To: Dave Favero (RACER) Ref. No.:

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1 February, 0 To: ave Favero (RACER) Ref. No.: 00 From: Subject: John-eric Pardys/wg/ Topsoil Characterization JSS identified a potential source of topsoil to be used at RACER's Saginaw Malleable Industrial Land (Site), in Saginaw, Michigan. The potential topsoil source is located at West Freeland Road, Freeland, Michigan as shown in Figure. JSS's topsoil subcontractor provided a letter indicating that this land has been virgin farmland for the past 0 years and that historical records do not identify and other land uses (Attachment A). In addition, JSS's subcontractor provided additional documentation from the Tittabawassee Township that supports the excavation and transportation of topsoil from West Freeland Road, Freeland, Michigan (Attachment B). On, January, 0, GH reached out to MEQ to obtain concurrence on an acceptable approach to characterizing the topsoil. On, January, 0, MEQ provided their concurrence on the approach to characterizing the topsoil which included: collecting discrete samples of the topsoil and analyzing for Pesticides (Method SW 0), Herbicides (Method SW ), Atrazine and Alachlor (Method SW 0), and Arsenic and Lead (Method 00). On January, 0, GH conducted a Site visit to inspect the topsoil pile and collect the discrete samples. Photos of the stockpile are included in Attachment C. The topsoil stockpile was approximately 00' x 0' x -0'. An excavator was used to dig through the surficial frozen soil, approximately - feet, at nine locations spread evenly around the stockpile. Field staff dug another -inches into the pile before collecting the samples. The approximate locations of the samples collected are identified on Figure. Samples were submitted to the laboratory on a -week turn. There were no detections reported for pesticides or herbicides. The only detections were for arsenic ranging between. to. mg/kg, which is below the statewide default background level (. mg/kg) and lead ranging between. to. mg/kg, which is below the statewide default background level ( mg/kg). A copy of the analytical report is provided in Attachment. Therefore, based on the characterization results, the topsoil is suitable for use at the Site. GH Colby rive Waterloo Ontario NV C Canada T 00 F 0 W

0 00 00ft ETAIL SCALE "=00' Source: Image 0

2 ft ETAIL SCALE "=00' Source: Image 0 Google LEGEN APPROXIMATE PROPERTY BOUNARY TOPSOIL ISCRETE SAMPLE LOCATION figure TOPSOIL SOURCE WEST FREELAN ROA, FREELAN, MICHIGAN 0-T0(MEMO)GN-WA00 JAN, 0

3 Attachment A GH 00Memo--TPs

4 EGGERS EXCAVATING, LLC PO Box 0 Saginaw, MI 0 () 0 July, 0 RE: Letter of Virgin Source To Whom It May Concern: Eggers Excavating, LLC recently purchased a piece of property located at West Freeland Road, Freeland, Michigan to develop as commercial property. Part of the development process is to remove the upper portion of the site soil which is topsoil. This site has been virgin farmland for the past 0 years. Historical records indicate that the land has never been utilized for any other purpose. If you should have any further questions please feel free to call me at () 0. Respectfully Submitted, EGGERS EXCAVATING LLC Bill Slaughter VP of Operations

5 Attachment B GH 00Memo--TPs

10 Attachment C GH 00Memo--TPs

11 Photo Topsoil Stockpile. ate //0 Site Photographs GH 00Memo- Page

12 Photo Topsoil Stockpile. ate //0 Site Photographs GH 00Memo- Page

13 Photo Topsoil Stockpile. ate //0 Site Photographs GH 00Memo- Page

14 Photo Topsoil Stockpile. ate //0 Site Photographs GH 00Memo- Page

15 Attachment GH 00Memo--TPs

Sheldon Road, Suite 00 Plymouth, Michigan 0 Attn: Rawa Fleisher 0 Authorized for release by: //0 :0: PM enise Heckler, Project Manager II (0)- denise.

16 ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Shuffel Street NW North Canton, OH 0 Tel: (0)- TestAmerica Job I: 0-0- Client Project/Site:, RACER SMI For: GH Services Inc. Sheldon Road, Suite 00 Plymouth, Michigan 0 Attn: Rawa Fleisher 0 Authorized for release by: //0 :0: PM enise Heckler, Project Manager II (0)- denise.heckler@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

17 Project/Site:, RACER SMI Table of Contents TestAmerica Job I: 0-0- Cover Page Table of Contents Case Narrative efinitions/glossary Sample Summary etection Summary Method Summary QC Association Summary QC Sample Results Surrogate Summary Lab Chronicle Certification Summary Chain of Custody Receipt Checklists Page of //0

18 Case Narrative TestAmerica Job I: 0-0- Project/Site:, RACER SMI Job I: 0-0- Laboratory: Narrative Comments No additional comments. Job Narrative 0-0- Receipt The samples were received on //0 :0 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 0.º C. GC/MS Semi VOA Method(s) 0: The following sample was diluted due to appearance and viscosity: S--0-SSH-0 (0-0-). Elevated reporting limits () are provided. Method(s) 0: The initial calibration curve analyzed in batch 0-0 was outside method criteria for the following analyte: Alachlor. A reporting limit () standard was analyzed, and the target analyte was detected. Since the associated samples were non-detect for this analyte, the data have been reported. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. GC Semi VOA Method(s) 0: The following samples required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by sulfur: S--0-SSH-0 (0-0-) and S--0-SSH-0 (0-0-).0, 0. 0 No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. Metals No analytical or quality issues were noted, other than those described in the efinitions/glossary page. General Chemistry No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Organic Prep Method(s) 0C: ue to the matrix, the following samples could not be concentrated to the final method required volume: S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), S--0-SSH-0 (0-0-), (0-0-C- MS) and (0-0-C- MS). The reporting limits (s) are elevated proportionately. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. Page of //0

19 Project/Site:, RACER SMI efinitions/glossary TestAmerica Job I: 0-0- s GC/MS Semi VOA escription U Indicates the analyte was analyzed for but not detected. GC Semi VOA U F F p Metals U Glossary Abbreviation escription Indicates the analyte was analyzed for but not detected. MS and/or MS Recovery is outside acceptance limits. MS/MS RP exceeds control limits The %RP between the primary and confirmation column/detector is >0%. The lower value has been reported. escription Indicates the analyte was analyzed for but not detected. These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid ER uplicate error ratio (normalized absolute difference) il Fac ilution Factor L, RA, RE, IN Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision level concentration MA Minimum detectable activity EL Estimated etection Limit MC Minimum detectable concentration Method etection Limit ML Minimum Level (ioxin) NC Not Calculated N Not detected at the reporting limit (or or EL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) 0 Page of //0

20 Project/Site:, RACER SMI Sample Summary TestAmerica Job I: 0-0- Lab Sample I Client Sample I Matrix Collected Received 0-0- S--0-SSH-0 0// 0:0 0// 0: S--0-SSH-0 0// 0: 0// 0: S--0-SSH-0 0// 0:0 0// 0: S--0-SSH-0 0// 0: 0// 0: S--0-SSH-0 0// 0:0 0// 0: S--0-SSH-0 0// 0: 0// 0: S--0-SSH-0 0// :00 0// 0: S--0-SSH-0 0// :0 0// 0: S--0-SSH-0 0// :0 0// 0:0 0 Page of //0

21 Project/Site:, RACER SMI etection Summary TestAmerica Job I: 0-0- Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 0 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- Result il Fac Method Prep Type Arsenic mg/kg 00 Lead mg/kg 00 This etection Summary does not include radiochemical test results. Page of //0

22 Project/Site:, RACER SMI Method Summary TestAmerica Job I: 0-0- Method Method escription Protocol Laboratory 0 Semivolatile Organic Compounds (GC/MS) SW TAL BUF 0A Organochlorine Pesticides (GC) SW TAL CAN 0 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW TAL CAN A Herbicides (GC) SW TAL CAN 00 Metals (ICP/MS) SW TAL CAN Moisture Percent Moisture EPA TAL CAN Protocol References: EPA = US Environmental Protection Agency SW = "Test Methods For Evaluating Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL BUF = TestAmerica Buffalo, 0 Hazelwood rive, Amherst, NY -, TEL ()-00 TAL CAN =, 0 Shuffel Street NW, North Canton, OH 0, TEL (0)- 0 Page of //0

23 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 ug/kg 0/0/ 0: 0// : Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// : Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// : -Fluorobiphenyl 0-0 0/0/ 0: 0// : -Fluorophenol (Surr) - 0 0/0/ 0: 0// : Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// : p-terphenyl-d (Surr) - 0/0/ 0: 0// : Phenol-d (Surr) - 0 0/0/ 0: 0// : il Fac 0 Page of //0

24 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 ug/kg 0/0/ 0: 0// :0 Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// :0 Analyzed,,-Tribromophenol (Surr) 0-0 0/0/ 0: 0// :0 -Fluorobiphenyl 0-0 0/0/ 0: 0// :0 -Fluorophenol (Surr) - 0 0/0/ 0: 0// :0 Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// :0 p-terphenyl-d (Surr) - 0/0/ 0: 0// :0 Phenol-d (Surr) - 0 0/0/ 0: 0// :0 il Fac 0 Page of //0

25 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 ug/kg 0/0/ 0: 0// :0 Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// :0 Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// :0 -Fluorobiphenyl 0-0 0/0/ 0: 0// :0 -Fluorophenol (Surr) - 0 0/0/ 0: 0// :0 Nitrobenzene-d (Surr) 0-0 0/0/ 0: 0// :0 p-terphenyl-d (Surr) - 0/0/ 0: 0// :0 Phenol-d (Surr) - 0 0/0/ 0: 0// :0 il Fac 0 Page 0 of //0

26 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 ug/kg 0/0/ 0: 0// : Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// : Analyzed,,-Tribromophenol (Surr) 0-0 0/0/ 0: 0// : -Fluorobiphenyl 0-0 0/0/ 0: 0// : -Fluorophenol (Surr) 0-0 0/0/ 0: 0// : Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// : p-terphenyl-d (Surr) - 0/0/ 0: 0// : Phenol-d (Surr) - 0 0/0/ 0: 0// : il Fac 0 Page of //0

27 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 ug/kg 0/0/ 0: 0// : Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// : Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// : -Fluorobiphenyl /0/ 0: 0// : -Fluorophenol (Surr) 0-0 0/0/ 0: 0// : Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// : p-terphenyl-d (Surr) - 0/0/ 0: 0// : Phenol-d (Surr) - 0 0/0/ 0: 0// : il Fac 0 Page of //0

28 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 ug/kg 0/0/ 0: 0// : Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// : Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// : -Fluorobiphenyl 0-0 0/0/ 0: 0// : -Fluorophenol (Surr) - 0 0/0/ 0: 0// : Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// : p-terphenyl-d (Surr) - 0/0/ 0: 0// : Phenol-d (Surr) - 0 0/0/ 0: 0// : il Fac 0 Page of //0

29 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// :00 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 00 U 00 0 ug/kg 0/0/ 0: 0// :0 Atrazine Surrogate 0 U %Recovery 0 0 ug/kg 0/0/ 0: 0// :0 Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// :0 -Fluorobiphenyl /0/ 0: 0// :0 -Fluorophenol (Surr) - 0 0/0/ 0: 0// :0 Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// :0 p-terphenyl-d (Surr) - 0/0/ 0: 0// :0 Phenol-d (Surr) - 0 0/0/ 0: 0// :0 il Fac 0 Page of //0

30 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 0 U 0 00 ug/kg 0/0/ 0: 0// : Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// : Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// : -Fluorobiphenyl 0-0 0/0/ 0: 0// : -Fluorophenol (Surr) - 0 0/0/ 0: 0// : Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// : p-terphenyl-d (Surr) 0-0/0/ 0: 0// : Phenol-d (Surr) - 0 0/0/ 0: 0// : il Fac 0 Page of //0

31 Project/Site:, RACER SMI Method: 0 - Semivolatile Organic Compounds (GC/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Alachlor 00 U ug/kg 0/0/ 0: 0// : Atrazine Surrogate 00 U %Recovery 00 ug/kg 0/0/ 0: 0// : Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// : -Fluorobiphenyl 0-0 0/0/ 0: 0// : -Fluorophenol (Surr) 0-0 0/0/ 0: 0// : Nitrobenzene-d (Surr) - 0 0/0/ 0: 0// : p-terphenyl-d (Surr) - 0/0/ 0: 0// : Phenol-d (Surr) 0-0 0/0/ 0: 0// : il Fac 0 Page of //0

32 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-. U F F.. ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene. U. U. U. U. U. U. U. U. U. U F. U F F. U F. U F. U F F. U. U. U. U U F F 0 U.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :..0 ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. 0. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : 0 Surrogate %Recovery Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene 0-0 0// 0: 0/0/ : il Fac Page of //0

33 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-. U.. ug/kg 0// 0: 0/0/ :0,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U U 0 U %Recovery.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0..0 ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ :0.. ug/kg 0// 0: 0/0/ :0. ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ :0 Tetrachloro-m-xylene 0-0 0// 0: 0/0/ :0 il Fac 0 Page of //0

34 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-.0 U.0. ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U U 0 U %Recovery.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0 0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :. ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene 0-0 0// 0: 0/0/ : il Fac 0 Page of //0

35 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-.0 U.0. ug/kg 0// 0: 0/0/ :0,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U U 0 U %Recovery.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0. ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ :0 Tetrachloro-m-xylene // 0: 0/0/ :0 il Fac 0 Page 0 of //0

36 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-.0 U.0. ug/kg 0// 0: 0/0/ :0,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U U 0 U %Recovery.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ :0.0. ug/kg 0// 0: 0/0/ :0. ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ :0 Tetrachloro-m-xylene 0-0 0// 0: 0/0/ :0 il Fac 0 Page of //0

37 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-. U.. ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U U 0 U %Recovery.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :..0 ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. 0. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene 0-0 0// 0: 0/0/ : il Fac 0 Page of //0

38 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// :00 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-. U.. ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U U 0 U %Recovery.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :..0 ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. 0. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : Analyzed CB ecachlorobiphenyl 0-0// 0: 0/0/ : Tetrachloro-m-xylene 0-0 0// 0: 0/0/ : il Fac 0 Page of //0

39 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-.0 U.0. ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U.0 U U 0 U %Recovery.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :.0 0. ug/kg 0// 0: 0/0/ :.0. ug/kg 0// 0: 0/0/ :. ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene // 0: 0/0/ : il Fac 0 Page of //0

40 Project/Site:, RACER SMI Method: 0A - Organochlorine Pesticides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,'-. U..0 ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U. U U 0 U %Recovery.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. 0. ug/kg 0// 0: 0/0/ :.. ug/kg 0// 0: 0/0/ :. ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene 0-0 0// 0: 0/0/ : il Fac 0 Page of //0

41 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ 0: Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ 0: ug/kg 0// 0: 0/0/ 0: ug/kg 0// 0: 0/0/ 0: 0 ug/kg 0// 0: 0/0/ 0: ug/kg 0// 0: 0/0/ 0: ug/kg 0// 0: 0/0/ 0: Analyzed Tetrachloro-m-xylene 0-0// 0: 0/0/ 0: CB ecachlorobiphenyl 0-0// 0: 0/0/ 0: il Fac 0 Page of //0

42 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ : Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ : CB ecachlorobiphenyl 0-0// 0: 0/0/ : il Fac 0 Page of //0

43 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ :0 Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ :0 CB ecachlorobiphenyl 0-0// 0: 0/0/ :0 il Fac 0 Page of //0

44 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ : Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ : CB ecachlorobiphenyl 0-0// 0: 0/0/ : il Fac 0 Page of //0

45 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ :0 Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ :0 CB ecachlorobiphenyl 0-0// 0: 0/0/ :0 il Fac 0 Page 0 of //0

46 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ : Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : 0 ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ : CB ecachlorobiphenyl 0 0-0// 0: 0/0/ : il Fac 0 Page of //0

47 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// :00 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ : Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : ug/kg 0// 0: 0/0/ : Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ : CB ecachlorobiphenyl 0-0// 0: 0/0/ : il Fac 0 Page of //0

48 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 U ug/kg 0// 0: 0/0/ :0 Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery U U U U U U ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 ug/kg 0// 0: 0/0/ :0 Analyzed Tetrachloro-m-xylene 00-0// 0: 0/0/ :0 CB ecachlorobiphenyl 0 0-0// 0: 0/0/ :0 il Fac 0 Page of //0

49 Project/Site:, RACER SMI Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Aroclor-0 0 U 0 ug/kg 0// 0: 0/0/ :0 Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery 0 U 0 U 0 U 0 U 0 U 0 U 0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 0 0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 0 ug/kg 0// 0: 0/0/ :0 Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ :0 CB ecachlorobiphenyl 0-0// 0: 0/0/ :0 il Fac 0 Page of //0

50 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :. ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid 0-0 0// 0:0 0// : il Fac 0 Page of //0

51 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t 0 U 0. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery 0 U 0 ug/kg 0// 0:0 0// : 0.0 ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// : il Fac 0 Page of //0

52 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :. ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// : il Fac 0 Page of //0

53 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :. ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// : il Fac 0 Page of //0

54 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :. ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// : il Fac 0 Page of //0

55 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t 0 U 0. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery 0 U 0 ug/kg 0// 0:0 0// : 0.0 ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// : il Fac 0 Page 0 of //0

56 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// :00 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U.0 ug/kg 0// 0:0 0// :0,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :0. ug/kg 0// 0:0 0// :0 Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// :0 il Fac 0 Page of //0

57 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U. ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :. ug/kg 0// 0:0 0// : Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// : il Fac 0 Page of //0

58 Project/Site:, RACER SMI Method: A - Herbicides (GC) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:.,,-t U. ug/kg 0// 0:0 0// :0,- Silvex (,,-TP) Surrogate 0 U %Recovery U 0 ug/kg 0// 0:0 0// :0. ug/kg 0// 0:0 0// :0 Analyzed,-ichlorophenylacetic acid - 0 0// 0:0 0// :0 il Fac 0 Page of //0

59 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page of //0

60 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page of //0

61 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page of //0

62 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ :0 Lead mg/kg 0// :0 0/0/ :0 0 Page of //0

63 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page of //0

64 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page of //0

65 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// :00 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page 0 of //0

66 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ : Lead mg/kg 0// :0 0/0/ : 0 Page of //0

67 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Arsenic mg/kg 0// :0 0/0/ :0 Lead mg/kg 0// :0 0/0/ :0 0 Page of //0

68 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

69 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

70 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

71 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

72 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// 0:0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

73 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// 0: ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

74 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// :00 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

75 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page 0 of //0

76 Project/Site:, RACER SMI General Chemistry Client Sample I: S--0-SSH-0 ate Collected: 0// :0 ate Received: 0// 0:0 Result TestAmerica Job I: 0-0- Lab Sample I: 0-0- Percent s:. Percent s % 0// 0: Percent Moisture % 0// 0: 0 Page of //0

77 Project/Site:, RACER SMI GC/MS Semi VOA Prep : 0 QC Association Summary TestAmerica Job I: 0-0- Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 0C 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-0/-A Method Blank LCS 0-0/-A Lab Control Sample 0-0- MS S--0-SSH MS S--0-SSH-0 Analysis : 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-0/-A Method Blank LCS 0-0/-A Lab Control Sample 0-0- MS S--0-SSH MS S--0-SSH-0 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C GC Semi VOA Prep : Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-/-A Method Blank LCS 0-/-A Lab Control Sample 0-0- MS S--0-SSH MS S--0-SSH-0 Page of //0

78 Project/Site:, RACER SMI GC Semi VOA (Continued) Prep : QC Association Summary TestAmerica Job I: 0-0- Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 0C 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-/0-A Method Blank LCS 0-/-A Lab Control Sample Prep : Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 0C 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-/-A Method Blank LCS 0-/-A Lab Control Sample 0-0- MS S--0-SSH-0 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0C 0 Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-/0-A Method Blank LCS 0-/-A Lab Control Sample Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 0A 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 0A 0A 0A 0A 0A 0A 0A Page of //0

79 Project/Site:, RACER SMI GC Semi VOA (Continued) Analysis : (Continued) QC Association Summary TestAmerica Job I: 0-0- Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 0A MB 0-/-A Method Blank LCS 0-/-A Lab Control Sample 0-0- MS S--0-SSH-0 Analysis : 00 0A 0A 0A Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 A 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-/-A Method Blank LCS 0-/-A Lab Control Sample 0-0- MS S--0-SSH MS S--0-SSH-0 Metals Prep : 00 A A A A A A A A A A A A 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 00B 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-00/-A ^ Method Blank LCS 0-00/-A ^ Lab Control Sample Analysis : 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 MB 0-00/-A ^ Method Blank LCS 0-00/-A ^ Lab Control Sample 00B 00B 00B 00B 00B 00B 00B 00B 00B 00B Page of //0

80 Project/Site:, RACER SMI General Chemistry Analysis : QC Association Summary TestAmerica Job I: 0-0- Lab Sample I Client Sample I Prep Type Matrix Method Prep 0-0- S--0-SSH-0 Moisture 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH U S--0-SSH-0 Moisture Moisture Moisture Moisture Moisture Moisture Moisture Moisture Moisture 0 Page of //0

81 Project/Site:, RACER SMI QC Sample Results Method: 0 - Semivolatile Organic Compounds (GC/MS) TestAmerica Job I: 0-0- Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis : 0 Prep : 0 MB MB Result Alachlor 0 U 0 ug/kg 0/0/ 0: 0// :0 Atrazine Surrogate %Recovery Analyzed il Fac 0 U 0 ug/kg 0/0/ 0: 0// :0 MB MB Analyzed,,-Tribromophenol (Surr) - 0 0/0/ 0: 0// :0 -Fluorobiphenyl /0/ 0: 0// :0 -Fluorophenol (Surr) - 0 0/0/ 0: 0// :0 Nitrobenzene-d (Surr) 0-0 0/0/ 0: 0// :0 p-terphenyl-d (Surr) - 0/0/ 0: 0// :0 Phenol-d (Surr) - 0 0/0/ 0: 0// :0 Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis : 0 Prep : 0 Spike LCS LCS %Rec. Added Result Atrazine 0 0 ug/kg Surrogate %Recovery LCS LCS,,-Tribromophenol (Surr) 0-0 -Fluorobiphenyl Fluorophenol (Surr) - 0 Nitrobenzene-d (Surr) - 0 p-terphenyl-d (Surr) - Phenol-d (Surr) - 0 %Rec il Fac 0 Lab Sample I: 0-0- MS Client Sample I: S--0-SSH-0 Prep Type: Analysis : 0 Prep : 0 Sample Sample Spike MS MS %Rec. Result Added Result Atrazine 00 U 0 0 ug/kg Surrogate %Recovery MS MS,,-Tribromophenol (Surr) - 0 -Fluorobiphenyl 0-0 -Fluorophenol (Surr) - 0 Nitrobenzene-d (Surr) - 0 p-terphenyl-d (Surr) - Phenol-d (Surr) - 0 Lab Sample I: 0-0- MS Client Sample I: S--0-SSH-0 Prep Type: Analysis : 0 Prep : 0 Sample Sample Spike MS MS %Rec. RP Result Added Result Atrazine 00 U 0 00 ug/kg %Rec %Rec RP Limit Page of //0

82 Project/Site:, RACER SMI QC Sample Results Method: 0 - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: 0-0- MS Client Sample I: S--0-SSH-0 Prep Type: Analysis : 0 Prep : 0 Surrogate %Recovery MS MS,,-Tribromophenol (Surr) - 0 -Fluorobiphenyl 0-0 -Fluorophenol (Surr) - 0 Nitrobenzene-d (Surr) - 0 p-terphenyl-d (Surr) - Phenol-d (Surr) - 0 Method: 0A - Organochlorine Pesticides (GC) Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Result,'-. U.. ug/kg 0// 0: 0/0/ :,'-E,'-T Aldrin alpha-bhc alpha-chlordane beta-bhc delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Analyzed il Fac. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U. 0.0 ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U. 0. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ :. U.. ug/kg 0// 0: 0/0/ : 00 U 00 ug/kg 0// 0: 0/0/ : 0 Surrogate %Recovery MB MB Analyzed CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene 0-0 0// 0: 0/0/ : Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : Spike LCS LCS %Rec. Added Result,'- 00. ug/kg - 0,'-E 00. ug/kg - 0 %Rec il Fac Page of //0

83 Project/Site:, RACER SMI QC Sample Results Method: 0A - Organochlorine Pesticides (GC) (Continued) TestAmerica Job I: 0-0- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : Spike LCS LCS %Rec. Added Result,'-T 00. ug/kg - 0 Aldrin ug/kg 0-0 alpha-bhc 00. ug/kg - 0 alpha-chlordane 00. ug/kg - 0 beta-bhc ug/kg - 0 delta-bhc 00. ug/kg - 0 ieldrin 00. ug/kg - 0 Endosulfan I 00. ug/kg - 0 Endosulfan II 00.0 ug/kg - 0 Endosulfan sulfate 00. ug/kg - 0 Endrin 00.0 ug/kg - Endrin aldehyde 00. ug/kg - 0 Endrin ketone 00. ug/kg - 0 gamma-bhc (Lindane) 00. ug/kg - 0 gamma-chlordane ug/kg 0-0 Heptachlor 00. ug/kg - 0 Heptachlor epoxide 00. ug/kg - 0 Methoxychlor 00. ug/kg - Surrogate %Recovery LCS LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene 0-0 %Rec 0 Lab Sample I: 0-0- MS Client Sample I: S--0-SSH-0 Prep Type: Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Added Result,'-. U F F. p ug/kg - 0,'-E. U. p ug/kg - 0,'-T. U. p ug/kg - Aldrin. U. p ug/kg - 0 alpha-bhc. U. p ug/kg 0-0 alpha-chlordane. U.0 p ug/kg - 0 beta-bhc. U. p ug/kg delta-bhc. U. ug/kg 0-0 ieldrin. U. p ug/kg - 0 Endosulfan I. U. p ug/kg 0-0 Endosulfan II. U F 0. p ug/kg - 0 Endosulfan sulfate. U F F. p ug/kg - 0 Endrin. U F 0. p ug/kg - Endrin aldehyde. U F.0 p ug/kg - 0 Endrin ketone. U F F. p ug/kg - 0 gamma-bhc (Lindane). U. ug/kg - 0 gamma-chlordane. U. ug/kg - 0 Heptachlor. U. ug/kg - 0 Heptachlor epoxide. U.0 ug/kg - 0 Methoxychlor U F F. p ug/kg - 0 %Rec Page of //0

84 Project/Site:, RACER SMI Surrogate %Recovery MS MS CB ecachlorobiphenyl 0 p - QC Sample Results Tetrachloro-m-xylene 0-0 Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography TestAmerica Job I: 0-0- Lab Sample I: MB 0-/0-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Result Aroclor-0 0 U 0 ug/kg 0// 0: 0/0/ : Aroclor- Aroclor- Aroclor- Aroclor- Aroclor- Aroclor-0 Surrogate %Recovery Analyzed il Fac 0 U 0 ug/kg 0// 0: 0/0/ : 0 U 0 ug/kg 0// 0: 0/0/ : 0 U 0 0 ug/kg 0// 0: 0/0/ : 0 U 0 ug/kg 0// 0: 0/0/ : 0 U 0 ug/kg 0// 0: 0/0/ : 0 U 0 ug/kg 0// 0: 0/0/ : MB MB Analyzed Tetrachloro-m-xylene - 0// 0: 0/0/ : CB ecachlorobiphenyl 0-0// 0: 0/0/ : Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : Spike LCS LCS %Rec. Added Result Aroclor ug/kg - 0 Aroclor ug/kg - 0 %Rec il Fac 0 Surrogate %Recovery LCS LCS Tetrachloro-m-xylene - CB ecachlorobiphenyl 0 - Method: A - Herbicides (GC) Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : 00 Prep : MB MB Result,,-T 0 U 0.0 ug/kg 0// 0:0 0// :,- Silvex (,,-TP) Surrogate %Recovery Analyzed il Fac 0 U 0 0 ug/kg 0// 0:0 0// : 0 U 0.0 ug/kg 0// 0:0 0// : MB MB Analyzed,-ichlorophenylacetic acid 0-0 0// 0:0 0// : il Fac Page of //0

85 Project/Site:, RACER SMI Method: A - Herbicides (GC) (Continued) QC Sample Results TestAmerica Job I: 0-0- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : 00 Prep : Spike LCS LCS %Rec. Added Result,,-T 0 00 ug/kg 0 -, ug/kg 0-0 Silvex (,,-TP) 0 ug/kg - 0 Surrogate %Recovery LCS LCS,-ichlorophenylacetic acid 0-0 Lab Sample I: 0-0- MS Client Sample I: S--0-SSH-0 Prep Type: Analysis : 00 Prep : Sample Sample Spike MS MS %Rec. Result Added Result,,-T U ug/kg 0-0,- 0 U 0 0 ug/kg 0-0 Silvex (,,-TP) U ug/kg - 0 Surrogate %Recovery MS MS,-ichlorophenylacetic acid - 0 Lab Sample I: 0-0- MS Client Sample I: S--0-SSH-0 Prep Type: Analysis : 00 Prep : Sample Sample Spike MS MS %Rec. RP Result Added Result,,-T U 0 ug/kg 0-0 0,- 0 U 0 00 ug/kg Silvex (,,-TP) U ug/kg - 0 %Rec %Rec %Rec RP Limit 0 Surrogate %Recovery MS MS,-ichlorophenylacetic acid - 0 Method: 00 - Metals (ICP/MS) Lab Sample I: MB 0-00/-A ^ Client Sample I: Method Blank Prep Type: Analysis : 0 Prep : 00 MB MB Result Arsenic.0 U mg/kg 0// :0 0/0/ : Lead Analyzed il Fac 0.0 U mg/kg 0// :0 0/0/ : Lab Sample I: LCS 0-00/-A ^ Client Sample I: Lab Control Sample Prep Type: Analysis : 0 Prep : 00 Spike LCS LCS %Rec. Added Result Arsenic 00. mg/kg 0-0 %Rec Page 0 of //0

86 Project/Site:, RACER SMI Method: 00 - Metals (ICP/MS) (Continued) QC Sample Results TestAmerica Job I: 0-0- Lab Sample I: LCS 0-00/-A ^ Client Sample I: Lab Control Sample Prep Type: Analysis : 0 Prep : 00 Spike LCS LCS %Rec. Added Result Lead 00 0 mg/kg Method: Moisture - Percent Moisture Lab Sample I: 0-0- U Analysis : Sample Sample Result U U Result %Rec Client Sample I: S--0-SSH-0 Prep Type: Percent s.. % 0. 0 Percent Moisture.. % 0 RP RP Limit 0 Page of //0

87 Project/Site:, RACER SMI Surrogate Summary Method: 0 - Semivolatile Organic Compounds (GC/MS) TBP FBP FP NBZ TPH PHL Lab Sample I Client Sample I (-0) (0-0) (-0) (-0) (-) (-0) 0-0- S--0-SSH MS S--0-SSH MS S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 LCS 0-0/-A MB 0-0/-A Surrogate Legend Lab Control Sample Method Blank TBP =,,-Tribromophenol (Surr) FBP = -Fluorobiphenyl FP = -Fluorophenol (Surr) NBZ = Nitrobenzene-d (Surr) TPH = p-terphenyl-d (Surr) PHL = Phenol-d (Surr) Method: 0A - Organochlorine Pesticides (GC) TestAmerica Job I: 0-0- Percent Surrogate Recovery (Acceptance ) Prep Type: Prep Type: 0 Percent Surrogate Recovery (Acceptance ) CB CB TCX TCX Lab Sample I Client Sample I (-) (-) (0-0) (0-0) 0-0- S--0-SSH MS S--0-SSH-0 0 p S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 LCS 0-/-A Lab Control Sample MB 0-/-A Method Blank Surrogate Legend CB = CB ecachlorobiphenyl TCX = Tetrachloro-m-xylene Page of //0

88 Project/Site:, RACER SMI Surrogate Summary Method: 0 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography TCX CB Lab Sample I Client Sample I (-) (0-) 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH-0 LCS 0-/-A MB 0-/0-A Surrogate Legend TCX = Tetrachloro-m-xylene CB = CB ecachlorobiphenyl Lab Control Sample Method Blank Method: A - Herbicides (GC) CPA CPA Lab Sample I Client Sample I (-0) (-0) 0-0- S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH S--0-SSH MS S--0-SSH MS S--0-SSH-0 LCS 0-/-A MB 0-/-A Lab Control Sample Method Blank TestAmerica Job I: 0-0- Percent Surrogate Recovery (Acceptance ) Percent Surrogate Recovery (Acceptance ) Prep Type: Prep Type: 0 Surrogate Legend CPA =,-ichlorophenylacetic acid Page of //0

89 Lab Chronicle TestAmerica Job I: 0-0- Project/Site:, RACER SMI Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// : LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ : BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ 0: LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0: ate Received: 0// 0:0 Lab Lab 0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Lab Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0: ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// :0 LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ :0 BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ : LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Lab Page of //0

90 Lab Chronicle TestAmerica Job I: 0-0- Project/Site:, RACER SMI Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// :0 LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ : BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ :0 LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0: ate Received: 0// 0:0 Lab Lab 0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Lab Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0: ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// : LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ :0 BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ : LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ :0 AS TAL CAN Lab Page of //0

91 Lab Chronicle TestAmerica Job I: 0-0- Project/Site:, RACER SMI Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// : LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ :0 BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ :0 LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0: ate Received: 0// 0:0 Lab Lab 0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Lab Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// 0: ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// : LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ : BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ : LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Lab Page of //0

92 Lab Chronicle TestAmerica Job I: 0-0- Project/Site:, RACER SMI Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// :00 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// :00 ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// :0 LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ : BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ : LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// :0 RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// :0 ate Received: 0// 0:0 Lab Lab 0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Lab Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// :0 ate Received: 0// 0:0 Percent s:. Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// : LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ : BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ :0 LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// : RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ : AS TAL CAN Lab Page of //0

93 Lab Chronicle TestAmerica Job I: 0-0- Project/Site:, RACER SMI Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// :0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyzed Analyst Analysis Moisture 0// 0: JWW TAL CAN Client Sample I: S--0-SSH-0 Lab Sample I: 0-0- ate Collected: 0// :0 ate Received: 0// 0:0 Percent s:. Prep Type Type Laboratory References: Method Run ilution Factor Number or Analyzed Analyst Prep 0C 0 0/0/ 0: RJS TAL BUF Analysis 0 0 0// : LMW TAL BUF Prep 0C 0// 0: SE TAL CAN Analysis 0A 0/0/ : BPM TAL CAN Prep 0C 0// 0: SE TAL CAN Analysis 0 0/0/ :0 LSH TAL CAN Prep 0// 0:0 SE TAL CAN Analysis A 00 0// :0 RTR TAL CAN Prep 00B 00 0// :0 EE TAL CAN Analysis /0/ :0 AS TAL CAN TAL BUF = TestAmerica Buffalo, 0 Hazelwood rive, Amherst, NY -, TEL ()-00 TAL CAN =, 0 Shuffel Street NW, North Canton, OH 0, TEL (0)- Lab Lab 0 Page of //0

94 Certification Summary TestAmerica Job I: 0-0- Project/Site:, RACER SMI Laboratory: All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate California State Program 0-0- * Connecticut State Program PH Florida NELAP E 0-0- Illinois NELAP Kansas NELAP E * Kentucky (UST) State Program 0-- * Kentucky (WW) State Program 0 -- * Minnesota NELAP Minnesota (Petrofund) State Program Nevada State Program OH-00000A 0-- New Jersey NELAP OH New York NELAP * Ohio VAP State Program CL Oregon NELAP * Pennsylvania NELAP Texas NELAP T USA Federal P Virginia NELAP Washington State Program 0 C 0-- West Virginia EP State Program 0 -- * Wisconsin State Program Laboratory: TestAmerica Buffalo All certifications held by this laboratory are listed. Not all certifications are applicable to this report. 0 Authority Program EPA Region Certification I Expiration ate Arkansas EQ State Program California State Program CA 0-0- Connecticut State Program PH Florida NELAP E 0-0- Georgia State Program N/A 0-- * Georgia State Program 0-- * Illinois NELAP Iowa State Program 0-0- * Kansas NELAP E-0-0- * Kentucky (W) State Program Kentucky (UST) State Program * Kentucky (WW) State Program * Louisiana NELAP Maine State Program NY Maryland State Program 0-- * Massachusetts State Program M-NY Michigan State Program 0-- * Minnesota NELAP New Hampshire NELAP Primary AB 0-- New Hampshire NELAP Secondary AB -- New Jersey NELAP NY 0-0- New York NELAP * North akota State Program R- 0-- * Oklahoma State Program 0-- * Certification renewal pending - certification considered valid. Page of //0

95 Certification Summary TestAmerica Job I: 0-0- Project/Site:, RACER SMI Laboratory: TestAmerica Buffalo (Continued) All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Oregon NELAP 0 NY Pennsylvania NELAP Rhode Island State Program LAO00-0- Tennessee State Program TN * Texas NELAP T USA Federal P Virginia NELAP Washington State Program 0 C 0-0- * West Virginia EP State Program 0-0- * Wisconsin State Program * Certification renewal pending - certification considered valid. Page 0 of //0

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