ANALYTICAL SUMMARY REPORT

Transcription

1 ANALYTICAL SUMMAY EPOT vember 01, st Ave N Lewistown, MT Work Order: Project Name: B MT Energy Laboratories Inc Billings MT received the following 1 sample for on 10/19/2018 for analysis. Lab ID Client Sample ID Collect Date eceive Date Matrix Test B Spigot By Distilled 10/18/18 13:00 10/19/18 Drinking Water Metals by ICP/ICPMS, Drinking Water Alkalinity Color Mercury, Drinking Water Fluoride Chloride Sulfate/Anions by Ion Chromatography Nitrogen, Nitrate + Nitrite Odor ph Metals Digestion by E200.2 Mercury Digestion by E245.1 Preparation for TDS A2540 C Solids, Total Dissolved Turbidity The analyses presented in this report were performed by Energy Laboratories, Inc., 1120 S 27th St., Billings, MT 59101, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical eport, the QA/QC Summary eport, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. eport Approved By: Page 1 of 21

2 LABOATOY ANALYTICAL EPOT Lab ID: B Client Sample ID: Spigot By Distilled PWS #: MT Name: LEHKINDS BIG SPING WATE Collection Date: 10/18/18 13:00 Facility ID: TP001 Date eceived: 10/19/18 SamplingPoint/Location: EP502 / Spigot By Distilled Matrix: Drinking Water Project ID:MT Federal ID#: MT00005 Collector's Name: Don Cates Contact Phone #: (406) Compliance Sample: YES Sample Type: T FDS Analyses esult Units L MCL/ QCL Method Analysis Date / By PHYSICAL POPETIES 1925 ph 7.8 s.u. H 0.1 A4500-H B ph Measurement Temp 13 C A4500-H B 1905 Color ND c.u. H 5 A2120 B 1920 Odor 1 T.O.N. A2150 B Odor Measurement Temp ph at Time of Color Analysis 60 C A2150 B 8.0 s.u. 0.1 A2120 B 0100 Turbidity ND NTU 0.1 A2130 B 1930 Solids, Total Dissolved 180 C 292 mg/l 10 A2540 C 10/20/18 11:50 / pjw 10/20/18 11:50 / pjw 10/22/18 16:08 / rco 10/19/18 09:55 / pjw 10/19/18 09:55 / pjw 10/22/18 16:08 / rco 10/20/18 11:32 / pjw 10/25/18 11:41 / klj INOGANICS 1927 Alkalinity, Total as CaCO3 163 mg/l 4 A2320 B 1928 Bicarbonate as HCO3 199 mg/l 4 A2320 B 1929 Carbonate as CO3 4 A2320 B 1017 Chloride 1 E Sulfate 84 mg/l 1 E Fluoride 0.6 mg/l 0.1 A4500-F C 10/24/18 21:00 / cke 10/24/18 21:00 / cke 10/24/18 21:00 / cke 10/23/18 19:43 / rco 10/23/18 19:43 / rco 10/25/18 11:24 / mmc NUTIENTS 1038 Nitrogen, Nitrate+Nitrite as N 0.17 mg/l E353.2 METALS, TOTAL 1002 Aluminum 0.03 E Antimony E Arsenic E Barium E Beryllium E Cadmium E Calcium 68 mg/l 1 E Chromium E Copper mg/l E Iron 0.02 E Lead E Magnesium 20 mg/l 1 E Manganese E Mercury E Nickel 0.01 E /22/18 10:37 / mjm 10/24/18 00:15 / by 10/24/18 00:15 / by 10/24/18 00:15 / by 10/24/18 00:15 / by 10/24/18 00:15 / by 10/24/18 00:15 / by 10/30/18 15:35 / trc 10/24/18 00:15 / by eport Definitions: QCL - ity control limit. H - Analysis performed past recommended holding time. MCL - Maximum contaminant level. Page 2 of 21

3 LABOATOY ANALYTICAL EPOT Lab ID: B Client Sample ID: Spigot By Distilled PWS #: MT Name: LEHKINDS BIG SPING WATE Collection Date: 10/18/18 13:00 Facility ID: TP001 Date eceived: 10/19/18 SamplingPoint/Location: EP502 / Spigot By Distilled Matrix: Drinking Water Project ID:MT Federal ID#: MT00005 Collector's Name: Don Cates Contact Phone #: (406) Compliance Sample: YES Sample Type: T FDS Analyses esult Units L MCL/ QCL Method Analysis Date / By METALS, TOTAL 1042 Potassium 1 E Selenium E Silica 6.0 mg/l 0.2 E200.7 SILI Silicon 2.8 mg/l 0.1 E Silver E Sodium 2 mg/l 1 E Thallium E Zinc 0.01 E /24/18 00:15 / by 10/24/18 00:15 / by 10/24/18 00:15 / by eport Definitions: QCL - ity control limit. MCL - Maximum contaminant level. Page 3 of 21

4 Method: A2120 B Batch: Lab ID: MB Method Blank un: MISC-WC_181022C 10/22/18 16:08 Color ND c.u. Lab ID: LCS Laboratory Control Sample un: MISC-WC_181022C 10/22/18 16:08 Color 24.0 c.u Lab ID: B ADUP 2 Sample Duplicate un: MISC-WC_181022C 10/22/18 16:08 Color 4.00 c.u ph at Time of Color Analysis 8.00 s.u ifiers: Page 4 of 21

5 Method: A2130 B Batch: A-TUB-W Lab ID: MBLK (DI H2O) Method Blank un: HACH2100N_181020A 10/20/18 11:30 Turbidity ND NTU 0.08 Lab ID: Turb - 20 NTU Laboratory Control Sample un: HACH2100N_181020A 10/20/18 11:30 Turbidity 20.4 NTU Lab ID: Turb NTU Laboratory Control Sample un: HACH2100N_181020A 10/20/18 11:31 Turbidity 1.06 NTU Lab ID: B ADUP Sample Duplicate un: HACH2100N_181020A 10/20/18 11:33 Turbidity NTU ifiers: Page 5 of 21

6 Method: A2150 B Batch: Lab ID: MB Method Blank un: MISC-WC_181019F 10/19/18 09:55 Odor ND T.O.N. Odor Measurement Temp 60 C ifiers: Page 6 of 21

7 Method: A2320 B Batch: Lab ID: MBLK Method Blank un: Metrohm 3_181024A 10/24/18 20:49 Alkalinity, Total as CaCO3 6 mg/l 0.7 Lab ID: LCS Laboratory Control Sample un: Metrohm 3_181024A 10/24/18 20:54 Alkalinity, Total as CaCO3 102 mg/l Lab ID: B ADUP 3 Sample Duplicate un: Metrohm 3_181024A 10/24/18 21:07 Alkalinity, Total as CaCO3 163 mg/l Bicarbonate as HCO3 199 mg/l Carbonate as CO Lab ID: B AMS Sample Matrix Spike un: Metrohm 3_181024A 10/24/18 21:32 Alkalinity, Total as CaCO3 136 mg/l Lab ID: B ADUP 3 Sample Duplicate un: Metrohm 3_181024A 10/24/18 21:43 Alkalinity, Total as CaCO mg/l Bicarbonate as HCO mg/l Carbonate as CO ifiers: Page 7 of 21

8 Method: A2540 C Batch: Lab ID: MB Method Blank un: BAL #SD-15_181024A 10/25/18 11:39 Solids, Total Dissolved 180 C 10 Lab ID: LCS Laboratory Control Sample un: BAL #SD-15_181024A 10/25/18 11:39 Solids, Total Dissolved 180 C 989 mg/l Lab ID: B A DUP Sample Duplicate un: BAL #SD-15_181024A 10/25/18 11:40 Solids, Total Dissolved 180 C 2780 mg/l ifiers: Page 8 of 21

9 Method: A4500-F C Analytical un: Metrohm 3_181025A Lab ID: ICV Initial Calibration Verification Standard 10/25/18 11:01 Fluoride 1.01 mg/l Method: A4500-F C Batch: Lab ID: MBLK Method Blank un: Metrohm 3_181025A 10/25/18 11:07 Fluoride 0.05 Lab ID: LFB Laboratory Fortified Blank un: Metrohm 3_181025A 10/25/18 11:13 Fluoride 1.25 mg/l Lab ID: B AMS Sample Matrix Spike un: Metrohm 3_181025A 10/25/18 11:30 Fluoride 1.82 mg/l Lab ID: B AMSD Sample Matrix Spike Duplicate un: Metrohm 3_181025A 10/25/18 11:36 Fluoride 1.78 mg/l ifiers: Page 9 of 21

10 Method: A4500-H B Analytical un: PHSC _101-B_181020A Lab ID: ph 8 2 Initial Calibration Verification Standard 10/20/18 10:37 ph 8.01 s.u ph Measurement Temp 19.2 C 0 0 Method: A4500-H B Batch: Lab ID: B ADUP 2 Sample Duplicate un: PHSC _101-B_181020A 10/20/18 11:32 ph 6.85 s.u ph Measurement Temp 12.0 C Lab ID: B ADUP 2 Sample Duplicate un: PHSC _101-B_181020A 10/20/18 12:01 ph 7.61 s.u ph Measurement Temp 14.1 C ifiers: Page 10 of 21

11 Method: E200.7 Analytical un: ICP203-B_181023A Lab ID: ICV 12 Continuing Calibration Verification Standard 10/23/18 10:14 Aluminum 2.44 mg/l Barium 2.46 mg/l Beryllium 1.21 mg/l Calcium 25.1 mg/l Copper 2.39 mg/l Iron 2.55 mg/l Magnesium 25.8 mg/l Potassium 26.1 mg/l Silicon 4.96 mg/l Sodium 25.7 mg/l Zinc 2.47 mg/l Silica 10.6 mg/l 0.21 Method: E200.7 Batch: Lab ID: MB-6500DIS181023A 12 Method Blank un: ICP203-B_181023A 10/23/18 10:21 Aluminum 0.03 Barium Beryllium Calcium 0.07 Copper Iron 0.02 Magnesium 0.02 Potassium 0.1 Silicon 0.07 Sodium 0.1 Zinc Silica 0.2 Lab ID: LFB-6500DIS181023A 11 Laboratory Fortified Blank un: ICP203-B_181023A 10/23/18 10:29 Aluminum 4.90 mg/l Barium mg/l Beryllium mg/l Calcium 49.3 mg/l Copper mg/l Iron 4.97 mg/l Magnesium 51.3 mg/l Potassium 51.5 mg/l Silicon 9.66 mg/l Sodium 50.8 mg/l Zinc mg/l Lab ID: B CMS2 12 Sample Matrix Spike un: ICP203-B_181023A 10/23/18 12:11 Aluminum 5.01 mg/l Barium 1.04 mg/l Beryllium mg/l ifiers: Page 11 of 21

12 Method: E200.7 Batch: Lab ID: B CMS2 12 Sample Matrix Spike un: ICP203-B_181023A 10/23/18 12:11 Calcium 127 mg/l Copper mg/l Iron 4.98 mg/l Magnesium 73.8 mg/l Potassium 54.9 mg/l Silicon 22.5 mg/l Sodium 70.3 mg/l Zinc 1.00 mg/l Silica 48.2 mg/l Lab ID: B CMSD 12 Sample Matrix Spike Duplicate un: ICP203-B_181023A 10/23/18 12:15 Aluminum 5.08 mg/l Barium 1.06 mg/l Beryllium mg/l Calcium 126 mg/l Copper mg/l Iron 5.03 mg/l Magnesium 74.5 mg/l Potassium 56.1 mg/l Silicon 22.8 mg/l Sodium 71.4 mg/l Zinc 1.01 mg/l Silica 48.7 mg/l ifiers: Page 12 of 21

13 Method: E200.8 Analytical un: ICPMS206-B_181022A Lab ID: QCS 10 Initial Calibration Verification Standard 10/23/18 19:45 Antimony mg/l Arsenic mg/l Cadmium mg/l Chromium mg/l Lead mg/l Manganese mg/l Nickel mg/l Selenium mg/l Silver mg/l Thallium mg/l Method: E200.8 Batch: Lab ID: LB 10 Method Blank un: ICPMS206-B_181022A 10/22/18 17:45 Antimony Arsenic Cadmium Chromium Lead Manganese Nickel Selenium Silver Thallium mg/l Lab ID: LFB 10 Laboratory Fortified Blank un: ICPMS206-B_181022A 10/23/18 08:11 Antimony mg/l Arsenic mg/l Cadmium mg/l Chromium mg/l Lead mg/l Manganese mg/l Nickel mg/l Selenium mg/l Silver mg/l Thallium mg/l Lab ID: B CMS 10 Sample Matrix Spike un: ICPMS206-B_181022A 10/24/18 00:01 Antimony mg/l Arsenic mg/l Cadmium mg/l Chromium mg/l Lead mg/l Manganese mg/l Nickel mg/l Selenium mg/l ifiers: Page 13 of 21

14 Method: E200.8 Batch: Lab ID: B CMS 10 Sample Matrix Spike un: ICPMS206-B_181022A 10/24/18 00:01 Silver mg/l Thallium mg/l Lab ID: B CMSD 10 Sample Matrix Spike Duplicate un: ICPMS206-B_181022A 10/24/18 00:06 Antimony mg/l Arsenic mg/l Cadmium mg/l Chromium mg/l Lead mg/l Manganese mg/l Nickel mg/l Selenium mg/l Silver mg/l Thallium mg/l ifiers: Page 14 of 21

15 Method: E245.1 Analytical un: HGCV202-B_191030A Lab ID: ICV Initial Calibration Verification Standard 10/30/18 14:03 Mercury mg/l Method: E245.1 Batch: Lab ID: MB Method Blank un: HGCV202-B_191030A 10/30/18 15:20 Mercury Lab ID: LCS Laboratory Control Sample un: HGCV202-B_191030A 10/30/18 15:22 Mercury mg/l Lab ID: B CMS Sample Matrix Spike un: HGCV202-B_191030A 10/30/18 15:25 Mercury mg/l Lab ID: B CMSD Sample Matrix Spike Duplicate un: HGCV202-B_191030A 10/30/18 15:27 Mercury mg/l ifiers: Page 15 of 21

16 Method: E300.0 Analytical un: IC METOHM 2_181022A Lab ID: ICV 2 Initial Calibration Verification Standard 10/22/18 11:27 Chloride 100 mg/l Sulfate 397 mg/l Method: E300.0 Batch: Lab ID: ICB 2 Method Blank un: IC METOHM 2_181022A 10/22/18 11:43 Chloride 0.05 Sulfate 0.03 Lab ID: LFB 2 Laboratory Fortified Blank un: IC METOHM 2_181022A 10/22/18 11:58 Chloride 25.1 mg/l Sulfate 99.5 mg/l Lab ID: B AMS 2 Sample Matrix Spike un: IC METOHM 2_181022A 10/23/18 21:16 Chloride 27.3 mg/l Sulfate 111 mg/l Lab ID: B AMSD 2 Sample Matrix Spike Duplicate un: IC METOHM 2_181022A 10/23/18 21:32 Chloride 28.8 mg/l S Sulfate 117 mg/l S ifiers: S - Spike recovery outside of advisory limits. Page 16 of 21

17 Method: E353.2 Analytical un: FIA203-B_181022A Lab ID: ICV Initial Calibration Verification Standard 10/22/18 09:49 Nitrogen, Nitrate+Nitrite as N mg/l Method: E353.2 Batch: Lab ID: MBLK Method Blank un: FIA203-B_181022A 10/22/18 09:50 Nitrogen, Nitrate+Nitrite as N Lab ID: LFB Laboratory Fortified Blank un: FIA203-B_181022A 10/22/18 09:51 Nitrogen, Nitrate+Nitrite as N mg/l Lab ID: B CMS Sample Matrix Spike un: FIA203-B_181022A 10/22/18 10:28 Nitrogen, Nitrate+Nitrite as N 1.18 mg/l Lab ID: B CMSD Sample Matrix Spike Duplicate un: FIA203-B_181022A 10/22/18 10:29 Nitrogen, Nitrate+Nitrite as N 1.17 mg/l ifiers: Page 17 of 21

18 Work Order eceipt Checklist B Login completed by: eviewed by: eviewed Date: ichard L. Shular BL2000\raschim 10/22/2018 Date eceived: 10/19/2018 eceived by: qej Carrier name: eturn-ups Ground Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as ph, DO, es Cl, Sulfite, Ferrous Iron, etc.) t Present t Present t Present Temp Blank received in all shipping container(s)/cooler(s)? t Applicable Container/Temp Blank temperature: 5.2 C Blue Ice Water - VOA vials have zero headspace? Water - ph acceptable upon receipt? VOA vials submitted t Applicable Standard eporting Procedures: Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as ph, Dissolved Oxygen and esidual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: The collection time indicated on the container label for sample Spigot By Distilled is 1:00pm and on the Chain of Custody it is 2:00pm. Proceeded with the collection date/time as indicated on the sample container. Page 18 of 21

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