Closed Cycle Cryostat Optical Cryostat for High cooling power and Ultra Low Vibration experiments.

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1 Closed Cycle Cryostat Optical Cryostat for High cooling power and Ultra Low Vibration experiments. DMX-20, ULV Interface. Cryostat Models (Cryocooler min. temperature): cs204a-x20 <9K cs204a(t)-x20 <9K Turbo For fast cooldown. cs204n-x20 <6K cs204s-x20 <4K Applications: High Cooling power for: Mossbauer Experiments Low Vibration Optical Experiments, SQUID Quantum Dot Photoluminescence, MicroRaman, Micro PL. Micro- Spectroscopy. Kerr Effect (MOKE), Ellipsometry. Design Features: Sample is isolated from cryocooler by soft rubber bellows (at room temperature) and helium exchange gas. See specifications for vibration level. Vibration level at sample with proper isolation is 3 to 5 Nanometers at 2.4 Hz. No line width broadening with proper installation. Sample temperature will be ~1-2K higher than the cryocooler temperature. Cooldown time of the interface is between 2.5 and 3 Hrs. 2 Window ports. (Optional 4 ports) Window materials for Mossbauer (Beryllium) or optical spectroscopy (Vis, UV,IR windows available. Compact optical shroud. Optical View = f 1.4 (1.75 in./1.25 in.) Sample space; 1.9 in. (ID) * 1.5 inches long. Sample in vacuum. Vacuum Shroud; Rotatable under vacuum. Double O-ring. Sample Holder, two component with groove for indium wire for improved thermal contact with sample. Metallized thermofoil heater for long heater life. One Instrumentation Port for temperature control instrumentation. Additional ports using T adapters DE-204AF with DMX-20 interface installed. vacuum shroud and radiation shield also shown. Cryocooler Specifications at 60 Hz. Cryo-cooler Model: DE-104(T) DE-204A DE-204A (T) DE-204N DE-204S Compressor Model. ARS-4HW ARS-4HW ARS-4HW ARS-4HW ARS-4HW Temperature Range <25K-350K <9K -350K <9K-350K <6K 350K <4K 350K Sample Temperature ~25K ~ K ~ 10-11K ~ 7-8 K ~ 5-6 K Cooling Power (2 nd Stage) 2 Watts/10K 2.7 Watts/10K 3 Watts/10K 0.2 Watts/4K 9 Watts /20K 12 Watts /20K 8 Watts /20K 8 Watts /20K Cooling Power (1 st Stage) 60 Watts/77K 18 Watts/77K 24 Watts/77K 18 Watts/77K 18 Watts/77K Vibrations at sample 3 to 5 nm Same Same Same Compressor Maintenance 12,000 Hrs. Ambient, Operating 12 C 40 C (54 F F) System Weight: Cryo-cooler 7.5 Kg. Compressor 73 Kg. Power Requirements: V, 60 Hz V, 50 Hz. Optional: 230V or 240V, 50 Hz. (With optional transformer) Notes: Hz operation will have reduced performance, see specifications for details. 2. These specifications (Except sample temperature and vibration data) are for the cryocooler only. Actual performance will depend on parasitic and experimental heat loads.

2 DE204/DE202 VIBRATION ISOLATION BELLOWS Instrumentation Ports: Typically 1 instrumentation port is supplied for 10 pin connector for tempewrature control temperature control instrumentation, installed at factory. For additional wiring, ARS offers T adaoters or additional welded ports as an option. 10-PIN FEEDTHROUGH ROTATABLE DOUBLE O-RING SEAL 3.38 UPPER VACUUM SHROUD DMX20 INTERFACE UPPER RADIATION SHIELD O-RING SEAL FOR REMOVABLE LOWER SHROUD 1.24 REMOVABLE LOWER RADIATION SHIELD OPTICAL RING SAMPLE HOLDER REMOVABLE LOWER VACUUM SHROUD Drawing showing the DMX-20 and vacuum shroud installed for optical or Mossbauer experiments. Windows are available for UV, Vis, IR experiments.

3 Mossbauer Spectra with DMX-20. Cryocooler Off: Fe cal T=RT (compressor off) 1.00 Cryocooler On. Fe cal T=10K (compressor on) 1.00 Relative transmission Relative transmission Velocity [mm/s] Velocity [mm/s] Calculated parameters: WID=0.269 mm/s W13=1.17 W23=1.08 ISO=0.000 mm/s BHF=32.94T Calibration spectrum: Measurement with metallic iron foil (thickness 25 μm) at room temperature (T=RT), compressor off Calculated parameters: WID=0.270 mm/s W13=1.21 W23=1.11 ISO= mm/s BHF=33.81T Calibration spectrum: Measurement with metallic iron foil (thickness 25 μm) at 10K (T=10K), compressor on When the system is properly mounted to the wall and the table and properly adjusted then the effect of vibrations induced by the working compressor is very small (almost negligible). The broadening (rather no broadening!) is fully reproducible and is well below 2%. Such broadening has practically no effect and in almost all cases can be ignored. However, compare the linewidths calculated in the same way! The Displex system is virtually vibration free! Prof. Dr. habil. Michal Kopcewicz Institute of Electronic Materials Technology WARSAW, Poland Mossbauer Cryostat, DMX-20 Prof. Dr. habil. Michal Kopcewicz

4 Vibration Spectra of DMX-20 Interface. Vibration level at the sample is 3 Nanometers at 2.4 Hz. The vibrations at the sample are in the range of 3-5 Nanometers at 2.4 Hz (60 Hz power supply). The vibrations from the cooler are isolated from the sample mount. Additional care is needed to minimize vibrations to the table from the floor. The picture shows the Displex and its interface. All items showing stainless steel in the photo are modifications to our JSM-5910 SEM. Please also note the published papers on my website, which demonstrate CL results that were acquired with this cooling system. The sample temperature, is between 40 K and 50 K. Courtesy; Prof. Dan Rich, Ben Gurion University, Beer Sheva, Israel. Image of a InGaN/GaN quantum well grown on a patterned GaN substrate. The patterning consists of stripes with a periodicity of 10 microns. Monochromatic CL image (Mag. 2000) taken with a 390 nm detection wavelength. The degradation of image quality from room temperature and 50K suggests that the vibration is less than 10nm. Courtesy; Prof. Dan Rich, Ben Gurion University, Beer Sheva, Israel.

5 Elastomeric Isolator at the cryocooler. DISPLEX CRYOCOOLER WITH LOW VIBRATION INTERFACE Low Vibration Table Transducer Detector Counter OPTICAL AXIS CRYOCOOLER STAND Elastomeric Isolators (qty. 4) Compact Air Mount, Low Vibration Legs. (qty. 4) Granite Plate 24" x 24" x 3" thk. (recommendation. reference only) For maximum isolation proper mounting of the system is important. ARS offers a special ULV stand to isolate the ultra low vibration cryostat from the vibrating components of the cooler and the floor vibrations. The cryocooler stand can be adjusted for the proper height, this holds the cooler. The cryostat is mounted on the low vibration table. which consists of a high mass granite block (User supplied), resting on 4 air legs (optional ARS offering). Additional elastomeric isolators additional filter the unwanted frequencies from the floor to the cryostat. System can be tested by shutting off the cryocooler only and watching the vibration effect on the experiment. DMX-20 for MicroRaman. DMX-20 for UHV (Bakeable to 200C) DE 202 or DE-204 Series Cryocoolers. He GAS INLET PORT (FITTINGS NOT SHOWN) PLCS BELLOWS, Soft Rubber TYP 2 PLCS Ø "* NONROTATABLE OR 6" OR 8" ROTATABLE CONFLAT 2 1/4-20 THD Ø 1.60 RAD. SHIELD 1.93 OD X.03 WL (NICKEL PLATED OFHC COPPER) Ø0.81 X.12 DP. C'BORE 1/4-28 THD. X.25 DP. Ø1.12 THRU 2 SIDES DMX-20 for Micro-Spectroscopy is shown on the left. Sample temperature as low as 8K can be expected DMX-20 for UHV. The cryostat can be removed during bakeout.

6 Direct Mounting: Understanding the ULV (DMX-20) Interface. Helium Gas. Static supply. Cryocooler, Pneumatic Drive. Mounted on a floor stand. Soft rubber bellows, minimize the vibrations transmitted to DMX-20 and sample, they keep the helium exchange gas DMX-20. Has no mechanical contact with the Cryocooler except the rubber bellows. Cold Tip of cryocooler has mechanical vibrations. No mechanical contact with the sample Helium Exchange gas gets cold and cools the sample Sample is installed on the DMX- 20. Has vibration in the 3-5 Nanometers at 2.4Hz. coming from the cryocooler. Windows for optical experiments Optical Table. Vibration isolated. DMX-20 can be direct mounted on the Cryocooler. The vibrations at the sample will go up to 140 nm. It can be useful if the sample has to be translated in XYZ. The ARS Low Vibration Closed Cycle Cryostat consists of two components: 1. The Closed Cycle Cryo-cooler determines the sample temperature. Typical vibrations of this cooler are microns. The Cryocooler is shown in red in the above sketch.. 2. The DMX-20 low vibration interface is not mechanically connected to the cryocooler. The thermal contact is through a helium exchange gas at the bottom of the DMX-20. The system has a sophisticated and patented heat transfer hardware at the bottom of the cryocooler but there is no mechanical contact. The space between the Cryo-cooler and the DMX-20 is filled (static, not continuous flow) with helium gas. 3. The soft rubber bellows contain the helium between the DMX-20 and the Cryo-cooler. The bellows are at room temperature and remain soft during operation, thus preventing vibrations from being transmitted to the DMX-20 and the sample. Cryocooler mounting Stand. Variable height.

7 DMX-20 for Magneto Electrical Experiments DMX-20 for Magneto Electrical Experiments DMX20B with 6" CF #990175A " CF (ref.) SHCS, SS, #5/16-24 x 2.25 long McMaster Carr#92196A354 (qty. 16) Plate Nut, K. Lesker# PN-0600 (qty. 8) #072028A Upper Vac. Shroud # Upper Rad. Shield SHCS, Brass, #4-40 x.50 long McMaster Carr#93465A110 (qty. 6) Lock Washer, Bronze,#4 McMaster Carr#93496A405 (qty. 6) # P5 Extension Indium foil O-Ring #2-036 SHCS, St. St., #4-40 x.25 long (qty. 6) Lock washer, #4 (qty. 6) 6.96 [177] #072029A Lower Vac. Shroud 4.97 [126] 1.06 [27] ID 1.57 [40] 1.50 [38] OD 3.25 [83] #072030A Lower Rad. Shield The vacuum shroud becomes narrow to permit sample insertion into a small magnet pole space. The vacuum shroud becomes narrow to permit sample insertion into a small magnet pole space. DMX-20 for Ellipsometry. DMX-20 for Ellipsometry. Low Vibration system for SOPRA Ellipsometer

8 DMX-20 for MOKE (Kerr Effect) DMX-20 for MOKE (Kerr Effect) #4-40 x 1/8"Lg SHSS w/nylon Tip,18-8 (X3) MCMSTR CARR PN: 90291A O-RING (X2) Vacuum Shroud 0.95 dia. 2 mm thk. Quartz Window.75 dia. view port epoxied to shroud Sample space ID, Rad. Shield dia. Radiation Shield 2.5 dia. Flange (DMX-4) Small diameter vacuum housing can be inserted into a narrow gap (high field). The optical window allows collection of light from the sample. The window can be very close to the sample for short focal length objective Low Vibration Side looking window can be placed in a MOKE, (Magneto Optical Kerr Effect). Sample can be located in any plane. The pole spacing can be as low as 1 inch. DMX-20 for FTIR. DMX-20 for FTIR. DMX-20B INTERFACE 4.5 CF 6.43 Vibration Isolation Soft Mount CF, Non-Rotatable (ref.) 3.10 Compressed Position Movable Side Z-Translator 4.5 CF both ends 2 inch stroke Fixed Side 4.5 CF, Non-Rotatable (ref.) Upper Vacuum Shroud Radiation Shield FTIR Cover Plate [103.3] 7.70 [195.5] Removable Lower Vacuum Shroud Long Optical Sample Holder 0.53 Low Vibration system for FTIR spectrometer. Sample holder with 3 samples can be translated in Z direction. Low Vibration system for BOMEM, DA8 FTIR spectrometer.

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