ANAMA Package & Container Testing Services, Inc.

Transcription

1 ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY Tel: (914) Fax: (914) DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING CERTIFICATION Page 1 of 34 Testing Performed by: ANAMA Package & Container Testing Services, Inc. (+CM) Approval 607 Fayette Avenue Mamaroneck, NY (914) Testing Performed for: County Road 1000 Godley, TX Mr. Matt Holzer (817) matt.holzer@corelab.com 4G Design Qualification Testing 350# DW Fibrebord Box With: Iteration 1: Grams Average Gross Weight Barrier Bags (JEC) Iteration 2: Grams & Kg Average Gross Weight Articles (CUT NT) u n 4G / Y 5.7 / S / ** USA / +CM0472 ** insert year the packaging is manufactured Anton Cotaj, Certification Officer

2 ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY Tel:(914) Fax: (914) SECTION 1 - CERTIFICATION Page 2 of 34 4G Design Qualification Testing of the, Godley, TX 350# DW Fibrebord Box With: Iteration 1: Grams Average Gross Weight Barrier Bags (JEC) Iteration 2: Grams & Kg Average Gross Weight Articles (CUT NT) Requesting Party: Tel: (817) County Road 1000, PO Box matt.holzer@corelab.com Godley, TX Attn: Mr. Matt Holzer ANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under and certifies that the, Godley, TX packaging prepared as for transport, referenced above and tested in September & October 2017 has passed the Standards of the US Department of Transportation, Title 49CFR, Performance Oriented Packaging Standards; Section 178. This package is also certified under IMDG and UN Recommendations of the Committee of Experts on the Transportation of Dangerous Goods. It is the responsibility of the shipper / end user to ensure appropriate use. The use of other packaging methods or components other than those documented in this report may render this report invalid. SUMMARY OF PERFORMANCE TESTS Test Specification Test Level Time Results Drop 49 CFR m N/A Pass Stacking 49 CFR kg 24 Hours Pass Cobb 49 CFR gr/m² 30 Minutes Pass Vibration 49 CFR CPM 60 Minutes Pass Test Report #0472 UN Marking (49 CFR ) 4G / Y 5.7 / S / ** USA / +CM0472 Package Identification Code 4G - Fibreboard Box (49 CFR ) Performance Standard Y - Packaging meets Packing Group II and III Tests Authorized Gross Mass 5.7 kg (12.54 lbs) "S" Designation Denotes Inner Packaging Year of Manufacture ** Insert year the packaging is manufactured Country Authorizing The Mark USA DOT UN Third-Party Certification Agency (+CM) ANAMA Package & Container Testing Services, Inc. Approval Third Party Packaging Identification Number +CM0472 Anton Cotaj, Certification Officer

3 Page 3 of 34 SECTION 2 - Description of The Tested Package Iteration 1 (Box JEC): Ten (10) 317 grams average gross solid product filled metal-in film laminate bags, inner packagings installed sideways 2 layers high within the center special slotted fibreboard container (International Box Code 0204) outer packaging backfilled with bubble sheets void space fillers and honeycomb top and bottom pads. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #1-1 (ESD Shielding Bag) Reference Section 8 for drawings Type Metal-in Film Laminate Bag Count 10 Style/Description Lead free RoHs Compliant, Stat Shielding bag with heat-sealed bottom and sides Type RoHs Compliant 0217/617 Desco Part # Owen Part # BAG-0715-F100 7 X 15 Foil Bag Manufacturer Desco Industries, Chino, CA Supplier Global Industrial, Item #T97B Material of Construction Metal-in film laminate, 3 Mil nominal gauge Minimum Thickness mm Nominal Thickness mm Dimension (mm, OD), W X L, flat 197 x 375 Dimension (mm, ID), W X L, flat 175 x 327 Side Seam Width, mm 9.9 mm Top Seam Width, mm 4.2 mm, 40 mm away from top edge Tare Weight 11.3 grams Average Gross Weight (as tested) 317 grams Print EMI/STATIC SHIELD Test material was inserted into bag. Air was expelled from bag, then bag was Method of Closure heat-sealed. Each bag contains 1 sand filled steel tube with plastic caps and 2 Desiccant bags. PRODUCT/ARTICLES - TEST MATERIAL DETAIL #1-1-1 Reference Section 8 for drawings Type Metal cylinder with plastic plugs Count 10 Style/Description Machined metal halo cylinder Material of Construction Steel Manufacturer Owen Oil Tools, Godley, TX Nominal Thickness 1.17 mm Dimension (mm, OD) 25.6 x Dimension (mm, ID) 23.0 x Average Tare Weight grams Average Gross Weight grams Plastic Plugs Count 2 Material of Construction Red plastic Manufacturer/Supplier Caplugs, Inc., Buffalo, NY Nominal Thickness 0.98 mm Dimension (mm, OD) 25.2 x 24.6 Tare Weight 2.2 grams each Test Material Sand Note These articles were inserted individually within the barrier bags

4 Page 4 of 34 INNER PACKAGING DETAIL # Reference Section 8 for drawings Desiccant Bag Count 40 Manufacturer Desiccare, Inc., Reno, NV Material Silica Gel, Indicating Silica Gel, Clay, Molecular Sieve and Carbon Owen Part # PAK Dimension (mm, OD), D X H 59.6 x 11.5 x 88.7 Weight 22.2 grams each Notes 2 desiccant bags were placed inside each barrier bag plus 20 bags were loose over the closed bags PRODUCT/ARTICLES ADDITIONAL WEIGHT TEST MATERIAL DETAIL #1-2 Type Metal Blocks Count 8 Style/Description Solid steel block 3 X 76 x 76 x 3.35, 141 grams each Dimension (mm, OD), D X H 1 X 76 x 76 x 9.4, 434 grams 20 X 46.5 x 43.6 x 1.6, 413 grams all Overall Gross Weight 9.41 kg Note These steel blocks and cylinders were placed on both sides and over the barrier bags (to reach the desired weight) Overall Inner Packaging Gross Weight (OIP1GW) 5.02 kg

5 Page 5 of 34 Iteration 2 (Box CUT NT): Eight (8) grams average gross weight each solid product filled foil/plastic laminate bags each folded and placed into 4 smaller & 3 larger spiral wound fiberboard tube rings primary inner packagings and one (1) 3.33 kg gross weight casing cutter assembly secondary inner packaging, all installed within a center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard top and bottom pads and fibreboard/honeycomb side fillers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #2-1 (Barrier Bag) Reference Section 8 for drawings Type Barrier Bag Count 8 Style/Description Laminated watervaporproof, greaseproof, flexible barrier bag with heat-sealed bottom and sides Part # 4.5 X 5 Foil Bag Type MIL-PRF-131K, Type 1, Class 1, Style 1 Manufacturer Ludlow Coated Products, Inc., Columbus, GA Supplier East Texas Seals, LLC, Dallas, TX Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S Owen Part # BAG-0305-F100 3 X 5 Foil Bag Material of Construction Plastic/foil/plastic laminate, 5 Mil nominal gauge Minimum Thickness mm (0.0045") Nominal Thickness mm (0.005") Bursting Strength 65 lbs/inch² Dimension (mm, OD), W X L, flat 5 X 105 x 138 & 3 X 105 x 205 Dimension (mm, ID), W X L, flat 5 X 85 x 122 & 3 X 85 x 182 Bottom Seam Width, mm 18.0 mm Side Seam Width, mm 8.5 mm Tare Weight 5 X 4.4 grams & 3 X 5.6 grams Average Gross Weight (as tested) grams Average Net Weight (as tested) grams Print INNERT Each bag was filled with solid product (putty). Top of bags was left open to Method of Closure place the putty, bag was then folded and placed individually in the center of each fibreboard tube ring (Refer to Section 7.2) INNERT TEST MATERIAL Count 8 Description White putty material Average Net Weight (as tested) grams Notes This material was placed inside each barrier bag

6 Page 6 of 34 INNER PACKAGING DETAIL #2-2 - Reference Section 8 for drawings Small Fiberboard Tube Rings Count (per outer packaging) 4 Style Spiral wound fiberboard Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN2.80 X 1.25 Owen Part # TUBE Material 26 Plies of High Density Paperboard Laminated with PVOH Adhesive Size (mm, OD) 97.7 x 31.2 Size (mm, ID) 70.5 x 31.2 Caliper 13.6 mm Tare Weight 76.4 grams each Notes Placed on each corner on top layer INNER PACKAGING DETAIL #2-3 - Reference Section 8 for drawings Large Fiberboard Tube Rings Count (per outer packaging) 2 Style Spiral wound fiberboard Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN3.45 X 1.25 Owen Part # TUBE Material 26 Plies of High Density Paperboard Laminated with PVOH Adhesive Size (mm, OD) x 31.2 Size (mm, ID) 87.3 x 31.2 Caliper 14.4 mm Tare Weight 98.2 grams each Notes These tubes were placed in the center between smaller tubes on top layer

7 Page 7 of 34 INNER PACKAGING DETAIL #2-4 Reference Section 8 for drawings Type Large Casing Cutter Count 1 Style/Description Machined steel cylindrical shape with steel cover Manufacturer Owen Oil Tools, Godley, TX Nominal Thickness 1.35 mm Dimension (mm, OD) 96.8 x 83.8 (without lid and plastic detail on the bottom) Dimension (mm, OD) x 85.8 (with lid and plastic detail on the bottom) Print/Label CUT RO; Gross Weight (as tested) 3.33 kg Lid Dimension (mm, OD) 88.3 x 38.8 Gross Weight (as tested) 909 grams Lid Screws Count 4 Style Allen screws Dimension (mm, OD) 7.8 x 17.0 Weight 2.7 grams each Note This article was placed on the bottom of shipper Overall Inner Packaging Gross Weight (OIP2GW) 4.55 kg

8 Page 8 of 34 OUTER PACKAGING - UN 4G (Reference Section 8 for drawings) Type Fiberboard Box Style Center Special Slotted Container (CSSC), FEDCO Style: 0204 Manufacturer/Supplier All Star Corrugated, Fort Worth TX Part # R&S-350 BC Spec. # Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA Dimension (mm, OD), L X W X H 305 x 305 x 190 Dimension (mm, ID), L X W X H 296 x 296 x 178 Stacking Height (mm) 190 Number of Walls - Flute Type Double-Wall BC-Flute Tare Weight 560 grams BMC (Box Marked Certification) 350# ( ) Tested Basis Weight (lbs/1000ft²) ( ) JEC ( ) CUT Tested Burst Strength (lbs/inch²) Minimum Tested Caliper 6.96 mm Method of Joining Panels Stitched with at least five (5) 12.5 mm wide staples Mfr's Joint Flap Size 35 mm Mfr's Joint Location 5-2 corner as per the ASTM diagram Top Flap Gap/Meet Inner: Meet Outer: Meet Bottom Flap Gap/Meet Inner: Meet Outer: Meet Print None Closure Method (Refer to Section 7 for Closing Instruction and Section 8 for Specs) Closure 3/4" C34 Stick Staples Description 18 mm (3/4") long, 31 mm (1-1/4") crown galvanized metal staples Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S-1396 Owen Part # STA S Four (4) staples along the flap seam, 38 mm (1-1/2") away from boxes outside Top Closure edges, 63.5 mm (2-1/2") apart on both sides & 100 mm (4") apart on center, 0.8 grams each Four (4) staples along the flap seam, 38 mm (1-1/2") away from boxes outside Bottom Closure edges, 63.5 mm (2-1/2") apart on both sides & 100 mm (4") apart on center, 0.8 grams each Method of Closure See Section 7.2

9 Page 9 of 34 OUTER PACKAGING DETAIL #1 - Reference Section 8 for drawings Plain Corrugated Pad Count Iteration 1: 0 Iteration 2: 7 Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Corrugate Manufacturer/Supplier All Star Corrugated, Fort Worth TX Part # Spec. # Size (mm, OD) 278 x 278 Caliper 6.78 mm Weight 80.9 grams each Pad Location Iteration 2: 1 pad is placed on top, 4 pads between the layers and 2 pads are placed on bottom OUTER PACKAGING DETAIL #2 - Reference Section 8 for drawings Large Honeycomb Pad Count Iteration 1: 3 Iteration 2: 0 Material Hexacomb Core Type 4 35# facing Manufacturer/Supplier Pregis Hexacomb Corporation Supplier All Star Corrugated, Fort Worth TX Part # 2 X 11 HEX Spec. # H Owen Part # PAD-HEX-100 Size (mm, OD) 285 x 280 Caliper 25.4 mm Weight 35.1 grams each Pad Location Iteration 1: 1 over and 2 bellow Metal-in Film Laminate Bags OUTER PACKAGING DETAIL #3 - Reference Section 8 for drawings Small Honeycomb Filler Count Iteration 1: 0 Iteration 2: 10 Material Hexacomb Core Type 4 35# facing Manufacturer/Supplier Pregis Hexacomb Corporation Supplier All Star Corrugated, Fort Worth TX Spec # H Owen Part # PAD-HEX-1X2 Size (mm, OD) 52 x 280 Caliper 25.4 mm Weight 13.4 grams each Pad Location Iteration 2: These honeycomb fillers were placed around the cutter casing

10 Page 10 of 34 OUTER PACKAGING DETAIL # Reference Section 8 for drawings Bubble Sheet Count Iteration 1: 1 Iteration 2: 0 Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Owen Part # WRAP Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16") Dimension (mm, OD) flat 305 x 1820 Tare Weight 23 grams Sheet Location Iteration 1: These bubble sheet were placed over and around the Metal-in Film Laminate Bags Overall Outer Package Tare Weight (OPTW) Iteration 1: grams Iteration 2: grams

11 Page 11 of 34 SECTION 3 - Test Description and Test Results Drop Test 49 CFR Test Specimen/Contents Characteristics Number of Packages Tested 10 (5 per iteration) Packing Group Number PG II State Solid Dummy Load (Solid) Steel disks or blocks Drop Height Multiplier 0.67 for PG III; 1 for PG II & 1.5 for PG I Drop Height 1.2 m Conditioning Temperature & Duration, 49 CFR (c) F & 50 % R.H. Content (Dummy Load) Test Temperature 73 F Drop Test Method: The inner packagings were filled to 98% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 7). Ten (10) assembled packages, 5 packages for each iteration, were subjected to a free fall drop test from a height of 1.2 meters onto a solid steel plated concrete floor as described below. Drops were conducted within 60 seconds of removal of the outer packagings from the conditioning chamber. Drop Test Results Iteration 1 Test Sample # Weight (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 2" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance

12 Page 12 of 34 Drop Test Results Iteration 2 Sample Test Weight # (kg) # Orientation Top (mfr's) corner (Corner 1-2-5) # Top surface (Face 1) # Long side (Face 2) # Short side (Face 6) # Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 2" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance Pass/Fail Criteria - A package is considered to successfully pass the drop tests if for each sample tested: For packaging containing liquid, there is no leakage of the filling substance from the inner packaging. There is no damage to the outer packaging likely to adversely affect safety during transport. Inner receptacles, inner packagings or articles must remain completely within the outer packaging. Any discharge from a closure is slight and ceases immediately after impact or pressure equalization with no further leakage. No rupture is permitted in packagings for materials in Class 1 which would permit spillage of loose explosive substances or articles from the outer packaging.

13 Page 13 of 34 Stacking Test - 49 CFR (See Section 5.2 for Calculation) Test Specimen/Contents Characteristics Number of Packages Tested Product State Dummy Load (Solid) Conditioning of Outer Packaging - 49 CFR (d) Test Temperature Test Method Test Duration Minimum calculated stacking test weight Actual stacking test weight Test Duration 10 (5 per iteration) Solid Steel disks or blocks F & 50 % R.H. 73 F & 50 % R.H. Free standing, static (dead weight) test 24 hours 85.5 kg (188.1 lbs) per package kg (225 lbs) per package 24 hours Stacking Test Method: The inner packagings were filled to 98% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 7). Stacking test load (dead weight) of kg was applied individually to the top of the three (3) assembled packages for each iteration using wood load spreaders and the weight was maintained for 24 hours. Stacking Test Results - Iteration 1 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance Stacking Test Results - Iteration 2 Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results # Hours # Hours # Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance Pass/Fail Criteria - A package is considered to successfully pass the stack tests if for each sample tested: No test sample shows any deterioration or distortion that could adversely affect safety during transport causing instability in stacks of packages, or cause damage to inner packagings that is likely to reduce safety in transport. There no leakage of the filling substance from the inner receptacle, or inner packaging

14 Page 14 of 34 Vibration Test - 49 CFR Test Specimen/Contents Characteristics Number of Packages Tested Product State Dummy Load (Solid) Conditioning of Outer Packaging - 49 CFR (d) Test Temperature Test Method Test Duration Test Frequency 10 (3 simultaneously, 3 per iteration) same samples used for stacking test Solid Steel disks or blocks F & 50 % R.H. Ambient ASTM D Rotary Motion Vibration 60 minutes 235 CPM Vibration Test Method: The inner packagings were filled to 98% overflow capacity with dummy load. The packages were re-assembled as per closing instruction (Reference Section 7). Three (3) assembled packages, for each iteration were simultaneously placed on a rotary vibration table platform having 25.4 mm peak-to-peak displacement and vibrated in normal shipping orientation for one (1) hour at 235 CPM such that a 1.6 mm thickness could be passed between the bottom of the samples and the platform. Immediately thereafter, the packages were removed from the platform and turned on its side for examination. Vibration Test Results - Iteration 1 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance Vibration Test Results - Iteration 2 Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results # # # There was no rupture or deterioration of boxes, there was no leakage of the filling substance

15 Page 15 of 34 Pass/Fail Criteria - A package is considered to successfully pass the vibration test, if for each sample tested after it was immediately removed from table platform and turned on its side: There is no leakage or rupture from any of the packaging. No test sample shows any deterioration which could adversely affect safety or container strength, during transport liable to reduce packaging strength. Cobb (Water Absorption) Test - 49 CFR [ISO International Standard (E)] Test Specimen/Contents Characteristics Number of Samples Tested 5 Test Duration 30 Minutes Test Intensity 100 ml Distilled Water Conditioning of Test Samples F & 50 % R.H. Test Method ISO 535, Cobb Method Cobb Test Results Sample # #1 #2 #3 #4 #5 Average Results grams/m² Pass Pass/Fail Criteria An increase in mass of greater than 155 grams/m² over the 30 minute duration of the tests represents an unacceptable level of water absorption. SECTION 4 - Shippers Responsibility It is the responsibility of the end shipper to determine authorization for use under these regulations. It is the shippers responsibility to determine if the packaging is compatible for products to be shipped. Use of the marking of this certification for any variations without further testing as allowed under US DOT 49 CFR Section will be at complete responsibility of the shipper. By continuing to place the UN Markings on Packagings, the packaging manufacturer or shipper is certifying that each packaging is constructed in the same manner as the originally tested and certified packaging, and that each packaging is capable of withstanding the prescribed performance tests. According to 49 CFR Section (1) Variation 1 - variations are permitted in inner packaging of a tested combination packaging without further testing of the package, provided an equivalent level of performance is maintained as described in (1) Variation 4 (i),(a),(b),(c),(d),(e) and (F) and (ii). According to US DOT 49 CFR Section (e), the packaging manufacturer shall achieve successful test results for the periodic retesting at intervals established by the manufacturer of sufficient frequency to ensure that each packaging produced by manufacturer is capable of passing the design qualification test. Changes in retest frequency are subject to the approval of the Associate Administrator for Hazardous Materials Safety. For combination packaging, the periodic retest must be conducted at least once every 24 months.

16 Page 16 of 34 SECTION 5 - Calculations 5.1 Certified Package Gross Mass Calculations Based on Test Level Overall Inner Package Gross Weight (OIPGW) Iteration 1: 5.02 kg Iteration 2: 4.55 kg Overall Outer Package Tare Weight (OPTW) Iteration 1: 695 grams Iteration 2: grams Test Material Specific Gravity (TMSG) - Packing Group Number II Minimum Package Weight as Tested (PGW) Iteration 1: 5.72 kg Iteration 2: 5.81 kg Packing Group Multiplication Factor (PMF) 1.0 Formula for Calculating Certified Gross Mass (CGW) Certified Package Marking CGW = Minimum PGW CGW = Minimum PGW = 5.72 kg CGW = 5.7 kg (12.54 lbs) Y = 5.7 (12.54 lbs) 5.2 Stacking Strength Test Calculations Test Load (TL) Overall Stacking Height of Packages (SH) Overall Stacking Height of Package (PH) TL (Static) TL = [(SH - PH) - 1] x CGW (static) TL = [(SH - PH) - 1] x CGW x 1.5 (dynamic) 3000 mm (10 feet) 190 mm TL = [(3000/190) - 1] x 5.7 = 15 (rounded up) x 5.7 TL = 85.5 kg (188.1 lbs) Rounded up to at kg (225 lbs) per package for test purposes

17 Page 17 of 34 Regulatory Standard References: Test Appendix A Regulatory & Industry Standard References CFR UN Regulation IMDG ICAO IATA Drop Test Stacking Test Hydrostatic Pressure (c) Cobb Test Vibration Test United States Code of Federal Regulations (CFR), Title 49, Transportation, Parts The United Nations Recommendations on The Transport of Dangerous Goods Model Regulations (Orange Book) 3. International Maritime Dangerous Goods Code (IMDG) 4. Technical Instructions for the Safe Transport of Dangerous Goods by Air (ICAO) 5. International Air Transport Association (IATA), Dangerous Goods Regulations Industry Standard References: Drop Test ASTM D5276 Standard Test Method for Drop Test of Loaded Containers by Free Fall Stacking Test ASTM D4577 Standard Test Method for Compression Resistance of a Container Under Constant Load Hydrostatic Standard Guide for Conducting Internal Pressure Tests on United Nations ASTM D7660 Pressure (UN) Packagings Cobb Test ISO 535 Paper and Board Determination of Water Absorption Cobb Method Vibration Test ASTM D999 Standard Test Method for Vibration Testing of Shipping Containers American Society for Testing and Materials (ASTM) International Organization for Standardization (ISO)

18 Page 18 of 34 Appendix B Test Equipment & Instrumentation No. Test Machine, Model # and Serial # Capacity Calibration Date Re-Calibration Date 1. Drop Table, Lansmont Corporation: Model #PDT-56-ED; Serial #M " 72" 2/27/2017 2/27/ Drop Table, Gaynes Eng. Inc., Serial #G " 120" 2/27/2017 2/27/ Vibration Table, Gaynes Eng. Inc.: Model #6000V 3000 lbs 2/27/2017 2/27/ Compression Machine, TechLab Systems: Model #Validator; S/N # T lbs 2/27/2017 2/27/ Digital Thermometer, Mannix: Model #DT721 (for Conditioning, Freezer), F 2/23/2017 2/23/ Paperless Temperature & Humidity Recorder, Dickson: Model #TH660 (for Cold Chamber) F 2/23/2017 2/23/ Paperless Temperature & Humidity Recorder, F, Dickson: Model #TH635 (for Hot Chamber) 0% 95% RH 2/23/2017 2/23/ Thermometer & Hygrometer, F, Omega Engineering: Model #RH520 10% 95% RH (for Conditioning Room) 2/23/2017 2/23/ Bench Scale, SeiKo Scale Division: Model #WA200001XP; S/N# mg 20 kg 5/16/2017 5/16/ Bench Scale, Mettler Toledo: Model #ICS4x9-1; S/N# mg 30 kg 5/16/2017 5/16/ Analytical Balance, PCA, Germany: Model #AB200; S/N # mg 200 g 5/16/2017 5/16/ Bench Scale, Ohaus: Serial # XZ lbm 5/16/2017 5/16/ Caliper, General Tools & Instruments: Model # , S/N: 81PCS " 5/16/2017 5/16/ Caliper, Fowler: Model # " 5/16/2017 5/16/ Electronic Torque-Meter, Kaps-All: Model #EB-650; S/N # inch-lbs 12/19/ /19/ Toque Wrench, CDI, Model No. 301LDIN 0 30 inch-lbs 5/17/2017 5/17/ General Purpose Digital Pressure Gauge, Omega Engineering: Model #DPG psi 5/15/2017 5/15/ General Purpose Digital Pressure Gauge, Omega Engineering: Model #DPG V psi 5/15/2017 5/15/ Winters Pressure Gauge, WG psi 5/15/2017 5/15/ Ashcrof Pressure Gauge, V/300 Psi Part # ; S/N: The Mullen Tester, B.F Perkins and Son: Serial # ECT Tester, Testing Machines, Inc.: S/N 5852X Measuring Tape, Ultra-Touch: ANAMA TM1 & TM2 Measuring Tape, Stanley Power Lock, ; ANAMA TM3 Measuring Tape, Made In China; ANAMA TM4 Presto Dart Impact Tester, Model No. PCN-230; S/N: psi 10/21/ /21/ psi 5/18/2017 5/18/ lbs 5/18/2017 5/18/ Feet 5/16/2017 5/16/ Feet 5/16/2017 5/16/ Feet 5/16/2017 5/16/ " 1.7 feet 2/28/2017 2/28/2018

19 Page 19 of 34 SECTION 6 Inner & Outer Packaging Photographs Primary Inner Packaging Components Iteration 1

20 Page 20 of 34 Primary Inner Packaging Details - Iteration 2

21 Page 21 of 34 Outer Packaging Components

22 Page 22 of 34 SECTION 7 - Packaging Assembly (Closing) Instruction) Note: Packages were re-assembled same way as received. Step-by-Step Packaging Assembly Demonstration - Iteration 1

23 Page 23 of 34 Step-by-Step Packaging Assembly Demonstration - Iteration 2

24 Page 24 of 34 Manufacturer s Closing Instructions: Iteration 1:

25 Page 25 of 34 Iteration 2:

26 Page 26 of 34 SECTION 8 - Package Specifications & Drawings Barrier Bag Specifications Iteration 2

27 Page 27 of 34 Small Fibreboard Tube Drawings Iteration 2

28 Page 28 of 34 Large Fibreboard Tube Drawings Iteration 2

29 Page 29 of 34 Desiccant Bag

30 Page 30 of 34 Outer Box Drawing & Specifications

31 Page 31 of 34 DW Corrugated Pad Drawing & Specifications

32 Page 32 of 34 Honeycomb Pad Drawing & Specification

33 Page 33 of 34 Anti-Static Sheet Specifications

34 Page 34 of 34 Carton Sealing Staples Specification