Aromatic amines and carcinogens acc. to COE Resolution ResAP(2008)1: Part 1a, Part 1b

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1 Krackser Straße Germany [Arrival date CTL] [Test] Aromatic amines and carcinogens acc. to COE Resolution ResAP(2008)1: Part 1a, Part 1b Part 1a Investigationn of aromatic amines with carcinogenic, mutagenic, reprotoxic and sensitising properties according to COE Resolution ResAP(2008)1 Detection limit: 1 ppm; Limit: as low as technically avoidable DIN EN 14362, 64 LFGB ,3,4,9 Amine EC-No. CAS-No. Amine EC-No. CAS-No. Biphenyl-4-ylamine ,3'-Dimethoxybenzidine Benzidine ,3'-Dimethylbenzidine Chloro-o-toluidine ,4'-Methylenedi-o-toluidine Naphthylamine Methoxy-m-toluidine o-aminoazotoluene ,4'-Methylenebis-(2-chloroaniline) Nitro-o-toluidine Methyl-m-phenylenediamine Chloroaniline o-anisidine Methoxy-m-phenylenediamine Aminoazobenzene ,4'-Methylenedianiline Amino-2-ethoxynaphthaline ,3'-Dichlorobenzidine Amino-3-fluorophenol Part 1b Investigationn of carcinogens classified in Categories 1, 2 and 3 by the Euro Commission and mentioned in the Council Directive 1967/548/EEC of 27 June opean 1967 according to COE Resolution ResAP(2008)1 Detection limit: 1 ppm DIN EN 14362, 64 LFGB ,3,4,9 Amine EC-No. CAS-No. Amine EC-No. CAS-No. 4,4'-Oxydianiline Para-phenylenediamine ,4'-Thiodianiline ,4 Xylidine o-toluidine ,6 Xylidine ,4,5-Trimethylaniline () = below detection limit

2 Krackser Straße Germany [Arrival date CTL] [Test] Dyestuffs acc. to COE Resolution ResAP(2008)1: Part 2 Part 2 Investigation of Dyestuffs according to COE Resolution ResAP(2008)1 Detection limit: 5 mg/l DIN in the up-to-date legislation TLC Analysis Colourant Cl-No. CAS-No. Colourant Cl-No. CAS-No. Acid Green Disperse Orange Acid Red Disperse Red Acid Violet Disperse Red Acid Violet Disperse Yellow Acid Yellow Disperse Yellow Basic Blue Pigment Orange Basic Green Pigment Red Basic Red Pigment Violet : Basic Red Pigment Violet : Basic Violet Solvent Blue Basic Violet Solvent Orange Basic Violet Solvent Red Disperse Blue Solvent Red : Disperse Blue Solvent Violet : Disperse Blue Solvent Yellow Disperse Blue Solvent Yellow Disperse Blue Solvent Yellow Disperse Orange () = below detection limit

3 Krackser Straße Germany [Arrival date CTL] [Test] Heavy Metals acc. to COE Resolution ResAP(2008)1: Part 3 Part 3 Investigation of Heavy Metals according to COE Resolution ResAP(2008)1 Method: Prior, G. (2014). Tattoo Inks: Analysis, Pigments, Legislation. Berlin: epubli. CTL Method 2, p. 83. Elements or compound Limit Detection limit Elements or compound Limit Detection limit < 1 Arsenic (As) < 2 1 < 0.1 Nickel (Ni) As low as technically achievable 0.1 < 5 Barium (Ba) < 50 5 < 1 Lead (Pb) < 2 1 < 0.1 Cadmium (Cd) < < 1 Selenium (Se) < 2 1 < 5 Cobalt (Co) < 25 5 < 1 Antimony (Sb) < 2 1 < 0.1 Chromium (Cr), VI < < 5 Tin (Sn) < 50 5 < 5 Copper (Cu), soluble < 25 5 < 5 Zinc (Zn) < 50 5 < 0.1 Mercury (Hg) <

4 Krackser Straße Germany [Arrival date CTL] [Test] PAH and BaP acc. to COE Resolution ResAP(2008)1: Part 4 Part 4 Investigation of Polycyclic aromatic hydrocarbons (PAH) and Benzo-a-pyrene (BaP) according to COE ResAP(2008)1 Detection limit: PAH: 0.05 ppm as total; Benzo-a-pyrene: 0.5 ppb Limit: PAH: 0.5 ppm as total; Benzo-a-pyrene: 5 ppb EPA, ZEK Elements or compound Elements or compound Naphthalene Benz(a)anthracene Acenaphthylene Chrysene Acenaphthene Benzo(b)fluoranthene Fluorene Benzo(k)fluoranthene Phenanthrene Dibenzo(a,h)anthracene Anthracene Indo (1,2,3-cd)pyrene Fluoranthene Benzo(g,h,i)perylene Pyrene Benzo-a-pyrene (BaP) Result as total: all below detection limit BIELEFELD, 15. JULY 2015 () = below detection limit

5 Krackser Straße Germany [Arrival date CTL] [Test] Sterility acc. to COE Resolution ResAP(2008)1; ASU 64 LFGB L ;- L : Part 5 tested on a single representative sample Part 5 Investigation of Sterility Detection limit: < 1.0 x 10 0 CFU/g Results Microbiological test: pseudomonads = King A, King B, Oxidase test acc. to COE ResAP(2008)1 Anaerobes sulfite-reducing sporulating bacteria acc. to ASU 64 LFGB L Aerobes mesophilic sporulating bacteria acc. to ASU 64 LFGB L BIELEFELD, 10. JULY 2015