Pilot processing line for manufacturing articles from bulk nanostructured ceramics/composites

Transcription

1 Pilot processing line for manufacturing articles from bulk nanostructured ceramics/composites 1. Analysis of nanopowders 2. Compacting of dry nano-, polydisperse powders 3. Analysis of green compacts 4. Sintering 5. Testing of articles XRD-7000S (Shimadzu) TEМ, JEM-2100F (JEOL) SEМ, JSM-7500F (JEOL) BET-analyzer Sorbi (META) Optical microscopes MMN-2 (LOMO) Software: SIAMS PDF-4 NEXSYS Ultrasonic and collector dies Press WK 18 (100 Tf), Press D2430B (100 Tf) Installation for plotting the compaction curves (Mitutoyo ID-F125/150; DM 5001EU, ) Ultrasonic generators UZG 6.3; UZG 3, IL Transducers PMS-15 Solid Works Mercury porosimeter Poremaster 33 (Quantachrome Co.) Ultrapycnometer 1000 (Quantachrome Co.) AFM, SPM Nanolaboratory Ntegra- Aura (NT-MDT) AFM, SPM training equipment NanoEducator (NT-MDT) TEM, JEM-2100F SEM, JSM-7500F XRD-7000S MMN-2 SIAMS PDF-4 NEXSYS Spark Plasma Sintering SPS 515S (Sumitomo) HTK-18 vacuum furnace (Nabertherm) VP 20/17 furnace (LAC) EMITRON furnace TGA/DSC/DTA analyzer SDT Q600 (Netzch) SIAMS PDF-4 NEXSYS Nanohardness meter DUH-2115 (Shimadzu) Microhardess meter PMT-3M (LOMO) Testing machine IP- 500M (ZIPO) JEM-2100F JSM-7500F AFM, Ntegra-Aura XRD-7000S; Poremaster 33 Ultrapycnometer 1000 MMN-2 SIAMS PDF-4 NEXSYS, etc.

2 Important characteristics of the equipment 1. SEM JEOL JSM-7500F with microanalyser EDXS (Japan) 2. TEM JEOL JEM-2100F with Ion Slicer EM-09100IS (Japan) 3. AFM, SPM nanolaboratory NT-MDT NTEGRA-Aura (Russia) 4. AFM, SPM training equipment NT-MDT NanoEducator (Russia) 5. X-Ray diffractometer Shimadzu XRD-7000S (Japan) including: HTK-2000 Heating Chamber with accessories (vacuum and gas atmosphere control) providing temperature range o C Polycapillary Optics Attachment PCL-1001 'Long Fine Focus : X-ray Tube, PW2273/20 (Philips, Cu), Micro-Measuring Attachment, MDA-1101 with video output Thin Film Analysis using Attachment, THA-1101 Large sample stage (R-Theta) providing analysis of large samples (350 mm diameter; 190 mm height) Stress Analysis Attachment SA-1101 Rotational Sample Stage, RS-1001 with option driver Theta-Theta Vertical Goniometer Cu Target, Broad Focus (BF) Type Min. Step Angle: deg. (2theta), deg. (theta) PDA-4+ Database Crystallite Size & Lattice Strain Software Crystallization Calculation Software

3 Important characteristics of the equipment 6. Mercury porosimeter Quantachrome Poremaster 33 (USA); provides the measurement of the pore size 7 nm with pore size distribution. 7. Helium pycnometer Quantachrome Ultrapycnometer 1000 (USA) 8. BET-analyzer Sorbi with the unit for thermo-treatment of samples (Russia); provides the measurement of the specific area ( m 2 /g), mean size of nanoparticles ( 1 nm ), pore volume (0.001 cm 3 /g). 9. Nanohardness meter Shimadzu DUH-2115 (Japan) 10. Microhardness meter LOMO PMT-3M (Russia) having digital video-camera 11. Binocular optical microscope LOMO MMN-2 (Russia) 12. Testing machine IP-500M (Russia) 13. Pressing equipment including: Hydraulic press WK 18 (Poland); the press force up to 100 tons; Digital sensor of microdisplacements Mitutoyo ID-F125/150 (Japan) to measure the punch displacements during pressing; Digital manometer DM 5001EU (Russia) to measure the pressure; Computer interface Hydraulic press D2430B (Russia); the press force up to 100 tons; working area about 800 x 800 x 700 mm. 14. Powerful ultrasonic equipment: Ultrasonic generators UZG 6.3, Russia (6 kw; khz); UZG 3, Russia (3 kw; 21 khz) Magnetostrictive transducers PMS-15, Russia (1.5 and 3 kw; 21 khz) Ultrasonic bath

4 Important characteristics of the equipment 15. The Spark Plasma Sintering (SPS) Machine Sumitomo 5T-1000A (Japan) 16. Vacuum furnace Nabertherm HTK-18 (Germany); provides the temperature range up to 2200 o C, vacuum of 10-5 mbar; the chamber volume of 8.1 liters. 17. Furnace LAC VP 20/17 (Czechia); provides the temperature range in air up to 1700 o C; the chamber volume of 10 liters. 18. Furnace EMITRON (Russia); provides the temperature range in air up to 1700 o C; the chamber volume of 6 liters.

5 TEM: JEM 2100F (JEOL) with the Ion Slicer SEM: JSM 7500F (JEOL) with the EDS microanalysis XRD-7000S (Shimadzu) with high-temperature chamber ( о С) Nanohardness meter DUH-211S (Shimadzu)

6 BET analyzer (Sorbi, Russia) Ultrasonic and collector molds (TPU, Russia) Ultrasonic generator (IL 100-6/10, Russia) AFM and SPM Nanolaboratory Ntegra-Aura (NT-MDT, Russia) Spark Plasma Sintering SPS 515S (Sumitomo, Japan) Vacuum furnace HTK-18 (Nabertherm, Germany)

7 Presses WK 18 (Poland), D2430B (Russia) Force of 100 Tonns Furnace VP20/17 (LAC, Czechia); о С Liquid nitrogen installation (LNP-10; USA) Chemical tools

8 Nanoporemeter Poremaster 33 (Quantachrome, USA); pore size range 7 nm 950 micrometers Testing machine IP-500М-auto (Russia) with the standard digital dynamometer and bending strength measurements Ultrapycnometer 1000 (Quantachrome, USA) Microhardessmeter PMT-3M (Russia) with CCD camera

9 Special software SIAMS (including :«SIAMS Photolab»; «SIAMS-CP Multiscale Modeling»; «S3D PoroStructure») PDF-4 (crystallographic database) Solid Works NEXSYS (image analysis) etc.

10 Some opportunities of the SIAMS software SIAMS NanoPack Modeling and design of nano-materials and composites. The formation of nanoparticle packing under different conditions. The SIAMS NanoPack considers the material properties, medium characteristics and manufacturing environment, provides modeling formation of multilayer multiphase materials with specified properties. SIAMS NanoSinter Sintering and production of nanoceramics. The sintering processes on nano-level at uniform heating the whole chamber, and using laser sintering, and under threedimensional loading.