Analytical Instrumentation in the F&B Industry

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1 ISAB/F&B Symp/ /Slide No. 1 National Symposium on Automation & Digital Transformation of Food & Beverage Industry 26 th & 27 th February 2016 Analytical Instrumentation in the F&B Industry Standards Certification Education & Training Publishing Conferences & Exhibits RAJIV DOSHETTY AGM Marketing ( Analysis ) Endress + Hauser ( India ) Pvt. Ltd. Rajiv.Doshetty@In.Endress.Com

2 Analytical Instrumentation in the F&B Industry FoodSafe, Bengaluru 27 th February 2016 Slide 2 / 36

3 Topics Analyser types Analytical measurements in Food process Analytical measurement in Utilities Analytical measurement in Waste-Water Automation & Digital Transformation in Analytical instruments Slide 3 / 36

4 Analyser types Manual measurements Laboratory analysers Portable analysers Automated measurements In-situ analysers Wet-chemistry analysers Slide 4 / 36

5 Classical off-line system REALITY TODAY Manual, discontinuous transport Plant sampling Transport of sample Laboratory Operational Time and Operational Risk Possible change of measured value during the transport caused by Shift of chemical equilibrium Absorption/out gassing of volatile compounds (eg. CO 2 ) Slide 5 / 36

6 Analytical measurements in the food process Operate & Control your processes in an effective, efficient & safe manner Slide 6 / 36

7 Properties required of sensors in F&B Cleanable Confirmation of hygienic design according to EHEDG Unbreakable parts : e.g. non-glass ph sensors e.g. ISFET, metal enamel Slide 7 / 36

8 ph applications - examples Quality control Release of products (bottling of beer, soft drinks, mineral water) Receiving of raw material (e.g. milk at a dairy) Process control ph in milk products : cheese, yogurt Mayo, Ketchup, marmalade, tomato sauce Slide 8 / 36

9 Conductivity applications - examples Core application: CIP control Phase separation Bottle cleaning Product monitoring Slide 9 / 36

10 Conductivity in CIP process Concentration monitoring of the cleansing agents Control of phase separation between water & cleansing agent in CIP return product product acid H 2 SO 4 NaOH rinsing water drain to filling system Slide 10 / 36

11 CIP examples Brewery CIP return Dairy CIP tank Slide 11 / 36

12 DO Applications Fillers (absence of Oxygen in Beer) Brewing processes Process control Fermentation Inertization Juice bottler Degasing of Juice Slide 12 / 36

13 DO in yeast propagation Controlled input of air / oxygen to control the growing of yeast in the brewery Slide 13 / 36

14 DO in juice bottling process Process: Juice bottling Application: O2 content before and after degasing process of different kinds of juices Customer benefit: Traceability of their process for their customers Slide 14 / 36

15 Process Photometers applications - examples Turbidity measurements Fermentation process - cell growth Crystallization processes monitoring and controlling the crystal formation Colour measurement Color scale measurement like APHA, Hazen, EBC, ASBC, ASTM, ICUMSA, Lovibond Turbidity measurements in dairy Milk/water phase detection Milk drain monitoring Slide 15 / 36

16 Process Photometers applications - examples Turbidity A good filtration results in a low turbidity Filtration system optimization through diatomaceous earth dosage Centrifuge control + Colour Color identification of Beer Syrup Colour Sugar Colour + Slide 16 / 36

17 Analytical measurements in Utilities Monitoring and Controlling to protect your processes & investments Slide 17 / 36

18 Application areas & parameters Application Areas Control of Reverse osmosis Control of ion exchangers Monitoring of steam condensate Control of cooling water Measuring parameters ph Conductivity Dissolved Oxygen Turbidity Chlorine Silica Sodium Phosphate Hydrazine Hardness Slide 18 / 36

19 SWAS Panels (Steam-Water-Analysis-System ) Slide 19 / 36

20 Disinfection control sampling point Static mixer dosing point flowmeter Transmitter CCA 250 Slide 20 / 36

21 Analytical measurements in Waste-Water Treatment Monitoring and Controlling to fulfill your environmental responsibilities Slide 21 / 36

22 What to control in each step? Inlet of WWTP Primary treatment Secondary Treatment / Biological Outlet WWTP - ph - Conductivity - TOC - Samplers - DO - Sludge level - NH4+, NO3 - Sludge concentration - PO4-, - Sludge Level - Sludge concentration - TOC/COD/BOD - ph - NH4+ - Chlorine - Samplers Slide 22 / 36

23 Why we should control this parameters? ph Assure the life of the microorganisms in the biological treatment, the water quality for the treatment and correct flocculation. Conductivity Salt and Metal content. Organic load(bod; COD; TOC) Treatment efficiency, meeting regulations requirements Dissolved oxygen Optimal source of oxygen for the microorganisms to be able to digest the organic load. NH 4, NO 3 y PO 4 3- Concentration Hazardous compounds for the ecosystem, efficiency monitoring in the Biological treatment Free Chlorine Disinfection, reduction of pathogen microorganisms Turbidity Bacteria content in the Biological treatment and Suspended solids content in the outlet Sludge level Clarifiers capacity and sludge management Sludge concentration Avoid recirculating water to the biological treatment and to the sludge treatment Flow Monitor of volume of waste in and out from the factory Slide 23 / 36

24 Automation & Digitisation in Analytical Measurements Slide 24 / 36

25 Automatic cleaning For all hygienic applications with frequent soiling of the sensor to maintain best measuring performance Safe money due to regular & automatic instead of time consuming manual cleaning Slide 25 / 36

26 Memosens Sensor with memory & digital signal Contactless, inductive signal and data transfer Fast and easy sensor change No chance for moisture, salt bridges and corrosion Maintenance and sensor change is done as planned Extremely high availability of the measuring point thanks to the possibility of sensor calibration in the laboratory inductive signal transfer inductive energy supply Memosens saves time and money Memosens increases safety and availability Slide 26 / 36

27 Calibration and Maintenance in the ideal conditions Sensors with Memosens technology are the first sensors to allow a calibration of the sensor independent from the actual measuring point. Slide 27 / 36

28 Time savings With Memosens technology calibration/adjustment away from the measuring point in the measuring lab is possible Expenditure of time for maintenance / recalibration Digital Memosens sensors Standard analogue sensors Error message: maintenance needed Take recalibrated sensor Remove sensor Install sensor Release measuring point Error message: maintenance needed Take cleaning agent Take buffers Take new sensors from shelf Remove sensor Clean/exchange sensor Calibrate sensor with buffer 1 Calibrate sensor with buffer 2 Install sensor Release measuring point Slide 28 / 36

29 Memosens Plus - Managment Software With Memobase Plus installed in your PC and Memosens sensors, you can easy: Measure Calibrate/adjust Document Calibrate Document Measure Slide 29 / 36

30 Multiparameter, Multichannel transmitters One transmitter for all parameters ph, ORP, conductivity, dissolved oxygen, turbidity, nitrate, chlorine, ISE, ultrasonic sludge level and SAC Makes you flexible thanks to modular concept Easy to use menu guidance and common operation concept Saves you time by quick sensor exchange with precalibrated Memosens sensors Comfortable remote access via web server using tablets or PCs Webbrowser Slide 30 / 36

31 Increased comfort by the Ethernet web server Remote measurement values via a standard WiFi/WLAN/GSM/3G Router Full access for device configuration, measured values, diagnostics, logbooks and service data Slide 31 / 36

32 Example: cyclic measured values via Modbus TCP Easy remote access via Modbus TCP Optional even wirelessly On all Memosens values & I/Os Via any Modbus TCP viewer Modbus TCP over Ethernet PLC Slide 32 / 36

33 Various possibilities for remote access and configuration Slide 33 / 36

34 Seamless integration into control systems FieldCare Every ma device with HART communication RS 485 based communication Profibus DP Modbus RS485 Ethernet based communication Modbus TCP Ethernet/IP Ethernet webserver for configuration use with standard web browsers like Internet Explorer, Firefox and others Connectable to standard PC/Ethernet equipment Slide 34 / 36

35 E+ H in Liquid Analytics Summary Analytical measurements Processes : operate your processes in an effective, efficient & safe manner Utilities : protect your processes and investments Waste-water treatment : fulfill your environmental responsibilities Newer analytical technologies / features : optimise and improve operational excellence Automatic sensor cleaning : eases sensor maintenance Digital sensor signal : help in reliable measurement and ease operation and maintenance efforts besides ensuring higher availability of measurement time Multiparameter/multichannel transmitters : increase flexibility and reduces cost-ofownership Digital output : Seamless integration of data communication with user s server Analytical instrumentation help you in achieving your objectives of digitisation and automation! Slide 35 / 36

36 Thank you very much for your attention Slide 36 / 36