Low viscosity, unfilled epoxy casting resin system, curing at room temperature. High filler addition possibility. Casting; vacuum casting.

Transcription

1 Advanced Materials Araldite DBF 100 pbw Aradur HY 956 EN 20 pbw Low viscosity, unfilled epoxy casting resin system, curing at room temperature. High filler addition possibility. Application Encapsulating or potting of low voltage and electronic components. Processing methods Casting; vacuum casting. Key Properties Good heat resistance. Good resistance to atmospheric and chemical degradation. August 2012 DBF / HY 956 EN Page 1 of 6

2 Product Data (Guideline Values) Araldite DBF Liquid epoxy resin modified by the addition of a plasticizer. Viscosity at 25 C ISO 2555 mpa*s * Specific Gravity at 25 C ISO 2811 g/cm³ 1.15 Appearance Visual Clear liquid* Epoxy content ISO 3001 Eq/kg * Aradur HY 956 EN Formulated, low viscosity polyamine hardener. Viscosity at 25 C ISO mpa*s * Specific Gravity at 25 C ISO 2811 g/cm³ 1.03 Appearance Visual Clear, liquid* *Specified range August 2012 DBF / HY 956 EN Page 2 of 6

3 Processing Data (Guideline Values) Mix Ratio Parts by weight Parts by volume Araldite DBF Resin HY 956 EN Hardener Gel Time, Viscosity and Curing Mix Viscosity at 25 C Araldite DBF / HY 956 EN Rheomat mpa*s 1800 Mix Viscosity at 40 C 1300 Pot life at 25 C Araldite DBF / HY956 EN Time to reach 5000 mpa*s min 70 Time to reach mpa*s min 120 Pot life at 40 C Araldite DBF / HY956 EN Time to reach 5000 mpa*s min 45 Time to reach mpa*s min 62 Gel time at 40 C Araldite DBF / HY956 EN Gelnorm min 62 Gel time at 60 C Gelnorm min 15 Minimum Curing Cycle hours at RT or 4 h at RT + 4 h at 60 C August 2012 DBF / HY 956 EN Page 3 of 6

4 Processing and Storage (Guideline Values) Mixing Measure (by weight or volume) the Araldite resin and the hardener. Add the hardener to the Araldite resin; making sure that the required amount of hardener is transferred to the resin. Stir thoroughly until mixing is complete. Air entrainment during mixing results in pores in the cured resin. Mixing under vacuum or in a metering-mixing machine is the most effective way to prevent air entrainment. Alternatively the static resin hardener mixture may be deaerated in a vacuum chamber allowing at least 200 % ullage for the foam to expand. Curing The chemical reaction initiated by mixing resin and hardener results in the generation of exothermic heat. The peak temperatures attained are determined by the starting temperature and the size and shape of the casting. Unfilled resin systems are suitable only for manufacturing castings weighing up to about 500 grams. Mineral filler should be added to dissipate heat and damp the exothermic reaction when producing large castings. There is very little exothermic reaction when producing very small castings or thin layers as the heat generated is rapidly dissipated. Cure is consequently delayed and the surfaces of castings may remain tacky. In such cases an infrared heater or oven at 40 C 60 C should be used to effect full cure. When casting thick sections special care is needed to avoid excessive exothermic temperature rise. Short high-temperature curing schedules should not be used unless preliminary trials with castings manufactured to the specific design, and in the specified moulds, produce no unacceptable exothermic effects. To determine whether cross-linking has been carried to completion and the final properties are optimal, it is necessary to carry out relevant measurements on the actual object or to measure the glass transition temperature. Different gel and cure cycles in the customer s manufacturing process could lead to a different degree of crosslinking and thus a different glass transition temperature. Storage Conditions Store the components in a dry place according to the storage conditions stated on the label in tightly sealed original containers. Under these conditions, the shelf life will correspond to the expiry date stated on the label. After this date, the product may be processed only after reanalysis. Partly emptied containers should be tightly closed immediately after use. For information on waste disposal and hazardous products of decomposition in the event of a fire, refer to the Material Safety Data Sheets (MSDS) for these particular products. August 2012 DBF / HY 956 EN Page 4 of 6

5 Mechanical and Physical Properties (Guideline Values) Determined on standard test specimen at 23 C. Cured for 6 hours at RT + 6 hours at 60 C. Color of casting Density ISO 1183 g/cm Glass transition temperature (DSC) ISO C 64 Flexural strength ISO 178 MPa 107 Elongation at break ISO 178 % 12 Yellow Flexural modulus ISO 178 MPa 2900 Hardness ISO 868 Shore D 80 Tensile strength ISO 527 MPa 58 Elongation at break ISO 527 % 6.4 Tensile modulus ISO 527 MPa 2880 Impact strength ISO 179 kj/m 2 69 Water absorption ISO day at 23 C 30 min at 100 C % by wt Electrical Properties (Guideline Values) Determined on standard test specimen at 23 C. Cured for 6 hours at RT + 6 hours at 60 C. Dielectric strength (2 mm specimen) IEC kv/mm 24 Dielectric loss factor (tan δ, 50Hz, 25 C) IEC % 0.8 Dielectric constant (εr, 50Hz, 25 C) IEC Volume resistivity (ρ, 25 C) IEC Ω cm 7 x Tracking resistance IEC 112/79 CTI > Electrolytic corrosion IEC grade A-1 August 2012 DBF / HY 956 EN Page 5 of 6

6 Legal Notice Huntsman Advanced Materials (Switzerland) GmbH Klybeckstrasse Basel Switzerland Tel: +41 (0) Fax: +41 (0) Huntsman Advanced Materials warrants only that its products meet the specifications agreed with the user. Specified data are analysed on a regular basis. Data which is described in this document as 'typical' or 'guideline' is not analysed on a regular basis and is given for information purposes only. Data values are not guaranteed or warranted unless if specifically mentioned. The manufacture of materials is the subject of granted patents and patent applications; freedom to operate patented processes is not implied by this publication. While all the information and recommendations in this publication are, to the best of Huntsman Advanced Material s knowledge, information and belief, accurate at the date of publication, nothing herein is to be construed as a warranty, whether express or implied, including but without limitation, as to merchantability or fitness for a particular purpose. In all cases, it is the responsibility of the user to determine the applicability of such information and recommendations and the suitability of any product for its own particular purpose. The behaviour of the products referred to in this publication in manufacturing processes and their suitability in any given end-use environment are dependent upon various conditions such as chemical compatibility, temperature, and other variables, which are not known to Huntsman Advanced Materials. It is the responsibility of the user to evaluate the manufacturing circumstances and the final product under actual end-use requirements and to adequately advise and warn purchasers and users thereof. Products may be toxic and require special precautions in handling. The user should obtain Safety Data Sheets from Huntsman Advanced Materials containing detailed information on toxicity, together with proper shipping, handling and storage procedures, and should comply with all applicable safety and environmental standards. Hazards, toxicity and behaviour of the products may differ when used with other materials and are dependent on manufacturing circumstances or other processes. Such hazards, toxicity and behaviour should be determined by the user and made known to handlers, processors and end users. Except where explicitly agreed otherwise, the sale of products referred to in this publication is subject to the general terms and conditions of sale of Huntsman Advanced Materials LLC or of its affiliated companies including without limitation, Huntsman Advanced Materials (Europe) BVBA, Huntsman Advanced Materials Americas Inc., Huntsman Advanced Materials (UAE) FZE, Huntsman Advanced Materials (Guangdong) Company Limited, and Huntsman Advanced Materials (Hong Kong) Ltd. Huntsman Advanced Materials is an international business unit of Huntsman Corporation. Huntsman Advanced Materials trades through Huntsman affiliated companies in different countries including but not limited to Huntsman Advanced Materials LLC in the USA and Huntsman Advanced Materials (Europe) BVBA in Europe. All trademarks mentioned are either property of or licensed to Huntsman Corporation or an affiliate thereof in one or more, but not all, countries. Copyright 2012 Huntsman Corporation or an affiliate thereof. All rights reserved. August 2012 DBF / HY 956 EN Page 6 of 6