Application Data Sheet for Polypropylene (PP)
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1 FR-20 Magnesium hydroxide [Mg(OH)2] Application Data Sheet for Polypropylene (PP) FR-20, a series of high purity grades magnesium hydroxide, is offered by ICL-IP as inorganic halogen free flame retardants (FR) recommended where use of halogenated products is limited or prohibited. FR-20 is particularly suitable for use with PP. As a result of its chemical nature, high purity and excellent thermal stability (Table 1 and 2), FR-20 exhibits inherent advantages over other halogenated free FR additives currently used for the same applications. Table 1: Properties of FR-20 FR-20 grade S5 S7 S10 CAS Number Assay, w% 99.6 Specific gravity 2.36 Molecular weight 58.3 Bulk density, g/ml Particle size, µm: (Malvern Mastersizer 2000) D D 90 < 6 Surface area (BET), m 2 /g Grades with special surface treatments to optimize processability and properties are recommended with PP applications.
2 The use of FR-20 is advantageous when the following properties are required: halogen-free flame retardancy low and non-toxic smoke high thermal and long term heat aging stabilities dimensional stability after injection molding acid scavenger and heat stabilizer reinforcing filler improving tracking index Thermal stability FR-20 has a high thermal stability up till C and its use is recommended where alumina trihydrate (ATH) is not sufficiently stable. Thermogravimetric analysis of FR-20 (Table 2) reflects its high thermal stability allowing high processing temperatures typical to PP. Its thermal stability combined with excellent resistance to degradation, makes it a product of choice when recycling is an issue. Table 2: Thermo gravimetric analysis (TGA-10 0 C/min in air) Weight loss, % Temperature, 0 C
3 Excellent smoke suppressant FR-20 is also a powerful smoke suppressant and it is one of its main advantages over halogen- and antimony- based FRs. Halogen based PP compounds burn with intense black smoke leading quickly to high values of smoke density in a NBS chamber (Figure 1). On the contrary, PP compounds flame retarded by FR-20 are generating very little quantities of smoke Figure 1: Smoke optical density of V-0 PP (NBS smoke chamber - ASTM E Flaming mode) Br FR + Sb2O3 (no FR-20) Optical density, DM Ref no FR 0 62% FR-20 (no Br FR) Time, min Surface treatment In order to cope with the high loadings needed to get class V-1 or V-0, surface treated grade FR is preferred for extrusion and injection moulding applications of PP. FR has indeed a good contribution to improve melt flow during injection molding (Figure 2).
4 Figure 2: Influence of surface treament on MFI (PP homo V-0 with 62% FR-20; 230 C kg) MFI, % PP ref. PP + FR PP + FR-20 untreated Processing conditions Tables 3 provides indicative formulations enabling to get class V-0 (1.6mm) with PP homo- and block copolymers flame retarded by FR and their properties. It may be advisable to feed FR in two steps: Circa 40% in the feeding zone The rest, 20-25%, at the end of the second third of the extruder via a sidefeeder. Typical processing conditions to compound and mold PP flame retarded with FR are as follow: Compounding: Compounding in a co-rotating twin-screw extruder (L/D = 32) Temperature profile, 0 C: Screw speed, Rpm: 430
5 Injection molding Temperature profile, 0 C Mold temperature, 0 C 80 Properties Properties achievable in PP homo- and block copolymers are summarized in Table 3. Applications The range of applications for FR in PP is very wide: E & E: switches, wire and cables, connectors Automotive: under the hood electrical parts, wire and cables, trimmings and cover panels Building: thermal insulation foam, panels, sheets, ceiling parts and films
6 Table 3: Properties of PP flame retarded by FR S-7 Type of PP PP Homo PP Block copo Ref. no FR FR Ref. no FR FR Composition, w%: PP FR Properties: Flame retardancy: UL 94 (3.2mm), class NR V-0 NR V-0 LOI MFI, g/10 min (230 0 C; 2.16kg) Tensile: Max. strength, MPa Elongation at break, % Modulus, MPa Impact IZOD notched, J/m
7 For further advice and assistance, contact our representatives in your area: Head Office ICL-IP Ltd. Phone: Fax: frinfo@icl-ip.com North America and Mexico ICL-IP America Inc. Asia Pacific China Phone: ICL China Fax: fr.nam@icl-ip.com Phone: Fax: South America fr.china@icl-ip.com ICL Brasil Ltda Japan Phone: ICL-IP Japan Ltd Fax: fr.sam@icl-ip.com Phone: Fax: Europe fr.japan@icl-ip.com Main Office Asia Pacific ICL-IP Europe B. V. ICL Asia Ltd Phone: Fax: Phone: fr.europe@icl-ip.com Fax: fr.asia@icl-ip.com Italy Other Parts of the World PM Chemicals Italy ICL-IP Sales Office Phone: Fax: Phone: fr.it@icl-ip.com Fax: fr.row@icl-ip.com Tecnet
Application Data Sheet for Polypropylene (PP)
FR-20 Magnesium hydroxide [Mg(OH)2] Application Data Sheet for Polypropylene (PP) F-37 FR-20, a series of high purity grades magnesium hydroxide, is offered by ICL-IP as inorganic halogen free flame retardants
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