TAMURA KAKEN (UK) LTD

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1 Product Information TAMURA KAKEN (UK) LTD Carbon Resin Conductive Paste Feb 3 CARBOLLOID MRX-713J DESCRIPTION CARBOLLOID MRX-713J is suitable for use in the production of printed key pads or jumper circuits, giving excellent printing characteristics. It is a single component system which requires no mixing. PHYSICAL PROPERTIES Dry Resistivity Ohms/square at 15 microns thickness High temperature Resistance ( C - 5hrs) -4% Humidity Resistance (6 C, 9%RH, 5hrs) - 11% resistivity change Copper Adhesion Cross Cut Tape test Solder Heat Resistance Adhesion on copper - 1% resistivity change Viscosity dpa.s at C RECOMMENDED PRINTING PARAMETERS Screen Squeegee Screen Cleaner mesh polyester or stainless steel screen (6 T) 65-8 Shore Hardness Toluene, Xylene, T.C.E. etc CURING 15 C for 15 minutes in an air oven. SHELF LIFE I f stored in the right conditions the solder paste should be for at least 12 months without the need fof If stored in a fridge, 3 months from date of manufacture. 1

2 TECHNICAL INFORMATION 1. MRJ-713J SPECIFIC AREA MRX-713J TECHNICAL INFORMATION Table 1 : MRX-713J Specific Data ITEMS DATA TEST CONDITION Viscosity dpa.s C, Viscotester VT-4 Sheet Resistivity Ohm / ٱ Adhesion on Copper Cross Cut Tape Test Solder Heat Resistances Change of Resistivity Adhesion on Copper -1% Change of Resistivity after PEELCOAT curing -2% Change of Resistivity after PEELCOAT curing and Solder Dipping -5% Pressure Cooker Test Solder Dipped - Change of Resistivity Not solder Dipped - Change of resistivity +6% -% 26 C, sec RA Flux 15 C, 7 min M- 15 C, 7 min M- 26 C, sec RS Flux Saturated Type 121 C, 8 hrs Adhesion on Overcoat PHOTOCOAT USR 2G-SH - On Laminate - On Copper PHOTOCOAT USR 11G-11 - On Laminate - On Copper Powder Dropping Passed 1W/cm, 3 lamps 7 m/min Printing Resolution Initial After Panels - On Laminate - On Copper - On Laminate - On Copper.4mm.4mm.4mm.4mm Pattern width.4mm C, 1. min left standing before curing Curing Condition : 165 C 3 min by IR furnace 2

3 Abrasion Resistance Change of Insulation Resistivity Powder Dropping Table 1 : MRX-713J Specific Data (Cont) ITEMS DATA TEST CONDITION Before / After Weight 5g, times 13 / 13 Ohm a little High Temperature Ageing - Solder Dipped - Not Solder Dipped High Humidity Oil Dipping Solder Dipped - Solder Dipped - Not Solder Dipped - Change of Resistivity Not Solder Dipped - Change of Resistivity Salt Water Spray Solder Dipped - Change of Resistivity Not Solder Dipped - Change of Resistivity Boiling Water Test Solder Dipped - Change of Resistivity Not Solder Dipped - Change of Resistivity Solder Heat Resistance - Change of Resistivity - 6% - 7% + 13% + 18% - 5% + % + 1% + 3% + 2% - 13% - 18% slight peeling C, 5 hrs 6 C, 9%RH, 5 hrs 26 C, sec, times 35 C, 5%NaCl, 96 hrs C, 2 hrs, 4 times C, 5 sec, times Curing Condition : 165 C 3 min by IR furnace 3

4 2. MRX-713J ADHESION OF OVERCOAT Table 2 : MRX-713J Adhesion Test Result Overcoat Resist Conveyor Speed On Laminate On Copper USR 2G-SH 3m/min 5m/min 7m/min poor poor USR-11B-11 3m/min 5m/min 7m/min Undercoat : USR 2G-SH in 1W/cm 3 lamps 5m/min acceptable superior acceptable superior 3. MRX-713J INTER-LAYER ADHESION Table 3 : Adhesion between Carbon & Overcoat Overcoat Resist Undercoat Resist USR 2G-SH USR 11B-11 USR 2G-SH On Laminate poor On Copper poor Curing parameter : 12W/cm 3 lamps 5m/min 4

5 4. MRX-713J : FILM THICKNESS EFFECTS 7 6 Resistivity Ω / 5 15 Film thickness (micron) Figure 1: Sheet Resistivity vs. Film Thickness Resistivity change (%) - Peelcoat curing resistance Solder Heat resistance - - Film Thickness (microns) Fig. 2 Film Thickness vs. Solder Heat Resistance & Peelcoat Curing Resistance 5

6 5. MRX-713J EFFECTS OF IR FURNACE PASSES Resistivity Ω / IR Furnace passes (165 O C, 3min.) Fig. 3: Sheet Resitivity vs. Furnace Passes 4 Resistivity Change (%) Peelcoat curing resistance Solder heat resistance -8 IR Furnace Passes (165 O C, 3 min.) Fig 4 Solder Heat Resistance and Peelcoat Curing Resistance vs. IR Furnace Passes 6

7 6. MRX-713J Continuous Printability Viscosity (dpa.s) 8 6 Panels printed Fig. 5 Change of Viscosity on Screen Resistivity Ω / 6 5 Panels printed Fig. 6 Change of Sheet Resistivity Resistivity Ω / Panels printed Fig. 7 Change of Film Thickness 7

8 7. MRX-713J Curing Conditions 6 5 Resistivity ( / ) 1 OC 1 OC 1 OC 15 OC 5 Curing time (min) Fig 8 Curing condition vs Resistivity (15 m) Resistivity change (%) OC 1 OC 1 OC 15 OC - 5 Curing time (min) Fig 9 Curing condition vs Resistivity change after soldering 8

9 Table 4 : MRX-713J Adhesion vs. IR Furnace Passes Solder Dipped Not Solder Dipped Pass Number 26 C, sec, 5 times.5 Times (double speed) Once Twice 3 times 8. MRX-713-J STUDY OF RE-USE Table 5 : Reuse of MRX-713J Units Initial Panels Kept 4 Days & Visco adjusted Viscosity ps 5-35 Sheet Resistivity ohm/sq Film Thickness micron Solder Heat Resistance - Change of Resistivity % % PEELCOAT curing resistance % PEELCOAT solder dipping - change of resistivity % Adhesion on Copper 9. ABRASION RESISTANCE When the Carbon paste is subject to abrasion due to a moving contact across the surface of the cured carbon layer the following items should be noted. The shape of the material in contact with the carbon layer should be as smooth as possible to reduce the abrasive effect. The end user should satisfy themselves under test conditions that the carbon layer will fulfil their requirements for abrasive resistance. These tests should be carried out to determine the reliability of the carbon layer and would hence be an indicator of the products performance under end user conditions Tamura Kaken is not liable for guaranteeing the abrasion resistance as each condition of use is different. 9