Discipline Chemical Testing Issue Date Certificate Number T-3553 Valid Until Last Amended on - Page 1 of 9

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1 Last Amended on - Page 1 of 9 I. ORES & MINERALS 1. Iron Ore Total Iron IS 1493: 1981 (RA 2006) 10 % to 70 % Silicon IS 1493: 1981 (RA 2006) 0.5 % to 25 % Aluminum IS 1493: 1981 (RA 2006) 0.5 % to 20 % Phosphorus IS 1493: 1981 (RA 2006) 0.02 % to 0.1 % Sulphur IS 1493: 1981 (RA 2006) % to 0.02 % Loss of Ignition IS 1493: 1959 (RA 2001) 0.5 % to 15 % Manganese IS 1493: 1959 (RA 2001) 0.1 % to 2 % Bulk density IS 5842: 1986 (RA 2014) 1 g/cc to 10 g/cc 2. Manganese Ore Manganese IS 1473: 2004 (RA 2008) 5 % to 50 % Manganese dioxide IS 1473: 2004 (RA 2008) 2 % to 40 % Silicon IS 1473: 2004 (RA 2008) 0.5 % to 15 % Iron IS 1473: 2004 (RA 2008) 1 % to 40 % Aluminum IS 1473: 2004 (RA 2008) 0.5 % to 10 % Phosphorus IS 1473: 2004 (RA 2008) 0.01 % to 0.1 % Sulphur IS 1473: 2004 (RA 2008) 0.01 % to 0.2 %

2 Last Amended on - Page 2 of 9 3. Bauxite Ore Aluminum IS 2000 (Part 3): 1985 (RA 2006) 1 % to 90 % Silicon IS 2000 (Part 2): 1985 (RA 2006) 0.5 % to 20 % Loss of Ignition IS 2000 (Part 1): 1985 (RA 2006) 0.5 % to 30 % Titanium IS 2000 (Part 5): 1985 (RA 2006) 0.5 % to 12.0 % Ferric Oxide IS 2000 (Part 4): 1985 (RA 2006) 1 % to 35.0 % 4. Limestone & Dolomite Loss of Ignition IS 1760 (Part 1): 1991 (RA 2001) 1 % to 50 % Silicon IS 1760 (Part 2): 1991 (RA 2001) 0.5 % to 15 % Ferric Oxide IS 1760 (Part 3): 1991 (RA 2001) 0.2 % to 2 % Calcium IS 1760 (Part 3): 1991 (RA 2001) 0.5 % to 40 % Magnesium IS 1760 (Part 3): 1991 (RA 2001) 0.2 % to 40 % Aluminum IS 1760 (Part 3): 1991 (RA 2001) 0.2 % to 5.0 % II. AIR, GASES & ATMOSPHERE 1. Stack Monitoring Particulate matter IS (Part 1): 1985 (RA 2003) 1.0 mg/nm 3 to 1000 mg/nm 3 Oxides of Sulphur IS (Part 2): 1985 (RA 2003) 3.0 mg/nm 3 to 500 mg/nm 3 Oxides of Nitrogen IS (Part 7): 2005 (RA 2012) 3.0 mg/nm 3 to 400 mg/nm 3 2. Ambient Air Quality Monitoring Particulate Matter (Size less than 10µm) or PM10 IS 5182 (Part 4): 1999 (RA 2010) 1.0 µg/m 3 to 1000 µg/m 3

3 Last Amended on - Page 3 of 9 Ambient Air Quality Monitoring Particulate Matter (Size less than 2.5µm) or PM 2.5 USEPA µg/m 3 to 500 µg/m 3 Sulphur Dioxide IS 5182 (Part 2): 2001 (RA 2012) 4.0 µg/m 3 to 200µg/m 3 (SO 2) µg/m 3 Nitrogen Dioxide IS 5182 (Part 6): 2006 (RA 2012) 6.0 µg/m 3 to 200 µg/m 3 (NO 2) µg/m 3 3. Ambient Noise Monitoring Ambient Noise IS 9989: 1981 (RA 2008) 35 dba to 100 dba III. WATER 1. Potable and Drinking Water ph Page to to 14 Total Hardness APHA (22 nd Edition) 2340 C Page to 2-46 Calcium Page to 3-68 Magnesium Page Chloride Page to 4-73 Total Alkalinity APHA (22 nd Edition) 2320 B Page to 2-36

4 Last Amended on - Page 4 of 9 Potable and Drinking Water Conductivity APHA (22 nd Edition) 2510 B Page µs/cm to µs/cm Total Dissolved Solids APHA (22 nd Edition) 2540 C Page mg/l to mg/l Sulphate APHA (22 nd Edition) 4500 E Page to Fluoride APHA (22 nd Edition) 4500 D Page to mg/l to 1.50 mg/l Nitrate APHA (22 nd Edition) 4500 Page to mg/l to 10 mg/l Nitrite Iron Turbidity Sodium Potassium Boron Total suspended solids Page to Page to 3-80 APHA (22 nd Edition) 2130 B Page to 2-15 Page to 3-98 Page to 3-88 Page to 4-26 APHA (22 nd Edition) 2540 D Page. 2-66t o mg/l to 20 mg/l 0.02 mg/l to 50 mg/l 0.01 NTU to 100 NTU 0.1 mg/l to 1000mg/l 0.1 mg/l to 100 mg/l 0.02 mg/l to 10 mg/l

5 Last Amended on - Page 5 of 9 Potable and Drinking Water Total Solids APHA (22 nd Edition) 2540 B Page Chromium APHA (22 nd Edition) 2540 B Page mg/l to 10 mg/l 2. Waste Water ph Page to to 14 Total Hardness Calcium Magnesium Chloride Total Alkalinity Conductivity Total Dissolved Solids Sulphate Fluoride APHA (22 nd Edition) 2340 C Page to 2-46 Page. 3-67to 3-68 Page Page to 4-73 APHA (22 nd Edition) 2320 B Page to 2-36 APHA (22 nd Edition) 2510 B Page APHA (22 nd Edition) 2540 C Page APHA (22 nd Edition) 4500 E Page to APHA (22 nd Edition) 4500 D Page to mg/l to mg/l 1 mg/l to mg/l 1 µs/cm to µs/cm 1 mg/l to 100 mg/l 0.05 mg/l to 10.0 mg/l

6 Last Amended on - Page 6 of 9 Waste Water Nitrate APHA (22 nd Edition) 4500 E Page to mg/l to 250 mg/l Nitrite Iron Turbidity Dissolved Oxygen Sodium Potassium Boron Chemical oxygen Demand Biological oxygen Demand Oil & Grease Total solids Page to Page to 3-80 APHA (22 nd Edition) 2130 B Page to 2-15 APHA (22 nd Edition) 4500N C Page to Page to 3-98 Page to 3-88 Page to 4-26 APHA (22 nd Edition) 5220 D Page. 5-20to 5-21 APHA (22 nd Edition) 5210 B Page to 5-10 APHA (22 nd Edition) 5520 B Page to 5-41 APHA (22 nd Edition) 2540 B Page mg/l to 50 mg/l 0.02 mg/l to 100 mg/l 0.01 NTU to 500 NTU 1.00 mg/l to 8.00 mg/l 1 mg/l to 500 mg/l 0.02 mg/l to 10 mg/l 2 mg/l to mg/l 4 mg/l to mg/l 5 mg/l to 100 mg/l

7 Last Amended on - Page 7 of 9 Waste Water Total suspended solids APHA (22 nd Edition) 2540 D Page to 2-67 IV. BUILDING MATERIALS 1. Soil Moisture Content (%) IS 2720 (Part 18): 1992 (RA 2011) 1 % to 50 % ph IS 2720 (Part 26): 1987 (RA 2011) 0.1 to 14.0 Conductivity IS 14767: 2000 (RA 2010) 1 µs/cm to 1000 µs/cm Organic Matter (%) IS 2720 (Part 22): 1972 (RA 2010) 1 % to 25 % V. POLLUTION & ENVIRONMENT 1. Effluents ph Page to 4-96 Total Hardness APHA (22 nd Edition) 2340 C Page to to 14 1 mg/l to mg/l Calcium Magnesium Chloride Total Alkalinity Conductivity Page. 3-67to 3-68 Page Page to 4-73 APHA (22 nd Edition) 2320 B Page to 2-36 APHA (22 nd Edition) 2510 B Page mg/l to mg/l 1 µs/cm to µs/cm

8 Last Amended on - Page 8 of 9 Effluents Total Dissolved Solids APHA (22 nd Edition) 2540 C Page Sulphate Fluoride Nitrate Nitrite Iron Turbidity Dissolved Oxygen Sodium Potassium Boron Chemical oxygen Demand APHA (22 nd Edition) 4500 E Page to APHA (22 nd Edition) 4500 D Page to 4-88 APHA (22 nd Edition) 4500 E Page to Page to Page to 3-80 APHA (22 nd Edition) 2130 B Page to 2-15 APHA (22 nd Edition) 4500N C Page to Page to 3-98 Page to 3-88 Page to 4-26 APHA (22 nd Edition) 5220 D Page. 5-20to mg/l to 100 mg/l 0.05 mg/l to 10.0 mg/l 0.1 mg/l to 250 mg/l 0.1 mg/l to 50 mg/l 0.02 mg/l to 100 mg/l 0.01 NTU to 500 NTU 1.00 mg/l to 8.00 mg/l 1 mg/l to 500 mg/l 0.02 mg/l to 10 mg/l 2 mg/l to mg/l

9 Last Amended on - Page 9 of 9 Effluents Biological oxygen Demand APHA (22 nd Edition) 5210 B Page to mg/l to mg/l Oil & Grease APHA (22 nd Edition) 5520 B Page to mg/l to 100 mg/l Total solids APHA (22 nd Edition) 2540 B Page Total suspended solids APHA (22 nd Edition) 2540 D Page to X-X-X-X-X-X-X-X-X-X-X-X-X-X-

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