Table of Contents. Quality Management LIMS System... Customer Services...
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- Barnard Pope
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1 2013 Price List
2 Inside Front
3 Inside Back
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5 Table of Contents Quality Management LIMS System... Customer Services... MINING SERVICES... Metallurgical Sample Receiving... Sample Pickup... Sample Submittal... Metallurgical Sample Preparation... Preparation... Extra Handling Charges... Sample Storage... Analytical Testing... Fire Assay... Geochemical Scans... Digestions... ICP-OES Scans... Individual Elements, ICP Element ICP Scans, Low to Medium Range Element ICP Scans, Trace Geochemistry... ICP-MS Element ICP Scans, Trace to Ultra-trace Geochemistry... ICP-MS Rare Earth... Mercury in Mine Sample by CVAFS... Mercury... Carbon and Sulfur by LECO... LECO... Ore Grade Assays... Flame Atomic Absorption (AA)... FAAS... Wet Chemistry... ENVIRONMENTAL SERVICES Sample Preparation... Analytical Services... Trace Metals by ICP-OES... EPA Toxicity Characteristic Leaching Procedure (TCLP)... & Synthetic Precipitation Leaching Procedure (SPLP)... Trace Metals by ICP-MS... Environmental Mercury by CVAFS... Anions... Acid-base Accounting... Additional Environmental Parameters...
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9 Quality Management American Analytical Services is committed to providing our customers with the highest quality analytical results. American Analytical Services, Inc. s metallurgical lab is ISO (Testing and Certification laboratory) certified. American Analytical Services, Inc. participates in wastewater pollution studies biannually and has had a minimum 90% passing score dating back to These WP study results place American Analytical Services, Inc. in compliance with the State of Washington Department of Ecology provisions set forth in Chapter WAC and is recognized by the Department of Ecology as an accredited laboratory for the analytical parameters listed on the Scope of Accreditation. The environmental laboratory is currently pursing Department of Defense environmental laboratory certification. This certification will meet and exceed NELAC standards. Expected completion of certification is spring American Analytical Services, Inc. is also in the process of applying to the State of Idaho for Drinking Water Certification. AAS has been audited by both public and private auditors insuring clients of our ability to match results with both internal and 3rd party laboratories. AAS met all tolerances of the tests performed. LIMS System: AAS is proud to introduce Perkin Elmer s Labworks LIMS into the laboratory in December The addition of a LIMS system will allow us to provide enhanced customer service by better tracking sample movement through the laboratory, optimizing work flow, and tracking quality control measures in real time. 5
10 Customer Services: American Analytical Services provides customers with superior customer service. As a small laboratory, we are able to respond quickly to the specific needs of our customers. We employ a full time customer service representative, Mary Jacobson, who is glad to address your concerns, large or small. Our laboratory and quality staff members are also available to answer any technical questions you have. AAS strives to be sure that our customers are fully satisfied. To better serve our clients, there are absolutely no hidden fees. You pay to have your sample prepared, digested, and analyzed; AAS does not charge reporting, check-in, or handling fees. All other charges (wet samples, overweight, long-term storage, etc. are noted in this price list). If you have any questions or concerns regarding pricing, please contact our customer service agent. AAS offers a standard two week turnaround from the date samples arrive in our lab. Rush returns of one-week or 48-hours are available for increased cost. Please contact the lab with samples that will require 48-hour turn around; this allows us to plan to fit your samples into our work flow. AAS also offers contract or bulk discounts for larger or recurring sample submittals; contact Mary Jacobson for details. Sample Submittal: Samples can be shipped to Silver Valley Road, Osburn, ID Samples should be accompanied by a chain of custody that includes customer name, address, phone number and analyses requested. Rush samples require prior approval from AAS. A blank chain of custody is included in the back of this booklet. Sample Pickup: AAS can arrange to pick up samples from our clients. Our pricing for sample pickup is based on AAS s cost to perform the pickup. For more information or to discuss pricing, please contact customer service. Service Sample pickup Price Price on request 6
11 Additional Environmental Parameters: AAS provides a range of environmental services. If your project requires a test not listed please contact us and we will make every effort to accommodate you. Parameter Reference Method Price, Soil Price, Water Acidity SM 2310 B na 15 Alkalinity, total SM 2320 B na 15 Alkalinity, CO3, HCO3, OH SM 2320 B na 25 Ammonia SM/EPA 4500/ Cation exchange capacity (CEC) ASA Mono 9 50 na Chlorine, free Hach na Chlorine, total Hach na Color na 15 Conductivity SM/EPA 2510 B/ Cyanide, total SM/EPA 4500 D F Cyanide, WAD SM 4500 C I Cyanide, amenable to chlorination na 75 Dissolved oxygen Hach na Fluoride SM/EPA 4500 F/ Hardness, total (as CaCO3) SM/EPA 2340 B/200.7 na 15 Hexavalent chromium Hach na Loss on ignition/organics EPA na Moisture (% solids) SM 2540G 15 na Carbon Soil I-LECO-06/ Oil & grease EPA na Orthophosphate Hach ph SM/EPA 4500 H/150.1/ Resistivity AASHTO T na Sieve analysis C117 & C na Solids, settleable EPA na 20 Solids, total EPA na 15 Solids, total dissolved SM/EPA 2540 C/160.1 na 15 Solids, total suspended SM/EPA 2540 D/160.2 na 15 Solids, total volatile EPA na 25 Specific gravity, soil Total Kjeldahl (TKN) EPA Thiocyanate EPA 300.0M na 50 Turbidity EPA na 15 23
12 Acid-base Accounting Acid-base accounting is performed to determine if waste rock has the ability to leach acids that might be damaging to the environment. Samples are measured for acid producing potential and for neutralization potential. Acid producing potential is determined from the total sulfur content. Neutralization potential is calculated by back titration with NaOH. There are varying levels of complexity to ABA that account for a variety of assumptions. Selection of method is usually based on the mineralogy of the rock. Consistent use of a single method within a project is important for internal comparability. There are varying levels of detail and consideration in ABA. The most basic is using total sulfur to determine AP. Additional analyses to determine the sulfur speciation can provide a more complete picture of the true acid producing potential of a sample. The use of the modified neutralization potential of Lawrence or the siderite correction of Skousen can provide a more accurate picture of the neutralization potential (NP) depending on the mineralogy of the sample. Test Reported parameters Price ABA-01: Net neutralization potential Net Neutralization Potential (NNP) $73.30 based on total sulfur Acid potential (AP) Neutralization potential (NP) NP:AP ratiov Paste ph ABA-01 with Lawrence NP Skousen correction ABA-02: Net neutralization potential Same as ABA-01 plus: based on total sulfur, HCl-leachable HCl leachable sulfate sulfate, and sulfide. Sulfide ABA-02 with: Lawrence NP Skousen correction ABA-03: Net neutralization potential Same as ABA-02 plus based on total sulfur, total sulfate, Total sulfate (carbonate leach) and sulfide. ABA-03 with: Lawrence NP Skousen correction ABA-04: Net neutralization potential Same as ABA-02 plus: based on total sulfur, HCl-leachable Inorganic Carbon (CO2) sulfate, and sulfide ABA-04 with: Lawrence NP Skousen correction ABA-05: Net neutralization potential Same as ABA-02 plus: based on total sulfur, total sulfate, Total sulfate (carbonate leach) sulfide and inorganic carbon. Inorganic Carbon (CO2) ABA-05 with: Lawrence NP Skousen correction
13 MINING SERVICES Metallurgical Sample Receiving AAS follows strict protocols to ensure that a representative sub-sample of each submission will be used for analysis. The rejected portion of the sample is returned to the original sample bag, saved and returned to the client. Between samples, barren rock is run through the crushing equipment to clean the crushers, and a sample preparation blank is run with the client s samples. During pulverization, silica sand is used between each sample to clean bowl and rings to prevent salting of samples. The pulp is placed in sample envelopes for the client s archiving purposes. Metallurgical Sample Preparation Overweight samples (>10 lbs) will incur a $10 surcharge. Excessively wet samples may be delayed due to increased drying time. Medium technique Method Price Rock or Core Dry, jaw, and cone crush to SP-M-01 $6 10 mesh, rings pulverize to 140 mesh (250 g) Soil / Sediment Dry and sieve to 80 mesh SP-S-02 $5 Soil / Sediment Dry and sieve to 80 mesh, SP-S-02 $8 save +80 fraction Extra Handling Charges Occasionally samples require extra handling and these services are priced as follows. If you have any questions regarding these charges, feel free to contact the lab. Handling Method Price Excessively wet samples Extra drying time $5/every 24 hours Composites $40/hour Splitting $40/hour 7
14 Sample Storage Samples submitted are stored free of charge for 30 days. Handling Long term sample storage Price price on request Analytical Testing: Ore Grade Assays: Fire Assay AAS is highly experienced in the use of fire assay to determine precious metals content. Our experience allows us to expediently handle a variety of sample types and yield accurate results. Gravimetric fire assay is used for ore grade material, while fire assay with an ICP finish is utilized for exploration and low level samples. Parameter technique Method Price Gold Fire Assay, Gravimetric FA-Ag/Au-01 $20 Silver Fire Assay, Gravimetric FA-Ag/Au Gold and Silver Fire Assay, Gravimetric FA-Ag/Au Gold and Silver Fire Assay, ICP Finish FA-ICP Gold and Silver (CN Solutions) Fire Assay FA-CN Gold and Silver (CN Solutions) Fire Assay, ICP Finish FA-CN-ICP Gold and Silver (Carbons) Fire Assay, Gravimetric FA-Au-C Gold and Silver (Bullion) Fire Assay, Gravimetric FA-Au-B Palladium Fire Assay, ICP Finish FA-ICP Platinum Fire Assay, ICP Finish FA-ICP Rhodium Fire Assay, ICP Finish FA-ICP PGMs (palladium, platinum, rhodium) Fire Assay, ICP Finish FA-ICP
15 Anions: AAS purchased a new Metrohom Anions Ion Chromatography (IC) instrument in We can measure any of the anions in EPA method parts A & B. Parameter Reference Method Price / A & B EPA $ / 300.1A EPA A / 300.1B EPA B 40 Bromide EPA A 10 Chloride EPA A 10 Floride EPA A 10 Nitrate EPA A 10 Nitrite EPA A 10 Ortho-phosphate, P EPA A 10 Sulfate EPA A 15 Bromate EPA B 15 Chlorate EPA B 15 Chlorite EPA B 15 21
16 Parameter Reference Method Price Cu - Copper EPA Pb - Lead EPA Mn - Manganese EPA Mo - Molybdenum EPA Ni - Nickel EPA Se - Selenium EPA Ag - Silver EPA Tl - Thallium EPA Th - Thorium EPA U - Uranium EPA V - Vanadium EPA Zn - Zinc EPA Environmental Mercury by CVAFS: AAS measures mercury by Cold Vapor Atomic Fluorescence Spectroscopy (CVAFS) via a Teledyne Leeman Hydra AF+ instrument. Using low level detection, AAS can measure to about 0.01 ppb. Parameter Reference Method Reporting Limit Price Mercury EPA / ppb $35 Mercury (low level) EPA / ppb 70 20
17 Metallic Screen (Native Gold) To analyze samples containing free gold, a metallic screen should be performed to decrease the possibility of anomalously high or low results. After a sample suspected to contain free gold is pulverized, it is screened. The free gold portion of the sample (the plus fraction ) will be fire assayed in its entirety while two samples from the minus fraction will be fired. The final result provided to the client will represent the composite of these three assays. Technique Metallic Screen plus fire assay Price $100 plus cost of fire assay A 48-hour turnaround is not available for metallic screens. Please contact the lab for 1 week options. 9
18 Wet Chemistry Ore grade assays (volumetric and gravimetric techniques) are used for highly accurate characterization of concentrates and ores that exceed the range of other instrumentation within reasonable dilution limits. Parameter technique Method Price Sb - Antimony Volumetric Vol-Sb-02 $30 As - Arsenic Volumetric Vol-As Cu - Copper Volumetric Vol-Cu Fe - Iron Volumetric Vol-Fe Pb - Lead Volumetric Vol-Pb Silicates (Insolubles) Gravimetric Grav-Si S - Sulfur (Total) Gravimetric Vol-S Zn - Zinc Volumetric Vol-Zn
19 Parameter Reference Method Price Ti -Titanium EPA V - Vanadium EPA Zn - Zinc EPA Toxicity Characteristic Leaching Procedure (TCLP) & Synthetic Precipitation Leaching Procedure (SPLP) Parameter Reference Method Price TCLP EPA 1311 Extraction Required for all analyses $25 Complete suite Ag, As, Ba, Cd, Cr, Pb, Se, Hg 95 Metals suite Ag, As, Ba, Cd, Cr, Pb, Se 70 Mercury Hg 25 Individual metals 10 SPLC EPA 1312 Extraction Required for all analyses 25 Complete suite Ag, As, Ba, Cd, Cr, Pb, Se, Hg 95 Metals suite Ag, As, Ba, Cd, Cr, Pb, Se 70 Mercury Hg 25 Individual metals 10 Trace metals by ICP-MS EPA methods (water) and EPA 6020 (soils) are designed to measure trace environmental metal contaminants. The ICP-MS is capable of measuring at much lower levels than the ICP- OES. This method is approved to meet many requirements of the Clean Water Act (NPDES) and the Safe Drinking Water Act (SDWA), check with your specific requirements. Parameter Reference Method Price Suite EPA $150 Al - Aluminum EPA Sb - Antimony EPA As - Arsenic EPA Be - Beryllium EPA Cd- Cadmium EPA Cr - Chromium EPA Co - Cobalt EPA
20 Analytical Services: American Analytical is a full service environmental laboratory. Commonly performed analyses are listed here but if your company requires a service not listed, please contact us and we ll be happy to accommodate your needs. Trace metals by ICP-OES EPA EPA methods (water) and 6010 (soils) are designed to measure trace metal contamination in environmental samples. This method is approved to meet many requirements of the Clean Water Act (NPDES) and the Safe Drinking Water Act (SDWA). Check with your specific regulatory requirements. Parameter Reference Method Price Suite (28 elements) EPA $120 Al - Aluminum EPA Sb - Antimony EPA As - Arsenic EPA Ba - Barium EPA Be - Beryllium EPA B - Boron EPA Cd - Cadmium EPA Ca - Calcium EPA Cr - Chromium EPA Co - Cobalt EPA Cu - Copper EPA Fe - Iron EPA Pb - Lead EPA Mg - Magnesium EPA Mn - Manganese EPA Mo - Molybdenum EPA Ni - Nickel EPA P - Phosphorus, Total EPA K- Potassium EPA Se - Selenium EPA Ag - Silver EPA Na - Sodium EPA Sr - Strontium EPA Tl - Thallium EPA Sn - Tin EPA
21 Flame Atomic Absorption (AA): AA is used for relatively high-concentration/ore-grade samples. This method will give accurate results in the percentage range for silver and most base metals. FAAS i-faas-01 Per Element Six elements suite: $10.00 $35.00 Element Reporting Limit upper Limit Ag Silver oz/ton Bi Bismuth % Cu Copper % Fe Iron % Pb Lead % Sb Antimony % Zn Zinc % 11
22 Geochemical Scans: ICP-OES Scans ICP-OES can be used to obtain a geochemical profile of samples collected in mining exploration. A basic ten-element package or a comprehensive thirty-five element package can be selected, based on a client s analytical needs. Clients may also create a custom package by working with customer service. All ICP Scan prices include digestion. Data from the Aqua Regia digestion represent the leachable portion of samples (although many base metals may dissolve entirely). Aqua Regia does not digest silicates. For a more complete digestion, we recommend the four acid digestion; this technique will completely dissolve most materials. Special Digestions: Some materials may require alternate digestions such as fusions for complete digestion at high concentrations. Special digestions for elements not fully recovered by Aqua Regia or 4-Acid Digestion at high concentrations (Tungsten, Niobium, et al.) are billed hourly at $35/ hour. ICP-OES Scan Options: Individual Elements, ICP Aqua Regia Digestion SD-01-ICP 4-Acid Digestion SD-4A-ICP $15 $22 Designed to meet the needs of working mines, the 12 Element ICP Scan offers a cost-effective way to characterize the content of mine samples. The samples are highly diluted, allowing higher concentrations to be analyzed. 12
23 Carbon and Sulfur by LECO AAS offers analysis by LECO s Infrared Radiation (IR) spectrometer specially designed to accurately analyze both low and high ranges of carbon and sulfur. LECO Element Method Reporting Limit (%) Price C & S Carbon & sulfur I-LECO $22.80 C Carbon I-LECO S Sulfur I-LECO ENVIRONMENTAL SERVICES Sample Preparation: Soil samples require preparation before they are sent to the environmental lab for analysis. Soil samples are dried in a dedicated oven to prevent contamination from mining samples. Water and soil digestion is required for instrumental analysis by ICP, ICP-MS and CVAFS. Parameter Reference Method Price Water Digestion SM 3005, 3010, 3052 $7 Soil Digestion SM/EPA 6010 B/ Soil Prep 80 mesh SM/EPA 6010 B/ Air Filters EPA 40CFR, part50, appg 7 17
24 ICP-MS Rare Earth MS-4A-RE $37.00 Element Reporting Limit (ppm) Ce- Cerium 1.00 Dy Dysprosium 1.00 Er Erbium 1.00 Eu - Europium 1.00 Gd Gadolinium 1.00 Hf Hafnium 5.00 Ho Holmium 1.00 La Lanthanum 1.00 Lu Lutetium 1.00 Nb Niobium 2.00 Nd Neodymium 1.00 Pr Praseodymium 1.00 Rb - Rubidium 1.00 Sm Samarium 2.00 Sn Tin 1.00 Ta Tantalum Tb Terbium 1.00 Th Thorium Tm Thulium 2.00 W - Tungsten 1.00 U Uranium Y Yttrium 1.00 Yb Ytterbium 2.00 Zr- Zirconium 1.00 Mercury in mine samples by CVAFS AAS uses Cold Vapor Atomic Fluorescence Spectroscopy (CVAFS) to detect ultra-trace levels of mercury. Mercury Element Method Reporting Limit (ppb) Price Hg Mercury I-CVAFS $12 16
25 12 Element ICP Scans, Low to medium range Aqua Regia Digestion SD-01-ICP $30.00 Element Reporting Limit (ppm) Upper Limit of Method As - Arsenic % Bi - Bismuth % Cd - Cadmium % Co - Cobalt % Cu - Copper % Fe - Iron % Mn - Manganese % Ni - Nickel % Pb - Lead % S - Sulfur % Sb - Antimony % Zn - Zinc % The 35 element scan is geared for samples taken from exploration and measures a wide range of trace element concentrations for a cost-effective way to broadly characterize a sample. 35 Element ICP Scans, Trace Geochemistry Aqua Regia Digestion SD-01-ICP 4-Acid Digestion SD-4A-ICP $20.00 $28.00 Element Reporting Limit (ppm) Al - Aluminum 50.0 As - Arsenic 5.00 Ba Barium 1.00 Be - Beryllium 1.00 Bi - Bismuth 5.00 Ca - Calcium 50.0 Cd - Cadmium 1.00 Ce Cerium 5.00 Co Cobalt 2.00 Cr - Chromium 2.00 Cu - Copper 2.00 Fe Iron 5.00 Ga Gallium 5.00 K - Potassium 50.0 La - Lanthanum
26 14 35 Element ICP Scans, Trace Geochemistry con t. Aqua Regia Digestion SD-01-ICP 4-Acid Digestion SD-4A-ICP Element $20.00 $28.00 Reporting Limit (ppm) Li Lithium 2.00 Mg - Magnesium 50.0 Mn - Manganese 2.00 Mo - Molybdenum 2.00 Nb - Niobium 5.00 Ni Nickel 2.00 P - Phosphorous 50.0 Pb Lead 5.00 S Sulfur 50.0 Sb - Antimony 5.00 Sc - Scandium 2.00 Sn Tin 5.00 Sr - Strontium 1.00 Ti - Titanium 5.00 V - Vanadium 2.00 W - Tungsten 5.00 Y Yttrium 2.00 Zn Zinc 2.00 Zr - Zirconium 2.00 ICP-MS ICP-MS is useful for trace-level geochemical scans in soils, sediments, or other samples that require a very low detection limit. 48 Element ICP-MS Scan, Trace to ultra-trace geochemistry ICP-MS-48 $42.00 Element Reporting Limit (ppm) Ag Silver 1.00 Al Aluminum 50.0 As Arsenic 1.00 Ba Barium 1.00 Be Beryllium 1.00 Bi Bismuth 10.0 Ca Calcium 50.0 Cd Cadmium 1.00 Ce Cerium 1.00
27 Element Reporting Limit (ppm) Co Cobalt 1.00 Cr Chromium 1.00 Cs Cesium 1.00 Cu Copper 1.00 Fe Iron 50.0 Ga Gallium 1.00 Ge Germanium 1.00 Hf - Hafnium 5.00 In Indium 1.00 K - Potassium 50.0 La Lanthanum 1.00 Li Lithium 1.00 Mg Magnesium 50.0 Mn Manganese 1.00 Mo Molybdenum 1.00 Na Sodium 50.0 Nb Niobium 2.00 Ni Nickel 1.00 P Phosphorous 50.0 Pb Lead 5.00 Rb Rubidium 1.00 Re Rhenium 1.00 S Sulfur 50.0 Sb Antimony 1.00 Sc Scandium 1.00 Se Selenium 1.00 Sn Tin 1.00 Sr Strontium 1.00 Ta Tantalum 10.0 Te Tellurium 1.00 Th Thorium 10.0 Ti Titanium 1.00 Tl Thallium 10.0 U Uranium V Vanadium 1.00 Y Yttrium 1.00 Zn Zinc 5.00 Zr Zirconium
28 Quality, customer focused analytical results since Silver Valley Road PO Box 748 Osburn, Idaho Phone: Fax:
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