ELECTROMETRIC MEASUREMENT CONDUCTANCE AT 25 DEGREES C ELECTROMETRIC OR PHENOLPHTHALEIN ENDPOINT TITRIMETRIC TITRIMETRIC (MERCURIC NITRATE)

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2 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 CLEAN WATER ACT DIOXINS AND FURANS CHLORINATED DIOXINS & FURANS-HRGC/HRMS EPA 1613B (1994) INORGANIC - DEMAND BIOCHEMICAL OXYGEN DEMAND(BOD) DISSOLVED OXYGEN SM 5210 B-2011 SM G DAY DO DEPLETION ELECTRODE INORGANIC - MINERAL ACIDITY ALKALINITY CHLORIDE CHLORIDE FLUORIDE FLUORIDE FLUORIDE HYDROGEN-ION CONC. (PH) SPECIFIC CONDUCTANCE SULFATE SM 2310 B-2011 SM 2320 B-2011 EPA (1993) SM 4500-CL- C-2011 EPA (1993) SM 4500-F B-2011 SM 4500-F C-2011 SM 4500-H B-2011 SM 2510 B-2011 EPA (1993) ELECTROMETRIC OR PHENOLPHTHALEIN ENDPOINT TITRIMETRIC TITRIMETRIC (MERCURIC NITRATE) MANUAL DISTILLATION ELECTRODE (MANUAL) ELECTROMETRIC MEASUREMENT CONDUCTANCE AT 25 DEGREES C INORGANIC - MISCELLANEOUS CYANIDE OIL&GREASE SULFIDE SULFIDE SURFACTANTS(MBAS) EPA (1993) EPA 1664B (2010) SM 4500-S2 B-2011 SM 4500-S2 D-2011 SM 5540 C-2011 SEMI-AUTOMATED COLORIMETRY OIL & GREASE - HEM/SGT-HEM SEPARATION OF SOLUBLE AND INSOLUBLE SULFIDES COLORIMETRIC (METHYLENE BLUE) COLORIMETRIC (METHYLENE BLUE) INORGANIC - NUTRIENT KJELDAHL-NITROGEN NITRATE-NITRITE (N02&N03) NITRATE-NITROGEN NITRITE-NITROGEN NITRITE-NITROGEN ORTHOPHOSPHATE PHOSPHORUS EPA (1993) EPA (1993) EPA (1993) EPA (1993) EPA (1993) SM 4500-P E-2011 EPA (1993) SEMI-AUTOMATED BLOCK DIGESTER COLORIMETRIC CADMIUM REDUCTION (AUTOMATED) CADMIUM REDUCTION (AUTOMATED) ASCORBIC ACID (MANUAL SINGLE REAGENT) ASCORBIC ACID (AUTOMATED) Page 1 of7

3 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 CLEAN WATER ACT INORGANIC - RESIDUE RESIDUE, FILTERABLE (TDS) RESIDUE, NON FILTERABLE (TSS) RESIDUE, SETTLEABLE (SS) RESIDUE, TOTAL (TS) RESIDUE, VOLATILE (VS) SM 2540 C-2011 SM 2540 D-2011 SM 2540 F-2011 SM 2540 B-2011 EPA (1979) GRAVIMETRIC (180) GRAVIMETRIC VOLUMETRIC (IMHOFF CONE) OR GRAVIMETRIC GRAVIMETRIC GRAVIMETRIC (550) INORGANIC -TRACE METAL ALUMINUM ANTIMONY ANTIMONY ARSENIC ARSENIC BARIUM BERYLLIUM BERYLLIUM BORON CADMIUM CADMIUM CALCIUM CHROMIUM CHROMIUM CHROMIUM, HEXAVALENT COBALT COPPER COPPER IRON LEAD LEAD MAGNESIUM MANGANESE MERCURY MERCURY MOLYBDENUM NICKEL NICKEL POTASSIUM SELENIUM SELENIUM SILVER EPA200.7 (1994) EPA (1994) EPA 1631 E (2002) EPA (1994) EPA (1994) PURGE AND TRAP CVAFS COLD VAPOR (MANUAL) Page2 of7

4 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 CLEAN WATER ACT INORGANIC - TRACE METAL SILVER SODIUM THALLIUM THALLIUM TIN VANADIUM ZINC SEMI-VOLATILES BASE/NEUTRALS AND ACIDS - GC/MS EPA625 VOLATILES (VOCS) PURGEABLES - GC/MS voes BY GC/FID voes BY ISOTOPE DILUTION (GC/MS) EPA 624 EPA 1671A EPA 1666A SAFE DRINKING WATER ACT INORGANIC - MINERAL HYDROGEN-ION CONC. (PH) HYDROGEN-ION CONC. (PH) EPA (1983) SM 4500HB (20TH) ELECTROMETRIC MEASUREMENT ELECTROMETRIC MEASUREMENT INORGANIC - NUTRIENT NITRITE-NITROGEN EPA (1993) INORGANIC - RESIDUE RESIDUE, FILTERABLE (TDS) SM 2540C (20TH) GRAVIMETRIC (180) INORGANIC - TRACE METAL ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM EPA (1994) EPA200.7 (1994) Page 3 of7

5 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 SAFE DRINKING WATER ACT INORGANIC -TRACE METAL BERYLLIUM CADMIUM CADMIUM CALCIUM CHROMIUM CHROMIUM COPPER COPPER IRON LEAD MAGNESIUM MANGANESE MERCURY NICKEL NICKEL SELENIUM SILVER SODIUM THALLIUM ZINC EPA (1994) EPA200.7 (1994) COLD VAPOR (MANUAL) TRIHALOMETHANES PURGEABLE ORGANICS - GC/MS EPA (1995) VOLATILES (VOCS) PURGEABLE ORGANICS - GC/MS EPA (1995) DIOXINS AND FURANS CHLORINATED DIOXINS & FURANS-HRGC/HRMS EPA 8290A INORGANIC - DEMAND TOTAL ORGANIC CARBON (TOG) EPA 9060A CARBONACEOUS ANALYZER Page4 of7

6 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 INORGANIC - HAZARDOUS WASTE CHARACTERISTICS IGNITABILITY SYNTHETIC PREC. LEACHING PROC. TCLP - BOTTLE EXTRACTION TCLP - ZERO HEADSPACE EPA 1010A EPA 1312 EPA 1311 EPA 1311 PENSKY-MARTENS CLOSED-CUP SYNTHETIC PRECIPITATION LEACHING PROCEDURE TOXICITY CHARACTERISTIC LEACHING PROCEDURE TOXICITY CHARACTERISTIC LEACHING PROCEDURE INORGANIC - MINERAL HYDROGEN-ION CONG. (PH) SPECIFIC CONDUCTANCE EPA9040C EPA 9050A ELECTROMETRIC WHEATSTONE BRIDGE INORGANIC - MISCELLANEOUS CYANIDE CYANIDE AMEN. TO CHLORINATION OIL&GREASE EPA 9012B EPA 9012B EPA 9071B TOTAL AND AMENABLE (COLORIMETRIC, AUTOMATED UV) TOTAL AND AMENABLE (COLORIMETRIC, AUTOMATED UV) HEM/SGT-HEM INORGANIC - NUTRIENT NITRATE-NITROGEN EPA 9056A INORGANIC - TRACE METAL ANTIMONY ANTIMONY ARSENIC ARSENIC BARIUM BERYLLIUM BERYLLIUM CADMIUM CADMIUM CALCIUM CHROMIUM CHROMIUM CHROMIUM, HEXAVALENT CHROMIUM, HEXAVALENT COBALT COPPER COPPER IRON EPA 6020A EPA6020A EPA 6020A EPA 6020A EPA6020A EPA 7196A EPA 7199 EPA 6020A COLORIMETRIC Page 5 of7

7 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 INORGANIC - TRACE METAL LEAD LEAD MANGANESE MERCURY MERCURY METALS DIGESTION METALS DIGESTION METALS DIGESTION METALS DIGESTION MOLYBDENUM NICKEL NICKEL SELENIUM SILVER STRONTIUM THALLIUM THALLIUM TIN VANADIUM ZINC EPA 6020A EPA 7470A EPA 7471B EPA 3005A EPA 3010A EPA 3050B EPA 3060A EPA6020A EPA 6020A COLD VAPOR TECHNIQUE LIQUID COLD VAPOR TECHNIQUE SOLID AQUEOUS ACID DIGESTION TOTAL OR DISSOLVED METALS FLAA OR ICP AQUEOUS ACID DIGESTION TOTAL METALS FLAA OR ICP SOLID ACID DIGESTION ALKALINE DIGESTION HEX CHROM SEMI-VOLATILES EDB & DBCP BY MICROEXTRACTION AND GC SEMIVOLATILE ORGANICS BY GC/MS SEMIVOLATILE ORGANICS BY GC/MS SEMIVOLATILE ORGANICS BY GC/MS SEMIVOLATILE ORGANICS BY GC/MS (SIM) SEMIVOLATILE ORGANICS BY GC/MS (SIM) TPH - DIESEL RANGE ORGANICS (ORO) TPH - DIESEL RANGE ORGANICS (ORO) EPA 8011 EPA EPA EPA EPA (SIM) EPA (SIM) EPA 8015C (ORO) EPA 8015C (ORO) EPA 3546 EPA3550C EPA3510C EPA 3546 EPA3510C EPA3550C EPA3510C VOLATILES (VOCS) OXYGENATE VOLATILE ORGANICS BY GC/MS TPH - GASOLINE RANGE ORGANICS (GRO) TPH - GASOLINE RANGE ORGANICS (GRO) VOLATILE ORGANICS BY GC/MS VOLATILE ORGANICS BY GC/MS VOLATILE ORGANICS BY GC/MS EPA 8260B-OXY EPA 8015C (GRO) EPA 8015C (GRO) EPA 8260B EPA 8260B EPA 8260B (SIM) EPA5030B EPA5035 EPA 5030B EPA5035 EPA 5030B EPA5030B Page 6 of7

8 SOUTH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENTAL CONTROL Laboratory Director: DUANE LUCKENBILL Certifying Authority: PA Certificate Number: Date of Issue: September 26, 2016 Expiration Date: January 31, 2017 VOLATILES (VOCS) VOLATILES BY GC/HALUPID EPA EPA Page 7 of7

9 Certifying Authority: PA Date of Issue: September 26, 2016 Certificate Number: Expiration Date: January 31, DIOXINS AND FURANS EPA 1613B (1994) 1,2,3,4,6,7,8-HPCDD 1,2,3,4,6,7,8-HPCDF 1,2,3,4,7,8,9-HPCDF 1,2,3,4, 7,8-HXCDD 1,2,3,4, 7,8-HXCDF 1,2,3,6,7,8-HXCDD 1,2,3,6,7,8-HXCDF 1,2,3,7,8,9-HXCDD 1,2,3,7,8,9-HXCDF 1,2,3,7,8-PECDD 1,2,3,7,8-PECDF 2,3,4,6,7,8-HXCDF 2,3,4,7,8-PECDF 2,3,7,8-TCDD 2,3,7,8-TCDF OCDD OCDF -----SEMI-VOLATILES- --- EPA 625 1,2,4-TRICHLOROBENZENE 2,3-DICHLOROANILINE 2,4,6-TRICHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 2,4-DINITROPHENOL 2,4-DINITROTOLUENE (2,4-DNT) 2,6-DINITROTOLUENE (2,6-DNT) 2-CHLORO 2-CHLOROPHENOL 2-METHYL-4,6-DINITROPHENOL 2-NITROPHENOL 3,3-DICHLOROBENZIDINE 4-BROMOPHENYLPHENYL ETHER 4-CHLOR0-3-METHYLPHENOL 4-CHLOROPHENYL PHENYL ETHER 4-NITROPHENOL ACENAPHTHENE ACENAPHTHYLENE ALPHA-TERPINEOL ANILINE ANTHRACENE SOUTH CAROLINA DEPARTMENT OF HEAL TH AND ENVIRONMENTAL CONTROL EPA 625 BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO(G,H,l)PERYLENE BENZO(K)FLUORANTHENE BENZYLBUTYLPHTHALATE BIS(2-CHLOR0-1-METHYLETHYL)ETHER BIS(2-CHLOROETHOXY)METHANE BIS(2-CHLOROETHYL)ETHER BIS(2-ETHYLHEXYL)PHTHALA TE CARBAZOLE CHRYSENE Dl-N-BUTYL PHTHALATE Dl-N-OCTYL PHTHALATE DIBENZO(A,H)ANTHRACENE DIETHYL PHTHALATE DIMETHYL PHTHALATE FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE INDEN0(1,2,3-CD)PYRENE ISOPHORONE N-DECANE N-NITROSODl-N-PROPYLAMINE N-NITROSODIMETHYLAMINE N-NITROSODIPHENYLAMINE N-OCTADECANE NITROBENZENE (NB) PENTACHLOROPHENOL PHENANTHRENE PHENOL PYRENE PYRIDINE -----VOLATILES (VOCS)-- EPA 1666A ETHYL ACETATE ISOBUTYRALDEHYDE ISOPROPANOL ISOPROPYL ACETATE CLEAN WATER ACT EPA 1666A ISOPROPYL ETHER METHYL FORMATE N-AMYL ACETATE N-AMYL ALCOHOL N-BUTYLACETATE N-HEPTANE N-HEXANE T-BUTYL ALCOHOL TETRAHYDROFURAN XYLENE, TOTAL EPA 1671A ACETONITRILE DIETHYLAMINE DIMETHYL SULFOXIDE ETHANOL METHANOL METHYL CELLOSOLVE N-PROPANOL (N-PROPYLALCHOHOL) TRIETHYLAMINE EPA624 1, 1, 1-TRICHLOROETHANE 1, 1,2,2-TETRACHLOROETHANE 1, 1,2-TRICHLOROETHANE 1, 1-DICHLOROETHANE 1, 1-DICHLOROETHENE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 2-CHLOROETHYLVINYL ETHER BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,3-DICHLOROPROPENE EPA 624 DICHLORODIFLUOROMETHANE ETHYLBENZENE METHYL TERT BUTYL ETHER (MTBE) METHYLENE CHLORIDE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL CHLORIDE XYLENE, TOTAL

10 SOUTH CAROLINA DEPARTMENT OF HEAL TH AND ENVIRONMENTAL CONTROL Certifying Authority: PA Date of Issue: September 26, 2016 Certificate Number: Expiration Date: January 31, 2017 SAFE DRINKING WATER ACT TRIHALOMETHANES EPA (1995) BROMODICHLOROMETHANE BROMOFORM CHLORODIBROMOMETHANE CHLOROFORM ----VOLATILES (VOCS) EPA (1995) 1, 1, 1-TRICHLOROETHANE 1, 1,2-TRICHLOROETHANE 1, 1-DICHLOROETHENE 1,2,4-TRICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,4-DICHLOROBENZENE BENZENE CARBON TETRACHLORIDE CHLOROBENZENE CIS-1,2-DICHLOROETHENE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRICHLOROETHENE VINYL CHLORIDE XYLENE, TOTAL

11 Certifying Authority: PA Date of Issue: September 26, 2016 Certificate Number: Expiration Date: January 31, DIOXINS AND FURANS EPA 8290A 1,2,3,4,6,7,8-HPCDD 1,2,3,4,6, 7,8-HPCDF 1,2,3,4, 7,8,9-HPCDF 1,2,3,4, 7,8-HXCDD 1,2,3,4,7,8-HXCDF 1,2,3,6,7,8-HXCDD 1,2,3,6,7,8-HXCDF 1,2,3,7,8,9-HXCDD 1,2,3,7,8,9-HXCDF 1,2,3,7,8-PECDD 1,2,3, 7,8-PECDF 2,3,4,6, 7,8-HXCDF 2,3,4,7,8-PECDF 2,3,7,8-TCDD 2,3,7,8-TCDF OCDD OCDF SEMI-VOLATILES----- EPA ,2-DIBROM0-3-CHLOROPROPANE(DBCP) 1,2-DIBROMOETHANE (EDS) EPA 8015C (ORO) EPA3510C TPH - HIGH BOIL. PT. (DIESEL) EPA 8015C (ORO) EPA 3550C TPH - HIGH BOIL. PT. (DIESEL) 1, 1 '-BIPHENYL EPA8270D EPA3510C 1,2,4,5-TETRACHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIPHENYLHYDRAZINE 1,3,5-TRINITROBENZENE (1,3,5-TNB) SOUTH CAROLINA DEPARTMENT OF HEAL TH AND ENVIRONMENTAL CONTROL EPA8270D EPA 3510C 1,3-DICHLOROBENZENE 1,3-DINITROBENZENE (1,3-DNB) 1,4-DICHLOROBENZENE 1,4-NAPHTHOQUINONE 1-NAPHTHYLAMINE 2,3,4,6-TETRACHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2,4,6-TRICHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 2,4-DINITROPHENOL 2,4-DINITROTOLUENE (2,4-DNT) 2,6-DICHLOROPHENOL 2,6-DINITROTOLUENE (2,6-DNT) 2-ACETYLAMINOFLUORENE 2-CHLORO 2-CHLOROPHENOL 2-METHYL 2-METHYLPHENOL 2-NAPHTHYLAMINE 2-NITROANILINE 2-NITROPHENOL 2-PICOLINE (2-METHYLPYRIDINE) 3,3-DICHLOROBENZIDINE 3,3-DIMETHYLBENZIDINE 3-METHYLCHOLANTHRENE 3-NITROANILINE 4,4-METHYLENEBIS(2-CHLORO.) 4,6-DINITR0-2-METHYLPHENOL 4-AMINOBIPHENYL 4-BROMOPHENYLPHENYL ETHER 4-CHLOR0-3-METHYLPHENOL 4-CHLOROANILINE 4-CHLOROPHENYL PHENYL ETHER 4-METHYLPHENOL 4-NITROANILINE 4-NITROPHENOL 4-NITROQUINOLINE-1-0XIDE 5-NITR0-0-TOLUIDINE 7, 12-DIMETHYLBENZ(A)ANTHRACENE ACENAPHTHENE ACENAPHTHYLENE ACETOPHENONE ANILINE ANTHRACENE EPA EPA 3510C ATRAZINE BENZIDINE BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO(G,H,l)PERYLENE BENZO(K)FLUORANTHENE BENZYL ALCOHOL BIS(2-CHLOR0-1-METHYLETHYL)ETHER BIS(2-CHLOROETHOXY)METHANE BIS(2-CHLOROETHYL)ETHER BIS(2-ETHYLHEXYL)PHTHALA TE BUTYLBENZYLPHTHALATE CARBAZOLE CHLOROBENZILA TE CHRYSENE Dl-N-BUTYL PHTHALATE 01-N-OCTYL PHTHALATE DIALLATE DIBENZO(A,H)ANTHRACENE DIBENZOFURAN DIETHYL PHTHALATE DIMETHOATE DIMETHYL PHTHALATE DIMETHYLAMINOAZOBENZENE ETHYL METHANESULFONATE FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE HEXACHLOROPROPENE INDEN0(1,2,3-CD)PYRENE ISODRIN ISOPHORONE ISOSAFROLE METHAPYRILENE METHYL METHANESULFONATE N-NITROSODl-N-BUTYLAMINE N-NITROSODl-N-PROPYLAMINE N-NITROSODIETHYLAMINE N-NITROSODIMETHYLAMINE N-NITROSODIPHENYLAMINE N-NITROSOMETHYLETHYLAMINE EPA EPA3510C N-NITROSOMORPHOLINE N-NITROSOPIPERIDINE N-NITROSOPYRROLIDINE NITROBENZENE (NB) 0,0,0-TRIETHYLPHOSPHOROTHIOATE 0-TOLUIDINE PENTACHLOROBENZENE PENTACHLORONITROBENZENE PENTACHLOROPHENOL PHENACETIN PHENANTHRENE PHENOL PRONAMIDE PYRENE PYRIDINE SAFROLE TETRAETHYL DITHIOPYROPHOSPHATE THIONAZIN EPA EPA3546 1, 1 '-BIPHENYL 1,2,4,5-TETRACHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIPHENYLHYDRAZINE 1,3-DICHLOROBENZENE 1,3-DINITROBENZENE (1,3-DNB) 1,4-DICHLOROBENZENE 1,4-DINITROBENZENE 1,4-NAPHTHOQUINONE 1-CHLORO 1-NAPHTHYLAMINE 2,3,4,6-TETRACHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2,4,6-TRICHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 2,4-DINITROPHENOL 2,4-DINITROTOLUENE (2,4-DNT) 2,6-DICHLOROPHENOL 2,6-DINITROTOLUENE (2,6-DNT) 2-ACETYLAMINOFLUORENE

12 SOUTH CAROLINA DEPARTMENT OF HEAL TH AND ENVIRONMENTAL CONTROL Certifying Authority: PA Date of Issue: September 26, 2016 Certificate Number: Expiration Date: January 31, SEMI-VOLATILES---- EPA8270D EPA CHLORO 2-CHLOROPHENOL 2-METHYL 2-METHYLPHENOL 2-NAPHTHYLAMINE 2-NITROANILINE 2-NITROPHENOL 2-PICOLINE (2-METHYLPYRIDINE) 3,3-DICHLOROBENZIDINE 3-METHYLCHOLANTHRENE 3-NITROANILINE 4,4-METHYLENEBIS(2-CHLORO.) 4,6-DINITR0-2-METHYLPHENOL 4-AMINOBIPHENYL 4-BROMOPHENYLPHENYL ETHER 4-CHLOR0-3-METHYLPHENOL 4-CHLOROANILINE 4-CHLOROPHENYL PHENYL ETHER 4-METHYLPHENOL 4-NITROANILINE 4-NITROPHENOL 4-NITROQUINOLINE-1-0XIDE 5-NITR0-0-TOLUIDINE 7, 12-DIMETHYLBENZ(A)ANTHRACENE ACENAPHTHENE ACENAPHTHYLENE ACETOPHENONE ANILINE ANTHRACENE ATRAZINE BENZALDEHYDE BENZI DINE BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO(G,H,l)PERYLENE BENZO(K)FLUORANTHENE BENZOIC ACID BENZVL ALCOHOL BIS(2-CHLOR0-1-METHYLETHYL)ETHER BIS(2-CHLOROETHOXY)METHANE BIS(2-CHLOROETHYL)ETHER BIS(2-ETHYLHEXYL)PHTHALA TE EPA8270D EPA 3546 BUTYLBENZYLPHTHALATE CAPROLACTAM CARBAZOLE CHLOROBENZILATE CHRYSENE Dl-N-BUTYL PHTHALATE Dl-N-OCTYL PHTHALATE DIALLATE DIBENZO(A,H)ANTHRACENE DIBENZOFURAN DIETHYL PHTHALATE DIMETHOATE DIMETHYL PHTHALATE DIMETHYLAMINOAZOBENZENE DINOSEB ETHYL METHANESULFONA TE FLUORANTHENE FLU ORE NE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE HEXACHLOROPROPENE INDEN0(1,2,3-CD)PYRENE ISODRIN ISOPHORONE ISOSAFROLE METHAPYRILENE METHYL METHANESULFONATE METHYL PARATHION N-NITROSODl-N-BUTYLAMINE N-NITROSODl-N-PROPYLAMINE N-NITROSODIETHYLAMINE N-NITROSODIMETHYLAMINE N-NITROSODIPHENYLAMINE N-NITROSOMETHYLETHYLAMINE N-NITROSOMORPHOLINE N-NITROSOPIPERIDINE N-NITROSOPYRROLIDINE NITROBENZENE (NB) 0,0,0-TRIETHYLPHOSPHOROTHIOATE 0-TOLUIDINE PARATHION PENTACHLOROBENZENE EPA 8270D EPA 3546 PENTACHLORONITROBENZENE PENTACHLOROPHENOL PHENACETIN PHENANTHRENE PHENOL PHORATE PRONAMIDE PYRE NE PYRIDINE SAFROLE TETRAETHYL DITHIOPYROPHOSPHATE THIONAZIN EPA8270D EPA 3550C 1, 1 '-BIPHENYL 1,2,4,5-TETRACHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,2-DICHLOROBENZENE 1,3,5-TRINITROBENZENE {1,3,5-TNB) 1,3-DICHLOROBENZENE 1,3-DINITROBENZENE (1,3-DNB) 1,4-DICHLOROBENZENE 1,4-NAPHTHOQUINONE 1-NAPHTHYLAMINE 2,3,4,6-TETRACHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2,4,6-TRICHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 2,4-DINITROPHENOL 2,4-DINITROTOLUENE (2,4-DNT) 2,6-DICHLOROPHENOL 2,6-DINITROTOLUENE (2,6-DNT) 2-ACETYLAMINOFLUORENE 2-CHLORO 2-CHLOROPHENOL 2-METHYL 2-METHYLPHENOL 2-NAPHTHYLAMINE 2-NITROANILINE 2-NITROPHENOL 2-PICOLINE (2-METHYLPYRIDINE) 3,3-DICHLOROBENZIDINE EPA 8270D EPA 3550C 3,3-DIMETHYLBENZIDINE 3-METHYLCHOLANTHRENE 3-NITROANILINE 4,6-DINITR0-2-METHYLPHENOL 4-AMINOBIPHENYL 4-BROMOPHENYLPHENYL ETHER 4-CHLOR0-3-METHYLPHENOL 4-CHLOROANILINE 4-CHLOROPHENYL PHENYL ETHER 4-METHYLPHENOL 4-NITROANILINE 4-NITROPHENOL 4-NITROQUINOLINE-1-0XIDE 5-NITR0-0-TOLUIDINE 7, 12-DIMETHYLBENZ(A)ANTHRACENE ACENAPHTHENE ACENAPHTHYLENE ACETOPHENONE ANILINE ANTHRACENE ATRAZINE BENZALDEHYDE BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO{G,H,l)PERYLENE BENZO(K)FLUORANTHENE BENZYL ALCOHOL BIS(2-CHLOR0-1-METHYLETHYL)ETHER BIS(2-CHLOROETHOXY)METHANE BIS{2-CHLOROETHYL)ETHER BIS(2-ETHYLHEXYL)PHTHALA TE BUTYLBENZYLPHTHALATE CAPROLACTAM CARBAZOLE CHLOROBENZILA TE CHRYSENE Dl-N-BUTYL PHTHALATE Dl-N-OCTYL PHTHALATE DIALLATE DIBENZO(A,H)ANTHRACENE DIBENZOFURAN DIETHYL PHTHALATE DIMETHOATE DIMETHYL PHTHALATE

13 Certifying Authority: PA Date of Issue: September 26, 2016 Certificate Number: Expiration Date: January 31, SEMI-VOLATILES EPA8270D EPA 3550C DIMETHYLAMINOAZOBENZENE ETHYL METHANESULFONATE FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE HEXACHLOROPROPENE INDEN0(1,2,3-CD)PYRENE ISODRIN ISOPHORONE ISOSAFROLE METHAPYRILENE METHYLMETHANESULFONATE N-NITROSODl-N-BUTYLAMINE N-NITROSODl-N-PROPYLAMINE N-NITROSODIETHYLAMINE N-NITROSODIMETHYLAMINE N-NITROSODIPHENYLAMINE N-NITROSOMETHYLETHYLAMINE N-NITROSOMORPHOLINE N-NITROSOPIPERIDINE N-NITROSOPYRROLIDINE NITROBENZENE (NB) 0,0,0-TRIETHYLPHOSPHOROTHIOATE 0-TOLUIDINE PENTACHLOROBENZENE PENTACHLORONITROBENZENE PENTACHLOROPHENOL PHENACETIN PHENANTHRENE PHENOL PRONAMIDE PYRE NE PYRIDINE SAFROLE TETRAETHYL DITHIOPYROPHOSPHATE THIONAZIN SOUTH CAROLINA DEPARTMENT OF HEAL TH AND ENVIRONMENTAL CONTROL EPA 8270D (SIM) EPA3510C 2-METHYL ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE, BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO(G,H,l)PERYLENE BENZO(K)FLUORANTHENE CH RYS ENE DIBENZO(A,H)ANTHRACENE FLUORANTHENE FLUORENE INDEN0{1,2,3-CD)PYRENE PHENANTHRENE PYRE NE EPA 8270D (SIM) EPA METHYL ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO(G,H,l)PERYLENE BENZO(K)FLUORANTHENE CHRYSENE DIBENZO{A,H)ANTHRACENE FLUORANTHENE FLUORENE INDEN0(1,2,3-CD)PYRENE PHENANTHRENE PYRENE ---VOLATILES (VOCS)----- EPA 8015C (GRO) EPA5030B TPH - LOW BOIL. PT. (GAS.) EPA 8015C (GRO) EPA5035 TPH - LOW BOIL. PT. (GAS.) EPA 8021B EPA 5030B BENZENE ETHYLBENZENE ISOPROPYLBENZENE METHYL TERT BUTYL ETHER (MTBE) TOLUENE XYLENE, TOTAL EPA EPA 5030B 1, 1, 1,2-TETRACHLOROETHANE 1, 1, 1-TRICHLOROETHANE 1, 1,2,2-TETRACHLOROETHANE 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE 1,1,2-TRICHLOROETHANE 1, 1-DICHLOROETHANE 1, 1-DICHLOROETHENE 1, 1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE(DBCP) 1,2-DIBROMOETHANE (EDB) 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,4-DIOXANE 2-CHLOR0-1,3-BUTADIENE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE ACETONITRILE ACROLEIN ACRYLONITRILE ALL YL CHLORIDE BENZENE BROMOCHLOROMETHANE EPA 8260B EPA 5030B BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE CYCLOHEXANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYL METHACRYLATE ETHYLBENZENE IODOMETHANE ISO BUTYL ALCOHOL ISOPROPYLBENZENE METHACRYLONITRILE METHYL ACETATE METHYL ETHYL KETONE (MEK) METHYL METHACRYLATE METHYL TERT BUTYL ETHER (MTBE) METHYLCYCLOHEXANE METHYLENE CHLORIDE P-ISOPROPYL TOLUENE PENTACHLOROETHANE PROPIONITRILE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRANS-1,4-DICHLOR0-2-BUTENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL ACETATE VINYL CHLORIDE XYLENE, TOTAL

14 SOUTH CAROLINA DEPARTMENT OF HEAL TH AND ENVIRONMENTAL CONTROL Certifying Authority: PA Date of Issue: September 26, 2016 Certificate Number: Expiration Date: January 31, VOLATILES (VOCS)--- EPA 8260B EPA , 1, 1,2-TETRACHLOROETHANE 1, 1, 1-TRICHLOROETHANE 1, 1,2,2-TETRACHLOROETHANE 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE 1, 1,2-TRICHLOROETHANE 1, 1-DICHLOROETHANE 1, 1-DICHLOROETHENE 1, 1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE(DBCP) 1,2-DIBROMOETHANE (EDB) 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 2-CHLOR0-1,3-BUTADIENE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE ACROLEIN ACRYLONITRILE ALL YL CHLORIDE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE CYCLOHEXANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE EPA8260B EPA5035 IODOMETHANE ISO BUTYL ALCOHOL ISOPROPYLBENZENE METHACRYLONITRILE METHYL ACETATE METHYL ETHYL KETONE (MEK) METHYL METHACRYLATE METHYL TERT BUTYL ETHER (MTBE) METHYLCYCLOHEXANE METHYLENE CHLORIDE P-ISOPROPYL TOLUENE PENTACHLOROETHANE PROPIONITRILE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRANS-1,4-DICHLOR0-2-BUTENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL CHLORIDE XYLENE, TOTAL 1,4-DIOXANE EPA 8260B (SIM) EPA 5030B EPA XY EPA5030B 3,3-DIMETHYL-1-BUTANOL DllSOPROPYL ETHER ETHANOL ETHYL TERT BUTYL ETHER T-AMYL ALCOHOL T-AMYL METHYL ETHER T-BUTYL ALCOHOL T-BUTYL FORMATE