I i I I I LII I. SSFL ANALYTICAL CHEMISTR Y Rockwell International, Rocketdyne Div. (818) D/392 S92 1 BNA

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1 I i I I I LII I BNA HDMSe SSFL ANALYTICAL CHEMISTR Y Rockwell International, Rocketdyne Div. (818) D/392 S Dept /Group : MAIL : T886 REPORT DATE : 11/19/9 2 Sample Descrption : Soil, Bins : 1102, 52338, 1317, 5277, B-2 9 Requested Analysis: 8080 Received : 11/17/92 Sampler : M. Halverson Sampler ID# : B Sampled : 11 / 8 :33 :0 0 ANALYTE RESULT UNITS METHOD/SOURCE PCB 1254 in soil 0.65 mg /Kg S11846, Method SPECIFICATION : ( PCB analysis ) SPECIAL NOTES : APPROVED : 4d. ;Z ~~ )! \ p Luti~S o~ SIGNED : Rocketdyne 5SF Analytical Chemistry Roc etdyne SSFL Anaical chemistr y

2 SSFL ANALYTICAL CHEMISTRY Dept/Group : MAIL : T REPORT DATE : 11/25/9 2 SAMPLE INFORMATIO N Sample Descrption : Soil, Bins : 1102, 52338, 1317, 5277, B-2 9 Requested Analysis: Metals Received: 11/17/9 2 Sampler: M. Halverson Sampler ID# : A Sampled : 8 :33 :0 0 ANALYTE RESULT UNITS METHOD / SOURCE Antimony ND mg/kg 6010/SW 84 6 Arsenic ND mg/kg 6010/SW 846 Barium 93 mg/kg 6010/SW 846 Beryllium ND mg/kg 6010/SW 846 Cadmium 0-67 mg/kg 6010/SW 84 6 Chromium 21 mg/kg 6010/SW 84 6 Cobalt 6.4 mg/kg 6010/SW 84 6 Copper 11 mg/kg 6010/SW 84 6 Lead ND mg/kg 6010/SW 84 6 Mercury 18 mg/kg 7471/SW 84 6 Molybdenum ND mg/kg 6010/SW 84 6 Nickel 12 mg/kg 6010/SW 846 Selenium ND mg/kg 6010/SW 846 Silver ND mg/kg 6010/SW 846 Thallium ND mg/kg 6010/SW 846 Vanadium 36 mg/kg 6010/SW 84 6 Zinc 71 mg/kg 6010/SW 84 6 SPECIFICATION : Title 22 (Hazardous Waste for TTLC (soil) ) SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances, Sec APPROVED : ] Rocketdyne SSFL Analytical Chemistry SIGNED : Rocketdyne SSFL Analytica Th stry I I II I i I I BNA H D M Se

3 SSFL ANALYTICAL CHEMISTRY (818) D/392 SS TO : Rocketdyne Environmental Protection Requester : Sodium Disposal Fac. Dept/Group : MAIL : T88 6 PHONE : REPORT DATE : 11/24/92 DATE OF ANALYSIS : 11/23/9 2 Sample Descrption : Soil, Bins : 52260, 52161, , B-30, Requested Analysis : 8240 Received : 11/16/92 Sampler : M. Halverson Sampler ID# : Sampled : :11 :0 0 ANALYTE per SW-846, #8240 RESULT, ug/kg MDL MC L Date Extracted 11/23/9 2 1,1,1-Trichloroethane (TCA) N.D ,1,2,2-Tetrachloroethane M.D ,1,2-Trichloroethane N.D ,1-Dichloroethane N.D ,1-Dichloroethylene N.D ,2-Dichlorobenzene N.D ,2-Dichloroethane N.D ,2-Dichloroethylene (cis) N.D ,2-Dichloroethylene (trans) N.D ,2-Dichloropropane N.D ,3-Dichlorobenzene N.D ,3-Dichloropropene (cis) N.D ,3-Dichloropropene (trans) N.D ,4-Dichlorobenzene Acetone N.D. 7.9 Benzene N.D. 0.7 Bromodichloromethane N.D. 0.6 Bromoform N.D. 0.5 Bromomethane N.D. 1.0 Carbon Tetrachloride N.D. 0.5 Chloroethane N.D. 1.0 Chloroform N.D. 0.8 Chloromethane N.D. 0.6 Di bromochloromethane N.D. 0.4 Ethylbenzene N.D. 0.8 Freon 113 N.D. 0.8 Methylene Chloride N.D. 2.9 Monochtorobenzene N.D. 0.6 Tetrachloroethylene N.D. 0.8 Toluene N.D. 0.7 Trichloroethylene (TCE) N.D. 0.6 Trichlorofluoromethane N.D. 0.8 Vinyl Chloride N-D. 0-4 Kytenes (Total) N.D. 1.4 SPECIFICATION : Title 22 (Soil for Method SW ) SPECIAL NOTES : Application not provided by requester, thus mcl is not specified. SIGNED : I I I II I I I I BNA HDMSe

4 SSFL ANALYTICAL CHEMISTR Y Dept/Group : MAIL : T REPORT DATE : 11/19/9 2 SAMPLE INFORMATIO N Sample Descrption : Soil, Bins : 52260, 52161, , B-30, Requested Analysis: 8080 Received : 11/16/92 Sampler : M. Halverson Sampler ID# : B Sampled : 14 :30 :0 0 ANALYTE RESULT UNITS METHOD / SOURCE PCB 1254 in soil 1.3 mg / Kg SW846, Method 8080 SPECIFICATION : (PCB analysis ) SPECIAL NOTES : APPROVED : Ir C. L l, -sil ti 1 ~..~Scn SIGNED : Rocketdyne SSFL Analytical Chemistry etdyne SSFL Anal ical Chemistry I i I I I I BNA H D M Se

5 I i I I I 9 BNA HDMSe SSFL ANALYTICAL CHEMISTRY Dept /Group : MAIL : T REPORT DATE : 11/25/9 2 Sample Descrption : Soil, Bins : 52260, 52161, , B-30, 1178 Re q uested Analysis : Metals Rece ive d : 11 / 16 / 92 Sampler : M. Halverson Sampler ID # : A Sampled : 11/16 / 14 :30 :0 0 ANALYTE RESULT UNITS METHOD/ SOURC E Antimony ND mg/kg 6010/SW 84 6 Arsenic ND mg/kg 6010/SW 846 Barium 92 mg/kg 60101SW 84 6 Beryllium ND mg /kg 6010/SW 84 6 Cadmium 0.75 mg/kg 6010/SW 84 6 Chromium 26 mg/kg 6010/SW 84 6 Cobalt 7.8 mg/kg 6010/SW 846 Copper 11 mg/kg 6010/SW 846 Lead NO mg / kg 6010/SW 846 Mercury 27 mg / kg 7471/SW 846 Molybdenum ND mg / kg 6010/SW 84 6 Nickel 24 mg / kg 6010/SW 84 6 Selenium NO mg / kg 6010/SW 84 6 Silver ND mg / kg 6010/SW 84 6 Thallium ND mg/kg 6010/SW 84 6 Vanadium 37 mg/ kg 6010/SW 846 Zinc 53 mg/ kg 6010/SW SPECIFICATION : Title 22 ( Hazardous Waste for TTLC (soil) ) SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances, Sec APPROVED : Al '~ oa-4~-~ SIGNED : Rocketdyne SSFL Analytical Chemistry Rocketdyne SSFL Analytical Chemistry