SSI Atomic Absorption Spectrophotometers AA-6300 Series Consumables

Transcription

1 SSI Atomic Absorption Spectrophotometers AA-6300 Series Consumables

2 Contents AA Burner ASSY... 3 Drain ASSY... 3 Maintenance parts... 4 ASC Maintenance Parts... 6 ASK Maintenance Parts... 6 GFA-EX7i... 7 Maintenance Parts... 7 Hydride Vapor Generator... 8 Consumables... 9 Maintenance Parts... 9 Atom Booster Chemical Compatibility AA ASC Lamps Single-Element Multi-Element Standards... 16

3 AA-6300 Burner ASSY Item Part Number Part Name cm Titanium Burner Head O-RING, 4D P O-Ring, AS56A PLUG FOR CHAMBER ASSY O-RING 4D P16,AA Mixer Paddle O-RING 4D P DRAIN JOINT O-RING 4D P Sleeve, PP CAP TUBING POLYETHYLENE CAPILLARY NEBULIZER BURNER SOCKET ELBOW RETAINTING PLATE HALF UNION Drain ASSY Item Part Number Part Name Tube, Super-Corn-Ace Level Switch Assy Drain Bottle Half Union, HZ10-02-PP Tubing DRAIN TUBING 3

4 Maintenance Parts: AA-6300 Part Name Part Number Remarks Replacement D2-Lamp Lamp, D2 L Deuterium lamp 1 Year O-Ring Sets O-Ring Set STD O-ring (Fluorine-containing rubber) O-Ring Set, Organics Perfluoroelastomer (FFKM) *See Chemical Compatibility *See Chemical Compatibility O-Ring Set, Silicon Silicon Rubber (VQM) *See Chemical Compatibility Burner Head Burner Head ASSY Titanium, 10 cm 3 Years High Temp Burner Head Titanium, N2O-C2H2, 5 cm 3 Years Hoses Hose, 8 2B-BK For support gas (Air/Argon), Black 3 Years Hose, 8 2B-R For fuel gas (C2H2), Red 3 Years Hose, 8 2B-G For support gas (N2O), Green 3 Years Atomizer Nebulizer Set With Impact bead & Nebulizer 2 Years Burner Socket Years Chamber ASSY Engineering plastic PP 6 Years Mixer Years Tubing Sampling tube Teflon tube for sample uptake *See Chemical Compatibility Sampling tube ASSY Polyethylene tube for sample uptake *See Chemical Compatibility Drain ASSY Overflow-type drainage trap Polyethylene capillary No For sealing the capillary PE tube, 8x Drain tube, connects to drain bottle. Specify 3 meters. Misc. WizAArd Win 7, 32-bit Software Agent Connection Kit Win 7, 32-bit Cleaning wire For cleaning the capillary Card For cleaning the burner/for checking the burner height Window Panel w(30)-q Optical windows, inside atomization chamber Seal Joint Assy Gas leak checking HCL Lamp Retainer Holds HCL in socket 4

5 ASC-6100 Item Part Number Part Name KNOB TURNTABLE FOR ASC NOZZLE ASSY, F COVER, TURN TABLE LITER RINSE BOTTLE BOTTLE HOLDER RS232C CABLE POWER CABLE CANOE CLIP-WHITE O-RING, 4D P8 ASK-6100 Item Part Number Part Name Item Part Number Part Name Port Guide, ASC Nut, AA Syringe Port Nipple, AA Syringe Tube Assy Teflon Tube LUER FITTING Filter SYRINGE, ASC PLUNGER PRESSER Clip, Hose Pump Head 5

6 Maintenance Parts: ASC-6100 Part Name Part Number Remarks Replacement Nozzles Nozzle ASSY, F Standard Nozzle ASSY, GFA, Micro Requires Pipette Tip ( ) Pipet tip For Dispensing Every 60 samples *4 Nozzle ASSY, G Optional Nozzle ASSY, HVG For HVG Syringe Parts Syringe Capacity 250 ul 5 years *3 Plunger Tip, TEF Plunger for syringe 1 year *3,5 Pump Parts Pump tube Tube for Peristaltic pump Pump Head Pump Head for Peristaltic pump 6 months *1,3,5 2 years *2,3,5 1 year *1,5 4 years *2,5 Vials & Cups 16 ml Sample vial Each, polypropylene, Flame Cont. *1: Flame continuous method 16 ml Sample vial /PK, polypropylene, Flame Cont. *2: Furnace/ micro sampling method 53 ml Glass Vial Each, glass, Flame Cont. *3: When distilled water is used 20 ml Vials Each, polypropylene, GFA, Micro. *4: Recommended for low conc. 2 ml Cup Each, polypropylene, GFA, Micro. *5: 60 samples per day usage 2 ml Cup /PK, Polystyrene, GFA, Micro. Glass sample cup (2 ml) ml Glass Glass Test tube (12 ml) ml Glass Misc. Rinse liquid bottle L plastic tank for rinse liquid Port Integrated port Fuse V, 3.15 A, Type T GFA-TV Assists with Nozzles Postioning GFA-TV 6

7 GFA-EX7i GFA Tubes Name Part Number High-density tube Extended Life High-denisty Pyrolytic coated tube Extended Life Pyrolytic coated Platform tube Item Part Name Part Number Replacement Item Part Name Part Number Replacement 1 Graphite Cap Years 8 O-ring, 4CP Years 2 Seal Years 9 Bolt Graphite Holder Years 10 Guide ASSY Socket ASSY Lid Window plate, W(16)-Q Slide Cover Years 6 O-ring, 4CP Years 13 Spring HOSE NIPPLE M 5H Electrode tool Maintenance Parts: GFA-EX7i Part Name Part Number Remarks Replacement Hose, 8 2B-BK For support gas (Air/Argon), Black 3 Years Wire band, for 14 mm Gas hose clamp Wire band, for 16 mm Cooling water hose clamp O-ring, 4CP Socket Assy 3 Years Extension tube ASSY Cooling Water Outlet 3 Years Cooling Water ASSY Cooling Water Inlet 3 Years Tetron Sleeve, 10 x For Cooling Water 3 Years TUBE ASSY, OUTER TUBE ASSY,TEMPSENS TUBE ASSY,INLET TUBE ASSY,OUTLET TUBE ASSY, INNER

8 Hydride Vapor Generator Item Part Name Part Number 1 Hydride vapor generator main body 2 Reagent bottle (poltethylene) Gas Hose Drain tube (Tygon) AC Cable ( V) Power cable ( V) Fluorinated rubber tube Guide plate Fuse 1 A ( V) Fuse 0.3 A ( V) Cell holder Absorption cell Hose clamp, 16 mm Pump tube 080 (reagent) Pump tube 130 (sample) Front cover Side cover Gas/liquid separator Manifold Reaction Coil Hose nipple O-ring, EPR Suction tube (yellow-marked) for NaBH Suction tube (blue-marked) for HCl Suction tube (not marked, 30 cm) for sample Suction tube (not marked, 80 cm) for ASC Wire mark (yellow) Wire mark (blue) Vinyl cover Grounding line Label (flow path diagram) Hose nipple, HN Hose clamp, 14 mm Instruction manual

9 Consumables: HVG Unit Part Name Part Number Appearance Pump tube 080 (reagent) Pump tube 130 (sample) Absorption cell Maintenance Parts: HVG Unit Part Name Part Number Appearance Gas/liquid separator Manifold (except for O-ring, hose nipple) Reaction Coil Suction tube (yellow-marked) for NaBH

10 Suction tube (blue-marked) for HCl Suction tube (not marked, 30 cm) for sample Suction tube (not marked, 80 cm) for ASC Fluorinated rubber tube Joint (reagent) Joint (sample) Atom Booster Item Part Number Part Name Atom Booster Assembly Quartz Tube Replacement 10

11 Chemical Compatibility AA-6300 Chemical Name Drain Tank Drain Tube O-Rings Chamber Conditions of (Polyethlyene) Standard Use Optional (PTFE) Standard FFKM VQM Nebulizer Water 1 A A A A A A A Ethanol B B B B B B B Hydrochloric acid B B B B B B B Nitric acid B B B B B B B Sulfuric acid B B B B B B B Hydrofluoric acid B B B B B X B Perchloric acid B B B B B X B Methanol B B B C B B B Sodium hydroxide B B B X B X B Gasoline C C B B B X B Petroleum C C B B B C B Change O-rings Change the drain tank once every month. Change the standard drain tube once every month, or replace it with the optional product Acetic acid C C B X B B B Change the O-rings to the optional products. MIBK C C B X B C B Butyl acetate C C B X B C B Acetone C C B X B C B Change the drain tank once every month. Change the standard drain tube once every month, or replace it with the optional product. 1: Acid concentration less than 0.5% A: Applicable. Replacement required once every 3 years B: Applicable. Replacement required once a year C: Applicable. Replacement required once a month X: Cannot be used 11

12 ASC

13 Lamps Single Element Lamps Name Symbol Part Number Name Symbol Part Number Aluminum Al Nickel Ni Antimony Sb Niobium Nb Arsenic As Palladium Pd Barium Ba Platinum Pt Beryllium Be Potassium K Bismuth Bi Rhenium Re Boron B Rhodium Rh Cadmium Cd Rubidium Rb Calcium Ca Ruthenium Ru Cerium Ce Selenium Se Cesium Cs Silicon Si Chromium Cr Silver Ag Cobalt Co Sodium Na Copper Cu Strontium Sr Dysprosium Dy Tantalum Ta Gallium Ga Tellurium Te Germanium Ge Thallium Tl Gold Au Tin Sn Iron Fe Titanium Ti Lanthanum La Tungsten W Lead Pb Vanadium V Lithium Li Zinc Zn Magnesium Mg Zirconium Zr Manganese Mn Mercury Hg Molybdenum Mo

14 Multi-Element-Special Order Items Base Element Amalgam Metal/s P/N Base Element Amalgam Metal/s P/N Aluminium Ca Chromium Co+Fe+Mn+Ni Ca + Fe + Mg Cu Ca + Mg Cu + Co Ca+Cu+Fe+Mg+Si+Zn Cu + Fe Mg Cu + Fe + Mn Si Cu + Fe + Ni Si + Ti Cu + Mn Antimony Arsenic Barium Cadmium Calcium Ti Cu + Mn + Ni As + Bi Cu + Ni Se + Te Cu + Ni + Ag Ca + Mg + Sr Cu+Fe+Mn+Ni Sr Cu+Fe+Ni+Ag Zn Fe Ba Fe + Mn Ba + Sr Fe + Mn + Ni Mg Fe + Ni Mg + Si Mn Mg + Zn Mn + Ni Si Mo Chromium Sr Ni Zn Cobalt Cu Co Cu + Fe Co + Cu + Fe Cu + Fe + Mn Co + Cu + Mn Cu + Fe + Ni Co + Cu + Ni Cu + Mn Co + Fe Cu + Mn + Ni Co + Fe + Mn Cu+Fe+Mn+Mo Co + Fe + Ni Cu+Fe+Mn+Ni Co + Mn Fe Co + Mn + Ni Fe + Mn + Ni Co + Ni Mn Co+Cu+Fe+Mn Mn + Ni Co+Cu+Fe+Mn+Mo Mo Co+Cu+Fe+Mn+Ni Ni Co+Cu+Fe+Ni Co+Cu+Mn+Ni

15 Multi-Element Special Order Items Base Element Amalgam Metal/s P/N Base Element Amalgam Metal/s P/N Copper Fe Molybdenum Co + Cu Fe + Mn Co + Cu + Fe Fe + Mn + Ni Co + Cu + Mn Fe + Mn + Zn Co + Fe Fe + Mo Co + Fe + Mn Fe + Ni Co + Mn Fe + Ni + Ag Cr + Co Fe + Zn Cr + Cu Mn Cr + Fe Mn + Ni Cr + Mn Mn + Zn Cu + Fe Mo Cu + Fe + Mn Ni Cu + Mn Gold Zn Fe + Mn Ag Platinum Ag Cu Silicon Ti Cu + Ni Silver Cr Ni Cr + Cu Pt Cu Iron Pt + Ag Cu + Ni Mn Sodium K Mn + Ni Mn + Zn Mo Ni Magnesium Manganese Zn Si Zn Mo Ni Zn

16 Single Element Standards 1000 mg/l, (ppm) Element Name Element Symbol & Matrix Part number Element Name Element Symbol & Matrix Part number Aluminum Al in 2% HNO Neodymium Nd in 2% HNO Antimony Sb in 5% HNO % HF Nickel Ni in 2% HNO Antimony Sb in 5% Tartaric Acid + 2% HNO Niobium Nb in 2% HNO % HF Arsenic As in 2% HNO Palladium Pd in 10% HNO3 + TrHF Barium Ba in 2% HNO Phosphorus P from KH2PO4 in 0.05% HNO Beryllium Be in 2% HNO Phosphorus P in 0.05% HNO Bismuth Bi in 2% HNO Potassium K in 1% HNO Cadmium Cd in 2% HNO Praseodymium Pr in 2% HNO Calcium Ca in 2% HNO Rhenium Re in 2% HNO Cerium Ce in 2% HNO Rubidium Rb in 1% HNO Cesium Cs in 1% HNO Samarium Sm in 2% HNO Chromium Cr in 2% HNO Scandium Sc in 2% HNO Cobalt Co in 2% HNO Selenium Se in 2% HNO Copper Cu in 2% HNO Silver Ag in 2% HNO Dysprosium Dy in 2% HNO Sodium Na in 1% HNO Erbium Er in 2% HNO Strontium Sr in 1% HNO Europium Eu in 2% HNO Tantalum Ta in 2% HNO % HF Gadolinium Gd in 2% HNO Tellurium Te in 2% HNO % HF Gallium Ga in 2% HNO Terbium Tb in 2% HNO Germanium Ge (NH4)2GeF5 in 1% HNO Thallium Tl in 2% HNO Germanium Ge in 2% HNO % HF Thorium Th in 2% HNO Hafnium Hf in 2% HNO % HF Thulium Tm in 2% HNO Holmium Ho in 2% HNO Tin Sn in 2% HNO % HF Indium In in 2% HNO Titanium Ti in 2% HNO % HF Iron Fe in 2% HNO Tungsten W in 2% HNO3 + 1% HF Lanthanum La in 2% HNO Uranium U in 2% HNO Lead Pb in 2% HNO Vanadium V in 2% HNO Lithium Li in 1% HNO Ytterbium Yb in 2% HNO Lutetium Lu in 2% HNO Yttrium Y in 2% HNO Magnesium Mg in 2% HNO Zinc Zn in 2% HNO Manganese Mn in 2% HNO Zirconium Zr from ZrO(NO3)2 in 0.5% HNO Mercury Hg in 2% HNO Zirconium Zr in 2% HNO % HF Molybdenum Mo in 2% HNO % HF

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