ORGANISATION EUROPÉENNE POUR LA RECHERCHE NUCLÉAIRE EUROPEAN ORGANIZATION FOR NUCLEAR RESEARCH. Technical Sheet. N Ed. 1 EDMS N :
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1 ORGANISATION EUROPÉENNE POUR LA RECHERCHE NUCLÉAIRE EUROPEAN ORGANIZATION FOR NUCLEAR RESEARCH Materials Technical Specification GS-IS & EN-MME Technical Sheet N Ed. 1 EDMS N : Stainless steel plates for the shells of the cold masses of superconductive dipole magnets X2CrNiMoN AISI 316LN This document specifies the CERN technical requirements for (X2CrNiMoN , AISI 316LN) stainless steel plates for the shells of the cold masses of superconductive dipole magnets Original : English
2 Table of content 1. NORMATIVE REFERENCES REQUIREMENTS MANUFACTURING PROCESS CHEMICAL COMPOSITION STRUCTURE INCLUSIONS CONTENT MECHANICAL PROPERTIES MAGNETIC PROPERTIES THERMAL CONTRACTION SURFACE QUALITY DIMENSIONS AND TOLERANCES INTERNAL SOUNDNESS INSPECTION AND TESTING GENERAL TEST METHODS IDENTIFICATION INSPECTION CERTIFICATE PACKING /7
3 1. NORMATIVE REFERENCES Unless stated in the present CERN specification or agreed by a written mention in the order, the material shall be in accordance with the following referenced documents. The latest edition applies. EN EN EN EN ASTM E112 ASTM E45 ISO ISO EN EN EN EN Stainless steels - Part 2: Technical delivery conditions for plate and strip of corrosion resisting steels for general purposes General technical delivery requirements for steel products Flat products made of steels for pressure purposes Part 1: General requirements Flat products made of steels for pressure purposes Part 7: Stainless steels Standard test methods for determining average grain size Standard test methods for determining the inclusion content of steel Metallic materials Tensile testing Part 1: Method of test at room temperature Metallic materials Charpy pendulum impact test Magnetic materials Part 15: Methods for the determination of the relative magnetic permeability of feebly magnetic materials Hot-rolled steel plates 3 mm thick or above Tolerances on dimensions and shape Non-destructive testing - Ultrasonic testing of austenitic and austenitic-ferritic stainless steels flat products of thickness equal to or greater than 6 mm (reflection method) Metallic products: Types of inspection documents 3/7
4 2. REQUIREMENTS 2.1. MANUFACTURING PROCESS The stringent requirements of this material specification for products intended for cryogenic purposes, impose to apply an adapted metallurgy and manufacturing process, aimed at meeting the structure, inclusion limits, mechanical and physical properties specified in this document. The plates shall be hot-rolled and solution annealed. Strips are not accepted for this application (delivery in coils), but only plates individually rolled CHEMICAL COMPOSITION The chemical composition requirements of the product analysis are given in the following table. Chemical composition (product analysis) Element % by mass Cr * Ni * Special requirements: Cobalt shall be present only as a trace or to a maximum content of 0.10%, including measuring tolerance. C Si max max. The nitrogen content 0.15% % is imperative. Mn 2.00 max. Mo * N * P max.* Content of impurity elements (P, S, B) shall reach the lowest achievable level. Elements not listed in this table shall not be intentionally added to the steel without the agreement of CERN. S Fe max.* Remainder * CERN requirement 2.3. STRUCTURE The structure after solution annealing shall be completely homogenous. Austenite shall be stable with regards to thermo-mechanical loads. Segregations, as well as presence of intermediate phases, such as Sigma, Chi, Laves, are not allowed in the final product. No traces of such phases shall be visible on micrographs up to a magnification of 500. Grain size shall be determined in accordance with the standard ASTM E112. The average grain size number shall be greater than 3 and homogeneous within the range of ± 1 equivalent grain size number around the true average value. 4/7
5 2.4. INCLUSIONS CONTENT Amount and definition shall meet standard ASTM E Micro-inclusions (indigenous inclusions detectable by microscopical test methods): method A is applicable. Severity level number shall be at most Macro-inclusions (exogenous inclusions from entrapped slag or refractories): they are strictly forbidden and are cause for rejection MECHANICAL PROPERTIES At room temperature (RT), after solution annealing in the transversal direction: Tensile strength R m min. 590 N.mm -2 R m max. 790 N.mm -2 Yield stress R p0.2% min. 290 N.mm -2 Elongation at break A 5 min. 40% The impact test shall be performed on 3 test pieces ISO-V notched. Each tests piece shall be taken transverse to the rolling direction and the notch, therefore, parallel to the direction of rolling and perpendicular to the plate surface. The test method shall assure that the temperature of the tests sample truly equals 4.2 K at the time of rupture. This is normally the case when, either the test sample is still immersed in liquid helium at the time of rupture, or the complete testing device operates at 4.2 K inside an adequate cryostat. This test shall be carried out by qualified laboratories, of which CERN may provide a list upon request. CERN s approval on the test procedure is required before proceeding to the tests. At cryogenic temperature (4.2 K), after solution annealing the average impact strength shall exceed 150 J cm -2. Each individual value shall exceed 120 J cm MAGNETIC PROPERTIES The relative magnetic permeability at RT after solution annealing shall be lower than or equal to for fields of over A.m -1 (equivalent to 1000 Oe) THERMAL CONTRACTION The integrated thermal contraction coefficient between RT and 4.2 K, both in transverse and longitudinal directions, shall exceed m/m. CERN will carry out the measurements of this physical property at its own expense. 5/7
6 2.8. SURFACE QUALITY According to EN , the plates shall be annealed and matt-pickled with on both faces a surface finish 1D. Surface marks, scratches, mill slivers or laminations, scales and any other deterioration or pollution of the surfaces during handling and/or manufacturing are forbidden. Any trace of coloured oxide shall be removed wherever necessary but the grinding operation shall be carried out smoothly in order not to provoke undesirable under-size areas (i.e. deep marks). In specific cases, dye penetrant tests might be requested DIMENSIONS AND TOLERANCES The dimensions, shape and tolerances shall meet the standard EN Class C shall be applied on the thickness, with a maximum thickness difference within a plate of 0.5 mm. Edge camber and out of squareness shall be limited so that is shall be possible to inscribe a rectangle with the dimensions of the ordered plate within the delivered size INTERNAL SOUNDNESS The homogeneity of the steel shall be ultrasonically inspected, according to EN 10307, quality class S 3. The 50 mm bandwidth zone along the edges shall be entirely checked and shall meet quality class E 4. Should any defect appear in the course of the above-mentioned checking, CERN reserves the right to increase the frequency of checks at its own expense. 3. INSPECTION AND TESTING 3.1. GENERAL Quality control shall be carried out in accordance with an Inspection and Test Plan (ITP) established between the manufacturer and CERN. CERN (or its representative) reserves the right to intervene during the different stages of fabrication. In case dye penetrant testing is requested, the test shall be performed in accordance with a written procedure that shall be submitted to CERN for approval prior to testing. 6/7
7 3.2. TEST METHODS The rolling direction shall be marked on each test sample. Test Applicable standard Test unit Chemical analysis Structural analysis (structure/ inclusions) Mechanical properties Using appropriate European Standards* Grain size: ASTM E112 Inclusions: ASTM E45, Method A Tensile test at RT: ISO Charpy test at 4.2 K: ISO Cast analysis and on final product For each batch** and each thickness within the batch By sampling on the plates For each batch** and each thickness within the batch By sampling on the plates Magnetic permeability EN or equivalent For each batch** and each thickness within the batch By sampling on the plates Ultrasonic EN 10307, quality classes S 3, E 4 For each plate Dimensions EN For each plate * The choice of a suitable method for the analysis is at the discretion of the manufacturer. The manufacturer shall declare the test method used if required. ** The batch is defined based on EN IDENTIFICATION Each plate shall be marked with: Cast number Manufacturer's name Type of material Traceability number between delivered lot and inspection documents The markings shall be shown every 20 cm, on one side only. It shall be possible to erase them easily using solvents INSPECTION CERTIFICATE The certificate shall be based on specific inspection 3.1, according to EN All the inspection documents shall be drawn up in accordance with the prevailing standards and shall be submitted to CERN for approval prior to delivery. 4. PACKING The packaging of the plates shall be strong enough to preserve the surface condition during transport. 7/7
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