does not comply with the requirements of this specification using methods described in CONTRACTOR's approved work plan. The work plan should describe required procedures for each of the following defects: a) Coating which is too heavy or too thick, b) Coating which is too light or too thin, the shear strength conforms to the minimum values given by the coating Manufacturer. 7.2 DEMONSTRATION The CONTRACTOR shall qualify his coating methods by coating a test pipe using methods and equipment described in his work plan. The demonstration shall include all aspects of the coating process, including surface preparation, coating application, curing, inspection, weighing and testing. This test shall be done at least four weeks before production begins, and production shall not begin until COMPANY approves his work plan after the demonstration. 7.3 IMPACT TESTING The CONTRACTOR shall perform an impact test on the demonstration pipe according to ASTM G 14. The coating must absorb at least 3 foot pounds of energy with no loss of adhesion or cracking. c) Coating which is not properly cured, d) Coating with localized damage 7. PRE QUALIFICATION TESTING 7.1 ADHESION TEST Before work begins, the CONTRACTOR shall do a prequalification test for the shear strength of the coating using the method of ASTM D , modified as follows. One of the plates used to test the shear strength shall be prepared by coating it with fusion bonded epoxy approximately the same thickness as the undercoating on the pipe. The cured fusion bonded epoxy shall then be roughened using the same method of sweep blasting that the CONTRACTOR proposes to use for roughing the FBE surface during production. The test shall show that Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 13 of 17

14 APPENDIX A SUMMARY OF TEST REQUIREMENTS Table 1 Powder Acceptance/Qualification Tests (if Powder is 3 to 6 months old) Stock inspection dates Appendix B {Verify} Shelf Life Adhesion Test Demonstration Impact Test Appendix B {Verify} {Sec. 7.1} {Sec. 7.2} {Sec. 7.2} Table 2 Frequency of Tests on Coated Pipe Visual Thickness Dry Weight Submerged Weight Frequency Each Joint 100% of joints 20% of joints {Sec } {Sec } {Sec } {Sec } Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 1 of 17

15 APPENDIX B VENDOR DATA REQUIREMENTS LIST (VDRL) CLIENT: P.O./S.C. NO.: LOCATION: Gulf of Mexico SELLER/SUBCONTRACTOR: EQUIPMENT TAG NO.(S): DESCRIPTION(S): Abrasion Resistant Coating of Line Pipe The seller's/subcontractor's quotation shall state his intended compliance with this listing, as regards to the type of data required and schedule for data submittal, as well as the quantity and data form (reproducible, prints, etc.) indicated in the inquiry and purchase order/subcontract standard clauses. The seller/subcontractor shall confirm responsibility for similar compliance by his subvendors and/or subcontractors. As a part of the seller's/subcontractor's quotation, any deviation(s) from the data submittal schedule shall be shown in the comments column. All data submitted shall be identified with equipment tag number, equipment description, buyer's job number, and purchase order/subcontract number. AFTER ORDER IS PLACED, UNLESS OTHERWISE NOTED IN THE COMMENTS COLUMN, the following data submittal schedule shall apply: FOR APPROVAL DATA DUE 3 WEEKS AFTER PURCHASE ORDER/SUBCONTRACT IS PLACED, CERTIFIED CORRECT DATA DUE 4 WEEKS AFTER BUYER'S APPROVAL, RECORD DATA DUE 8 WEEKS AFTER PURCHASE ORDER/SUBCONTRACT IS PLACED. ABBREVIATIONS: Q = With Quotation, A = Approval, C = Certified by CONTRACTOR, R = Record, P = Prints, RP = Reproducible, M = Microfilm, S = Shotdown Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 1 of 17

16 VENDOR DATA REQUIREMENTS LIST (VDRL) Data Data Required Code Data Description/Definition Q A C R Comments CONTRACTOR Data Schedule 3P Production Schedule 3P Equipment Condition 3P QA/QC Plan 3P Pipe Handling Pipe Inspection Procedure Stock Inspection Certificate Shelf Life Surface Preparation Procedure 3P Coating Application Procedure 3P Coated Pipe Handling Procedure Repair Procedure Adhesion Test Demonstration Test Impact Test Visual Inspection Thickness Test Coated Pipe Weights Coated Pipe Submerged Weight Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 2 of 17

17 APPENXI C INSPECTION MATRIX 1. Observed/Verify by Inspection 2. Review of Documentation 3. Obtain Certification/Test Documents ACTIVITIES COMMENTS 1 Pre Coating Meeting X QA rep. to attend meeting 2 Specifications X 3 Contractor's Quality Plan X Sec Materials Certificates X Appendix B 5 Locate Abrasion Coating X Appendix B Materials, Trace To Certificates, Verify Marking/Age 6 Transportation, Handling X X Sec Storage 7 Segregating Damaged Pipe X Sec Method of Application X Sec Equipment: Type/Condition X Sec Inspection and cleaning X Sec End Caps/Internal Protection X Sec ; Masking X Sec Abrasive Cleaning X Sec Final Surface Preparation X Sec Multiple coats X Sec Curing X Sec Marking X Sec Visual Inspection X Sec Thickness X Sec Weighing X Sec Repairs X Sec. 6.5 Qualification Tests 22 Adhesion Test X X Sec Demonstration Test X X Sec Impact Test X X Sec Tag pipes to release for shipment X Sec Loading and Shipping procedures X Sec Loading/Shipping X Sec Specification for Material and Application of Abrasive Resistant Coating on Steel Line Pipe 1 of 17