Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005

Transcription

1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: Framatome GmbH Heiße Zellen, Radiochemische Analyse, Inkorporationsüberwachung, Chemische Analyse Paul-Gossen-Straße 100, Erlangen Tests in the fields: mechanical-technological materials testing and metallography for metallic materials; radiochemical analysis within the scope of emission and immission monitoring, investigation of process samples and waste samples and of fluence detectors, in addition to the testing of sorptive material for filtration system (without sampling); radioactive material content analysis of human excretions and other biological samples (without sampling) in addition to the determination of incorporated radionuclides by body counter measurements; physical, physicochemical and selected chemical investigations of water and waste water; selected investigations of steel and iron materials; investigation of operating materials Abbreviations used: see last page The testing laboratory is entitled to freely choose between the standard procedures listed here and standard-equivalent testing procedures with different version numbers without requiring previous information and approval of the DAkkS. A current list of all testing procedures in the flexible accreditation area is available from the testing laboratory. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/12

2 In the "Hot Cells" laboratory: 1 Mechanical-technological materials testing, fracture mechanics and hardness testing 1.1 Tensile testing of metallic materials DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ASTM E 8/E 8M-13a ASTM E Destructive tests on welds in metallic materials - Transverse tensile test Metallic materials - Tensile testing - Part 1: Method of test at room temperature (Methods A and B) Metallic materials - Tensile testing - Part 2: Method of test at room temperature (Methods A and B) Metallic materials - Tensile testing - Part 3: Method of test at low temperature (Methods A and B) Metallic materials - Tube - Ring tensile test Brazing - Destructive tests of brazed joints Standard Test Methods for Tension Testing of Metallic Materials Standard Test Methods for Elevated Temperature Tension Tests of Metallic Materials 1.2 Fracture mechanical testing of metallic materials ISO DIN EN ISO ASTM E ASTM E ASTM E Metallic materials - Unified method of test for the determination of quasistatic fracture toughness Metallic materials - Determination of plane-strain fracture toughness [standard withdrawn] Standard Test Method for Linear-Elastic-Plane-Strain Fracture Toughness K IC of Metallic Materials Standard Test Method for K-R-Curve Determination Standard Test Method for Measurement of Fatigue Crack Growth Rates Period of validity: to Translation - 2/12

3 ASTM E 740 /E 740M ASTM E a ASTM E ASTM E ASTM E NF A FAW-R 0025C Standard Practice for Fracture Testing with Surface-Crack Tension Specimens Standard Test Method for Determining Plane-Strain Crack- Arrest Fracture Toughness, K la, of Ferritic Steels Standard Guide for Reconstitution of Irradiated Charpy-Sized Specimens Standard Test Method for Measurement of Fracture Toughness Standard Test Method for Determination of Reference Temperature, T 0, for Ferritic Steels in the Transition Range Evaluation of the J a cracking resistance curve for the determination of the conventional parameters J 0 and dj/da for crack propagation by ductile failure (English translation of the original French standard) [standard withdrawn] Herstellung und Prüfung von elektronenstrahlgeschweißten 10 x 10 DPB-Verbundproben (B = 10 mm, W = 10 mm) (Production and testing of electron beam welded 10 x 10 three-point bending test samples (L = 10 mm, W = 10 mm)) 1.3 Impact bending testing of metallic materials DIN EN ISO DIN EN ISO ASTM E 23-12c ASTM E ASTM E ASTM E a Metallic materials - Charpy pendulum impact test - Part 1: Test method Steel - Charpy V-notch pendulum impact test - Instrumented test method Standard Test Methods for Notched Bar Impact Testing of Metallic Materials Standard Test Method for Dynamic Tear Testing of Metallic Materials Standard Guide for Reconstitution of Irradiated Charpy-Sized Specimens Standard Test Methods for Instrumented Impact Testing of Metallic Materials Period of validity: to Translation - 3/12

4 FAW-R 0016E Herstellung und Prüfung von elektronenstrahlgeschweißten Verbund- Kerbschlagproben (Production and testing of electron beam welded composite impact test samples) 1.4 Hardness testing of metallic materials DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO DIN EN ISO ASTM E b ASTM E Steels - Determination and verification of the depth of carburized and hardened cases Sintered metal materials, excluding hard metals - Determination of apparent hardness and microhardness Sintered ferrous materials, carburized or carbonitrided - Determination and verification of case-hardening depth by a microhardness test Metallic and other inorganic coatings - Vickers and Knoop microhardness tests Metallic materials - Vickers hardness test - Part 1: Test method Metallic materials - Vickers hardness test - Part 2: Verification and calibration of testing machines (Table 5 only) Metallic materials - Vickers hardness test - Part 4: Tables of hardness values Destructive tests on welds in metallic materials - Hardness testing - Part 1: Hardness test on arc welded joints Destructive tests on welds in metallic materials - Hardness testing - Part 2: Microhardness testing of welded joints Standard Hardness Conversion Tables for Metals Standard Test Method for Knoop and Vickers Hardness of Materials Period of validity: to Translation - 4/12

5 2 Metallography DIN EN ISO DIN EN ISO ASTM E Metallic and oxide coatings - Measurement of coating thickness - Microscopical method Metallic and other inorganic coatings - Review of methods of measurement of thickness Standard Test Method for Macroetching Metals and Alloys In the "Radiochemical Analysis" laboratory: 3 Emission and immission monitoring and production and waste samples from nuclear power plants DIN H DIN H AV D AV C AV D AV D AV D German standard methods for the examination of water, waste water and sludge; parameters characterizing effects and substances (group H); determination of total dry residue, filtrate dry residue and residue on ignition (H 1) German standard methods for the examination of water, waste water and sludge; parameters characterizing effects and substances (group H); determination of filterable matter and the residue on ignition (H 2) Determination of the strontium isotopes Sr-89 and Sr-90 in process and waste samples and environmental and incorporation monitoring samples by the liquid scintillation method Determination of uranium, thorium, plutonium, americium and curium isotopes by liquid-liquid extraction in process and waste samples and environmental monitoring samples Determination of tritium on molecular sieve samples by the liquid scintillation method Determination of C-14 on molecular sieve samples by the liquid scintillation method Determination of strontium 89 and strontium 90 on aerosol filters by the Beta integral method (gas flow proportional counter) Period of validity: to Translation - 5/12

6 AV D AV D AV D AV C AV C AV C AV D AV D AV D AV D AV D AV E AV C AV C Determination of strontium 89 and strontium 90 on aerosol filters by the beta integral method (gas flow proportional counter) Fast method Nuclide-specific determination of alpha-emitting radionuclides on filter and wipe test samples by direct measurement with the grid ionisation chamber Determination of Cl-36 in process and waste samples by the liquid scintillation method Determination of silver 108m activity in process and waste samples by gamma spectrometry Determination of total alpha activity concentration in process and waste samples by the gas flow proportional counter method Determination of total beta activity concentration in process and waste samples by the gas flow proportional counter method Determination of C-14 in process and waste samples by the liquid scintillation method following chemical separation Determination of tritium (HTO) by liquid scintillation in aqueous media: process water, waste water, waste material, environmental and urine samples Determination of iodine 129 in process and waste samples by gamma spectrometry following chemical separation Determination of Fe-55 in process and waste samples by liquid scintillation or gamma spectrometry Determination of Ni-63 in process and waste samples by the liquid scintillation method Determination of Pu-241 in process and waste samples and environmental monitoring samples by liquid scintillation following chemical separation Determination of total gamma activity concentration in process and waste samples with the NaI detector Determination of tritium in aqueous samples by the liquid scintillation method following extraction chromatography (separator column Period of validity: to Translation - 6/12

7 AV A AV E AV C AV A AV A AV B AV A AV A AV D AV A AV B AV B AV A Determination of Tc-99 in process and waste samples by the liquid scintillation method Determination of radionuclides in process and waste samples and environmental monitoring samples by gamma spectrometry Extraction-chromatographic separation of uranium, plutonium, americium and curium isotopes in process and waste samples and environmental monitoring samples and determination by alpha spectrometry Gamma-spectrometric determination of I-131 activity concentration in fresh milk following concentration on anion exchange resins Determination of Sr-90 concentration in fresh milk by the liquid scintillation method Determination of Sr-90 concentration and nuclide-specific determination of gamma-emitting radionuclides in foods (e.g. fruits, vegetables and grains) by liquid scintillation and gamma spectrometry Determination of Fe-55 and Ni-63 in primary coolants, waste water and other aqueous solutions by extraction chromatography Separation of niobium for activity determination in process and waste samples by gamma spectrometry Digestion of process and waste samples and environmental monitoring samples with the aid of the START 1500 and the Ethos 1600 microwave systems Digestion of evaporator concentrate and ion exchange samples with Na-K carbonate melt Leaching method for the analysis of uranium, thorium, plutonium and curium isotopes in soil and plant samples Preparation of soil and plant samples by drying and ignition Leaching method for soil and plant samples with the help of the microwave system Period of validity: to Translation - 7/12

8 4 Fluence detectors DIN DIN DIN DIN DIN DIN ASTM E ASTM E ASTM E ASTM E AV C AV C AV C Neutron fluence measurement - Part 1: Fast-neutron fluence determination with activation and fission detectors Neutron fluence measurement - Part 2: Fast-neutron fluence determination with iron activation detectors Neutron fluence measurement - Part 3: Fast-neutron fluence determination with nickel activation detectors Neutron fluence measurement - Part 4: Fast-neutron fluence determination with niobium activation detectors Neutron fluence measurement - Part 5: Fast-neutron fluence determination with copper activation detectors Neutron fluence measurement - Part 6: Fast-neutron fluence determination with thorium fission detectors Standard Test Method for Measuring Fast-Neutron Reaction Rates by Radioactivation of Iron Standard Test Method for Measuring Fast-Neutron Reaction Rates by Radioactivation of Copper Standard Test Method for Measuring Fast-Neutron Reaction Rates by Radioactivation of Nickel Standard Test Method for Measuring Fast-Neutron Reaction Rates by Radioactivation of Niobium Radiochemical evaluation of iron fluence detectors for the determination of Mn-54 decay rates in the measurement of the fast neutron fluence Radiochemical evaluation of niobium fluence detectors for the determination of Nb-93m decay rates in the measurement of the fast neutron fluence Radiochemical evaluation of material samples for the determination of Mn-54 and Nb-93m in the measurement of the fast neutron fluence Period of validity: to Translation - 8/12

9 5 Active charcoal testing (laboratory and on-site testing) Determination of iodine retention by the I-131 methyl iodide tracer DIN DIN AV E AV C AV C AV D Testing of solid fuels - Determination of the bulk density of solid fuels Testing of solid fuels - Determination of the water content and the moisture of analysis sample Synthesis of I-131-doped methyl iodide Grain size analysis of iodine sorption materials (sieve analysis) Laboratory testing of iodine sorption materials with I-131-doped methyl iodide Leakage rate testing of iodine sorption filter systems with I-131- doped methyl iodide (on-site testing) In the "Incorporation Monitoring" laboratory: 6 Radioactive material content analysis of human excretions and other biological samples (without sampling) in addition to the determination of incorporated radionuclides by body counter measurements AV F FAW R0029C Alpha-spectrometric determination of uranium, thorium, plutonium and curium in urine and faecal samples Performance of gamma-spectrometric body counter measurements In the "Chemical Analysis" laboratory: 7 Physical, physicochemical and selected chemical investigations of water and waste water 7.1 Physical and physicochemical parameters DIN EN ISO (C 5) Water quality - Determination of ph Period of validity: to Translation - 9/12

10 DIN EN (C 8) Water quality; determination of electrical conductivity 7.2 Anions DIN EN ISO (D 20) DIN D DIN D Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate German standard methods for the examination of water, waste water and sludge; anions (group D); determination of dissolved silicate by spectrometry German standard methods for the examination of water, waste water and sludge; anions (group D); photometric determination of chromium(vi) using 1,5-diphenylcarbonohydrazide 7.3 Cations DIN EN ISO (E 22) DIN EN ISO (E 29) DIN EN ISO (E 34) Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (extended to include: Au, Eu, Gd, Hf, La, Nb, Nd, Pd, Pt, Ta, Tl, Th, U) Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 2: Determination of 62 elements (extended to include: Am, Cm, Tc, Np, Pu) Water quality - Determination of dissolved Li+, Na+, NH₄+, K+, Mn²+, Ca²+, Mg²+, Sr²+ and Ba²+ using ion chromatography - Method for water and waste water 7.4 Sum effects and parameters DIN H DIN H German standard methods for the examination of water, waste water and sludge; parameters characterizing effects and substances (group H); determination of total dry residue, filtrate dry residue and residue on ignition (H 1) German standard methods for the examination of water, waste water and sludge; parameters characterizing effects and substances (group H); determination of filterable matter and the residue on ignition Period of validity: to Translation - 10/12

11 DIN EN 1484 (H 3) DIN EN ISO (H 53) Water analysis - Guidelines for the determination of total organic carbon (TOC) and dissolved organic carbon (DOC) Water quality - Determination of hydrocarbon oil index - Part 2: Method using solvent extraction and gas chromatography 7.5 Individual components MB Isotopenverhältnisbestimmung in wässrigen Lösungen mittels ICP-MS (Determination of the isotopic ratio by ICP-MS in aqueous solutions) 8 Investigations of steel and iron materials DIN EN ISO DIN EN ISO DIN EN DIN EN ASTM E ASTM E MB Steel and iron - Determination of total carbon and sulfur content - Infrared absorption method after combustion in an induction furnace (routine method) Steel and iron - Determination of nitrogen content - Thermal conductimetric method after fusion in a current of inert gas (routine method) Chemical analysis of ferrous materials - Determination of oxygen in steel and iron - Part 1: Sampling and preparation of steel samples for oxygen determination Chemical analysis of ferrous materials - Determination of oxygen content in steel and iron - Part 2: Infrared method after fusion under inert gas Standard Test Method for Analysis of Carbon and Low-Alloy Steel by Spark Emission Spectrometry (extended range of elements and working steps) Standard Test Method of Austenitic Stainless Steel by Spark Emission Spectrometry (extended range of elements and working steps) Hot extraction determination of hydrogen in zircaloy, titanium and steel Period of validity: to Translation - 11/12

12 9 Investigation of operating materials ISO MB Surface active agents; Washing powders; Determination of total boron content; Titrimetric method High-temperature digestion for the determination of Cl, F and S in solid and liquid samples Abbreviations used ASTM AV DIN EN FAW ICP-MS ICP-OES IEC ISO MB NF TOC American Society for Testing and Materials Analysenvorschrift der AREVA GmbH (Analytical instruction of the AREVA GmbH) Deutsches Institut für Normung (German Institute for Standardization) European norm Fachanweisung der AREVA GmbH (Technical instruction of the AREVA GmbH) Inductively coupled plasma mass spectrometry Inductively coupled plasma optical emission spectrometry International Electrotechnical Commission International Organization for Standardization Methodenbeschreibung der AREVA GmbH (Method description of the AREVA GmbH) Norme française (French standard) Total organic carbon Period of validity: to Translation - 12/12