A great fermentation step, now what?

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1 A great fermentation step, now what? Mathieu Bailly / Daniel Bar 4th Bio-based Chemicals Summit Del Mar, CA January 29 th, 2013

2 Eurodia / Ameridia designs and implements complete process solutions for purification and fractionation. EURODIA INDUSTRIE S.A. Established 1988 Shareholder 99% Tokuyama Corp. (Japan) Turnover MM Total staff 60 EURODIA in North America Ameridia (New Jersey, USA) since 1999 EURODIA in Russia Eurodia Kuban (Krasnodar, Kuban State) EURODIA in China Lixus Separation Technologies (Shanghai) TOKUYAMA CORPORATION A leading producer of specialty chemicals Established 1918 Turnover Billions USD Employees 4700 Subsidiaries 107 (including EURODIA) 2

3 OUR TECHNOLOGIES ADVANCED SEPARATION TECHNOLOGIES Electrodialysis (conventional & bipolar) Membrane filtration systems (MF, UF, NF, RO) COMPLETE PROCESS SOLUTIONS Chromatography & ion exchange resins 3

4 OUR APPLICATIONS MAIN INDUSTRIES DAIRY Whey processing / demineralization Proteins fractionation Milk standardization STARCH AND SUGAR WINE Tartrate stabilization of wines and juices ph adjustment of wines and juices Alcohol removal from wines Liquid sugar production Sugar decalcification Demineralization, clarification & decoloration of syrups Purification of specialty sugars and polyols Production of glucose & fructose Purification of oligosaccharides 4

5 OUR APPLICATIONS MAIN INDUSTRIES (cont.) GREEN CHEMISTRY Purification of organic acids Gluconic Acid Lactic Acid (PLA production / Bioplastics) Succinic Acid (Building block: BDO / PBS / others Acetic Acid (Vitamins) Ketogulonic Acid (Vitamin C) others Demineralization and purfication of amino acids Glycine Purification of plant proteins From peas From potatoes others 5

6 EURODIA : INTERNATIONAL REFERENCES Canada Europe Russia USA North Africa Middle East Japan Mexico China Brazil Chile Australa Argentina South Africa New Zealand 6

7 The right purification process GREEN CHEMISTRY Meets the stringent purity requirements of the chemical industry Gives a high product yield Has low operating costs Minimizes the capital investment Has the lowest effluent load The right process solution is often an optimized combination of several separation techniques

8 GREEN CHEMISTRY SUGARS FERMENTATION A good fermentation (or catalytic reaction) is only the start to obtain bio-based chemicals meeting the industry purity requirements. CLARIFICATION CROSS-FLOW MF and UF PURIFICATION BIPOLAR MEMBRANE ED ION EXCHANGE RESINS CHROMATOGRAPHY NANOFILTRATION CONCENTRATION The right purification process is key!

9 GREEN CHEMISTRY Other constraints Effluent specifications Initial product quality & quantity Process solution 15 years of R&D programs and feedback from industrial successes Final Product quality Selection based on know-how or from R&D studies Production costs Investment costs Calculations based on dedicated files / data base 9

10 GREEN CHEMISTRY FOCUS ON A GREEN TECHNOLOGY: BIPOLAR MEMBRANE ELECTRODIALYSIS (EDBM) An efficient production of acid and base from salts (e.g. Lactic acid / NH 4 OH from Ammonium Lactate) Driving force : electricity no chemicals, no effluents Recently: Development of high temperature EDBM (65 C) Minimization of energy footprint (by >25%) e.g vs 0.95 kwh/kg of lactic acid Improved control of bacterial contamination of DSP Possibility to process viscous and specific streams (e.g. Succinic Acid)

11 GREEN CHEMISTRY BIPOLAR MEMBRANE ELECTRODIALYSIS (EDBM): PRINCIPLE «WATER SPLITTING» MEMBRANE Bipolar membrane CEL + OH - H H + 2 O - AEL

12 GREEN CHEMISTRY BIPOLAR MEMBRANE ELECTRODIALYSIS (EDBM): PRINCIPLE TWO-COMPARTMENT STACK FOR ORGANIC ACID PRODUCTION NaOH Organic acid HX (+NaAc) Anode K BP K BP K BP K BP K BP K Na + Na + Na + Na + OH - H + OH - H + OH - H + OH - H + OH - H + Cathode + - X - X - X - X - X - Water Organic Salt (NaAc) K: cation exchange membrane BP: bipolar membrane

13 SOME EDBM INDUSTRIAL REFERENCES GREEN CHEMISTRY

14 :THE FUTURE IS NOW GREEN CHEMISTRY

15 GREEN CHEMISTRY THE KEY FOR PURIFICATION: COMBINING VARIOUS TECHNIQUES Filtration Ceramic TAMI membranes / UF: to optimize DSP Organic membranes / NF: as part of polishing steps Ion Exclusion Chromatography Removal of salts, color, sugar, AA Separation of organic salts from acids Ion Exchange Resins (conventional or continuous) Key Polishing steps to remove last traces of impurities Combination with complementary technologies: crystallization, evaporation, distillation, etc.

16 GREEN CHEMISTRY THE KEY FOR PURIFICATION: THE COMBINATION OF VARIOUS TECHNIQUES SOME INDUSTRIAL REFERENCES

17 GREEN CHEMISTRY CONCLUSIONS Eurodia/Ameridia has the expertise in bio-based organic acids to develop the most suitable downstream purification processes With our pilot facilities and simulation software, we have the tools to guarantee performance for our clients specific feedstreams We work under strict confidentiality obligations.

18 Thank you for your attention

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