Hitech Healthcare Laboratory and Research Centre, 201, Sahaj Arcade, Science City Road, Ahmedabad, Gujarat

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1 Last Amended on Page 1 of 20 I. WATER 1. Packaged Packaged Natural Mineral Water, Treated Water, Colour IS 3025 (Part 4): 1983 (RA 2002), Amd. 1: March 2007 Odour IS 3025 (Part 5): 1983 (RA 2002) Taste IS 3025 (Part 8): 1984 (RA 2002) Turbidity IS 3025 (Part 10): 1984 (RA 2002) Total Dissolved Solids IS 3025 (Part 16): 2002, (RA 2006) Amd. 1: Dec ph IS 3025 (Part 11): 1983 (RA 2002) Barium (As Ba) IS 13428: 2005 Amd. 4: 2011 Annexure F Chloride (As Cl) IS 3025 (Part 32): 1988, [Argenometric Method] Alkalinity IS 3025 (Part 23): 1986 Amd. 2, 2006 (1 to 500) Hazen unit Qualitative (Agreeable/ Disagreeable) Qualitative (Agreeable/ Disagreeable) 0.1 NTU to 1000 NTU 5 mg/l to 500 mg/l 500 mg/l to mg/l 02 to mg/l to 2000 mg/l 0.5 mg/l to mg/l 0.5 mg/l to mg/l

2 Last Amended on Page 2 of 20 Packaged Packaged Natural Mineral Water, Treated Water, Calcium (As Ca) IS 3025 (Part 40): 1991 Amd. 1: 2004 Magnesium (As Mg) IS 3025 (Part 46): 1994 Amd. 2: March 2003 Residual Free Chlorine IS 3025 (Part 26): 1986 Amd. 1: Feb Nitrate (As NO 3 ) IS 3025 (Part 34): 1988 / APHA (22 nd Edition) 4500 NO 3 - B Nitrite (As NO 2 ) IS 3025 (Part 34): 1988 Sulphide (As H 2 S) IS 3025 (Part 29): 1986 / APHA (22 nd Edition) 4500-S - - D,F Antimony IS 13428: 2005 Amd. 4: 2011, Annexure G IS 15303: 2003, USEPA Phenolic Compounds IS 3025 (Part 43): mg/l to 5000 mg/l 0.1 mg/l to 5000 mg/l 0.05 mg/l to 20 mg/l 0.1 mg/l to 1000 mg/l 0.01 mg/l to 500 mg/l 0.01 mg/l to 100 mg/l mg/l to 100 mg/l 0.01 mg/l to 50 mg/l

3 Last Amended on Page 3 of 20 Packaged Packaged Natural Mineral Water, Treated Water, Mineral Oil IS 3025 (Part 39) (FTIR): 1991 Amd. 2: 2013 Anionic Surface Active Agents IS 13428: 2005 Amd. 4: 2011 Annexure K Borates IS 13428: 2005 Amd. 4: 2011 Annexure H Cyanide IS 3025 (Part 27): 1986, Amd. 1: April 2003 (RA 2009) 0.05 mg/l to 100 mg/l 0.1 mg/l to 20 mg/l 0.5 mg/l to 50 mg/l 0.01 mg/l to 50 mg/l Aluminum IS 3025 (Part 55): mg/l to 10 mg/l Silver IS 13428: 2005, Amd. 4: 2011, Annexure J USEPA Sulphate IS 3025 (Part 24): 1986 [Turbidity method] Total Hardness (As CaCO 3 ) IS 3025 (Part 21): 1983 (RA 2009) Fluoride (As F) IS 3025 (Part 60): 2008/ APHA (22 nd Edition) 4500-F ˉD mg/l to 50 mg/l 0.5 mg/l to 2000 mg/l 1 mg/l to 5000 mg/l 0.10 mg/l to 50 mg/l Manganese (As Mn) IS 3025 (Part 59): mg/l to 10 mg/l Zinc (As Zn) IS 3025 (Part 49): mg/l to 50 mg/l

4 Last Amended on Page 4 of 20 Packaged Packaged Natural Mineral Water, Treated Water, Copper (As Cu) IS 3025 (Part 42): 1992 /USEPA mg/l to 20 mg/l Iron (As Fe) IS 3025 (Part 53): mg/l to 50 mg/l Selenium (As Se) IS 3025 (Part 56): 2003 / USEPA Mercury (As Hg) IS 3025 (Part 48): 1994, Amd. 1: Oct mg/l to 20mg/l mg/l to 20 mg/l Sodium (As Na) IS 3025 (Part 45): 1993 Amd. 1: 2003 Cadmium (As Cd) IS 3025 (Part 41): 1992 / USEPA Arsenic (As As) IS 3025 (Part 37): 1988 / USEPA Lead (As Pb) IS 3025 (Part 47): 1994, (RA 2009) Amd: 2003/ USEPA Chromium (As Cr) IS 13428: 2005, Amd. 4: 2011,J / USEPA Nickel (As Ni) IS 13428: 2005, Amd. 4: 2011, L / USEPA mg/l to 2000 mg/l mg/l to 10 mg/l mg/l to 20 mg/l mg/l to 20 mg/l mg/l to 20 mg/l mg/l to 20 mg/l

5 Last Amended on Page 5 of 20 Packaged Packaged Natural Mineral Water, Treated Water, PAH (Polynuclear Aromatic Hydrocarbons) Naphthalene Acenaphthylene 2-Bromonaphthalene Acenaphthene SOP No. HTL/WI-TST/C/040, Issue. 01, Dated APHA (22 nd Edition) 6440, EPA 525.2) 0.01 mg/l to 2000 µg/l Fluorene Anthracene Phenanthrene Fluoranthene Pyrene Benz[A]Anthracene Chrysene Benzo[B]Fluoranthene Benzo[A]Pyrene Indeno[1,2,3-Cd]Pyrene Dibenz[A,H]Anthracene Benzo[G,H,I]Perylene

6 Last Amended on Page 6 of 20 Packaged Packaged Natural Mineral Water, Treated Water, PCBs (Polychlorinated Biphenyl) PCB-(Bz #28) PCB-(Bz #52) PCB-(Bz #101) PCB-(Bz #153) SOP No. HTL/WI-TST/C/040, Issue. 01, Dated APHA (22 nd Edition) 6440, EPA µg/l to 2000 µg/l PCB-(Bz #138) PCB-(Bz #180) Pesticide Residues Analysis O,P-DDD O,P' DDT O,P' DDE SOP No. HTL/WI-TST/C/041, Issue. 01, Dated (USEPA 508, 1657A, 525.2, 8141A, 507, 527) P,P' DDD P,P' DDT P,P' DDE Lindane a-hch 0.01 µg/l to 5000 µg/l b-hch 0.01 µg/l to 5000 µg/l d-hch

7 Last Amended on Page 7 of 20 Packaged Packaged Natural Mineral Water, Treated Water, Endosulfan A Endosulfan B Endosulfan Sulphate Ethion Chlorpyrifos SOP No. HTL/WI-TST/C/041, Issue. 01, Dated (USEPA 508, 1657A, 525.2, 8141A, 507, 527) Butachlor Phorate Phorate Sulfone Alachlor Atrazine Malathion Aldrin Dieldrin Methyl Parathion Malaoxon Methyl Paraoxon SOP No. HTL/WI-TST/C/042, Issue. 01, Dated (USEPA 8141A, 527 ) Monocrotophos 0.05 µg/l to 5000 µg/l Phorate Sulphoxide 0.05 µg/l to 5000 µg/l

8 Last Amended on Page 8 of 20 Packaged Packaged Natural Mineral Water, Treated Water, Isoproturon 2,4-D SOP No. HTL/WI- TST/C/043/A, Issue. 01, Dated (USEPA 532) SOP No. HTL/WI-TST/C/043, Issue. 01, Dated (USEPA 555, 515.1) 0.05 µg/l to 5000 µg/l 0.05 µg/l to 5000 µg/l Bromates (As Bro 3 ) ISO 15061: mg/l to 20 mg/l 2. Waste Water, Effluent Water Total Hardness (As CaCO 3 ) IS 3025 (Part 21): 1983 (RA 2009) Total Dissolved Solids IS 3025 (Part 16): 2002 (RA 2006),Amd. 1: Dec Chloride (As Cl) IS 3025 (Part 32): 1988 [Argenometric Method] Alkalinity IS 3025 (Part 23): 1986 Amd. 2: 2006 Residual Free Chlorine IS 3025 (Part 26): 1986 Amd. 1: Feb Nitrate (As NO 3 ) IS 3025 (Part 34): 1988 / APHA (22 nd Edition) 4500 NO 3 - B 1 mg/l to 5000 mg/l 5 mg/l to 500 mg/l 500 mg/l to mg/l 0.5 mg/l to mg/l 0.5 mg/l to mg/l 0.05 mg/l to 20 mg/l 0.1 mg/l to 1000 mg/l

9 Last Amended on Page 9 of 20 Waste Water, Effluent Water Nitrite (As NO 2 ) IS 3025 (Part 34): 1988 Sulphide (As H 2 S) IS 3025 (Part 29): 1986 / APHA (22 nd Edition) 4500-S - - D,F Antimony IS 13428: 2005, Amd. 4: 2011 Annexure G, IS 15303: 2003, USEPA mg/l to 500 mg/l 0.01 mg/l to 100 mg/l mg/l to 100 mg/l Aluminum IS 3025 (Part 55): mg/l to 10 mg/l Silver IS 13428: 2005, Amd. 4: 2011, Annexure J,USEPA Sulphate IS 3025 (Part 24): 1986 [Turbidity method] Fluoride (As F) IS 3025 (Part 60): 2008/ APHA (22 nd Edition) 4500-F ˉD mg/l to 50 mg/l 0.5 mg/l to 2000 mg/l 0.10 mg/l to 50 mg/l Manganese (As Mn) IS 3025 (Part 59): mg/l to 10 mg/l Zinc (As Zn) IS 3025 (Part 49): 1994 Copper (As Cu) IS 3025 (Part 42): 1992 /USEPA mg/l to 50 mg/l mg/l to 20 mg/l Iron (As Fe) IS 3025 (Part 53): mg/l to 50 mg/l

10 Last Amended on Page 10 of 20 Waste Water, Effluent Water Selenium (As Se) IS 3025 (Part 56): 2003 / USEPA Mercury (As Hg) IS 3025 (Part 48): 1994, Amd. 1: Oct Sodium (As Na) IS 3025 (Part 45): 1993 Amd. 1: 2003 Cadmium (As Cd) IS 3025 (Part 41): 1992 / USEPA Arsenic (As As) IS 3025 (Part 37): 1988 / USEPA Lead (As Pb) IS 3025 (Part 47): 1994, Amd: 2003 (RA 2009)/ USEPA mg/l to 20mg/l mg/l to 20 mg/l 1 mg/l to 2000 mg/l mg/l to 10 mg/l mg/l to 20 mg/l mg/l to 20 mg/l Chromium (As Cr) Nickel (As Ni) IS 13428: 2005, J Amd. 4: 2011 / USEPA IS 13428: 2005, L Amd. 4: 2011/ USEPA mg/l to 20 mg/l mg/l to 20 mg/l 3. Waste Water, Effluent Water, Dissolved Oxygen (Do) IS 3025 (Part 38): 1989 / APHA (22 nd Edition) O/CPCB Manual (SOP No. HTL/WI-TST/C/151, Issue. 01, Dated ) 0.5 mg/l to 18 mg/l

11 Last Amended on Page 11 of 20 Waste Water, Effluent Water, Biochemical Oxygen Demand (Bod) IS 3025 (Part 44): 1993 (RA 2009)/ APHA (22 nd Edition) 5210 / CPCB Manual (SOP No. HTL/WI-TST/C/152, Issue. 01, Dated ) 0.5 mg/l to mg/l Chemical Oxygen Demand (Cod) IS 3025 (Part 58): 2006 / APHA (22 nd Edition) 5220/CPCB Manual (SOP No. HTL/WI-TST/C/153, Issue. 01, Dated ) Total Suspended Solids IS 3025 (Part 17): 1984, (RA 2012) Amd. 1: Dec /APHA (22 nd Edition) D/CPCB Manual (SOP No. HTL/WI-TST/C/155, Issue. 01, Dated ) Total Solids IS 3025 (Part 15): 1984, (RA 2009) Amd. 1: Jan /APHA (22 nd Edition) B/CPCB Manual (SOP No. HTL/WI-TST/C/154, Issue. 01, Dated ) Acidity IS 3025 (Part 22): 1986 / APHA (22 nd Edition) 2310/CPCB Manual (SOP No. HTL/WI-TST/C/158, Issue. 01, Dated ) 1.0 mg/l to mg/l 5 mg/l to mg/l 5 mg/l to mg/l 5 mg/l to mg/l

12 Last Amended on Page 12 of 20 Waste Water, Effluent Water, Settleable Solids APHA (22 nd Edition) F/CPCB Manual (SOP No. HTL/WI-TST/C/156, Issue. 01, Dated ) Non Settleable Solids APHA (22 nd Edition) F/CPCB Manual (SOP No. HTL/WI-TST/C/157, Issue. 01, Dated ) Fixed Solids APHA (22 nd Edition) 2540-E (SOP No. HTL/WI-TST/C/205, Issue. 01, Dated ) Volatile Solids APHA (22 nd Edition) E(SOP No. HTL/WI- TST/C/205, Issue. 01, Dated ) Silica APHA (22 nd Edition) 4500-SiO 2 (SOP No. HTL/WI-TST/C/210, Issue. 01, Dated )/ IS 3025 (Part 35): 1988 Ammonical Nitrogen IS 3025 (Part 34): 1988 / APHA (22 nd Edition) 4500-NH 3 (SOP No. HTL/WI-TST/C/199, Issue. 01, Dated ) Chloramines IS 3025 (Part 26): 1986 Amd. 1: Feb mg/l to mg/l 0.1 ml/l to 100 ml/l 5 mg/l to 5000 mg/l 0.1 ml/l to 100 ml/l 10 mg/l to mg/l 10 mg/l to mg/l 0.2 mg/l to 1000 mg/l 5 mg/l to 300 mg/l 0.1 mg/l to 10 mg/l

13 Last Amended on Page 13 of 20 Waste Water, Effluent Water, Phosphorous IS 3025 (Part 31): 1988 / APHA (22 nd Edition) 4500-P (SOP No. HTL/WI-TST/C/207, Issue. 01, Dated ) Potassium IS 3025 (Part 45): 1993, Amd. 1: April 2003 /APHA (22 nd Edition) 3500-K (SOP No. HTL/WI-TST/C/208, Issue. 01, ) Electric Conductance APHA (22 nd Edition) 2510 (SOP No. HTL/WI-TST/C/204, Issue. 01, Dated )/ IS 3025 (Part 14) : 2013 Temperature APHA (22 nd Edition) 2550 (SOP No. HTL/WI-TST/C/212, Issue. 01, ) Salinity APHA (22 nd Edition) 2520 (SOP No. HTL/WI-TST/C/209, Issue. 01, ) Carbon Dioxide APHA (22 nd Edition) 4500-CO 2 (SOP No. HTL/WI-TST/C/202, Issue. 01, Dated ) Oil And Grease APHA (22 nd Edition) 5520/ IS 3025 (Part 39) (FTIR): 1991 Amd. 2: mg/l to 500 mg/l 1 mg/l to mg/l 5 mho/cm to mho/cm 10 C to 110 C 10 mg/l to mg/l 2 mg/l to 500 mg/l 1 mg/l to 5000 mg/l

14 Last Amended on Page 14 of 20 II. PLASTIC AND PLASTIC PRODUCTS 1. (Water Filled In PE Pouches, Container, Pet Jar And Bottles Potability Test For Odour IS 3025 (Part 5): 1983 (RA 2002) Potability Test For Taste IS 3025 (Part 8): 1984 (RA 2002) Qualitative (Agreeable/Disagreeable) Qualitative (Agreeable/Disagreeable) 2. (Water Filled In PE Pouches, Container, Pet Jar And Bottles, Caps And Closures Of Containers) Overall Migration IS 9845: mg/l to 100 mg/l 0.1 mg/dm 2 to 100 mg/dm 2 Colour Migration IS 9845: 1998 Qualitative (Visual Observation) III. FOOD AND AGRICULTURAL PRODUCTS 1. Namkeen Moisture IS 15271: 2003 (RA 2009) Amd. 2: July 2009 Annexure B Acid Insoluble Ash IS 15271: 2003 (RA 2009) Amd. 2: July 2009 Annexure C Fat IS 15271: 2003 (RA 2009) Amd. 2: July 2009 Annexure D Acid Value Of Extracted Fat IS 15271: 2003 (RA 2009) Amd. 2: July 2009 Annexure E 2. Biscuits Moisture IS 1011: 2002 (RA 2009) Amd. 1: Feb 2006 Appendix B 0.2 % to 20 % 0.01 % to 1 % 0.5 % to 70 % 0.1 to % to 25 %

15 Last Amended on Page 15 of 20 Biscuits Acid Insoluble Ash IS 1011: 2002 (RA 2009) Amd. 1: Feb 2006 Appendix C Acidity Of Extracted Fat IS 1011: 2002 (RA 2009) Amd. 1: Feb 2006 Appendix D 3. Oils & Fats Moisture & Volatile Matter IS 548 (Part 1): 1964 (RA 2010) Free Fatty Acid IS 548 (Part 1): 1964 (RA 2010) Acid Value IS 548 (Part 1): 1964 (RA 2010) Saponification Value IS 548 (Part 1): 1964 (RA 2010) Unsaponifiable Matter IS 548 (Part 1): 1964 (RA 2010) Reichet Missel Value IS 548 (Part 1): 1964 (RA 2010) Boudin Test IS 548 (Part 1): 1964 (RA 2010) 0.01 % to 1 % 0.2 % to 5 % 0.01 % to 5 % 0.01 % to 15 % 0.02 to 25 5 to % to 20 % 10 to 50 Qualitative (Present/Absent) Belleir Turbidity Temperature Test IS 548 (Part 1): 1964 (RA 2010) 5 C to 50 C Insoluble Impurities IS 548 (Part 1): 1964 (RA 2010) 0.01 % to 20 %

16 Last Amended on Page 16 of 20 Oils & Fats Test For Mineral Oil IS 548 (Part 2): 1976 (RA 2010) Amd. 7: July 1996, Iodine Value IS 548 (Part 1): 1964 (RA 2010) Peroxide Value IS 548 (Part 1): 1964 (RA 2010) Specific Gravity IS 548 (Part 1): 1964 (RA 2010) Refractive Index IS 548 (Part 1): 1964 (RA 2010) Qualitative (Present/Absent) 0.5 to meq/ kg to 20 meq/ kg 0.5 g/ml to 1.3 g/ml 1.3 to Iodized Salt / Refined Iodized Salt /Common Salt/ Iron Fortified Salt Moisture IS 7224: 2006 / IS 253 Annexure A Water Insoluble Matter IS 7224: 2006, Amd. 1: Jan 2009 Annexure C / IS 253 (RA 2009), Amd. 1: June 2006 Chlorine Content (As Nacl %) IS 7224: 2006 Amd. 1: Jan 2009 Annexure D / IS 253 (RA 2009), Amd. 1: June % to 5 % 0.1 % to 5 % 0.5 % to 100 % Matter Soluble In Water Other Than Nacl IS 7224: 2006, Amd. 1: Jan 2009 Annexure E,/ IS 253 (RA 2009), Amd. 1: June % to 5 %

17 Last Amended on Page 17 of 20 Iodized Salt / Refined Iodized Salt /Common Salt/ Iron Fortified Salt Ca % IS 7224: 2006, Amd. 1: Jan 2009 Annexure F Mg % IS 7224: 2006, Amd. 1: Jan 2009 Annexure F Sulphate % IS 7224: 2006, Amd. 1: Jan 2009 Annexure G 0.01 % to 2 % 0.01 % to 2 % 0.01 % to 2 % 5. Honey Optical Density At 660 Nm IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure H Specific Gravity IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure A Ash IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure D Refractive Index IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure B Colour IS 4941: 1994 (RA 2002), Amd. 1: April 2011 Acidity As Formic Acid IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure E Moisture IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure B 0.01 % to to % to 20 % 1.3 to 1.7 Visual Observation 0.01 % to 10 % 0.1 % to 75 %

18 Last Amended on Page 18 of 20 Honey Reducing Sugar % IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure C Total Reducing Sugar % IS 4941: 1994 (RA 2002), Amd. 1: April 2011, Annexure C 6. Tea, Coffee Moisture IS 13853: 1994 (RA 1999)/ IS 3077: 1992 (RA 1998), Annexure E Total Ash IS 3077: 1992 (RA 1998), Annexure F / IS :1994 (RA 1999) Acid Insoluble Ash IS :1993 (RA 1998) / IS 3077: 1992 (RA 1998), Annexure G Water Soluble Ash IS 3077: 1992 (RA 1998), Annexure H / IS : 1993 (RA 1998) Alkalinity Of Water Soluble Ash IS : 1993 (RA 1998)/ IS 3077: 1992 (RA 1998), Annexure J Water Extract IS 3077: 1992 (RA 1998), Annexure K / IS 13862: 1999 Petroleum Ether Extract IS 3077: 1992 (RA 1998), Annexure M 0.1 % to 90 % 0.1 % to 95 % 0.01 % to 30 % 0.01 % to 20 % 0.01 % to 5 % 0.01 % to 20 % 10 % to 80 % 0.1 % to 10 % 1 % to 80 % 0.1 % to 20 %

19 Last Amended on Page 19 of Spices And Condiments (Turmeric, Cumin, Ginger And Mix Masala) Moisture & Volatile Matter IS 5453 (Part 2): 1996 (RA 2012) Alcohol Soluble Extract IS 1797: 1985 (RA 2009) Amd. 2: Nov Cold Water Soluble Extract IS 1797: 1985 (RA 2009) Amd. 2: Nov Total Ash IS 1797: 1985 (RA 2009) Amd. 2: Nov Acid Insoluble Ash IS 1797: 1985 (RA 2009) Amd. 2: Nov % to 30 % 0.1 % to 50 % 0.1 % to 50 % 0.1 % to 10 % 0.01 % to 10 % Curcumine Content IS 10925: 1984 (RA 2012) 0.1 % to 10 % Lead Chromate IS 3576: 2010 Annexure A Qualitative (Present/Absent) 8. Heavy Metal Analysis In Food And Food Products (Turmeric, Cumin, Ginger And Mix Masala, Namkeen, Biscuits, Tea, Coffee Non Volatile Ether Extract IS 1797: 1985 (RA 2009) Amd. 2: Nov Lead DGHS Lab Manual 9, Sec. 2 /AOAC (19 th Edition) Cadmium DGHS Lab Manual 9, Sec. 2 /AOAC (19 th Edition) Copper DGHS Lab Manual 9, Sec. 2 /AOAC (19 th Edition) % to 10 % 0.1 µg/g to 1000 µg/g 0.1 µg/g to 1000 µg/g 0.1 µg/g to 1000 µg/g

20 Last Amended on Page 20 of 20 Heavy Metal Analysis In Food And Food Products (Turmeric, Cumin, Ginger And Mix Masala, Namkeen, Biscuits, Tea, Coffee 9. Nutritional Information Of Food Products Namkeen, Biscuits Zinc DGHS Lab Manual 9, Sec. 2 /AOAC (19 th Edition) Iron DGHS Lab Manual 9, Sec. 2 /AOAC (19 th Edition) Energy Value UNFAO, Food Energy Method of analysis and conversion factor, Paper 77 Fat % IS 15271: 2003 (RA 2009) Amd. 2: July 2009 Annexure D, IS 1011: 2002 (RA 2009), Amd. 1, µg/g to 1000 µg/g 01 µg/g to 1000 µg/g 20 kcal to 2000 kcal 0.5 % to 70 % Carbohydrate % UNFAO Method, Chapter % to 100 % Protein % IS 7219: 1973 (RA 2005) 0.1 % to 40 % Sugar % DGHS Lab Manual 5, Sec % to 40 % -X-X-X-X-X-X-X-X-X-X-X-X-X-X- NOTE: The Laboratory has demonstrated competence for the stated scope for WATER. This however does not fully cover the specification requirements of BIS for the Packaged Drinking Water as per IS:14543 and the Packaged Natural Mineral Water IS:13428.