CONTENTS. Brass plating solutions. Bronze plating solutions

Transcription

1 CONTENTS \c A Volumetric - Complexometric Methods A1 Antimony plating solutions A1 1 Determination of antimony using potassium permanganate A1 2 Determination of antimony using potassium bromate A1 3 Determination of free acid Brass plating solutions Determination of copper Determination of copper and zinc Determination of free sodium cyanide Determination of sodium carbonate Determination of sodium hydroxide - method 1 Determination of sodium hydroxide - method 2 Determination of sodium carbonate and sodium hydroxide Determination of sodi~rm sulphite Bronze plating solutions Determination of copper and tin Determination of copper Determination of sodium cyanide Determination of free sodium hydroxide Determination of carbonate Cadmium plating solutions Electrolytic determination of cadmium Determination of cadmium using ferrocyanide Complexometric determination of cadmium - method 1 Complexometric determination of cadmium - method 2 Complexometric determination of cadmium - method 3 Determination of free sodiurrl cyanide Determination of total sodium cyanide - method 1 Determination of total cyanide - method 2 Determination of sodium carbonate Determination of sodium hydroxide and sodium carbonate - method Determination of sodium hydroxide and sodium carbonate - method

2 A5 Chromium plating solutions Determination of chromium trioxide Determination of trivalent chromium - ~nethod 1 Determination of trivalent chromium - method 2 Gravimetric determination of sulphate Complexometric determination of sulphate lodometric determination of sulphate Determination of iron - niethod 1 Determination of iron - method 2 Determination of copper - method 1 Determination of copper - method 2 Determination of nickel Determination of chloride Complexometric determination of copper, nickel and zinc Complexometric determination of fluoride Determination of fluoride Determination of fluorides A6 Cobalt plating solutions A6 1 Complexometric determination of cobalt method 1 A6 2 Complexometric determination of cobalt - method 2 A6 3 Complexometric determina'tion of cobalt - method 3 A6 4 Determination of chloride A6 5 Determination of boric acid A7 Copper plating solutions (acid) A7 1 Electrolytic determination of copper A7 2 Volumetric determination of copper A7 3 Determination of free sulphuric acid A7 4 Gravimetric determination of chloride A7 5 Cornplexometric determination of chloride A7 6 Determination of iron A8 Copper plating solutions (cyanide) A8 1 Electrolytic determination of copper A8 2 Volumetric determination of copper A8 3 Complexometric deterqination of copper - methcd 1

3 Complexometric determination of copper - method 2 Determination of cyanide content Determination of total cyanide content Determination of carbonate - method 1 Determination of carbonate - method 2 Determination of hydroxide content Determination of the sulphite ion Determination of cyanide Com~lexometric determination of zinc Cornplexometric determination of iron Complexometric determination of Rochelle salt Determination of tensides Determination of thiocyanate A9 Copper fluoborate plating solutions A9 1 Determination of copper A9 2 Determination of free fluoboric acid A1 0 Copper pyrophosphate plating solutions A10 1 Complexometr~c determination of copper A10 2 Determination of total hydrofluoric acid A1 1 All 1 All 2 All 3 A11 4 A11 5 All 6 All 7 All 8 All 9 All 10 All 11 All 12 All 13 Degreasing solutions Determination of sodium hydroxide Determination of sodium carbonate Determination of sodium metasi licate Determination of trisodium phosphate Determination of sodium or potassium cyanide Determination of sodium carbonate, sodi um hydroxide and sodium phosphate Determination of sodium hydroxide and sodium phosphate Determination of sodium phosphate, sodium silicate and sodium cyanide Determination of sodium cyanide and sodium hydroxide Determination of sodium carbonate and sodium cyanide Determination of sodium phosphate and sodium carbonate Determination of chloride ion Determination of sodium cyanate

4 A1 2 Gold plating solutions Electrolytic determination of gold Determination of gold Gravimetric determination of gold Titrimetric determination of gold using iodine Complexometric determination of gold Determination of silver Determination of copper and nickel - method 1 Determination of copper and nickel - method 2 Determination of free sodium cyanide using silver nitrate Determination of free sodium cyanide using nickel sulphate Determination of sodium carbonate Determination of chloride A1 3 Iron plating solutions A13 1 Complexometric determination of iron A13 2 Oxydimetric determination of iron A13 3 Determination of manganese A13 4 Determination of manganese after separation of iron A13 5 Determination of ammonium salts A13 6 Determination of chloride A13 7 Determination of free hydrochloric acid A1 4 Lead and Tin-Lead plating solutions A14 1 Complexonletric determination of lead - method 1 A14 2 Complexometric determination of lead -method 2 A14 3 Determination of lead using sodium dichromate A14 4 Determination of lead using potassium dichrpate A14 5 Determination of tin in tin-lead plating solutions A14 6 Determination of fcee acid A1 5 Nickel plating solutions A15 1 Electrolytic determination of nickel A15 2 Complexometric determination of nickel A15 3 Determination of nickel using sodium cyanide A15 4 Determination of chloride content - method 1 A15 5 Determination of chloride content - method 2 A15 6 Determination of boric acid -method 1

5 Determination of boric acid - method 2 Determination of saccharine Determi nation of ptol uene su l phonamide Determination of sodium formate Determination of formaldehyde content Determination of iron content Complexometric determination of iron Determination of ammonia Complexometric determi nation of copper Complexometric determination of cobalt and nickel Complexometric determination of zinc concentration below 2 g/l Complexometric determination of lead Determination of magnesium Determination of sulphur-containing brightening agents Determination of wetting agent Palladium plating solutions Complexometric determination of palladium - method 1 Complexometric determination of palladium - method 2 Complexometric determination of palladium - method 3 Determi nation of chloride Determination of nitrite Determination of ammonia Silver plating solutions Electrolytic determination of silver Determination of silver as silver chloride Titrimetric determination of silver using thiocyanate - method 1 Titrimetric determination of silver using thiocyanate - method 2 Complexometric determination of silver Determination of free cyanide using silver nitrate Determination of free cyanide using nickel sulphate Determination of sodium carbonate - method 1 Determination of sodium carbonate - method 2 Complexometric determination of copper and nickel Complexometric determination of nickel Tin plating solutions (alkaline) lodometric determination of tin Complexometric determination of tin Determination of free sodium hydroxide Determination of sodium carbonate Determination of chloride Determination of tin (IV) Determination of free hydroxide

6 A18 8 Determination of total alkali A1 9 Tin plating solutions (acid) Complexometric determination of total tin Electrolytic determination of tin Determination of tin as metastannic acid lodometric determination of tin(ll) Complexometric determination of tin(ll) Complexometric determi nation of tin Titrimetric determination of tinill) using ferric chloride soln. Determination of the free acid - method 1 Determination of the free acid - method 2 Determination of chloride content A20 Zinc plating solutions (alkaline) Electrolytic determination of zinc Complexometric determination of zinc - method 1 Complexometric determination of zinc - method 2 Complexometric determination of zinc - method 3 in the presence of iron using potassium ferrocyanide Determination of total sodium cyanide Determination of sodium cyanide. Liebig method Determination of sodium hydroxide - method 1 Determination of sodium hydroxide - method 2 Determination of sodium carbonate Complexometric determination of sodium carbonate Determination of iron and aluminium Determination of iron and copper Determination of sodium sulphite A21 Zinc plating solutions (acid) Electrolytic determination of zinc Complexometric determination of zinc - method 1 Complexometric determination of zinc - method 2 Complexometric determination of zinc - method 3 Determination of chloride content Determination of sulphate content Determination of ammonia Determination of fluoboric acid Complexometric determination of iron and aluminium Complexometric determination of iron Determination of boric acid Tables - Section A

7 B Photometric Analysis 81 Antimony plating solutions B1 1 Determination of lead 82 Brass plating solutions P 82 1 Determination of iron 83 Cadmium plating solutions B3 1 Determination of iron 83 2 Determination of titanium B3 3 B3 4 Determination of copper 83 5 Determination of nickel Chromium plating solutions Determination of iron Determination of copper Determination of nickel Determination of selenium Copper plating solutions (acid) Determination of chloride ions Determination of iron Determination of anion-active surfactants Determination of thiocarbamate 86 Copper plating solutions (alkaline),- B6 1 Determination of selenium B6 2 Determination of iron

8 Degreasing solutions Determi nation of sodium metasi licate Determination of tri sodium phosphate Determination of cyanide Determination of chromate Determination of copper Determination of nickel Gold plating solutions Determination of nickel Determination of ind ium Determination of copper Determination of iron Determination of phosphate Determination of cobalt Determination of gold - method 1 Determination of gold - method 2 Determination of gold - method 3 Determination of thallium - method 1 Determination of thaliium - method 2 Iron plating solutions Determination of manganese Determination of ammonia Lead and Tin-Lead plating solutions Determination of lead Bll Bll 811 B11 Bl B1 1 B Nickel plating solutions Determination of chromate Determination of chromium Determination of coumarin Determination of ammonia - method 1 Determination of ammonia - method 2 Determination of copper - method 1 Determination of copper - method 2 Determination of total iron Determination of anion-active surfactants Determination of nitrate content Determination of cobalt Determination of pyridine and pyridine derivatives

9 Palladium plating solutions Determination of palladium - method 1 Determination of palladium - method 2 Determination of palladium - method 3 Determination of palladium - method 4 Determination of palladium - method 5 Determination of nitrite Determination of ammonia Determination of chromium(vl) Determination of total chromium? 813 Silver plating solutions Determination of copper using tetra amine Determination of copper using pyridine thiocyanate Determination of copper using oxaly ldihydrazide Determination of nickel using dimethyl glyoxime Determination of nickel using rubianic acid Determination of antimony Determination of nitrate 81 4 Tin plating solutions (acid) Determination of iron Determination of copper A 815 Tin plating solutions (alkaline) ~etermination of copper Determination of lead Determination of nitrate Analysis of water B16 1 Determination of chromium(vl) Determination of nitrate Determination of nitrite B16 4 Determination of phosphate - B16 5 Determination of cyanide Determinationofchlorine B16 7 Determination of nickel

10 Determination of copper - method 1 Determination of copper - method 2 Determi nation of iron Determination of lead Determination of aluminium Determination of boron Determination of anion-active detergents Determi nation of si licic acid 817 Zinc plating solutions (alkaline) Determination of copper Determination of iron Determination of molybdenum - method Determination of molybdenum - method Determination of sulphide B18 Zinc plating solutions (acid) B1 8 1 Determination of iron - method 1 B18 2 Determination of iron - method 2 B18 3 Determination of iron - method 3 B18 4 Determination of copper Tables - Section B C Polarographic Analysis C1 Antimony plating solutions C1 1 Determination of lead C1 2 Determination of tin C1 3 Determination of copper and zinc C2 Brass plating solutions C2 1 Determination of lead and cadmium

11 -. C3 Cadmium plating solutions C3 1 Determination of copper and lead C3 2 C3 3 Determination of tin C3 4 Determination of titanium C3 5 Determination of nickel C4 Chromium plating solutions C4 1 Determination of strontium C4 2 Determination of potassium r' C4 3 Determination of sulphate C4 4 Determination of chloride C4 5 Determination of copper, nickel and zinc C4 6 Determination of selenium C5 Cobalt platlng solutions C5 1 C5 2 Determination of copper C5 3 Determination of nickel C6 Copper plating solutions (acid) C6 1 Determination of chlorlde F~ C7 Copper plating solutions (alkaline) C7 1 Determinationofzinc C7 2 Determination of lead C7 3 Determination of iron C7 4 Determination of formaldehyde C8 Copper-Ti n plating solutions C8 1 C8 2 Determination of lead

12 C9 Degreasing solutions C9 1 Determination of copper, nickel, zinc and chromate C10 Gold plating solutions C10 1 Determination of copper, nickel and zinc C10 2 Determination of indium C10 3 Determination of nickel C10 4 Determination of cobalt C10 5 Determination of thallium ClO 6 Determination of cadmium C11 Iron plating solutions C11 1 Determination of manganese C12 Lead and Tin-Lead plating solutions C12 1 Determination of copper C12 2 Determination of cadmium, nickel and zinc C13 Nickel plating solutions Determination of copper and lead Determination of chromate Determination of sodium hypophosphate Determination of cadmium Determination of sodium Determination of palladium Determination of pyridine derivatives Determination of cobalt C14 Palladium plating solutions C14 1 Determination of palladium C14 2 Determination of nitrite C14 3 Determination of chromium(lll) C14 4 Determination of chromium(vi)

13 CIS Silver plating solutions C15 1 Determination of antimony C15 2 Determination of copper and nickel C16 Tin platlng solutions (acid) C16 1 Determination of tin(lv) C16 2 Determination of copper, nickel and zinc C17 Tin plating solutions (alkaline) C17 1 Determination of lead C17 2 Determination of cadmium, zinc and copper C18 Water analysis Determination of copper Determination of chromate Determination of chromium(1 ll) Determination of nickel Determination of tin Determi nation of cadmium Determination of palladium and rhodium.-. C19 Zinc plating solutions (acid) C19 1 Determination of copper, iron, lead and cadmium C20 Zinc plating solutions (alkaline) C20 1 Determination of lead and cadmium C20 2 Determination of copper C20 3 Determination of vani IIin C20 4 Determination of copper and tin C20 5 Determinationofmo~lybdenum C20 6 Determination of sulphide ion n Tables - Section C

14 D Potentiometric and other methods D4 Chromium plating solutions D4 1 Potentiometric determination of chromium D4 2 Conductometric determination of sulphate D4 3 Potentiometric determination of chloride Copper plating solutions (acid) Potentiometric determination of chloride Copper plating solutions (alkaline) Potentiometric determination of cyanide Potentiometric determination of alkali and carbonate Degreaslng solutions Potentiometric determination of chloride Determination of degreasing efficiency Gold plating solutions Potentiornetric determination of si lver Potentiometric determination of nickel Simultaneous determination of gold and copper Nickel plating solutions Determination of copper, zinc and cadmium and/or cadmium Determination of cobalt in nickel-cobalt solutions Determination of surface tension Potentiometric determination of boric acid Potentiometric determination of chloride Silver plating solutions Potentiometric determination of silver. Potentiometric determination of antimony Zinc plating solutions Dl9 1 Potentiometric determination of zinc using potassium hexacyanoferrate