Clean-up of Tank Battery Impoundments & Well Head Areas is Now a Reality. DeepEarth Technologies, Inc.

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1 Clean-up of Tank Battery Impoundments & Well Head Areas is Now a Reality William L. Lundy,, Principal DeepEarth Technologies, Inc.

2 Site Background Tank Battery Site - 1,000 cubic feet of crude oil impacted soil, heavily saturated Release occurred approximately 5 years ago Site underlain with a hard clay layer at 6 Well Head Approx. 20 sq ft. of aspaltines around well head where ground was impacted by hydrocarbons over time

3 Work Scope

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5 Challenges: Persistent Small Leaks Smelly and Unsightly Weathered crude oil takes on characteristics of asphalt paving

6 Plan of Action: Kill the strong odors at the site Jump start the remediation process at the weathered site Demonstrate the Cool-Ox Technology to: - Kill Odors upon contact - emulsify crudes and allow them to be separated from the soil mass to be recovered or simply disposed of in a fuel program.

7 Application: DTI s Field Crew applied approximately 175 gallons of Cool-Ox reagent to each site DTI s Hydro-Dart Tooling mixed the soils and applied the reagent to penetrate the depth of contamination

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13 How Does it Work? Cool-Ox generates hydrogen peroxide from solid peroxygens that are injected into the soil or groundwater in an aqueous suspension. Once in place, the peroxygens react with the water to produce hydrogen peroxide. The low solubility of the peroxygens allows them to be distributed throughout the sub-surface prior to reaction and increases the probability of contact with the contaminant!

14 Results

15 What Happened? Saw good results after treatment but A second release occurred on the site

16 Additional Sites Soil samples treated with Cool-Ox from Natural Gas Production Facilities in Colorado. Please note the great reduction in the SAR levels!

17 Garfield County, CO Sample # #1 #2 #3 Reactor Description Time PA 32-3 (Contaminated Soil ph EC SAR Benzene Toluene TRPH Day "0" Day ND ND % 100% 80% PA (EC Sludge) Day "0" ND ND 2,530 Day ND ND % Suicide Day "0" ND ND ND Day ND ND ND #4 #5 #6 Suicide (Frac Day "0" ,580 83,600 Day ND ,500 % reduction 100% 77% 56.30% RPW (Old Reserve Pit Day "0" ,800 Day ND ND % 100% 99.8% PA (Frac Day "0" ,340 90, Day ND 2, % 97.3% 64.8%

18 Garfield County, CO Sample # #7 #8 #9 #10 #11 Description Reactor Time ph EC SAR Benzene Toluene TRPH Workover Waste (Piles of Day "0" ND ND 796 Day ND ND % Frac Sand (10 - Day "0" ND 121 3,330 Day ND ND 1, % 52.6% Condensate & Produced Day "0" ND ND 158 Day ND ND % Cuttings 5200 D Day "0" Day ND ND % 100% 95.8% Evap Facility (Tank Day "0" ,000 4,330, ,000 Day , ,000 79, % 92.6% 65.2%

19 Contaminants & Sites Contaminants Free Product (NAPL) BTEX Coal Tars Vinyl Chloride & DCE Chlorobenzenes PAHs Creosote Jet Fuel Gas Condensate Fuel Oil (GRO/DRO/TPH) Herbicides Pesticides Pentachlorophenol (PCP) Dioxins Chlorinated Solvents PCBs Ethylene dibromide (EDB) Sites Service Stations Railroads Pipelines Agchem Formulators Mfg. Gas Plants (MGP) Wood Treating Military Bases Dry Cleaners Marine Bulk Terminals Slabs & Basements Sediments Mixed Plumes Refineries & Chem Plants Steel Mills

20 Contact is Everything Field Application Techniques DPT Injection Hydro-Dart Grizzly Soil Blending Twister Pit-Stop (over spray) Experience The value of DTI Turn-Key Installations

21 The Cool-Ox Process (Producing Hydrogen Peroxide In-Situ) CaO 2 + H 2 0 Ca(OH) 2 + H 2 O 2 (Chelates Activate Intrinsic Catalysts) H 2 O 2 + Fe +2 (OH) - + [OH] + Fe H 2 O 2 + Fe +3 (OH) - + [OOH] + Fe +2 (Radicals React with Contaminants) [OH] & [OOH] + C x C x (OH) y (Reaction by-products are CO2 and Calcium Carbonate that is not distinguishable from natural Calcium (Limestone) thus, not traceable!) The only totally Green and Sustainable Process!

22 Questions? Thank You! J. Bradley Stephenson Conestoga-Rover & Associates for DeepEarth Technologies, Inc. Alsip, IL