CERTIFICATE OF ANALYSIS
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1 BAY 3, TH STREET NE CALGARY, AB CANADA T2L 7C3 MAXXAM JOB #: A Received: 2008/04/02, 13:15 Matrix: Water # s Received: 1 This report supersedes all previous reports with the same Maxxam job number CERTIFICATE OF ANALYSIS Date Date Analyses Quantity Extracted Analyzed Laboratory Method Analytical Method Alkalinity (pp, total), CO3,HCO3,OH 1 N/A 2008/04/03 CAL SOP SM 2320-B Chloride by Automated Colourimetry 1 N/A 2008/04/02 CAL SOP EPA Conductivity 1 N/A 2008/04/03 CAL SOP SM 2510-B Hardness 1 N/A 2008/04/02 CAL WI AEMM, Method 423 Elements by ICP - Dissolved 1 N/A 2008/04/03 CAL SOP EPA SW B Elements by ICPMS - Dissolved 1 N/A 2008/04/02 CAL SOP EPA SW A Ion Balance 1 N/A 2008/04/02 CAL WI SM 1030E Nitrate + Nitrite-N (calculated) 1 N/A 2008/04/03 CAL SOP SM 4110B Nitrogen, (Nitrite, Nitrate) by IC 1 N/A 2008/04/03 CAL SOP SM 4110-B ph (Alkalinity titrator) 1 N/A 2008/04/03 CAL SOP (PCT) SM 4500-H B CAL SOP (MANUAL) Sulphate by Automated Colourimetry 1 N/A 2008/04/02 CAL SOP EPA Total Dissolved Solids (Calculated) 1 N/A 2008/04/02 CAL WI Encryption Key Please direct all questions regarding this Certificate of Analysis to your Project Manager. SUE RAYNARD, Sue.Raynard@maxxamanalytics.com Phone# (403) ==================================================================== Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format. Total cover pages: 1 Page 1 of 7
2 Maxxam Job #: A Client Project #: EXTENDED METALS SCAN ON WATER -DISSOLVED (WATER) Maxxam ID J38190 Sampling Date Units 25/08 RDL QC Batch Elements Dissolved Aluminum (Al) mg/l < Dissolved Antimony (Sb) mg/l < Dissolved Arsenic (As) mg/l < Dissolved Barium (Ba) mg/l Dissolved Beryllium (Be) mg/l < Dissolved Boron (B) mg/l Dissolved Cadmium (Cd) mg/l < Dissolved Calcium (Ca) mg/l Dissolved Chromium (Cr) mg/l < Dissolved Cobalt (Co) mg/l < Dissolved Copper (Cu) mg/l Dissolved Iron (Fe) mg/l < Dissolved Lead (Pb) mg/l < Dissolved Lithium (Li) mg/l Dissolved Magnesium (Mg) mg/l Dissolved Manganese (Mn) mg/l Dissolved Molybdenum (Mo) mg/l < Dissolved Nickel (Ni) mg/l < Dissolved Phosphorus (P) mg/l Dissolved Potassium (K) mg/l Dissolved Selenium (Se) mg/l Dissolved Silicon (Si) mg/l Dissolved Silver (Ag) mg/l < Dissolved Sodium (Na) mg/l Dissolved Strontium (Sr) mg/l Dissolved Sulphur (S) mg/l Dissolved Thallium (Tl) mg/l < Dissolved Tin (Sn) mg/l < Dissolved Titanium (Ti) mg/l < Dissolved Uranium (U) mg/l Dissolved Vanadium (V) mg/l < Dissolved Zinc (Zn) mg/l < RDL = Reportable Detection Limit Page 2 of 7
3 Maxxam Job #: A Client Project #: ROUTINE WATER (WATER) Maxxam ID J38190 Sampling Date Units 25/08 RDL QC Batch Calculated Parameters Hardness (CaCO3) mg/l Ion Balance N/A Total Dissolved Solids mg/l Misc. Inorganics Conductivity us/cm ph N/A Anions Alkalinity (PP as CaCO3) mg/l < Alkalinity (Total as CaCO3) mg/l Bicarbonate (HCO3) mg/l Carbonate (CO3) mg/l < Hydroxide (OH) mg/l < Dissolved Sulphate (SO4) mg/l < Dissolved Chloride (Cl) mg/l Nutrients Dissolved Nitrate (N) mg/l Nitrate plus Nitrite (N) mg/l Dissolved Nitrite (N) mg/l < RDL = Reportable Detection Limit Page 3 of 7
4 Maxxam Job #: A Client Project #: General Comments J : Anion - Cation balance exceeds normal acceptance limits, major ions reanalyzed, possible matrix interference EXTENDED METALS SCAN ON WATER -DISSOLVED (WATER) Comments J Elements by ICP - Dissolved: Detection limit raised to bring results within linear range for Na J Elements by ICPMS - Dissolved: Detection limits raised due to sample matrix. ROUTINE WATER (WATER) Comments J Chloride by Automated Colourimetry: Detection limit raised to bring results within linear range J Nitrogen, (Nitrite, Nitrate) by IC: Detection limits raised due to matrix interference Results relate only to the items tested. Page 4 of 7
5 Quality Assurance Report Maxxam Job Number: CA Client Project #: P.O. #: Site Reference: QA/QC Date Batch Analyzed Num Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits GK1 Calibration Check Dissolved Sulphate (SO4) 2008/04/ % MATRIX SPIKE Dissolved Sulphate (SO4) 2008/04/02 NC % BLANK Dissolved Sulphate (SO4) 2008/04/02 <0.5 mg/l RPD Dissolved Sulphate (SO4) 2008/04/ % KC1 Calibration Check Dissolved Antimony (Sb) 2008/04/ % Dissolved Arsenic (As) 2008/04/02 90 % Dissolved Beryllium (Be) 2008/04/02 93 % Dissolved Cadmium (Cd) 2008/04/02 94 % Dissolved Cobalt (Co) 2008/04/02 94 % Dissolved Copper (Cu) 2008/04/ % Dissolved Lead (Pb) 2008/04/02 95 % Dissolved Molybdenum (Mo) 2008/04/02 96 % Dissolved Nickel (Ni) 2008/04/02 99 % Dissolved Selenium (Se) 2008/04/02 89 % Dissolved Silver (Ag) 2008/04/02 98 % Dissolved Thallium (Tl) 2008/04/02 98 % Dissolved Tin (Sn) 2008/04/ % Dissolved Titanium (Ti) 2008/04/ % Dissolved Uranium (U) 2008/04/02 89 % Dissolved Vanadium (V) 2008/04/02 98 % Dissolved Zinc (Zn) 2008/04/02 99 % MATRIX SPIKE Dissolved Antimony (Sb) 2008/04/ % Dissolved Arsenic (As) 2008/04/ % Dissolved Beryllium (Be) 2008/04/ % Dissolved Cadmium (Cd) 2008/04/ % Dissolved Cobalt (Co) 2008/04/ % Dissolved Copper (Cu) 2008/04/ % Dissolved Lead (Pb) 2008/04/ % Dissolved Molybdenum (Mo) 2008/04/ % Dissolved Nickel (Ni) 2008/04/ % Dissolved Selenium (Se) 2008/04/02 97 % Dissolved Silver (Ag) 2008/04/ % Dissolved Thallium (Tl) 2008/04/ % Dissolved Tin (Sn) 2008/04/ % Dissolved Titanium (Ti) 2008/04/ % Dissolved Uranium (U) 2008/04/ % Dissolved Vanadium (V) 2008/04/ % Dissolved Zinc (Zn) 2008/04/ % BLANK Dissolved Antimony (Sb) 2008/04/02 < mg/l Dissolved Arsenic (As) 2008/04/02 <0.001 mg/l Dissolved Beryllium (Be) 2008/04/02 <0.001 mg/l Dissolved Cadmium (Cd) 2008/04/02 < mg/l Dissolved Cobalt (Co) 2008/04/02 < mg/l Dissolved Copper (Cu) 2008/04/ , RDL= mg/l Dissolved Lead (Pb) 2008/04/02 < mg/l Dissolved Molybdenum (Mo) 2008/04/02 < mg/l Dissolved Nickel (Ni) 2008/04/02 < mg/l Dissolved Selenium (Se) 2008/04/ , RDL=0.001 mg/l Dissolved Silver (Ag) 2008/04/02 < mg/l Dissolved Thallium (Tl) 2008/04/02 < mg/l Dissolved Tin (Sn) 2008/04/02 <0.001 mg/l Dissolved Titanium (Ti) 2008/04/02 <0.001 mg/l Dissolved Uranium (U) 2008/04/02 < mg/l Dissolved Vanadium (V) 2008/04/02 <0.001 mg/l Dissolved Zinc (Zn) 2008/04/02 <0.003 mg/l Page 5 of 7
6 Quality Assurance Report (Continued) Maxxam Job Number: CA Client Project #: P.O. #: Site Reference: QA/QC Date Batch Analyzed Num Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits KC1 RPD Dissolved Antimony (Sb) 2008/04/02 NC % 20 Dissolved Beryllium (Be) 2008/04/02 NC % 20 Dissolved Cobalt (Co) 2008/04/02 NC % 20 Dissolved Copper (Cu) 2008/04/02 NC % 20 Dissolved Lead (Pb) 2008/04/02 NC % 20 Dissolved Molybdenum (Mo) 2008/04/02 NC % 20 Dissolved Nickel (Ni) 2008/04/02 NC % 20 Dissolved Silver (Ag) 2008/04/02 NC % 20 Dissolved Thallium (Tl) 2008/04/02 NC % 20 Dissolved Tin (Sn) 2008/04/02 NC % 20 Dissolved Titanium (Ti) 2008/04/02 NC % 20 Dissolved Uranium (U) 2008/04/02 NC % 20 Dissolved Vanadium (V) 2008/04/02 NC % 20 Dissolved Zinc (Zn) 2008/04/02 NC % SE2 Calibration Check Dissolved Nitrate (N) 2008/04/ % Dissolved Nitrite (N) 2008/04/ % BLANK Dissolved Nitrate (N) 2008/04/03 <0.003 mg/l Dissolved Nitrite (N) 2008/04/03 <0.003 mg/l SP8 Calibration Check Alkalinity (Total as CaCO3) 2008/04/03 99 % RPD Alkalinity (PP as CaCO3) 2008/04/03 NC % 20 Alkalinity (Total as CaCO3) 2008/04/ % 20 Bicarbonate (HCO3) 2008/04/ % 20 Carbonate (CO3) 2008/04/03 NC % 20 Hydroxide (OH) 2008/04/03 NC % SP8 Calibration Check ph 2008/04/ % RPD ph 2008/04/ % SP8 Calibration Check Conductivity 2008/04/03 99 % SPIKE Conductivity 2008/04/ % BLANK Conductivity 2008/04/03 <1 us/cm RPD Conductivity 2008/04/03 0 % GK1 Calibration Check Dissolved Chloride (Cl) 2008/04/ % MATRIX SPIKE Dissolved Chloride (Cl) 2008/04/ % BLANK Dissolved Chloride (Cl) 2008/04/03 0.8, RDL=0.5 mg/l RPD Dissolved Chloride (Cl) 2008/04/03 NC % FL1 Calibration Check Dissolved Aluminum (Al) 2008/04/ % Dissolved Barium (Ba) 2008/04/03 93 % Dissolved Boron (B) 2008/04/ % Dissolved Calcium (Ca) 2008/04/ % Dissolved Chromium (Cr) 2008/04/03 94 % Dissolved Iron (Fe) 2008/04/03 95 % Dissolved Lithium (Li) 2008/04/03 99 % Dissolved Magnesium (Mg) 2008/04/ % Dissolved Manganese (Mn) 2008/04/ % Dissolved Phosphorus (P) 2008/04/ % Dissolved Potassium (K) 2008/04/ % Dissolved Silicon (Si) 2008/04/03 99 % Dissolved Sodium (Na) 2008/04/ % Dissolved Strontium (Sr) 2008/04/03 94 % MATRIX SPIKE Dissolved Aluminum (Al) 2008/04/03 96 % Dissolved Barium (Ba) 2008/04/03 87 % Dissolved Boron (B) 2008/04/03 94 % Dissolved Calcium (Ca) 2008/04/03 NC % Dissolved Chromium (Cr) 2008/04/03 87 % Dissolved Iron (Fe) 2008/04/03 88 % Dissolved Lithium (Li) 2008/04/03 90 % Page 6 of 7
7 Quality Assurance Report (Continued) Maxxam Job Number: CA Client Project #: P.O. #: Site Reference: QA/QC Date Batch Analyzed Num Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits FL1 MATRIX SPIKE Dissolved Magnesium (Mg) 2008/04/03 88 % Dissolved Manganese (Mn) 2008/04/03 93 % Dissolved Phosphorus (P) 2008/04/ % Dissolved Potassium (K) 2008/04/03 92 % Dissolved Silicon (Si) 2008/04/03 87 % Dissolved Sodium (Na) 2008/04/03 96 % Dissolved Strontium (Sr) 2008/04/03 89 % SPIKE Dissolved Sulphur (S) 2008/04/03 96 % BLANK Dissolved Aluminum (Al) 2008/04/03 <0.04 mg/l Dissolved Barium (Ba) 2008/04/03 <0.01 mg/l Dissolved Boron (B) 2008/04/03 <0.02 mg/l Dissolved Calcium (Ca) 2008/04/03 <0.3 mg/l Dissolved Chromium (Cr) 2008/04/03 <0.01 mg/l Dissolved Iron (Fe) 2008/04/03 <0.06 mg/l Dissolved Lithium (Li) 2008/04/03 <0.02 mg/l Dissolved Magnesium (Mg) 2008/04/03 <0.2 mg/l Dissolved Manganese (Mn) 2008/04/03 <0.004 mg/l Dissolved Phosphorus (P) 2008/04/03 <0.1 mg/l Dissolved Potassium (K) 2008/04/03 <0.3 mg/l Dissolved Silicon (Si) 2008/04/03 <0.1 mg/l Dissolved Sodium (Na) 2008/04/03 <0.5 mg/l Dissolved Strontium (Sr) 2008/04/03 <0.02 mg/l Dissolved Sulphur (S) 2008/04/03 <0.2 mg/l RPD Dissolved Barium (Ba) 2008/04/ % 20 Dissolved Boron (B) 2008/04/03 NC % 20 Dissolved Calcium (Ca) 2008/04/ % 20 Dissolved Iron (Fe) 2008/04/03 NC % 20 Dissolved Lithium (Li) 2008/04/03 NC % 20 Dissolved Magnesium (Mg) 2008/04/ % 20 Dissolved Manganese (Mn) 2008/04/03 NC % 20 Dissolved Phosphorus (P) 2008/04/03 NC % 20 Dissolved Potassium (K) 2008/04/ % 20 Dissolved Silicon (Si) 2008/04/ % 20 Dissolved Sodium (Na) 2008/04/ % 20 Dissolved Strontium (Sr) 2008/04/ % 20 Dissolved Sulphur (S) 2008/04/ % 20 NC = Non-calculable RPD = Relative Percent Difference Page 7 of 7
Appendix C: Water Quality Data
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