ANALYTICAL RESULTS Print Date: 20-Jul-JJ. Advanced Technology Laboratories. 6 of 13. Figure G

Transcription

1 Advanced Technology Laboratories ANALYTICAL RESULTS Print Date: 20-Jul-JJ Lab Order: LabID: -003A Client ID: M-114 Collection Date: 7112/ :00:00 AM Matrix: GROUWATER Analyses PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUS BY GC/MS EPA8260B RunlO: MS2_110713A QC Batch: Q11VW129 PrepOate: Analyst: SLL cis-1,3-0ichloropropene J.lg/L 7/13/ :43 AM Oibromochloromethane J.lg/L 7/13/ :43 AM Oibromomethane J.lg/L 7/13/ :43 AM Oichlorodifiuoromethane J.lg/L 7/13/ :43 AM Ethylbenzene J.lg/L 7/13/ :43 AM Hexachlorobutadiene J.lg/L 7/13/ :43 AM Isopropylbenzene J.Jg/L 7/13/ :43 AM m,p-xylene 1.0 J.lg/L 7/13/ :43 AM Methylene chloride 1.0 J.lg/L 7/13/ :43 AM n-butylbenzene J.lg/L 7/13/ :43 AM n-propylbenzene J.lg/L 7/13/ :43 AM Naphthalene J.lg/L 7/13/ :43 AM o-xylene J.lg/L 7/13/ :43 AM sec-butylbenzene J.lg/L 7/13/201111:43 AM Styrene J.Jg/L 7/13/201111:43 AM tert-butylbenzene J.lg/L 7/13/ :43 AM Tetrachloroethene J.lg/L 7/13/ :43 AM Toluene J.lg/L 7/13/ :43 AM trans-1,2-0ichloroethene J.lg/L 7/13/ :43 AM T richloroethene J.lg/L 7/13/ :43 AM Trichlorofiuoromethane J.lg/L 7/13/ :43 AM Vinyl chloride IJg/L 7113/ :43 AM Hexane 1.0 J.lg/L 7/13/ :43 AM Surr: 1,2-0ichloroethane-d %REC 7/13/201111:43 AM Surr: 4-Bromofiuorobenzene %REC 7/13/ :43 AM Surr: Oibromofiuoromethane %REC 7/13/ :43 AM Surr: Toluene-d %REC 7/13/ :43 AM B detected in the associated Method Blank E Value above quantitation range Not Detected at the Reporting Limit s are wet unless otherwise specified Advanced Technology Laboratories 3275 Walnut Avenue 6 of 13 Signal Hill, CA Tel: Fax: Figure G

2 Advanced Technology Laboratories ANALYTICAL RESULTS Print Date: 20-Jul-II Lab Order: Lab ID: -003B Client ID: M-114 Collection Date: 7/12/ :00:00 AM Matrix: GROUWATER Analyses PQL Qual Units DF Date Analyzed DISSOLVED GASES IN WATER RSK175 RunlD: GC18_110713A QC Batch: Z11A033 PrepDate: Analyst: DMP Methane ug/l 7/13/201111:31 AM B detected in the associated Method Blank S Spike/Surrogate outside oflimits due to matrix interference Not Detected at the Reporting Limit s are wet unless otherwise specified Advanced Technology Laboratories 3275 Walnut Avenue 7 of 13 Signal Hill, CA Tel: Fax: Figure G

3 ;;t. t-< l:l <'l <:J- s:; l:l.. E?, Cl <'l.s Cl '"... Advanced Technology Laboratories ID: Q110713LCS1 LCS Client ID: LCSW Batch ID: Q11VW129 Date: 20-Jul-// TestCode: 8260_ WP+HEX_LL TestCode: 8260_WP+HE Units: Ilg/L Prep Date: Run No: EPA 8260B Analysis Date: 7/13/2011 SeqNo: u... N "- ;:s ;;:... ;;t. ;:s ;;: V:l 00' ;:s!?. 1.1-Dichloroethene Benzene Chlorobenzene Toluene Trichloroethene Surr: 1.2-Dichloroethane d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 ID: Q110713MB3MS Client ID: ZZZZZZ MS Batch ID: Q11VW TestCode: 8260_WP+HE Units: Ilg/L Prep Date: RunNo: EPA 8260B Analysis Date: 7/13/2011 SeqNo: r- Q a v, 1.1-Dichloroethene Benzene Chlorobenzene Toluene Trichloroethene Surr: 1.2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene v, 00.h. Surr: Dibromofluoromethane Surr: Toluene-d8 ID: Q110713MB3MSD Client ID: ZZZZZZ MSD Batch ID: Q11VW TestCode: 8260_WP+HE Units: Ilg/L Prep Date: Run No: EPA 8260B Analysis Date: 7/13/2011 SeqNo: v, B detected in the associated Method Blank '.v, 00.h. a Not Detected at the Reporting Limit 8 of 13 S Spike/Surrogate outside of limits due to I11Mrixinterference Figure G

4 MTA Westside, 4953-\ TestCode: 8260 WP+HEX LL : Q110713MB3MSD Client 10: ZZZZZZ MSD Batch 10: Q11VW129 TestCode: 8260_WP+HE Units: Ilg/L Prep Date: RunNo: EPA 8260B Analysis Date: 7/13/2011 SeqNo: ,1-0ichloroethene Benzene Chlorobenzene Toluene T richloroethene Surr: 1,2-0ichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Oibromofluoromethane Surr: Toluene-d PQl SPK value SPK Ref Val %REC lowlimit HighLimit RPO Ref Val %RPO RPOLimit Qual : Q110713MB3 TestCode: 8260_WP+HE Units: Ilg/L Prep Date: RunNo: Client 10: PBW Batch 10: Q11VW129 EPA 8260B Analysis Date: 7/13/2011 SeqNo: ,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2- Tetrachloroethane 1,1,2-Trichloroethane 1,1-0ichloroethane 1,1-0ichloroethene 1,1-0ichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-0ibromo-3-chloropropane 1,2-0ibromoethane 1,2-0ichlorobenzene 1,2-0ichloroethane 1,2-0ichloropropane PQl SPK value SPK Ref Val %REC lowlimit HighLimit RPO Ref Val %RPO RPOLimit Qual B detected in the associated Method Blank Not Detected at the Reporting Limit 9 of 13 Figure G

5 TestCode: 8260_ WP+HEX_LL ID: Q110713MB3 TestCode: 8260_WP+HE Units: Ilg/L Prep Date: RunNo: Client ID: PBW Batch ID: Q11VW129 EPA 8260B Analysis Date: 7/13/2011 SeqNo: PQl SPK value SPK Ref Val %REC lowlimit HighLimit RPD Ref Val %RPD RPDLimit Qual Trimethylbenzene 1.3-Dichlorobenzene 1.3-Dichloropropane 1A-Dichlorobenzene 2.2-Dichloropropane 2-Chlorotoluene 4-Chlorotoluene 4-lsopropyltoluene Benzene Bromobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1.2-dichloroethene cis-1.3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachlorobutadiene Isopropyl benzene m,p-xylene Methylene chloride n-butylbenzene n-propylbenzene B detected in the associated Method Blank Not Detected at the Reporting Limit 10 of 13 Figure G

6 TestCode: 8260 WP+HEX LL 10: Q110713MB3 TestCode: 8260_WP+HE Units: ijg/l Prep Date: Run No: Client 10: PBW Batch 10: Q11VW129 EPA 8260B Analysis Date: 7/13/2011 SeqNo: PQl SPK value SPK Ref Val %REC lowlimit HighLimit RPD Ref Val %RPD RPDLimit Qual Naphthalene o-xylene sec-butylbenzene Styrene tert-butylbenzene Tetrachloroethene Toluene trans-1,2-dichloroethene T richloroethene Trichlorofluoromethane Vinyl chloride Hexane 1.0 Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d B detected in the associated Method Blank Not Detected at the Reporting Limit H Holding times lor preparation or analysis exceeded 11 of 13 Figure G

7 TestCode: D1946 ID: MB-Z11A033 TestCode: D1946 Units: ppmv Prep Date: Run No: Client ID: ZZZZZZ Batch ID: Z11A033 ASTM Analysis Date: 7/13/2011 SeqNo: Methane 10 ID: LCS-Z11A033 Client ID: ZZZZZZ LCS Batch ID: Z11A033 TestCode: Units: ppmv Prep Date: RunNo: ASTM Analysis Date: 7/13/2011 SeqNo: Methane ID: LCSO-Z11A033 Client 10: ZZZZZZ LCSO Batch ID: Z11 A033 TestCode: Units: ppmv Prep Date: Run No: ASTM Analysis Date: 7/13/2011 SeqNo: PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPOLimit Qual Methane '. B detected in the associated Method Blank Not Detected at the Reporting Limit 12 of 13 Figure G

8 TestCode: RSK175 ATL ID: MB-Z11A033 TestCode: RSK175_ATL Units: ug/l Prep Date: Run No: Client ID: PBW Batch ID: Z11A033 RSK175 Analysis Date: 7/13/2011 SeqNo: PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Methane 1.0 ID: LCS-Z11A033 LCS TestCode: RSK175_ATL Units: ug/l Prep Date: Run No: Client ID: LCSW Batch ID: Z11A033 RSK175 Analysis Date: 7/13/2011 SeqNo: PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Methane ID: LCSD-Z11A033 LCSD TestCode: RSK175_ATL Units: ug/l Prep Date: Run No: Client ID: LCSS02 Batch ID: Z11A033 RSK175 Analysis Date: 7/13/2011 SeqNo: Methane PQL SPK value SPK Ref Val o %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual B detected in the associated Method Blank Not Detected at the Reporting Limit 13 of 13 Figure G

9 IECHLOGY Page 1 of 3 C July 21, 2011 Advanced Technology Laboratories A TTN: Rachelle Arada 3275 Walnut Ave. Signal HilI, CA ADE-1461 EPA Methods TO-3, T014A,T015 81M & Scan, A8TM FL Cert E8784/LA Cert EPA Melhods T03, T014A, T015, 25C/3C, RSK 175 TX Cert Tl TX EPA Methods T014A, TO-IS LABORATORY TEST RESULTS Project Reference: Lab Number: C Enclosed are results for sample(s) received 7/13111 by Air Technology Laboratories. Analyses were performed according to specifications on the chain of custody provided with the sample(s). Report Narrative: - analyses were performed within method performance criteria, and meet all requirements of the NELAC Standards. - All results are reported without qualifications unless otherwise noted. - The enclosed results relate only to the sample(s). ATL appreciates the opportunity to provide testing services to your company. If you have any questions regarding these results, please call me at (626) Sincerely, ;t1 Mark Johnson Operations Manager MJ ohnson@airtechlabs,com Enclosures Note: The cover letter is an integral part of this analytical report E. Gale Avenue, Suite City of/ndustry, CA Ph: (626) Fx: (626) Figure G