Technical Report No Dated

Transcription

1 Applicant: Durable plastic limited Address: 105 Middle Badda, Gpo Box# Dhaka, Bangladesh Attn.: Mr. Nahid Hasan Sample Description: 100gram+5pcs samples Supplier/Manufacturer: Durable plastic limited Country of Origin: Bangladesh Sample Receive Date: Test Period: From to Test Requested and Conclusion: As specified by client, to test per the selected requirement(s) for the tested item(s) as stated in the German Food & Feed Acts LFGB ( 30 & 31) and Regulation (EC) No.1935/ For material: Plastics or coating Overall migration test for compliance with Regulation (EU) No. 10/2011 and its amendment Regulation (EU) 2016/1416 for plastic materials and article intended to come into contact with foodstuffs. 2. For material: Plastics or coating Specific Migration of Primary Aromatic Amine 3. For material: Plastics or coating Specific migration of Heavy metal(al, Ba, Co, Cu, Fe, Li, Mn, Zn) 4. For material: Silicone Extractable components 5. For material: Silicone Total platinum content No extract, abridgment or abstraction from a test report may be published or used to advertise a product without the written consent of the Director of TÜV SÜD Certification and Testing (China) Co., Ltd. Shenzhen Branch. The results contained herein apply only to the particular sample tested and to the specific test carried out and not to samples of the current production line. Page: 1 of 9

2 6. For material: Rubber / silicone / plastics Peroxide value 7. For material: Rubber / silicone Volatile Organic Matters 8. For material: Polypropylene (PP)/ Polyethylene (PE) Total Chromium, Vanadium, Zirconium and Hafnium content 9. Sensory test With reference to DIN Test Results: Refer to following page(s) Remark : - The result relates only to the items tested. - The test item was specified by the client. No extract, abridgment or abstraction from a test report may be published or used to advertise a product without the written consent of the Director of TÜV SÜD Certification and Testing (China) Co., Ltd. Shenzhen Branch. The results contained herein apply only to the particular sample tested and to the specific test carried out and not to samples of the current production line. Page: 2 of 9

3 1. TESTED SUBJECT DESCRIPTION SAMPLE NUMBER TESTED MATERIAL DESCRIPTION PHOTO 001 Transparent PP plastic cover & Body 002 Blue silicone rings 003 Whole product Page: 3 of 9

4 2. TEST RESULT 2.1. OVERALL MIGRATION TEST Test method: As specified in Regulation (EU) No. 10/2011 ANNEX III and V then test with reference to: EN :2002 (Guide to the selection of conditions and test methods for overall migration) EN :2002 (Article Filling method) EN :2002 (Substitute Test method) SIMULANT USED TEST CONDITIONS RESULT [mg/dm²] SAMPLE 001 LIMIT [mg/dm²] 10% Ethanol 100 for 2 hours < % Acetic Acid 100 for 2 hours < % Ethanol 60 for 3.5 hours < Iso-octane 60 for 1.5 hours denotes degree Celsius - mg/dm 2 denotes milligram per square decimeter 2.2. SPECIFIC MIGRATION OF PRIMARY AROMATIC AMINE TEST Test method: With reference to EN : 2002, followed by Kunststoffe im Lebensmittelvekehr, Book 2, Teil B II, XXI, The sample(s) were tested in 3% acetic acid at 100 for 2 hours, follow by UV spectrophotometer. Migration of Primary Aromatic Amine RESULT [mg/kg] SAMPLE 001 < mg/kg denotes milligram per kilogram - denotes degree Celsius - The specification was quoted from Regulation (EU) No. 10/2011 LIMIT [mg/kg] Not Detected (< 0.01 mg/kg) Page: 4 of 9

5 2.3. SPECIFIC MIGRATION OF HEAVY METAL (AL,BA, CO, CU, FE, LI, MN, ZN) Test method: As specified in Regulation (EU) No. 10/2011 ANNEX III and V, The samples were tested in 3% acetic acid at 100 for 2 hours, followed by Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES). RESULT[mg/kg] SAMPLE 001 LIMIT [mg/kg] Aluminium (Al) < Barium (Ba) < Cobalt (Co) < Copper (Cu) < Iron (Fe) < Lithium (Li) < Manganese (Mn) < Zinc (Zn) < denotes degree Celsius - mg/kg denotes milligram per kilogram - The specification was quoted from Regulation (EU) No. 10/2011 and its amendment Regulation (EU) 2016/1416 Page: 5 of 9

6 2.4. EXTRACTABLE COMPONENTS TEST Test method: With reference to Bundesgesundheitsbl 46(2003)362 and followed by gravimetric method. SIMULANT USED TEST CONDITIONS RESULTS [%] SAMPLE 002 LIMIT [%] Distilled water Reflux for 5 hours < % Acetic Acid Reflux for 5 hours < % Ethanol Reflux for 5 hours < Note : - % denotes percentage by weight Lebensmittelverkehr Part XV Silicone 2.5. TOTAL PLATINUM CONTENT Test method: Microwave digestion, followed by Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES). RESULT [m/kg] SAMPLE 002 LIMIT [mg/kg] Platinum < mg/kg denotes milligram per kilogram Lebensmittelverkehr Part XV Silicone Page: 6 of 9

7 2.6. PEROXIDE VALUE TEST Test method : With reference to 58th Communication on the testing of plastics, Bundesgesundheitsbl. 40 (1997) 412. RESULT SAMPLE 002 LIMIT Peroxide Value Absent Absent Lebensmittelverkehr Part XV and Part VI 2.7. VOLATILE ORGANIC MATTER TEST Test Method: With reference to Bundesgesundheitsbl 46 (2003) 362. The samples were tested at 100 for 2 hours. RESULT [%] SAMPLE 002 LIMIT [%] Volatile Organic Matter denotes degree Celsius - % denotes percentage by weight Lebensmittelverkehr Part XV Silicones Page: 7 of 9

8 2.8. TOTAL CHROMIUM, VANADIUM, ZIRCONIUM AND HAFNIUM CONTENT TEST Test method: Microwave digestion, followed by Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES). RESULT [mg/kg] SAMPLE 001 LIMIT [mg/kg] Chromium (Cr) < 5 10 Vanadium (V) < Zirconium (Zr) < Hafnium (Hf) < mg/kg denotes milligram per kilogram Lebensmittelverkehr Part VII Polypropylene Page: 8 of 9

9 2.9. SENSORY TEST Test method: With reference to DIN The submitted sample was treated with distilled water at 100 for 2 hours. After this treatment, treated water was examined by panels with regard to any divergence in smell and taste. GRADING RESULT SAMPLE 003 RECOMMENDED LEVEL Transfer of Taste 1 < 2.5 Transfer of Smell 1 < Explanation for grading are listed as below: Grading 0: No perceptible taste/smell deviation Grading 1: Just perceptible taste/smell deviation Grading 2: Weak taste/smell deviation Grading 3: Clear taste/smell deviation Grading 4: Strong taste/smell deviation ************ TÜV SÜD Certification and Testing (China) Co., Ltd. Shenzhen Branch Prepared by: Reviewed by: Ken Chen Senior Project Coordinator Brady Yu Section Manager Page: 9 of 9