04-H Rocky Lake Tap Water 04/09/30 04/09/ B nd. nd nd nd nd. nd nd

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1 norganic Parameters page: 1. ANALYTCAL SERVCES : Alpha Chemical Ltd. NS B3B 1T8 pac Project NUmber H Project Number FAX # : Printed: 2004/10/07 (Event 669) Reported. 2004/10/07 Matrix Philip Sampled Received Water 04-H Rocky Lake Tap Water Analyte BQL Total Water Sodium Potassium Calcium Magnesium Digest Alkalinity (as CaCO3) Sulfate Chloride Reactive Silica (as SiO2) Ortho Phosphate (as P) Phosphorus Nitrate + Nitrite (as N) Nitrate (as N) Nitrite Ammonia (as N) B Color TCU Total Org. Carbon (by UV)mg!L 0.5 Turbidity NTU Couctance (RCAp) us!cm Note Lege BQL = Bstimated Quantitation Limit is the minimum concentration that can be reliably reported. t is not a regulatory limit. HD. Not Detected, instrument did not detect anything above staard BQL. HD ( ). Not Detected at the elevated BQL specified, due to matrix interferences or sample pre-dilution. - - Dash is reported when parameter not requested in sample. Soil results are expressed as air dry weight basis. Biota re.ults are expressed on a wet weight basi. unless otherwise stated. page verified -L Z~8lUfWAERROAD,SUfTe 105, BEDfORD, NOVA SCOTA, C/\NADA B4&J.Gf,>'T'~ 4~~Q~, f9q W icol.com

2 PSC Analytical Services Bedford, HS Canada B4B 1G9 Pax (902) norganic Parameters page i : Alpha Chemical Ltd. NS B3B TS PSC Project NUmber: B Project NUmber: 2 RAWDNG, FAX # Printed Reported : :. PAUL /10/ /10/07 Matrix Philip Sampled Received Water 04-H Rocky Lake Tap Water Analyte ph EQL ( Continued from previous page) Hardness (as CaCO]) Bicarbonate (a8 CaCO3) Carbonate (as CaCO3) TDS (Calculated) Cation Sum Anion Sum on Balance Langlier Langlier Saturation < meq/l meq/l, Saturation Aluminum Antimony Arsenic Barium ph a 20C 10' 2~ Beryllium Bismuth Boron Cadmium Chromi urn s. 0.3 Lege BQL. Bstimated Quantitation Limit is the min~ concentration that can be reliably reported. t is not a regulatory limit. ND. Not Detected, instrument did not detect anything above staard BQL. ND ( ). Not Detected at the elevated BQL specified, due to matrix interferences or sample pre-dilution. -. Dash is reported when parameter not requested in sample. Note : Soil results are expressed as air dry weight basis. : Biota results are expressed on a wet weight basis unless otherwi.e stated. page verified -L-

3 ~ pac Analytical Services Bedford, NS Canada B4B 1G9 "ax (902) norganic Parameters page : Alpha Chemical Ltd. NS B3B l.t8 PSC Project Number: 04l.7932B Project Number: 3 PAX # Printed Reported /3.0/ /3.0/07 B669 Matrix Philip Analyte Sampled Received Water 04-B Rocky Lake Tap Water units BQL ( Continued fram previous page) Cobalt Copper ron Lead Manganese Molybdenum Nickel Selenium Silver Strontium Thallium Tin Titanium Uranium Vanadium Zinc 1.4. Note Lege BQL - Bstimated Quantitation Ltmit is the mintmum concentration that can be reliably reported. t ia not a regulatory ltmit. ND - Not Detected, instrument did not detect anything above.taard BQL. ND ( ). Not Detected at the elevated BQL specified, due to matrix interferences or sample pre-dilution. - = Dash is reported when parameter not requested in sample. Soil results are expressed as air dry weight ba.i.. Biota results are expressed on a wet weight basis unless otherwi.e stated. page verified --.L1--

4 norganic Parameters page : 4 PSC Analytical Service. Bedford, NS Canada B4B 1G9 Fax (902) z Alpha Chemical Ltd. Uni t 8, 75 MacDonald Ave NS B3B lt8 FAX # PSC Project Number: H Printed 2004/10/07 B669 proj ec t Number: Reported 2004/10/07 Certificate of Analysis Method Swmnaries:.~ ~ Alkalinity: Roche Cobas Fara/BMC Hitachi 911 Automated Colorimetric Analyser. Ref: USEPA Method #310.2 Chloride: Roche Cobas Fara/BMC Hitachi 911 Automated Colorimetric Analyser. Ref: USEPA Method #321 ~ Colour: Roche Cobas Fara/BMC Hitachi 911 Automated Colorimetric Analyser. Ref: Staard Methods, 16th Edition, 1985 ~ Couctance (RCAp): Electrometric. 25 C, values >300 US/cm diluted for validation purposes. Ref: Staard Methods 4500-H+, 19th Edition, 199,~ Total Organic Carbon: UV Digestion/Technicon AAl Analyser. Ref: Staard Methods, 19th Edition, 1995 ~~ Total Recoverable Metals Digest: Homogenization/Digestion. Ref: USBPA Method # NO2/NO3: Roche Cobas Fara/BMC Hitachi 911 Automated Colormetric Analyser. Ref. USEPA Method # ph: 25 C. Ref: USEPA Method #15 SOP 1007 V1Rl / 1011 V1R2 ~ Phosphorus: PE Optima 3000 CP-OBS. Ref: USBPA Method # Reactive Silica: Roche Cobas Fara/BMC Hitachi 911 Automated Colorimetric Analyser. Ref: USEPA Method #37 ~. Sulphate: Automated Turbidimetric. Ref: USBPA Method #374 or on Chromatography. Ref: USBPA Method #30 Turbidity: Nephelometric. Ref: USBPA Method Ortho Phosphorus: Roche Cobas Fara/BMC Hitachi 911 Automated Colorimetric Analyser. Ref: USEPA Method #361 SOP 2160 V1R2 / 2165 V1Rl.. Trace Metals in Aqueous Samples: Elan 5000 CP-MS. Ref: USBPA Method #200.8 ~ Ammonia (NH3 plus NH4+): Roche Cobas Fara/BMC Hitachi 911 Automated Colorimetric Analyser. Ref: USBPA 35 Determination of Ammonia ( Colorimetric, Automated Phenate) Revision 0, SOP 2100 V1R2 / 2105 V1R2 Nitrite. Roche Cobas/BMC Hitachi 911 Automated Colormetric Analyser. Ref: USEPA Method #354.1 Major Metals in Aqueous Samples: PB Optima 3000 CP-OES. Ref: USBPA Method #200.7 Total Metals in Water: Digestion/CP-MS. Ref: USEPA 200.8

5 norganic Parameters page z 5 PSC Analytical S.rvice. Bedford, NS Canada B4B 109 Fax (902) Alpha Chemical Ltd. RAWDNG, PAm. unit 8, 75 MacDonald Ave NS B3B J.T8 FAX # pac Project Number: H Printed 2004/10/07 B669 Project Number: Reported 12004/10/07 Certificate of Analysis Conversions: part per million (ppm) part per billion (ppb) All work recorded herein has been done in accordance with normal professional staards using accepted testing technologies, quality assurance a quality control procedures except where otherwise agreed to by the client a testing company in writing. The results relate only to the items tested. Liability for any a all use of these test results shall be limited to the actual cost of the pertinent analysis perfo~ed. There is no other warranty expressed or implied. Excess sample will be di8carded upon expiry of hold time. Analyses reviewed by: norganics Manager:.~ ~ ~_o~ c;:rrry Ar8novich

6 Microbiology Parameters page J 1 ANALYTCAL SERVCES Alpha Chemical Ltd. NS B3B 1T8 PSC Project Number: H Project Number: RAWDNG, FAX # Printed Reported PAUL /~O/O7 (Event 67~) 2004/10/07 04-H Rocky Lake Tap Water Sampled: 20 Time Sampled: 8:30 Received: 20 E. coli (Colilert) Absent Total Coliform (Colilert) Absent 200 BlUEWATER ROAD, SUTE 105, BEDFORD, NOVA SCOTA, CANADA B4B 1 G9 T J;~~A~~t2 W

7 Microcrobiology Parameters page z 2 PSC Analytical Services Bedford, NS Canada B4B Pax (902) P.o. lag : Alpha Chemical Ltd. NS B3B lt8 pac Project Number B Project NUmber: Printed, 2004/10/07 Reported 200t/1O/O7 Certificate of Analysis Method SUlarie8: Total 19th Coliform Edition, a E. 199 coli: Defined Substrate Test. Ref: Staard Methods, Conversions: 1 = part per million (ppm), part per billion (ppb) All work recorded herein has been done in accordance with normal professional staards using accepted testing technologies, quality assurance a quality control procedures except where otherwise agreed to by the client a testing company in writing. The results relate only to the items tested. Liability for any a all use of these test results shall be limited to the actual cost of the pertinent analysis performed. There is no other warranty expressed or implied. Bxcess sample will be discarded upon expiry of hold time. Analyses reviewed byz Microbiology Supervisor: /.<! DeA.-re f../.