SUBJECT DATE PAGE Item No Mineral EPA 13B. EPA 13A Chlorinated Hydrocarbons EPA TO-14A EPA TO-15 EPA TO-17 EPA TO-14A EPA TO-15

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1 Approved Methods: Air and Emissions 03/30/ of 19 Autonomous Detection Systems Biological Critical Agents 99 NYSDOH Approved Method 9900 Chemical Critical Agents 99 NYSDOH Approved Method 9900 Radioactive Critical Agents 99 NYSDOH Approved Method 9900 Mineral Fluoride, Total 99 EPA 14A 4389 COLOR EPA 13B IC EPA 26 POT EPA 13A Chlorinated Hydrocarbons Hexachlorobutadiene NIOSH GC-ELCD 40 CFR PART Method 18 Hexachloroethane GC-ELCD 40 CFR PART Method 18 1,2,4-Trichlorobenzene NIOSH GC-ELCD 40 CFR PART Method

2 Approved Methods: Air and Emissions 03/30/ of 19 Metals I Lead, Total CVAAS EPA FAAS EPA 29 FAAS NIOSH 7082 GFAAS EPA 29 GFAAS EPA 7010 ICP-AES EPA 29 (6010) ICP-AES NIOSH 7300 ICP-AES NIOSH 7303 ICP-MS 40 CFR PART APP G ICP-MS EPA 29 (6020) ICP-MS Inter-Mountain TSP Lead PREP 40 CFR PART 50 APP G Priority Pollutant Phenols Pentachlorophenol HPLC-UV NIOSH 5512 Phenol GC-FID NIOSH Chlorinated Hydrocarbon Pesticides Alachlor Aldrin NIOSH 4, VOL NYS DOH APC

3 Approved Methods: Air and Emissions 03/30/ of 19 Chlorinated Hydrocarbon Pesticides alpha-bhc beta-bhc Lindane NIOSH 4, VOL Chlordane Total NIOSH 5510 NYS DOH APC-34 4,4'-DDD 4,4'-DDE 4,4'-DDT NIOSH 2, VOL. 3 S274 Dieldrin NIOSH 2, VOL. 3 S283 NYS DOH APC-34 Endrin NIOSH 5519 Heptachlor

4 Approved Methods: Air and Emissions 03/30/ of 19 Chlorinated Hydrocarbon Pesticides Heptachlor epoxide Metolachlor Toxaphene NIOSH Trifluralin Metals II Mercury, Total CVAAS 40 CFR 61 Method CVAAS CVAAS EPA 102 CVAAS EPA CFR 61 Method 101A CVAAS NIOSH 6009 CVAAS CVAFS NYS DOH APC-16 Frontier Sorbent Total Mercury Beryllium, Total FAAS 40 CFR Method Metals III ICP-AES NIOSH 7300 ICP-AES NIOSH 7303 Chromium, Total FAAS 40 CFR C METH FAAS 40 CFR PART APP. A METH 3 FAAS 40 CFR PART APP A METH 12 FAAS ICP-AES 40 CFR PART 63 APP A 306,A,B 40 CFR PART 63 APP A 306,A,B

5 Approved Methods: Air and Emissions 03/30/ of 19 Metals III Chromium, Total ICP-AES NIOSH ICP-AES NIOSH 7303 ICP-MS 40 CFR PART APP. A METH 3 Polychlorinated Biphenyls PCBs and Aroclors NIOSH 5503 NYS DOH Purgeable Halocarbons Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride GC-ELCD 40 CFR PART Method 18 EPA TO-1 EPA TO-2 Chloroform GC-ELCD 40 CFR PART Method 18 GC-ELCD EPA TO

6 Approved Methods: Air and Emissions 03/30/ of 19 Purgeable Halocarbons Chloroform EPA TO-1 EPA TO-2 Chloroethane Chloromethane 3-Chloropropene (Allyl chloride) Dibromochloromethane Dichlorodifluoromethane 1,2-Dibromoethane 1,2-Dibromo-3-chloropropane 1,1-Dichloroethane GC-ELCD 40 CFR PART Method 18 1,2-Dichloroethane GC-ELCD 40 CFR PART Method

7 Approved Methods: Air and Emissions 03/30/ of 19 Purgeable Halocarbons 1,2-Dichloroethane GC-ELCD EPA TO EPA TO-1 EPA TO-2 cis-1,2-dichloroethene GC-ELCD 40 CFR PART Method 18 trans-1,2-dichloroethene 1,1-Dichloroethene GC-ELCD 40 CFR PART Method 18 GC-ELCD EPA TO-3 EPA TO-2 1,2-Dichloropropane NIOSH GC-ELCD 40 CFR PART Method 18 EPA TO-1 cis-1,3-dichloropropene

8 Approved Methods: Air and Emissions 03/30/ of 19 Purgeable Halocarbons cis-1,3-dichloropropene trans-1,3-dichloropropene Methylene chloride GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH 1005 EPA TO-2 1,1,2,2-Tetrachloroethane GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH 1019 Tetrachloroethene GC-ELCD 40 CFR PART Method 18 GC-ELCD EPA TO-3 GC-ELCD NYS DOH METH GC-ELCD NYS DOH METH EPA TO

9 Approved Methods: Air and Emissions 03/30/ of 19 Purgeable Halocarbons 1,1,1-Trichloroethane GC-ELCD 40 CFR PART Method 18 1,1,2-Trichloroethane GC-ELCD 40 CFR PART Method 18 Trichloroethene GC-ELCD 40 CFR PART Method 18 GC-ELCD NYS DOH METH Trichlorofluoromethane 1,1,2-Trichloro-1,2,2-Trifluoroethane Vinyl bromide Vinyl chloride GC-ELCD 40 CFR PART Method 18 GC-ELCD 40 CFR, PART APP. B METH 1 GC-FID NIOSH 1007 EPA TO

10 Approved Methods: Air and Emissions 03/30/ of 19 Volatile Chlorinated Organics Benzyl chloride GC-ELCD 40 CFR PART Method 18 Epichlorohydrin GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH 1010 Polynuclear Aromatics Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(b)fluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Benzo(a)pyrene GC-FID NIOSH Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH

11 Approved Methods: Air and Emissions 03/30/ of 19 Polynuclear Aromatics Naphthalene GC-FID NIOSH HPLC-UV NIOSH 5506 Phenanthrene Pyrene Purgeable Aromatics Benzene GC-ELCD 40 CFR PART Method 18 GC-ELCD EPA TO-3 GC-FID NIOSH 1501 EPA TO-1 EPA TO-2 Chlorobenzene GC-ELCD 40 CFR PART Method 18 GC-ELCD EPA TO-3 2-Chlorotoluene 1,2-Dichlorobenzene GC-ELCD 40 CFR PART Method

12 Approved Methods: Air and Emissions 03/30/ of 19 Purgeable Aromatics 1,2-Dichlorobenzene 1,4-Dichlorobenzene GC-ELCD 40 CFR PART Method 18 1,3-Dichlorobenzene Ethyl benzene GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH 1501 EPA TO-1 Isopropylbenzene Toluene GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH 1501 EPA TO-1 EPA TO

13 Approved Methods: Air and Emissions 03/30/ of 19 Purgeable Aromatics Total Xylenes GC-ELCD 40 CFR PART Method 18 GC-FID NIOSH 1501 EPA TO-1 o-xylene GC-FID NIOSH m/p-xylenes GC-FID NIOSH ,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Styrene GC-FID NIOSH Chlorophenoxy Acid Pesticides 2,4-D

14 Approved Methods: Air and Emissions 03/30/ of 19 Chlorophenoxy Acid Pesticides 2,4-D HPLC-UV NIOSH ,4,5-T HPLC-UV NIOSH Miscellaneous Asbestos TEM 40 CFR 763 APX A No. III 4588 TEM NIOSH 7402 TEM YAMATE,AGARWAL GIBB Fibers PCM NIOSH 7400 A RULES 4587 Formaldehyde NIOSH HPLC-FLUOR HPLC-UV EPA IP-6A HPLC-UV NIOSH 2016 Nitrogen Dioxide COLOR 40 CFR 60 Method COLOR COLOR COLOR 40 CFR 60 Method 7B 40 CFR 60 Method 7C 40 CFR 60 Method 7E COLOR NIOSH 6700 IC IC 40 CFR 60 Method 7A 40 CFR 60 Method 7D Nitrogen Oxide COLOR 40 CFR 60 Method COLOR COLOR COLOR IC IC 40 CFR 60 Method 7B 40 CFR 60 Method 7C 40 CFR 60 Method 7E 40 CFR 60 Method 7A 40 CFR 60 Method 7D

15 Approved Methods: Air and Emissions 03/30/ of 19 Miscellaneous Sulfuric Acid TITR 40 CFR 60 Method Sulfur Dioxide COLOR 40 CFR 60 Method 6C 6046 GRAV GRAV 40 CFR 60 Method 6A 40 CFR 60 Method 6B TITR 40 CFR 60 Method 6 TITR 40 CFR 60 Method 8 Suspended Particulates GRAV 40 CFR 60 APP A Method GRAV GRAV 40 CFR PART 50 APP B 40 CFR PART 50 APP J (PM10) Particulates GRAV 40 CFR 60 APP A Method GRAV GRAV EPA 17 GRAV EPA 201 GRAV 40 CFR PART 50 APP B EPA 201A GRAV EPA 5 GRAV NIOSH 0500 Radon 99 Alpha Track 7035 Fuels PROP CNT PROP CNT PROP CNT SCIN CNT VOLT Charcoal canister Continuous Radon Monitor Continuous Working level monitor Charcoal - Liquid Scintillation Electret B.T.U. 99 ASTM D ASTM D

16 Approved Methods: Air and Emissions 03/30/ of 19 Fuels B.T.U. 99 ASTM D ASTM D5865 TITR ASTM D4239 Percent Sulfur TITR ASTM D TITR XRF XRF Volatile Organics ASTM D4239 ASTM D2622 ASTM D4294 Acetaldehyde GC-ELCD 40 CFR PART Method 18 HPLC-UV Acetone GC-ELCD 40 CFR PART Method 18 HPLC-UV Acrolein (Propenal) HPLC-UV Benzaldehyde HPLC-UV 1,3-Butadiene 2-Butanone (Methylethyl ketone) Butyraldehyde HPLC-UV

17 Approved Methods: Air and Emissions 03/30/ of 19 Volatile Organics Carbon Disulfide Crotonaldehyde HPLC-UV Cyclohexane 1,2-Dichlorotetrafluoroethane 2,5-Dimethylbenzaldehyde HPLC-UV 1,4-Dioxane GC-ELCD 40 CFR PART Method 18 Hexanaldehyde HPLC-UV Hexane GC-ELCD 40 CFR PART Method 18 n-heptane Isopropanol Isovaleraldehyde HPLC-UV Methanol GC-ELCD 40 CFR PART Method 18 Methyl iodide 4-Methyl-2-Pentanone Methyl tert-butyl ether Nitrobenzene

18 Approved Methods: Air and Emissions 03/30/ of 19 Volatile Organics Propionaldehyde HPLC-UV tert-butyl alcohol 2,2,4-Trimethylpentane m-tolualdehyde HPLC-UV o-tolualdehyde HPLC-UV p-tolualdehyde HPLC-UV Valeraldehyde HPLC-UV Vinyl acetate Acrylates Acetonitrile GC-ELCD 40 CFR PART Method 18 Acrylonitrile Ethyl acrylate Methyl methacrylate Dioxins and Furans 2,3,7,8-Tetrachlorodibenzofuran GC-HRMS EPA 23 2,3,4,7,8-Pentachlorodibenzofuran GC-HRMS EPA 23 1,2,3,7,8-Pentachlorodibenzofuran GC-HRMS EPA 23

19 Approved Methods: Air and Emissions 03/30/ of 19 Dioxins and Furans 1,2,3,4,7,8-Hexachlorodibenzofuran GC-HRMS EPA 23 1,2,3,6,7,8-Hexachlorodibenzofuran GC-HRMS EPA 23 1,2,3,7,8,9-Hexachlorodibenzofuran GC-HRMS EPA 23 2,3,4,6,7,8-Hexachlorodibenzofuran GC-HRMS EPA 23 1,2,3,4,6,7,8-Heptachlorodibenzofuran GC-HRMS EPA 23 1,2,3,4,7,8,9-Heptachlorodibenzofuran GC-HRMS EPA 23 1,2,3,4,6,7,8,9-Octachlorodibenzofuran GC-HRMS EPA 23 2,3,7,8-Tetrachlorodibenzo-p-dioxin GC-HRMS EPA 23 1,2,3,7,8-Pentachlorodibenzo-p-dioxin GC-HRMS EPA 23 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin GC-HRMS EPA 23 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin GC-HRMS EPA 23 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin GC-HRMS EPA 23 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin GC-HRMS EPA 23 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin GC-HRMS EPA 23