Test item Unit Test results Test method Remarks TS C 2/20 rpm
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1 Technical Data February 17, 2003 Three Bond Co., Ltd. ThreeBond 3114 UV-curing epoxy resin 1. Outline ThreeBond 3114 is an epoxy resin-based solvent-free ultraviolet-curing resin. Since the resin cures through optical cationic polymerization, it is not inhibited from curing by oxygen, and it excels in surface curability. Hereinafter, ThreeBond is abbreviated to TB. 2. Features (1) The resin can be cured by irradiation of ultraviolet light (wavelength: 200 to 400 nm) for several seconds to several tens of seconds. (2) Its shrinkage factor during curing is low. (3) It excels in surface curability. (4) It exhibits good adhesion to various materials, such as glass, metals and plastics. (5) It does not need to be heated after irradiated by ultraviolet light. 3. Uses (1) The resin is suitable for bonding and securing optical components, such as optical pickup component parts. (2) The resin is suitable for precisely bonding and securing electrical and electronic parts. 4. Description 4.1 Description Table 1 Description Appearance Grayish white 3TS Viscosity Pa s 26 3TS C 20 rpm Structural viscosity ratio 3.0 3TS C 2/20 rpm Specific gravity TS C Rotor used to measure the viscosity and structural viscosity ratio: No.6-1 ED030501
2 4.2 Fluidity curves (rheometer) 10 4 TB3114 Viscosity TB3114 Shear Stress Temperature Viscosity(Pa s) Shear Stress(Pa) Shear rate (1/s) Fig. 1 Viscosity curve and fluidity curve 10-1 Viscosity(Pa s) TB3114 Viscosity(Pa s) Shear Rate =1.0(1/s) Temperature( ) Fig. 2 Temperature-viscosity curve - 2 ED030501
3 5. Properties of cured resin 5.1 Physical properties Table 2 Physical properties Hardness D 80 3TS C Cure shrinkage % 1.2 3TS g Water absorption % 1.0 * 3TS g Thick film curability mm 2.0 3TS kj/m 2 * Boiling: 2 hrs. 5.2 Viscoelastic properties Table 3 Viscoelastic properties Measuring frequency: 1 Hz tan δ peak C TS Storage elastic Pa modulus TS C 5.3 Linear expansion coefficient and glass transition temperature Table 4 Linear expansion coefficient and glass transition temperature Item Unit Property value Measuring method Remarks Linear expansion coefficient (α1) / C TS to 0 C Linear expansion coefficient (α2) / C TS to 150 C Glass transition temperature C TS TMA method - 3 ED030501
4 6. Tensile shear bond strength test Tested material PPS Glass 4.8 Table 5 Tensile shear bond strength Test results Test method: 3TS Remarks (details of substrate) PPS GS-40, Toso Corporation LCP Glass 3.5 VECTRA E130, Polyplastics Zinc die casting Glass 6.2 ZDC-2 (JIS H 5301) Glass Glass 7.7 (Material rupture) 7. Usage Standard curing condition: As for the details of the resin curing procedures, consult our sales engineers. 8. Instructions for use (1) The curing speed depends on the type of light source and the irradiation distance. Carefully check the conditions prior to use. (2) The resin in areas not exposed to ultraviolet light or in areas in the shadow does not cure in principle. Before using it, sufficiently examine whether the applying method and the purpose of use are appropriate. (3) A little gas is generated during application and ultraviolet curing. Forcedly ventilate the working area and the ultraviolet light irradiation area. Wear appropriate protective means, such as a mask, gloves (not permeable) and goggles, as necessary, and use the resin in a place provided with a local exhaust system. (4) It is forbidden to inhale or drink the resin. It is harmful to the health. Never inhale or drink it. If it if drunk, immediately put the sufferer under medical treatment. (5) The resin is toxic. Do not touch it directly or inhale its vapor. Adhesion of the resin to the skin can cause an inflammation. If it adheres to the skin, immediately wipe it off with cloth or paper, and wash the skin with soap and water. If it enters the eyes, wash the eyes with fresh water for about 15 minutes, and make arrangements for medical treatment. (6) If any abnormality is found in the human body, quit handling it, and make arrangements for medical treatment. Persons who have allergies or sensitive skin should avoid handling it. (7) Some materials are deteriorated by the product. Ascertain in advance whether it affects the materials to be bonded. If they are affected, do not use the product. (8) Do not pour the product into other containers. Do not return the product left unused to its container. (9) After using it, cover the container tight to prevent deterioration or entry of foreign matter. (10) Use and keep it out of reach of children. - 4 ED030501
5 9. Storage Store under (10 25 ºC) place where dose not shine direct rays of the sun and where humidity is low. 10. Disposal consideration Consign the disposal of the product to an authorized professional disposal trader for industrial wastes. 11. Precautions for use For industrial use Never use for household use. Acknowledge the following terms of sales before use of the product. (1) As for the technical data listed herein, the values are the test values in accordance with the test methods of our company, and we cannot warrant absolutely for the accuracy and completeness. Users are requested to infallibly decide the application and purpose by themselves and bear all of the accompanying responsibilities and risks. The coverage of warranty is limited to the replacement of for a clearly defective product with new item. (2) We cannot bear any responsibility for injuries and losses caused by mishandling of the product. (3) We cannot bear any responsibility for the matters not listed in this data book unless otherwise so specified in the contract - 5 ED030501
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