Appendix D Analytical Results-1 of 2

Transcription

1 Appendix D Analytical Results-1 of 2

2 ATTN: Clifton Samoiloff Commerce Drive Winnipeg MB R3P 0Y7 Phone: Date Received: Report Date: Version: 05-OCT-10 15:38 (MT) FINAL REV. 2 Certificate of Analysis Lab Work Order #: L Project P.O. #: NOT SUBMITTED ob Reference: Legal Site Desc: C of C Numbers: Comments: ADDITIONAL 28-SEP-10 13:41 05-OCT-10: Robert S. Kitlar Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 1329 Niakwa Road East, Unit 12, Winnipeg, MB R2 3T4 Canada Phone: Fax: MANITOBA TECHNOLOGY CENTRE LTD. Part of the ALS Group A Campbell Brothers Limited Company

3 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 2 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL4-F10-WQ1 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) SK, CH, MH, M on 10-SEP-10 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Color, True Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total < < < < < < <0.50 < < <0.50 < < <0.0 < < <0.00 < T.C.U. NTU 11-SEP SEP SEP SEP SEP SEP-10 R R R R R R R R R R14693 R R R R14693 R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

4 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 3 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL4-F10-WQ1 Sampled By: Matrix: SK, CH, MH, M on 10-SEP-10 WATER Total Metals by ICP-MS Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved < < < < < < R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

5 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 4 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: UL4-F10-WQ1 SK, CH, MH, M on 10-SEP-10 WATER Dissolved Metals by ICP-MS Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < < < ug/l ug/l ABS Ratio umhos/cm ph units 11-SEP SEP SEP-10 R R R R R R14651 R14651 R14651 R14651 R14651 R14651 L Sampled By: UL4-F10-WQ2 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) SK, CH, MH, M on 10-SEP-10 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Color, True Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total < < < < < < <0.50 < < <0.50 < T.C.U. NTU 11-SEP SEP SEP SEP SEP SEP-10 R R R R R R R R R R14693 R R R R14693 R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

6 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 5 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL4-F10-WQ2 Sampled By: Matrix: SK, CH, MH, M on 10-SEP-10 WATER Total Metals by ICP-MS Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved < < <0.0 < < <0.00 < < < < < < < < R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

7 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 6 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL4-F10-WQ2 Sampled By: Matrix: SK, CH, MH, M on 10-SEP-10 WATER Dissolved Metals by ICP-MS Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph 19.1 < <0.00 < < < ug/l ug/l ABS Ratio umhos/cm ph units 11-SEP SEP SEP-10 R R R R R R R R R R R R R R R R R R R R R R R R R R14651 R14651 R14651 R14651 R14651 R14651 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

8 Reference Information L CONTD... PAGE 7 of 9 QC Samples with Qualifiers & Comments: QC Type Description Parameter Matrix Spike Total Kjeldahl Nitrogen Qualifier MS-B Applies to Sample Number(s) L , -2 Test Method References: ALS Test Code Matrix Test Description Method Reference** ACIDITY-LOW-WP Acidity APHA Method 2310B ALK-TOT-WP Alkalinity APHA 23B Alkalinity of water is a measure of its acid neutralizing capacity. Alkalinity is imparted by bicarbonate, carbonate and hydroxide components of water. It is determined by titration with a standard solution of strong mineral acid to the successive HCO3- and H2CO3 endpoints indicated electrometrically. ANIONS5-IC-WP Anions scan (IC) EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". BR-IC-WP Bromide EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". C-DIS-ORG-WP Dissolved Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-INORG-WP Total Inorganic Carbon APHA 5310 B-Instrumental This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-ORG-CL Total Organic Carbon APHA 5310 C-Instrumental C-TOT-ORG-WP Total Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. CHL/A,PHEO/A-ACET-WP Chlorophyll-a & Pheophytin-a APHA H, /750NM Chlorophyll-a is filtered from the sample, then extracted with 90 (v/v) acetone. Absorbance is measured spectrophotometrically at 664 nm and 750 nm. The extract is then acidified, converting chlorophyll-a to phaeophytin-a. Absorbance is determined again after acidification. The chlorophyll-a concentration is determined from the decrease in absorbance upon acidification. When a detection limit of 0.5 ug/l is required, the volume of sample filtered is doubled to 700mL. Samples with an OD664 before/od665 after acidification ratio (664b/665a) of 1.70 are considered to contain no pheophytin a and to be in excellent physiological condition. Solutions of pure pheophytin show no reduction in OD665 upon acidification and have a 664b/665a ratio of Thus, mixtures of chlorophyll a and pheophytin a have absorption peak ratios ranging between and 1.7. These ratios are based on the use of 90 acetone as solvent.

9 Reference Information L CONTD... PAGE 8 of 9 Test Method References: ALS Test Code Matrix Test Description Method Reference** COL-TRU-WP True Colour APHA, AWWA, WPCF Colour is measured by visual comparison against a routinely calibrated color disk. True color is the color of water from which turbidity has been removed by centrifugation. CONSULT-BOD-CBOD- WP Carbonaceous BOD APHA 5210 B-5 day Incub.-O2 electrode A sample of water is incubated for 5 days at degrees Celcius. Comparison of dissolved oxygen content at beginning and end of incubation provides a measure of Biochemical oxygen demand. If carbonaceous BOD is requested, TCMP is added to the sample to chemically inhibit nitrogenous oxygen demand. If soluble BOD is requested, the sample is filtered prior to analysis. EC-WP Conductivity APHA 2510B Conductivity of an aqueous solution refers to its ability to carry an electric current. Conductance of a solution is measured between two spatially fixed and chemically inert electrodes. ETL-HARDNESS-DIS-WP ETL-HARDNESS-TOT-WP HG-D-CVAF-WP Hardness Calculated Hardness Calculated Mercury Dissolved Calculated Calculated EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. HG-T-CVAF-WP Mercury Total EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. MET-D-L-MS-WP Dissolved Metals by ICP-MS U.S. EPA 0.8-DL Dissolved Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the Examination of and Wastewater method 3030B for filtration through a 0.45 um filter and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. MET-T-L-MS-WP Total Metals by ICP-MS U.S. EPA 0.8-TL Total Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the examination of and Wastewater Method 3030E and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. N-TOTK-WP Total Kjeldahl Nitrogen Quickchem method E Lachat Samples are digested with a sulphuric acid solution, cooled, diluted with water, and analyzed for ammonia. Total Kjeldahl nitrogen is the sum of freeammonia and organic nitrogen compounds which are converted to ammonium sulphate through this digestion process. Analysis is performed by Flow Injection Analysis (FIA). The ph of the digested sample is raised to a known, basic ph by neutralization with a concentrated buffer solution. This neutralization converts the ammonium cation to ammonia. The ammonia produced is heated with saliclyate and hypochlorite to produce blue colour which is proportional to the ammonia concentration. NH3-COL-WP Ammonia by colour APHA 4500 NH3 F Ammonia - Colourimeric using Salicylate-nitroprusside and hypochlorite, in an alkaline phosphate buffer. NO2+NO3-CALC-WP Nitrate+Nitrite CALCULATION P-TOTAL-WP Phosphorus, Total APHA, 18 P-T Samples are digested using a sulphuric acid-persulfate mixture to convert organic phosphorous to orthophosphate. The samples are analyzed by either the Flow Injection Analysis (FIA) or the Segmented Flow Analysis (SFA) method. The absorbance measured by the instrument is proportional to the concentration of orthophosphate in the sample, and is reported as phosphorous.

10 Reference Information L CONTD... PAGE 9 of 9 Test Method References: ALS Test Code Matrix Test Description Method Reference** PH-WP ph APHA 4500H ph of a sample is the determination of the activity of the hydrogen ions by potentiometric measurement using a standard hydrogen electrode and a reference electrode. SILICATE-COL-VA Silicate by Colourimetric analysis APHA 4500-SIO2 D. This analysis is carried out using procedures adapted from APHA Method 4500-SiO2 D. "Silica". Silicate (molybdate-reactive silica) is determined by the molybdosilicate-heteropoly blue colourimetric method. SOLIDS-TDS-WP Total Dissolved Solids APHA 2540 The residue remaining in a prepared casserole after passing the sample through a 1.2 um Whatman GF/C glass microfibre filter and drying at 180 degrees C. Samples may be dried at 105 degrees C if the client specifically requests this drying temperature. SOLIDS-TOTSUS-WP Total Suspended Solids APHA 2540 The residue retained by a prepared 1.5 um Whatman 934-AH glass microfibre filter dried at 105 degrees C. TURBIDITY-WP Turbidity APHA, 18, 2130B A strong light beam is sent through a transparent tube containing the sample. Light that is reflected at 90 degrees to the axis by suspended particles is detected by the photocell. The electrical response is proportional to the sample turbidity. ** ALS test methods may incorporate modifications from specified reference methods to improve performance. The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code WP VA CL Laboratory Location ALS LABORATORY GROUP - WINNIPEG, MANITOBA, CANADA ALS LABORATORY GROUP - VANCOUVER, BC, CANADA ALS LABORATORY GROUP - CALGARY, ALBERTA, CANADA Chain of Custody Numbers: GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

11 Workorder: L Report Date: 05-OCT-10 Page 1 of Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ACIDITY-LOW-WP Batch R WG CVS Acidity (as CaCO3) ALK-TOT-WP Batch R14651 WG CVS Alkalinity, Total (as CaCO3) WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) L < < ANIONS5-IC-WP Batch R WG LCS Chloride Nitrite-N Nitrate-N Sulfate WG Chloride Nitrite-N Nitrate-N Sulfate MB <0.50 < < < BR-IC-WP Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 C-DIS-ORG-WP Batch R WG CCV Dissolved Organic Carbon SEP-10 WG CVS

12 Workorder: L Report Date: 05-OCT-10 Page 2 of C-DIS-ORG-WP Batch R WG CVS Dissolved Organic Carbon 29-SEP-10 WG MB Dissolved Organic Carbon < 1 29-SEP-10 C-TOT-INORG-WP Batch R WG CCV Total Inorganic Carbon WG CVS Total Inorganic Carbon WG MB Total Inorganic Carbon < 1 C-TOT-ORG-WP Batch R WG CCV Total Organic Carbon 01-OCT-10 WG CVS Total Organic Carbon 30-SEP-10 WG MB Total Organic Carbon < 1 30-SEP-10 CHL/A,PHEO/A-ACET-WP Batch R WG CVS Chlorophyll a WG Chlorophyll a CVS COL-TRU-WP Batch R WG DUP Color, True L T.C.U SEP-10 WG Color, True MB <5.0 T.C.U SEP-10 CONSULT-BOD-CBOD-WP Batch R WG DUP BOD Carbonaceous L < < WG IRM 61-GG

13 Workorder: L Report Date: 05-OCT-10 Page 3 of CONSULT-BOD-CBOD-WP Batch R WG IRM BOD Carbonaceous 61-GG WG MB BOD Carbonaceous < 1 EC-WP Batch R14651 WG CCV Conductivity WG Conductivity CVS WG Conductivity DUP L umhos/cm HG-D-CVAF-WP Batch R WG DUP L WG LCS WG MB WG MB WG MS L WG MS L HG-T-CVAF-WP Batch R WG DUP L

14 Workorder: L Report Date: 05-OCT-10 Page 4 of HG-T-CVAF-WP Batch R WG LCS WG MB WG MS L WG MS L WG MS L WG MS L MET-D-L-MS-WP Batch R WG CCV Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved

15 Workorder: L Report Date: 05-OCT-10 Page 5 of MET-D-L-MS-WP Batch R WG CCV Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved 104 WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved

16 Workorder: L Report Date: 05-OCT-10 Page 6 of MET-D-L-MS-WP Batch R WG CVS Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved

17 Workorder: L Report Date: 05-OCT-10 Page 7 of MET-D-L-MS-WP Batch R WG CVS Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG LCS

18 Workorder: L Report Date: 05-OCT-10 Page 8 of MET-D-L-MS-WP Batch R WG LCS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved

19 Workorder: L Report Date: 05-OCT-10 Page 9 of MET-D-L-MS-WP Batch R WG LCS Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG MB Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved <0.00 < < < < < <0.00 < < <0.0 < <

20 Workorder: L Report Date: 05-OCT-10 Page 10 of MET-D-L-MS-WP Batch R WG MB Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved <0.00 < Batch R WG CCV Copper (Cu)-Dissolved WG CVS Copper (Cu)-Dissolved WG CVS Copper (Cu)-Dissolved MET-T-L-MS-WP Batch R WG CCV Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 94

21 Workorder: L Report Date: 05-OCT-10 Page 11 of MET-T-L-MS-WP Batch R WG CCV Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total 93 94

22 Workorder: L Report Date: 05-OCT-10 Page 12 of MET-T-L-MS-WP Batch R WG CVS Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total 104

23 Workorder: L Report Date: 05-OCT-10 Page 13 of MET-T-L-MS-WP Batch R WG CVS Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG LCS Aluminum (Al)-Total 95

24 Workorder: L Report Date: 05-OCT-10 Page 14 of MET-T-L-MS-WP Batch R WG LCS Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total

25 Workorder: L Report Date: 05-OCT-10 Page 15 of MET-T-L-MS-WP Batch R WG LCS Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 93 WG MB Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total < < < < <0.0 < <0.00 < < <0.00 <0. <0.0 < <

26 Workorder: L Report Date: 05-OCT-10 Page 16 of MET-T-L-MS-WP Batch R WG MB Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total < < Batch R WG CCV Copper (Cu)-Total WG CVS Copper (Cu)-Total WG CVS Copper (Cu)-Total N-TOTK-WP Batch R WG CCV Total Kjeldahl Nitrogen WG CVS Total Kjeldahl Nitrogen WG LCS Total Kjeldahl Nitrogen WG MB Total Kjeldahl Nitrogen < WG MS Total Kjeldahl Nitrogen L MS-B - NH3-COL-WP Batch R WG CCV Ammonia as N WG Ammonia as N LCS WG Ammonia as N MB < 0.05 P-TOTAL-WP

27 Workorder: L Report Date: 05-OCT-10 Page 17 of P-TOTAL-WP Batch R WG CCV Phosphorus, Total WG CCV Phosphorus, Total WG CVS Phosphorus, Total 95 WG CVS Phosphorus, Total WG CVS Phosphorus, Total 106 WG CVS Phosphorus, Total 104 WG MS Phosphorus, Total L PH-WP Batch R14651 WG CCV ph WG ph CVS - WG ph DUP L ph units SILICATE-COL-VA Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 SOLIDS-TDS-WP Batch R14693 WG CVS Total Dissolved Solids WG MB Total Dissolved Solids <5.0 5

28 Workorder: L Report Date: 05-OCT-10 Page 18 of SOLIDS-TOTSUS-WP Batch R14693 WG CVS Total Suspended Solids WG MB Total Suspended Solids <5.0 5 TURBIDITY-WP Batch R WG CCV Turbidity 11-SEP-10 WG Turbidity CCV SEP-10 WG Turbidity CVS 11-SEP-10 WG Turbidity CVS 11-SEP-10 WG Turbidity MB < NTU SEP-10

29 Workorder: L Report Date: 05-OCT-10 Page 19 of Legend: Limit Confidence Interval (Laboratory Control Limits) DUP Duplicate RPD Relative Percent Difference Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description Duplicate results and limits are expressed in terms of absolute difference. MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. Relative Percent Difference Not Available due to result(s) being less than detection limit.

30 Workorder: L Report Date: 05-OCT-10 Page of Hold Time Exceedances: ALS Product Description Physical Tests ph Anions and Nutrients Anions scan (IC) Bromide Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: Sample ID Sampling Date Date Processed Rec. HT Actual HT SEP SEP SEP SEP SEP SEP-10 12:52 12:52 15:19 15:19 15:19 15:19 Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L were received on 10:00. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS Units hours hours hours hours hours hours Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units). Qualifier EHTR-FM EHTR-FM EHTR EHTR EHTR EHTR The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

31

32 ATTN: CLIFF SAMOILOFF COMMERCE DRIVE WINNIPEG MB R3P 0Y7 Phone: Date Received: Report Date: Version: 21-OCT-10 13:33 (MT) FINAL REV. 3 Certificate of Analysis Lab Work Order #: L Project P.O. #: NOT SUBMITTED ob Reference: Legal Site Desc: C of C Numbers: Comments: ADDITIONAL -OCT-10 14:47 ADDITIONAL 13-OCT-10 12:15 ADDITIONAL 28-SEP-10 13:42 18-OCT-10: 21-OCT-10: Robert S. Kitlar Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 1329 Niakwa Road East, Unit 12, Winnipeg, MB R2 3T4 Canada Phone: Fax: MANITOBA TECHNOLOGY CENTRE LTD. Part of the ALS Group A Campbell Brothers Limited Company

33 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 2 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL5-F10-WQ1 Sampled By: CLIENT on 12-SEP-10 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total < < < < < <0.50 < < < <0.50 < < < <0.0 < < <0.00 < CU NTU 30-SEP-10 -OCT OCT SEP-10 R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

34 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 3 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL5-F10-WQ1 Sampled By: Matrix: CLIENT on 12-SEP-10 WATER Total Metals by ICP-MS Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved < < < < < < < < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

35 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 4 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: UL5-F10-WQ1 CLIENT on 12-SEP-10 WATER Dissolved Metals by ICP-MS Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < < < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: UL5-F10-WQ2 CLIENT on 12-SEP-10 Matrix: WATER Miscellaneous Parameters Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total < < < < <0.50 < < < <0.50 < CU NTU 30-SEP-10 -OCT OCT SEP-10 R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

36 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 5 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL5-F10-WQ2 Sampled By: Matrix: CLIENT on 12-SEP-10 WATER Total Metals by ICP-MS Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved < <0.0 < < <0.00 < < < < < < < < < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

37 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 6 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: UL5-F10-WQ2 CLIENT on 12-SEP-10 WATER Dissolved Metals by ICP-MS Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph.2 < <0.00 < < < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: UL3-F10-WQ1 CLIENT on 12-SEP-10 Matrix: WATER Miscellaneous Parameters Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N < < CU 30-SEP-10 -OCT-10 R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

38 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 7 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL3-F10-WQ1 Sampled By: Matrix: CLIENT on 12-SEP-10 WATER Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < < < < < <0.0 < <0.00 < < NTU 15-OCT SEP-10 R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

39 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 8 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL3-F10-WQ1 Sampled By: Matrix: CLIENT on 12-SEP-10 WATER Total Metals by ICP-MS Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity < < < < < < < < < < ug/l ug/l ABS Ratio umhos/cm R1475 R1475 R1475 R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

40 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 9 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: ph ph UL3-F10-WQ1 CLIENT on 12-SEP-10 WATER 8.53 ph units R L Sampled By: UL3-F10-WQ2 CLIENT on 12-SEP-10 Matrix: WATER Miscellaneous Parameters Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total < < < < < < < < <0.0 < CU NTU 30-SEP-10 -OCT OCT SEP-10 R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

41 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 10 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL3-F10-WQ2 Sampled By: Matrix: CLIENT on 12-SEP-10 WATER Total Metals by ICP-MS Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved <0.00 < < < < < < < < < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

42 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 11 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UL3-F10-WQ2 Sampled By: Matrix: CLIENT on 12-SEP-10 WATER Dissolved Metals by ICP-MS Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

43 Reference Information L CONTD... PAGE 12 of 14 Qualifiers for Individual Samples Listed: Sample Numbe Client ID Qualifier Description L UL3-F10-WQ2 EHT Silicate analyses past hold time - Exceeded Recommended Holding Time Prior To Analysis Test Method References: ALS Test Code Matrix Test Description Method Reference** ACIDITY-LOW-WP Acidity APHA Method 2310B ALK-TOT-WP Alkalinity APHA 23B Alkalinity of water is a measure of its acid neutralizing capacity. Alkalinity is imparted by bicarbonate, carbonate and hydroxide components of water. It is determined by titration with a standard solution of strong mineral acid to the successive HCO3- and H2CO3 endpoints indicated electrometrically. ANIONS5-IC-WP Anions scan (IC) EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". BR-IC-WP Bromide EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". C-DIS-ORG-WP Dissolved Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-INORG-WP Total Inorganic Carbon APHA 5310 B-Instrumental This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-ORG-WP Total Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. CHL/A,PHEO/A-ACET-WP Chlorophyll-a & Pheophytin-a APHA H, /750NM Chlorophyll-a is filtered from the sample, then extracted with 90 (v/v) acetone. Absorbance is measured spectrophotometrically at 664 nm and 750 nm. The extract is then acidified, converting chlorophyll-a to phaeophytin-a. Absorbance is determined again after acidification. The chlorophyll-a concentration is determined from the decrease in absorbance upon acidification. When a detection limit of 0.5 ug/l is required, the volume of sample filtered is doubled to 700mL. Samples with an OD664 before/od665 after acidification ratio (664b/665a) of 1.70 are considered to contain no pheophytin a and to be in excellent physiological condition. Solutions of pure pheophytin show no reduction in OD665 upon acidification and have a 664b/665a ratio of Thus, mixtures of chlorophyll a and pheophytin a have absorption peak ratios ranging between and 1.7. These ratios are based on the use of 90 acetone as solvent.

44 Reference Information L CONTD... PAGE 13 of 14 Test Method References: ALS Test Code Matrix Test Description Method Reference** COLOUR-TRUE-WP Colour, True APHA 4500 COLOR This analysis is carried out using procedures adapted from APHA 21 "Color". Colour (True Colour) is determined by filtering a sample through a 0.45 micron membrane filter followed by analysis of the filtrate using the platinum-cobalt colourimetric method. Colour is ph dependent. Unless otherwise indicated, reported colour results pertain to the ph of the sample as received to within +/- 1 ph unit. CONSULT-BOD-CBOD- WP Carbonaceous BOD APHA 5210 B-5 day Incub.-O2 electrode A sample of water is incubated for 5 days at degrees Celcius. Comparison of dissolved oxygen content at beginning and end of incubation provides a measure of Biochemical oxygen demand. If carbonaceous BOD is requested, TCMP is added to the sample to chemically inhibit nitrogenous oxygen demand. If soluble BOD is requested, the sample is filtered prior to analysis. EC-WP Conductivity APHA 2510B Conductivity of an aqueous solution refers to its ability to carry an electric current. Conductance of a solution is measured between two spatially fixed and chemically inert electrodes. ETL-HARDNESS-DIS-WP ETL-HARDNESS-TOT-WP HG-D-CVAF-WP Hardness Calculated Hardness Calculated Mercury Dissolved Calculated Calculated EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. HG-T-CVAF-WP Mercury Total EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. MET-D-L-MS-WP Dissolved Metals by ICP-MS U.S. EPA 0.8-DL Dissolved Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the Examination of and Wastewater method 3030B for filtration through a 0.45 um filter and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. MET-T-L-MS-WP Total Metals by ICP-MS U.S. EPA 0.8-TL Total Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the examination of and Wastewater Method 3030E and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. N-TOTK-WP Total Kjeldahl Nitrogen Quickchem method E Lachat Samples are digested with a sulphuric acid solution, cooled, diluted with water, and analyzed for ammonia. Total Kjeldahl nitrogen is the sum of freeammonia and organic nitrogen compounds which are converted to ammonium sulphate through this digestion process. Analysis is performed by Flow Injection Analysis (FIA). The ph of the digested sample is raised to a known, basic ph by neutralization with a concentrated buffer solution. This neutralization converts the ammonium cation to ammonia. The ammonia produced is heated with saliclyate and hypochlorite to produce blue colour which is proportional to the ammonia concentration. NH3-COL-WP Ammonia by colour APHA 4500 NH3 F Ammonia - Colourimeric using Salicylate-nitroprusside and hypochlorite, in an alkaline phosphate buffer. NO2+NO3-CALC-WP Nitrate+Nitrite CALCULATION P-TOTAL-WP Phosphorus, Total APHA, 18 P-T Samples are digested using a sulphuric acid-persulfate mixture to convert organic phosphorous to orthophosphate. The samples are analyzed by either the Flow Injection Analysis (FIA) or the Segmented Flow Analysis (SFA) method. The absorbance measured by the instrument is proportional to the concentration of orthophosphate in the sample, and is reported as phosphorous.

45 Reference Information L CONTD... PAGE 14 of 14 Test Method References: ALS Test Code Matrix Test Description Method Reference** PH-WP ph APHA 4500H ph of a sample is the determination of the activity of the hydrogen ions by potentiometric measurement using a standard hydrogen electrode and a reference electrode. SILICATE-COL-VA Silicate by Colourimetric analysis APHA 4500-SIO2 D. This analysis is carried out using procedures adapted from APHA Method 4500-SiO2 D. "Silica". Silicate (molybdate-reactive silica) is determined by the molybdosilicate-heteropoly blue colourimetric method. SOLIDS-TDS-WP Total Dissolved Solids APHA 2540 The residue remaining in a prepared casserole after passing the sample through a 1.2 um Whatman GF/C glass microfibre filter and drying at 180 degrees C. Samples may be dried at 105 degrees C if the client specifically requests this drying temperature. SOLIDS-TOTSUS-WP Total Suspended Solids APHA 2540 The residue retained by a prepared 1.5 um Whatman 934-AH glass microfibre filter dried at 105 degrees C. TURBIDITY-WP Turbidity APHA, 18, 2130B A strong light beam is sent through a transparent tube containing the sample. Light that is reflected at 90 degrees to the axis by suspended particles is detected by the photocell. The electrical response is proportional to the sample turbidity. ** ALS test methods may incorporate modifications from specified reference methods to improve performance. The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code WP VA Laboratory Location ALS LABORATORY GROUP - WINNIPEG, MANITOBA, CANADA ALS LABORATORY GROUP - VANCOUVER, BC, CANADA Chain of Custody Numbers: GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

46 Workorder: L Report Date: 21-OCT-10 Page 1 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF ACIDITY-LOW-WP Batch R WG CVS Acidity (as CaCO3) WG DUP Acidity (as CaCO3) L ALK-TOT-WP Batch R WG CVS Alkalinity, Total (as CaCO3) WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < ANIONS5-IC-WP Batch R WG LCS Chloride Fluoride Nitrite-N Nitrate-N Sulfate WG Chloride MB < Fluoride < 0.1 Nitrite-N < 0.05 Nitrate-N < 0.05 Sulfate < BR-IC-WP

47 Workorder: L Report Date: 21-OCT-10 Page 2 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF BR-IC-WP Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 C-DIS-ORG-WP Batch R WG CCV Dissolved Organic Carbon SEP-10 WG CVS Dissolved Organic Carbon 29-SEP-10 WG DUP Dissolved Organic Carbon L SEP-10 WG MB Dissolved Organic Carbon < 1 29-SEP-10 C-TOT-INORG-WP Batch R WG CCV Total Inorganic Carbon 105 WG CVS Total Inorganic Carbon WG DUP Total Inorganic Carbon L SEP-10 WG MB Total Inorganic Carbon < 1 C-TOT-ORG-WP Batch R WG CCV Total Organic Carbon 01-OCT-10 WG CVS Total Organic Carbon 30-SEP-10 WG MB Total Organic Carbon < 1 30-SEP-10 CHL/A,PHEO/A-ACET-WP Batch R1475 WG CVS Chlorophyll a WG CVS

48 Workorder: L Report Date: 21-OCT-10 Page 3 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF CHL/A,PHEO/A-ACET-WP Batch R1475 WG CVS Chlorophyll a WG Chlorophyll a MB < ug/l 1 Phaeophytin a < ug/l 1 COLOUR-TRUE-WP Batch R WG DUP Colour, True L CU 0.1 WG Colour, True DUP L CU 2.2 WG Colour, True LCS WG Colour, True MB <5.0 CU 5 CONSULT-BOD-CBOD-WP Batch R WG DUP BOD Carbonaceous L WG IRM BOD Carbonaceous 61-GG WG MB BOD Carbonaceous < 1 EC-WP Batch R WG CCV Conductivity WG Conductivity CVS WG Conductivity DUP L umhos/cm HG-D-CVAF-WP Batch R WG DUP L WG DUP L

49 Workorder: L Report Date: 21-OCT-10 Page 4 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF HG-D-CVAF-WP Batch R WG DUP L WG DUP L WG LCS WG MB WG MB WG MS L WG MS L WG MS L HG-T-CVAF-WP Batch R WG DUP L WG DUP L WG DUP L WG DUP L

50 Workorder: L Report Date: 21-OCT-10 Page 5 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF HG-T-CVAF-WP Batch R WG DUP L WG LCS WG MB WG MS L WG MS L WG MS L WG MS L MET-D-L-MS-WP Batch WG CCV Aluminum (Al)-Dissolved 105 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved 104 Cobalt (Co)-Dissolved 104

51 Workorder: L Report Date: 21-OCT-10 Page 6 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CCV Copper (Cu)-Dissolved 104 Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved 105 Manganese (Mn)-Dissolved 104 Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 106 Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved 107 Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 93 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 94 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved

52 Workorder: L Report Date: 21-OCT-10 Page 7 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CVS Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 95 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved 105 Antimony (Sb)-Dissolved 95

53 Workorder: L Report Date: 21-OCT-10 Page 8 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CVS Arsenic (As)-Dissolved Barium (Ba)-Dissolved 95 Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved 106 Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved

54 Workorder: L Report Date: 21-OCT-10 Page 9 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CVS Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG DUP Aluminum (Al)-Dissolved WG <0.00 <0.00 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < Cadmium (Cd)-Dissolved < < Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < < Lead (Pb)-Dissolved < < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < < Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved

55 Workorder: L Report Date: 21-OCT-10 Page 10 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG DUP Thallium (Tl)-Dissolved WG Thorium (Th)-Dissolved 26 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved <0.00 <0.00 Zirconium (Zr)-Dissolved < < WG LCS Aluminum (Al)-Dissolved 107 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved 104 Barium (Ba)-Dissolved 108 Beryllium (Be)-Dissolved 105 Bismuth (Bi)-Dissolved Boron (B)-Dissolved 105 Cadmium (Cd)-Dissolved 104 Calcium (Ca)-Dissolved 104 Cesium (Cs)-Dissolved 110 Chromium (Cr)-Dissolved 106 Cobalt (Co)-Dissolved 111 Copper (Cu)-Dissolved 106 Iron (Fe)-Dissolved 107 Lead (Pb)-Dissolved Lithium (Li)-Dissolved 105 Magnesium (Mg)-Dissolved 108 Manganese (Mn)-Dissolved 108 Molybdenum (Mo)-Dissolved 109 Nickel (Ni)-Dissolved 105 Phosphorus (P)-Dissolved 112 Potassium (K)-Dissolved 105 Rubidium (Rb)-Dissolved 111

56 Workorder: L Report Date: 21-OCT-10 Page 11 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG LCS Selenium (Se)-Dissolved 105 Silicon (Si)-Dissolved 117 Silver (Ag)-Dissolved 108 Sodium (Na)-Dissolved 108 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved 106 Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved 104 Titanium (Ti)-Dissolved 105 Tungsten (W)-Dissolved 104 Uranium (U)-Dissolved 107 Vanadium (V)-Dissolved 108 Zinc (Zn)-Dissolved 104 Zirconium (Zr)-Dissolved 107 WG MB Aluminum (Al)-Dissolved < Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < 0.01 Cadmium (Cd)-Dissolved < Calcium (Ca)-Dissolved < 0.05 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < 0.01 Lead (Pb)-Dissolved < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved < 0.01 Manganese (Mn)-Dissolved

57 Workorder: L Report Date: 21-OCT-10 Page 12 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG MB Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < 0.1 Potassium (K)-Dissolved < Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved < 0.05 Silver (Ag)-Dissolved Sodium (Na)-Dissolved < Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved < Zirconium (Zr)-Dissolved < Batch WG CCV Silicon (Si)-Dissolved 95 Vanadium (V)-Dissolved WG CVS Silicon (Si)-Dissolved 93 Vanadium (V)-Dissolved WG CVS Silicon (Si)-Dissolved Vanadium (V)-Dissolved MET-T-L-MS-WP

58 Workorder: L Report Date: 21-OCT-10 Page 13 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CCV Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 95 Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total 104 Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total

59 Workorder: L Report Date: 21-OCT-10 Page 14 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CCV Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total 104 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 95 Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total 95 Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total

60 Workorder: L Report Date: 21-OCT-10 Page 15 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CVS Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total 104 Copper (Cu)-Total Iron (Fe)-Total 106 Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total 104

61 Workorder: L Report Date: 21-OCT-10 Page 16 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CVS Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total 105 Zinc (Zn)-Total Zirconium (Zr)-Total WG DUP Aluminum (Al)-Total WG ,G Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total <0.0 <0.0 Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total

62 Workorder: L Report Date: 21-OCT-10 Page 17 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Manganese (Mn)-Total WG Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total < < WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total

63 Workorder: L Report Date: 21-OCT-10 Page 18 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Cobalt (Co)-Total WG Copper (Cu)-Total Iron (Fe)-Total <0.0 <0.0 Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total 7 Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG DUP Aluminum (Al)-Total WG < < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total

64 Workorder: L Report Date: 21-OCT-10 Page 19 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Bismuth (Bi)-Total WG Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < <

65 Workorder: L Report Date: 21-OCT-10 Page of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Zirconium (Zr)-Total WG < < WG DUP Aluminum (Al)-Total WG < < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26

66 Workorder: L Report Date: 21-OCT-10 Page 21 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Tin (Sn)-Total WG Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG LCS Aluminum (Al)-Total Antimony (Sb)-Total 104 Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total 104 Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total 95 Chromium (Cr)-Total 105 Cobalt (Co)-Total Copper (Cu)-Total 106 Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 95 Magnesium (Mg)-Total 106 Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total 105

67 Workorder: L Report Date: 21-OCT-10 Page 22 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG LCS Silver (Ag)-Total Sodium (Na)-Total 105 Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total 95 Vanadium (V)-Total 104 Zinc (Zn)-Total Zirconium (Zr)-Total WG LCS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total 109 Barium (Ba)-Total Beryllium (Be)-Total 113 Bismuth (Bi)-Total 92 Boron (B)-Total 119 Cadmium (Cd)-Total Calcium (Ca)-Total 90 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total 85 Lead (Pb)-Total 89 Lithium (Li)-Total 88 Magnesium (Mg)-Total Manganese (Mn)-Total 93 Molybdenum (Mo)-Total Nickel (Ni)-Total

68 Workorder: L Report Date: 21-OCT-10 Page 23 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG LCS Phosphorus (P)-Total 94 Potassium (K)-Total 88 Rubidium (Rb)-Total 89 Selenium (Se)-Total 109 Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 90 Tellurium (Te)-Total Thallium (Tl)-Total 93 Thorium (Th)-Total 90 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total 95 Uranium (U)-Total 84 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 90 WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total < Lead (Pb)-Total <

69 Workorder: L Report Date: 21-OCT-10 Page 24 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG MB Lithium (Li)-Total < Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total < Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total Sodium (Na)-Total < Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total

70 Workorder: L Report Date: 21-OCT-10 Page 25 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG MB Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total < Lead (Pb)-Total < Lithium (Li)-Total < Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total < Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total Sodium (Na)-Total < Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < Batch WG CCV Silicon (Si)-Total 95 Vanadium (V)-Total WG CVS Silicon (Si)-Total 93

71 Workorder: L Report Date: 21-OCT-10 Page 26 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CVS Vanadium (V)-Total WG CVS Silicon (Si)-Total Vanadium (V)-Total N-TOTK-WP Batch R WG CCV Total Kjeldahl Nitrogen WG CVS Total Kjeldahl Nitrogen WG DUP Total Kjeldahl Nitrogen L WG LCS Total Kjeldahl Nitrogen WG MB Total Kjeldahl Nitrogen < WG MS Total Kjeldahl Nitrogen L NH3-COL-WP Batch R WG CCV Ammonia as N WG Ammonia as N DUP L WG Ammonia as N LCS WG Ammonia as N MB < 0.05 P-TOTAL-WP Batch R WG CCV Phosphorus, Total 104 WG CCV Phosphorus, Total WG CVS Phosphorus, Total 105

72 Workorder: L Report Date: 21-OCT-10 Page 27 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF P-TOTAL-WP Batch R WG CVS Phosphorus, Total WG DUP Phosphorus, Total L WG MB Phosphorus, Total < 0.01 WG MS Phosphorus, Total L PH-WP Batch R WG CCV ph WG ph CVS - WG ph DUP L ph units SILICATE-COL-VA Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK OCT-10 WG CRM Silicate (as SIO2) VA-SIO2-CSPK OCT-10 WG CRM Silicate (as SIO2) VA-SIO2-CSPK OCT-10 WG DUP Silicate (as SIO2) L < < 15-OCT-10 WG DUP Silicate (as SIO2) L OCT-10 WG DUP Silicate (as SIO2) L OCT-10 WG MB Silicate (as SIO2) < 1 15-OCT-10 WG MB Silicate (as SIO2) < 1 15-OCT-10 WG MB Silicate (as SIO2) < 1 16-OCT-10 SOLIDS-TDS-WP

73 Workorder: L Report Date: 21-OCT-10 Page 28 of 30 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF SOLIDS-TDS-WP Batch R WG CVS Total Dissolved Solids WG DUP Total Dissolved Solids L WG DUP Total Dissolved Solids L WG MB Total Dissolved Solids <5.0 5 SOLIDS-TOTSUS-WP Batch R WG CVS Total Suspended Solids WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG MB Total Suspended Solids <5.0 5 TURBIDITY-WP Batch R WG CCV Turbidity WG Turbidity CCV 104 WG Turbidity CVS WG Turbidity CVS WG Turbidity DUP L NTU WG Turbidity LCS WG Turbidity MB < NTU 0.1

74 Workorder: L Report Date: 21-OCT-10 Page 29 of 30 Legend: Limit Confidence Interval (Laboratory Control Limits) DUP Duplicate RPD Relative Percent Difference Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description Duplicate results and limits are expressed in terms of absolute difference. Relative Percent Difference Not Available due to result(s) being less than detection limit.

75 Workorder: L Report Date: 21-OCT-10 Page 30 of 30 Hold Time Exceedances: ALS Product Description Physical Tests ph Anions and Nutrients Anions scan (IC) Silicate by Colourimetric analysis Aggregate Organics Carbonaceous BOD Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: Sample ID Sampling Date Date Processed Rec. HT Actual HT SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP SEP-10 16:27 16:27 16:27 16:27 15:19 15:19 15:19 15:19 15-OCT-10 16:30 15-OCT-10 16:30 15-OCT-10 16:32 15-OCT-10 16:33 12:18 12:18 12:18 12: Units hours hours hours hours hours hours hours hours days days days days hours hours hours hours Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units). Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L were received on 09:05. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS. Qualifier EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTL EHTL EHTL EHTL EHT EHT EHT EHT EHTL EHTL EHTL EHTL The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

76

77 ATTN: Clifton Samoiloff Commerce Drive Winnipeg MB R3P 0Y7 Phone: Date Received: Report Date: Version: 21-OCT-10 14:00 (MT) FINAL REV. 3 Certificate of Analysis Lab Work Order #: L Project P.O. #: NOT SUBMITTED ob Reference: Legal Site Desc: C of C Numbers: Comments: ADDITIONAL -OCT-10 14:48 ADDITIONAL 28-SEP-10 13:43 08-OCT-10: 21-OCT-10: Robert S. Kitlar Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 1329 Niakwa Road East, Unit 12, Winnipeg, MB R2 3T4 Canada Phone: Fax: MANITOBA TECHNOLOGY CENTRE LTD. Part of the ALS Group A Campbell Brothers Limited Company

78 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 2 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL1-F10-WQ1 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) CLIENT 10:00 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total < < < < < < < <0.50 < < <0.0 < <0.00 < CU NTU 30-SEP-10 -OCT OCT-10 R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

79 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 3 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL1-F10-WQ1 Sampled By: Matrix: CLIENT 10:00 WATER Total Metals by ICP-MS Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved < < < < < < < R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

80 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 4 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: VL1-F10-WQ1 CLIENT 10:00 WATER Dissolved Metals by ICP-MS Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < < < ug/l ug/l ABS Ratio umhos/cm ph units R R1475 R1475 R1475 R R R R R R L Sampled By: VL1-F10-WQ2 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) CLIENT 10:00 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total < < < < < < < CU NTU 30-SEP-10 -OCT OCT-10 R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

81 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 5 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL1-F10-WQ2 Sampled By: Matrix: CLIENT 10:00 WATER Total Metals by ICP-MS Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < <0.0 < <0.00 < < < < < R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

82 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 6 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: VL1-F10-WQ2 CLIENT 10:00 WATER Dissolved Metals by ICP-MS Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < <0.00 < < < ug/l ug/l ABS Ratio umhos/cm ph units R R1475 R1475 R1475 R R R R R R L Sampled By: VL2-F10-WQ1 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) CLIENT 14:00 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) < < < CU 30-SEP-10 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

83 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 7 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL2-F10-WQ1 Sampled By: Matrix: CLIENT 14:00 WATER Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total < < < < <0.50 < < < <0.0 < <0.00 < NTU -OCT OCT-10 R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

84 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 8 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL2-F10-WQ1 Sampled By: Matrix: CLIENT 14:00 WATER Total Metals by ICP-MS Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) < < < < < < < <0.00 < < ug/l ug/l ABS Ratio R R R R1475 R1475 R1475 R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

85 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 9 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: VL2-F10-WQ1 CLIENT 14:00 WATER Alkalinity Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph 3.73 < umhos/cm ph units R R R R L Sampled By: VL2-F10-WQ2 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) CLIENT 14:00 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Inorganic Carbon Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total < < < < < < < < < < CU NTU 30-SEP-10 -OCT OCT-10 R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

86 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 10 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL2-F10-WQ2 Sampled By: Matrix: CLIENT 14:00 WATER Total Metals by ICP-MS Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved 0.0 < <0.00 < < < < < < < < R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

87 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 11 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L VL2-F10-WQ2 Sampled By: Matrix: CLIENT 14:00 WATER Dissolved Metals by ICP-MS Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < < ug/l ug/l ABS Ratio umhos/cm ph units R R1475 R1475 R1475 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

88 Reference Information L CONTD... PAGE 12 of 14 Test Method References: ALS Test Code Matrix Test Description Method Reference** ACIDITY-LOW-WP Acidity APHA Method 2310B ALK-TOT-WP Alkalinity APHA 23B Alkalinity of water is a measure of its acid neutralizing capacity. Alkalinity is imparted by bicarbonate, carbonate and hydroxide components of water. It is determined by titration with a standard solution of strong mineral acid to the successive HCO3- and H2CO3 endpoints indicated electrometrically. ANIONS5-IC-WP Anions scan (IC) EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". BR-IC-WP Bromide EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". C-DIS-ORG-WP Dissolved Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-INORG-CL Total Inorganic Carbon APHA 5310 C-Instrumental C-TOT-ORG-CL Total Organic Carbon APHA 5310 C-Instrumental C-TOT-ORG-WP Total Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. CHL/A,PHEO/A-ACET-WP Chlorophyll-a & Pheophytin-a APHA H, /750NM Chlorophyll-a is filtered from the sample, then extracted with 90 (v/v) acetone. Absorbance is measured spectrophotometrically at 664 nm and 750 nm. The extract is then acidified, converting chlorophyll-a to phaeophytin-a. Absorbance is determined again after acidification. The chlorophyll-a concentration is determined from the decrease in absorbance upon acidification. When a detection limit of 0.5 ug/l is required, the volume of sample filtered is doubled to 700mL. Samples with an OD664 before/od665 after acidification ratio (664b/665a) of 1.70 are considered to contain no pheophytin a and to be in excellent physiological condition. Solutions of pure pheophytin show no reduction in OD665 upon acidification and have a 664b/665a ratio of Thus, mixtures of chlorophyll a and pheophytin a have absorption peak ratios ranging between and 1.7. These ratios are based on the use of 90 acetone as solvent. COLOUR-TRUE-WP Colour, True APHA 4500 COLOR This analysis is carried out using procedures adapted from APHA 21 "Color". Colour (True Colour) is determined by filtering a sample through a 0.45 micron membrane filter followed by analysis of the filtrate using the platinum-cobalt colourimetric method. Colour is ph dependent. Unless otherwise indicated, reported colour results pertain to the ph of the sample as received to within +/- 1 ph unit. CONSULT-BOD-CBOD- WP Carbonaceous BOD APHA 5210 B-5 day Incub.-O2 electrode A sample of water is incubated for 5 days at degrees Celcius. Comparison of dissolved oxygen content at beginning and end of incubation provides a measure of Biochemical oxygen demand. If carbonaceous BOD is requested, TCMP is added to the sample to chemically inhibit nitrogenous oxygen demand. If soluble BOD is requested, the sample is filtered prior to analysis. EC-WP Conductivity APHA 2510B Conductivity of an aqueous solution refers to its ability to carry an electric current. Conductance of a solution is measured between two spatially fixed and chemically inert electrodes.

89 Reference Information L CONTD... PAGE 13 of 14 Test Method References: ALS Test Code Matrix ETL-HARDNESS-DIS-WP ETL-HARDNESS-TOT-WP HG-D-CVAF-WP Test Description Hardness Calculated Hardness Calculated Mercury Dissolved Method Reference** Calculated Calculated EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. HG-T-CVAF-WP Mercury Total EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. MET-D-L-MS-WP Dissolved Metals by ICP-MS U.S. EPA 0.8-DL Dissolved Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the Examination of and Wastewater method 3030B for filtration through a 0.45 um filter and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. MET-T-L-MS-WP Total Metals by ICP-MS U.S. EPA 0.8-TL Total Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the examination of and Wastewater Method 3030E and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. N-TOTK-WP Total Kjeldahl Nitrogen Quickchem method E Lachat Samples are digested with a sulphuric acid solution, cooled, diluted with water, and analyzed for ammonia. Total Kjeldahl nitrogen is the sum of freeammonia and organic nitrogen compounds which are converted to ammonium sulphate through this digestion process. Analysis is performed by Flow Injection Analysis (FIA). The ph of the digested sample is raised to a known, basic ph by neutralization with a concentrated buffer solution. This neutralization converts the ammonium cation to ammonia. The ammonia produced is heated with saliclyate and hypochlorite to produce blue colour which is proportional to the ammonia concentration. NH3-COL-WP Ammonia by colour APHA 4500 NH3 F Ammonia - Colourimeric using Salicylate-nitroprusside and hypochlorite, in an alkaline phosphate buffer. NO2+NO3-CALC-WP Nitrate+Nitrite CALCULATION P-TOTAL-WP Phosphorus, Total APHA, 18 P-T Samples are digested using a sulphuric acid-persulfate mixture to convert organic phosphorous to orthophosphate. The samples are analyzed by either the Flow Injection Analysis (FIA) or the Segmented Flow Analysis (SFA) method. The absorbance measured by the instrument is proportional to the concentration of orthophosphate in the sample, and is reported as phosphorous. PH-WP ph APHA 4500H ph of a sample is the determination of the activity of the hydrogen ions by potentiometric measurement using a standard hydrogen electrode and a reference electrode. SILICATE-COL-VA Silicate by Colourimetric analysis APHA 4500-SIO2 D. This analysis is carried out using procedures adapted from APHA Method 4500-SiO2 D. "Silica". Silicate (molybdate-reactive silica) is determined by the molybdosilicate-heteropoly blue colourimetric method. SOLIDS-TDS-WP Total Dissolved Solids APHA 2540 The residue remaining in a prepared casserole after passing the sample through a 1.2 um Whatman GF/C glass microfibre filter and drying at 180 degrees C. Samples may be dried at 105 degrees C if the client specifically requests this drying temperature. SOLIDS-TOTSUS-WP Total Suspended Solids APHA 2540

90 Reference Information L CONTD... PAGE 14 of 14 Test Method References: ALS Test Code Matrix Test Description Method Reference** The residue retained by a prepared 1.5 um Whatman 934-AH glass microfibre filter dried at 105 degrees C. TURBIDITY-WP Turbidity APHA, 18, 2130B A strong light beam is sent through a transparent tube containing the sample. Light that is reflected at 90 degrees to the axis by suspended particles is detected by the photocell. The electrical response is proportional to the sample turbidity. ** ALS test methods may incorporate modifications from specified reference methods to improve performance. The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code WP VA CL Laboratory Location ALS LABORATORY GROUP - WINNIPEG, MANITOBA, CANADA ALS LABORATORY GROUP - VANCOUVER, BC, CANADA ALS LABORATORY GROUP - CALGARY, ALBERTA, CANADA Chain of Custody Numbers: GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

91 Workorder: L Report Date: 21-OCT-10 Page 1 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ACIDITY-LOW-WP Batch R WG CVS Acidity (as CaCO3) WG DUP Acidity (as CaCO3) L ALK-TOT-WP Batch R WG CVS Alkalinity, Total (as CaCO3) WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP L

92 Workorder: L Report Date: 21-OCT-10 Page 2 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ALK-TOT-WP Batch R WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < ANIONS5-IC-WP Batch R WG DUP Chloride L Fluoride < < Nitrite-N < < Nitrate-N < < Sulfate WG Chloride LCS Fluoride Nitrite-N Nitrate-N Sulfate WG Chloride MB < Fluoride < 0.1 Nitrite-N < 0.05 Nitrate-N < 0.05 Sulfate < WG Chloride MS L Fluoride Nitrite-N Nitrate-N Sulfate BR-IC-WP

93 Workorder: L Report Date: 21-OCT-10 Page 3 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff BR-IC-WP Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 C-DIS-ORG-WP Batch R WG CCV Dissolved Organic Carbon 01-OCT-10 WG CVS Dissolved Organic Carbon 30-SEP-10 C-TOT-INORG-CL Batch R WG LCS Total Inorganic Carbon 95 WG MB Total Inorganic Carbon < 1 C-TOT-ORG-WP Batch R WG CCV Total Organic Carbon 02-OCT-10 WG CVS Total Organic Carbon 01-OCT-10 WG DUP Total Organic Carbon L OCT-10 WG MB Total Organic Carbon < 1 01-OCT-10 CHL/A,PHEO/A-ACET-WP Batch R1475 WG CVS Chlorophyll a WG Chlorophyll a CVS COLOUR-TRUE-WP Batch R WG DUP Colour, True L CU 0.1 WG DUP L

94 Workorder: L Report Date: 21-OCT-10 Page 4 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff COLOUR-TRUE-WP Batch R WG DUP Colour, True L CU 2.2 WG Colour, True LCS WG Colour, True MB <5.0 CU 5 CONSULT-BOD-CBOD-WP Batch R WG DUP BOD Carbonaceous L WG IRM BOD Carbonaceous 61-GG WG MB BOD Carbonaceous < 1 EC-WP Batch R WG CCV Conductivity WG Conductivity CVS WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm HG-D-CVAF-WP Batch R WG DUP L WG DUP L

95 Workorder: L Report Date: 21-OCT-10 Page 5 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-D-CVAF-WP Batch R WG DUP L WG DUP L WG LCS WG MB WG MB WG MS L WG MS L WG MS L HG-T-CVAF-WP Batch R WG DUP L WG DUP L WG DUP L WG DUP L

96 Workorder: L Report Date: 21-OCT-10 Page 6 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-T-CVAF-WP Batch R WG DUP L WG LCS WG MB WG MS L WG MS L WG MS L WG MS L MET-D-L-MS-WP Batch WG CCV Aluminum (Al)-Dissolved 93 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved 90 Bismuth (Bi)-Dissolved Boron (B)-Dissolved 94 Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved 95 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved

97 Workorder: L Report Date: 21-OCT-10 Page 7 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CCV Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved 91 Magnesium (Mg)-Dissolved 95 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 95 Potassium (K)-Dissolved 95 Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved 95 Silicon (Si)-Dissolved 95 Silver (Ag)-Dissolved Sodium (Na)-Dissolved 95 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved 92 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved

98 Workorder: L Report Date: 21-OCT-10 Page 8 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved 93 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 94 Potassium (K)-Dissolved 95 Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved 93 Silver (Ag)-Dissolved Sodium (Na)-Dissolved 91 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 92 Tungsten (W)-Dissolved Uranium (U)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved 95 Arsenic (As)-Dissolved 95 Barium (Ba)-Dissolved Beryllium (Be)-Dissolved

99 Workorder: L Report Date: 21-OCT-10 Page 9 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved 94 Cobalt (Co)-Dissolved 92 Copper (Cu)-Dissolved 93 Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved 95 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved 94 Phosphorus (P)-Dissolved 93 Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved 95 Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 92 Tungsten (W)-Dissolved Uranium (U)-Dissolved Zinc (Zn)-Dissolved 95 Zirconium (Zr)-Dissolved WG DUP Aluminum (Al)-Dissolved WG <0.00 <0.00

100 Workorder: L Report Date: 21-OCT-10 Page 10 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Antimony (Sb)-Dissolved WG Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < < Lead (Pb)-Dissolved < < Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < < Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 26 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved

101 Workorder: L Report Date: 21-OCT-10 Page 11 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Tungsten (W)-Dissolved WG Uranium (U)-Dissolved Zinc (Zn)-Dissolved <0.00 <0.00 Zirconium (Zr)-Dissolved < < WG LCS Aluminum (Al)-Dissolved 111 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved 109 Beryllium (Be)-Dissolved 109 Bismuth (Bi)-Dissolved Boron (B)-Dissolved 108 Cadmium (Cd)-Dissolved 105 Calcium (Ca)-Dissolved 105 Cesium (Cs)-Dissolved 112 Chromium (Cr)-Dissolved 105 Cobalt (Co)-Dissolved 109 Copper (Cu)-Dissolved Iron (Fe)-Dissolved 112 Lead (Pb)-Dissolved Lithium (Li)-Dissolved 111 Magnesium (Mg)-Dissolved 111 Manganese (Mn)-Dissolved 106 Molybdenum (Mo)-Dissolved 109 Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 110 Potassium (K)-Dissolved 104 Rubidium (Rb)-Dissolved 113 Selenium (Se)-Dissolved Silicon (Si)-Dissolved 110 Silver (Ag)-Dissolved 106 Sodium (Na)-Dissolved 114 Strontium (Sr)-Dissolved 105 Tellurium (Te)-Dissolved 106

102 Workorder: L Report Date: 21-OCT-10 Page 12 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG LCS Tellurium (Te)-Dissolved 106 Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 107 Tungsten (W)-Dissolved 105 Uranium (U)-Dissolved 110 Zinc (Zn)-Dissolved 104 Zirconium (Zr)-Dissolved 108 WG MB Aluminum (Al)-Dissolved < Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < 0.01 Cadmium (Cd)-Dissolved < Calcium (Ca)-Dissolved < 0.05 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < 0.01 Lead (Pb)-Dissolved < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved < 0.01 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < 0.1 Potassium (K)-Dissolved < Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved 0.001

103 Workorder: L Report Date: 21-OCT-10 Page 13 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG MB Silicon (Si)-Dissolved < 0.05 Silver (Ag)-Dissolved Sodium (Na)-Dissolved < Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Zinc (Zn)-Dissolved < Zirconium (Zr)-Dissolved < Batch R WG CCV Cadmium (Cd)-Dissolved Silicon (Si)-Dissolved Vanadium (V)-Dissolved WG CVS Cadmium (Cd)-Dissolved Silicon (Si)-Dissolved Vanadium (V)-Dissolved WG CVS Cadmium (Cd)-Dissolved 106 Silicon (Si)-Dissolved 104 Vanadium (V)-Dissolved 104 MET-T-L-MS-WP Batch WG CCV Aluminum (Al)-Total 92 Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total

104 Workorder: L Report Date: 21-OCT-10 Page 14 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CCV Bismuth (Bi)-Total Boron (B)-Total 104 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total 95 Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total 94 Selenium (Se)-Total Silicon (Si)-Total 95 Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total 94 Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total 95 Uranium (U)-Total 91 Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total

105 Workorder: L Report Date: 21-OCT-10 Page 15 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CVS Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total

106 Workorder: L Report Date: 21-OCT-10 Page 16 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CVS Uranium (U)-Total 95 Zinc (Zn)-Total Zirconium (Zr)-Total 95 WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total 106 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total 105 Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 106 Tellurium (Te)-Total Thallium (Tl)-Total

107 Workorder: L Report Date: 21-OCT-10 Page 17 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CVS Thorium (Th)-Total Tin (Sn)-Total 104 Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 104 WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total

108 Workorder: L Report Date: 21-OCT-10 Page 18 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG DUP Silver (Ag)-Total WG Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Tungsten (W)-Total Uranium (U)-Total Zinc (Zn)-Total Zirconium (Zr)-Total < < WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0.

109 Workorder: L Report Date: 21-OCT-10 Page 19 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG DUP Potassium (K)-Total WG Rubidium (Rb)-Total Selenium (Se)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG LCS Aluminum (Al)-Total Antimony (Sb)-Total 105 Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total 105 Bismuth (Bi)-Total Boron (B)-Total 109 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 94 Magnesium (Mg)-Total

110 Workorder: L Report Date: 21-OCT-10 Page of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG LCS Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total 104 Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 93 Tellurium (Te)-Total 109 Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total 92 Zinc (Zn)-Total Zirconium (Zr)-Total WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total

111 Workorder: L Report Date: 21-OCT-10 Page 21 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG MB Iron (Fe)-Total < Lead (Pb)-Total < Lithium (Li)-Total < Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total < Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total Sodium (Na)-Total < Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < Batch R WG CCV Cadmium (Cd)-Total Silicon (Si)-Total Vanadium (V)-Total WG CVS Cadmium (Cd)-Total Silicon (Si)-Total Vanadium (V)-Total WG CVS

112 Workorder: L Report Date: 21-OCT-10 Page 22 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CVS Cadmium (Cd)-Total 106 Silicon (Si)-Total 104 Vanadium (V)-Total 104 N-TOTK-WP Batch R WG CCV Total Kjeldahl Nitrogen 104 WG CVS Total Kjeldahl Nitrogen WG DUP Total Kjeldahl Nitrogen L WG DUP Total Kjeldahl Nitrogen L WG LCS Total Kjeldahl Nitrogen WG MB Total Kjeldahl Nitrogen < WG MB Total Kjeldahl Nitrogen < WG MS Total Kjeldahl Nitrogen L NH3-COL-WP Batch R WG CCV Ammonia as N WG Ammonia as N DUP L WG Ammonia as N LCS WG Ammonia as N MB < 0.05 P-TOTAL-WP Batch R WG CCV Phosphorus, Total WG CCV

113 Workorder: L Report Date: 21-OCT-10 Page 23 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff P-TOTAL-WP Batch R WG CCV Phosphorus, Total 92 WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG DUP Phosphorus, Total L WG DUP Phosphorus, Total L WG MB Phosphorus, Total < 0.01 WG MS Phosphorus, Total L WG MS Phosphorus, Total L PH-WP Batch R WG CCV ph WG ph CVS - WG ph DUP L ph units WG ph DUP L ph units WG ph DUP L ph units SILICATE-COL-VA Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG DUP Silicate (as SIO2) L WG DUP Silicate (as SIO2) L < <

114 Workorder: L Report Date: 21-OCT-10 Page 24 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff SILICATE-COL-VA Batch R WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 SOLIDS-TDS-WP Batch R WG CVS Total Dissolved Solids WG DUP Total Dissolved Solids L WG DUP Total Dissolved Solids L WG MB Total Dissolved Solids <5.0 5 SOLIDS-TOTSUS-WP Batch R WG CVS Total Suspended Solids WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG MB Total Suspended Solids <5.0 5 TURBIDITY-WP Batch R WG CCV Turbidity WG Turbidity CCV 104 WG Turbidity CVS WG CVS

115 Workorder: L Report Date: 21-OCT-10 Page 25 of 27 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff TURBIDITY-WP Batch R WG CVS Turbidity WG Turbidity DUP L NTU WG Turbidity DUP L NTU WG Turbidity LCS WG Turbidity MB < NTU 0.1

116 Workorder: L Report Date: 21-OCT-10 Page 26 of 27 Legend: Limit Confidence Interval (Laboratory Control Limits) DUP Duplicate RPD Relative Percent Difference Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description Duplicate results and limits are expressed in terms of absolute difference. Relative Percent Difference Not Available due to result(s) being less than detection limit.

117 Workorder: L Report Date: 21-OCT-10 Page 27 of 27 Hold Time Exceedances: ALS Product Description Physical Tests ph Anions and Nutrients Anions scan (IC) Organic / Inorganic Carbon Total Inorganic Carbon Aggregate Organics Carbonaceous BOD Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: Sample ID Sampling Date Date Processed Rec. HT Actual HT :00 10:00 14:00 14:00 10:00 10:00 10:00 10:00 14:00 14:00 10:00 10:00 11:30 11:30 11:30 11:30 14:35 14:35 00:00 00:00 00:00 00:00 12:18 12: Units hours hours hours hours hours hours hours hours hours hours hours hours Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units). Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L were received on 09:30. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS. Qualifier EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTL EHTL EHTR EHTR EHTR EHTR EHTL EHTL The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

118

119 ATTN: Clifton Samoiloff Commerce Drive Winnipeg MB R3P 0Y7 Phone: Date Received: Report Date: Version: 25-OCT-10 10:15 (MT) FINAL Certificate of Analysis Lab Work Order #: L Project P.O. #: NOT SUBMITTED ob Reference: Legal Site Desc: C of C Numbers: Paul Nicolas Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 1329 Niakwa Road East, Unit 12, Winnipeg, MB R2 3T4 Canada Phone: Fax: MANITOBA TECHNOLOGY CENTRE LTD. Part of the ALS Group A Campbell Brothers Limited Company

120 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 2 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC2-F10-WQ1 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) CLIENT 16:00 Note: Initial ph > Titration endpoint(ph 8.300) Ammonia as N Bromide (Br) BOD Carbonaceous Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < < < < < < < < <0.00 < NTU 29-SEP SEP-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

121 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 3 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC2-F10-WQ1 Sampled By: Matrix: CLIENT 16:00 WATER Total Metals by ICP-MS Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved < < < < < < < < < R14763 R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

122 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 4 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: UC2-F10-WQ1 CLIENT 16:00 WATER Dissolved Metals by ICP-MS Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: UC3-F10-WQ1 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous CLIENT 13:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < < < < < < < < < NTU 30-SEP SEP-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

123 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 5 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC3-F10-WQ1 Sampled By: Matrix: CLIENT 13:00 WATER Total Metals by ICP-MS Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved < < <0.00 < < < < < < < < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

124 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 6 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: UC3-F10-WQ1 CLIENT 13:00 WATER Dissolved Metals by ICP-MS Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < <0.00 < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: WHC-F10-WQ1 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous CLIENT 10:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids < < < < < SEP-10 R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

125 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 7 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L WHC-F10-WQ1 Sampled By: Matrix: CLIENT 10:00 WATER Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved < < < < < < < < < <0.00 < < < < NTU 30-SEP-10 R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

126 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 8 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L WHC-F10-WQ1 Sampled By: Matrix: CLIENT 10:00 WATER Dissolved Metals by ICP-MS Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < < < <0.00 < < < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

127 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 9 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L GRR-F10-WQ2 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous CLIENT 10:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total < < < < < < < < < < <0.00 < NTU 30-SEP SEP SEP-10 R R R R R R R R R R R R R R R R R R R R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

128 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 10 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L GRR-F10-WQ2 Sampled By: Matrix: CLIENT 10:00 WATER Total Metals by ICP-MS Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved < < < < < < < <0.00 < R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

129 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 11 of 14 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L GRR-F10-WQ2 Sampled By: Matrix: CLIENT 10:00 WATER Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

130 Reference Information L CONTD... PAGE 12 of 14 QC Samples with Qualifiers & Comments: QC Type Description Parameter Matrix Spike Total Kjeldahl Nitrogen Matrix Spike Total Kjeldahl Nitrogen Matrix Spike Total Kjeldahl Nitrogen Matrix Spike Total Kjeldahl Nitrogen Matrix Spike Ammonia as N Qualifier MS-B MS-B MS-B MS-B MS-B Applies to Sample Number(s) L , -2, -3 L , -2, -3 L L L , -2, -3, -4 Qualifiers for Individual Samples Listed: Sample Numbe L L Client ID UC2-F10-WQ1 WHC-F10-WQ1 Qualifier EHR EHR Description Exceeded Recommended Holding Time On Receipt: Proceed With Analysis As Requested Exceeded Recommended Holding Time On Receipt: Proceed With Analysis As Requested Test Method References: ALS Test Code Matrix Test Description Method Reference** ACIDITY-LOW-WP Acidity APHA Method 2310B ALK-TOT-WP Alkalinity APHA 23B Alkalinity of water is a measure of its acid neutralizing capacity. Alkalinity is imparted by bicarbonate, carbonate and hydroxide components of water. It is determined by titration with a standard solution of strong mineral acid to the successive HCO3- and H2CO3 endpoints indicated electrometrically. ANIONS5-IC-WP Anions scan (IC) EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". BR-IC-WP Bromide EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". C-DIS-ORG-WP Dissolved Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-ORG-WP Total Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. CHL/A,PHEO/A-ACET-WP Chlorophyll-a & Pheophytin-a APHA H, /750NM Chlorophyll-a is filtered from the sample, then extracted with 90 (v/v) acetone. Absorbance is measured spectrophotometrically at 664 nm and 750 nm. The extract is then acidified, converting chlorophyll-a to phaeophytin-a. Absorbance is determined again after acidification. The chlorophyll-a concentration is determined from the decrease in absorbance upon acidification. When a detection limit of 0.5 ug/l is required, the volume of sample filtered is doubled to 700mL. Samples with an OD664 before/od665 after acidification ratio (664b/665a) of 1.70 are considered to contain no pheophytin a and to be in excellent physiological condition. Solutions of pure pheophytin show no reduction in OD665 upon acidification and have a 664b/665a ratio of Thus, mixtures of chlorophyll a and pheophytin a have absorption peak ratios ranging between and 1.7. These ratios are based on the use of 90 acetone as solvent.

131 Reference Information L CONTD... PAGE 13 of 14 Test Method References: ALS Test Code Matrix Test Description Method Reference** CONSULT-BOD-CBOD- WP Carbonaceous BOD APHA 5210 B-5 day Incub.-O2 electrode A sample of water is incubated for 5 days at degrees Celcius. Comparison of dissolved oxygen content at beginning and end of incubation provides a measure of Biochemical oxygen demand. If carbonaceous BOD is requested, TCMP is added to the sample to chemically inhibit nitrogenous oxygen demand. If soluble BOD is requested, the sample is filtered prior to analysis. EC-WP Conductivity APHA 2510B Conductivity of an aqueous solution refers to its ability to carry an electric current. Conductance of a solution is measured between two spatially fixed and chemically inert electrodes. ETL-HARDNESS-DIS-WP ETL-HARDNESS-TOT-WP HG-D-CVAF-WP Hardness Calculated Hardness Calculated Mercury Dissolved Calculated Calculated EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. HG-T-CVAF-WP Mercury Total EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. MET-D-L-MS-WP Dissolved Metals by ICP-MS U.S. EPA 0.8-DL Dissolved Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the Examination of and Wastewater method 3030B for filtration through a 0.45 um filter and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. MET-T-L-MS-WP Total Metals by ICP-MS U.S. EPA 0.8-TL Total Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the examination of and Wastewater Method 3030E and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. N-TOTK-WP Total Kjeldahl Nitrogen Quickchem method E Lachat Samples are digested with a sulphuric acid solution, cooled, diluted with water, and analyzed for ammonia. Total Kjeldahl nitrogen is the sum of freeammonia and organic nitrogen compounds which are converted to ammonium sulphate through this digestion process. Analysis is performed by Flow Injection Analysis (FIA). The ph of the digested sample is raised to a known, basic ph by neutralization with a concentrated buffer solution. This neutralization converts the ammonium cation to ammonia. The ammonia produced is heated with saliclyate and hypochlorite to produce blue colour which is proportional to the ammonia concentration. NH3-COL-WP Ammonia by colour APHA 4500 NH3 F Ammonia - Colourimeric using Salicylate-nitroprusside and hypochlorite, in an alkaline phosphate buffer. NO2+NO3-CALC-WP Nitrate+Nitrite CALCULATION P-TOTAL-WP Phosphorus, Total APHA, 18 P-T Samples are digested using a sulphuric acid-persulfate mixture to convert organic phosphorous to orthophosphate. The samples are analyzed by either the Flow Injection Analysis (FIA) or the Segmented Flow Analysis (SFA) method. The absorbance measured by the instrument is proportional to the concentration of orthophosphate in the sample, and is reported as phosphorous. PH-WP ph APHA 4500H ph of a sample is the determination of the activity of the hydrogen ions by potentiometric measurement using a standard hydrogen electrode and a reference electrode.

132 Reference Information L CONTD... PAGE 14 of 14 Test Method References: ALS Test Code Matrix Test Description Method Reference** SILICATE-COL-VA Silicate by Colourimetric analysis APHA 4500-SIO2 D. This analysis is carried out using procedures adapted from APHA Method 4500-SiO2 D. "Silica". Silicate (molybdate-reactive silica) is determined by the molybdosilicate-heteropoly blue colourimetric method. SOLIDS-TDS-WP Total Dissolved Solids APHA 2540 The residue remaining in a prepared casserole after passing the sample through a 1.2 um Whatman GF/C glass microfibre filter and drying at 180 degrees C. Samples may be dried at 105 degrees C if the client specifically requests this drying temperature. SOLIDS-TOTSUS-WP Total Suspended Solids APHA 2540 The residue retained by a prepared 1.5 um Whatman 934-AH glass microfibre filter dried at 105 degrees C. TURBIDITY-WP Turbidity APHA, 18, 2130B A strong light beam is sent through a transparent tube containing the sample. Light that is reflected at 90 degrees to the axis by suspended particles is detected by the photocell. The electrical response is proportional to the sample turbidity. ** ALS test methods may incorporate modifications from specified reference methods to improve performance. The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code WP VA Laboratory Location ALS LABORATORY GROUP - WINNIPEG, MANITOBA, CANADA ALS LABORATORY GROUP - VANCOUVER, BC, CANADA Chain of Custody Numbers: GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

133 Workorder: L Report Date: 25-OCT-10 Page 1 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ACIDITY-LOW-WP Batch R WG CVS Acidity (as CaCO3) WG DUP Acidity (as CaCO3) L ALK-TOT-WP Batch R WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) L < Bicarbonate (HCO3) < Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < Batch R WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < ANIONS5-IC-WP Batch R WG LCS Chloride Fluoride Nitrite-N Nitrate-N Sulfate WG Chloride MB < Fluoride < 0.1 Nitrite-N < 0.05 Nitrate-N < 0.05 Sulfate <

134 Workorder: L Report Date: 25-OCT-10 Page 2 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ANIONS5-IC-WP Batch R WG DUP Chloride L Fluoride Nitrite-N < < Nitrate-N < < Sulfate WG Chloride LCS Fluoride Nitrite-N Nitrate-N Sulfate WG Chloride MB < Fluoride < 0.1 Nitrite-N < 0.05 Nitrate-N < 0.05 Sulfate < WG Chloride MS L Fluoride Nitrite-N Nitrate-N Sulfate BR-IC-WP Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 C-DIS-ORG-WP

135 Workorder: L Report Date: 25-OCT-10 Page 3 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff C-DIS-ORG-WP Batch R WG CCV Dissolved Organic Carbon SEP-10 WG CVS Dissolved Organic Carbon 29-SEP-10 WG DUP Dissolved Organic Carbon L SEP-10 WG MB Dissolved Organic Carbon < 1 29-SEP-10 C-TOT-ORG-WP Batch R WG CCV Total Organic Carbon 29-SEP-10 WG CVS Total Organic Carbon 29-SEP-10 WG DUP Total Organic Carbon L SEP-10 WG MB Total Organic Carbon < 1 29-SEP-10 CHL/A,PHEO/A-ACET-WP Batch R1475 WG CVS Chlorophyll a WG Chlorophyll a CVS CONSULT-BOD-CBOD-WP Batch R WG DUP BOD Carbonaceous L WG IRM BOD Carbonaceous 61-GG WG MB BOD Carbonaceous < 1 EC-WP Batch R WG CCV Conductivity WG CVS

136 Workorder: L Report Date: 25-OCT-10 Page 4 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff EC-WP Batch R WG CVS Conductivity WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm 10 WG Conductivity DUP L umhos/cm Batch R WG CCV Conductivity WG Conductivity CVS WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm 10 HG-D-CVAF-WP Batch R WG DUP L WG DUP L WG DUP L WG LCS WG MB WG MB

137 Workorder: L Report Date: 25-OCT-10 Page 5 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-D-CVAF-WP Batch R WG MS L WG MS L WG MS L Batch R WG DUP L WG DUP L WG LCS WG MB WG MB WG MS L WG MS L HG-T-CVAF-WP Batch R WG DUP L WG DUP L

138 Workorder: L Report Date: 25-OCT-10 Page 6 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-T-CVAF-WP Batch R WG DUP L WG DUP L WG LCS WG MB WG MS L WG MS L WG MS L Batch R WG DUP L WG DUP L WG DUP L WG LCS WG MB

139 Workorder: L Report Date: 25-OCT-10 Page 7 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-T-CVAF-WP Batch R WG MB WG MS L WG MS L WG MS L MET-D-L-MS-WP Batch WG CCV Aluminum (Al)-Dissolved 95 Antimony (Sb)-Dissolved 95 Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved 105 Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved 92 Chromium (Cr)-Dissolved 95 Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved

140 Workorder: L Report Date: 25-OCT-10 Page 8 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CCV Potassium (K)-Dissolved 94 Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved 95 Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 94 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved 104 Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved 104 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved 104 Lead (Pb)-Dissolved Lithium (Li)-Dissolved

141 Workorder: L Report Date: 25-OCT-10 Page 9 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved 94 Selenium (Se)-Dissolved Silicon (Si)-Dissolved 95 Silver (Ag)-Dissolved 95 Sodium (Na)-Dissolved Strontium (Sr)-Dissolved 95 Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved 91 WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved 106 Boron (B)-Dissolved 108 Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved

142 Workorder: L Report Date: 25-OCT-10 Page 10 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved 106 Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved 95 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 93 Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG DUP Aluminum (Al)-Dissolved WG Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved

143 Workorder: L Report Date: 25-OCT-10 Page 11 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Bismuth (Bi)-Dissolved WG Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved < < Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 26 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved

144 Workorder: L Report Date: 25-OCT-10 Page 12 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Zirconium (Zr)-Dissolved WG WG LCS Aluminum (Al)-Dissolved 108 Antimony (Sb)-Dissolved 111 Arsenic (As)-Dissolved 109 Barium (Ba)-Dissolved 109 Beryllium (Be)-Dissolved 116 Bismuth (Bi)-Dissolved 104 Boron (B)-Dissolved 111 Cadmium (Cd)-Dissolved 104 Calcium (Ca)-Dissolved 108 Cesium (Cs)-Dissolved 108 Chromium (Cr)-Dissolved 115 Cobalt (Co)-Dissolved 115 Copper (Cu)-Dissolved 109 Iron (Fe)-Dissolved 116 Lead (Pb)-Dissolved 106 Lithium (Li)-Dissolved 111 Magnesium (Mg)-Dissolved 109 Manganese (Mn)-Dissolved 105 Molybdenum (Mo)-Dissolved 109 Nickel (Ni)-Dissolved 105 Phosphorus (P)-Dissolved 111 Potassium (K)-Dissolved 109 Rubidium (Rb)-Dissolved 113 Selenium (Se)-Dissolved 107 Silicon (Si)-Dissolved 113 Silver (Ag)-Dissolved 104 Sodium (Na)-Dissolved 113 Strontium (Sr)-Dissolved 104 Tellurium (Te)-Dissolved 115 Thallium (Tl)-Dissolved 105 Thorium (Th)-Dissolved 106 Tin (Sn)-Dissolved 108

145 Workorder: L Report Date: 25-OCT-10 Page 13 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG LCS Titanium (Ti)-Dissolved 109 Tungsten (W)-Dissolved 107 Uranium (U)-Dissolved Vanadium (V)-Dissolved 111 Zinc (Zn)-Dissolved 109 Zirconium (Zr)-Dissolved 106 WG MB Aluminum (Al)-Dissolved < Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < 0.01 Cadmium (Cd)-Dissolved < Calcium (Ca)-Dissolved < 0.05 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < 0.01 Lead (Pb)-Dissolved < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved < 0.01 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < 0.1 Potassium (K)-Dissolved < Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved < 0.05 Silver (Ag)-Dissolved Sodium (Na)-Dissolved <

146 Workorder: L Report Date: 25-OCT-10 Page 14 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG MB Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved < Zirconium (Zr)-Dissolved < Batch WG CCV Aluminum (Al)-Dissolved 94 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved 95 Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved

147 Workorder: L Report Date: 25-OCT-10 Page 15 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CCV Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 95 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 95 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved 92 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved

148 Workorder: L Report Date: 25-OCT-10 Page 16 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 95 Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silver (Ag)-Dissolved 95 Sodium (Na)-Dissolved 95 Strontium (Sr)-Dissolved 95 Tellurium (Te)-Dissolved 95 Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 95 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 94 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved 94 WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved 105 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved

149 Workorder: L Report Date: 25-OCT-10 Page 17 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG DUP Aluminum (Al)-Dissolved WG <0.00 <0.00 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved

150 Workorder: L Report Date: 25-OCT-10 Page 18 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Calcium (Ca)-Dissolved WG Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < < Lead (Pb)-Dissolved < < Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < < Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 26 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved <0.00 <0.00 Zirconium (Zr)-Dissolved < < WG LCS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved

151 Workorder: L Report Date: 25-OCT-10 Page 19 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG LCS Barium (Ba)-Dissolved 106 Beryllium (Be)-Dissolved 108 Bismuth (Bi)-Dissolved Boron (B)-Dissolved 104 Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved 108 Chromium (Cr)-Dissolved 106 Cobalt (Co)-Dissolved 106 Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved 104 Magnesium (Mg)-Dissolved 105 Manganese (Mn)-Dissolved 106 Molybdenum (Mo)-Dissolved 105 Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 109 Potassium (K)-Dissolved Rubidium (Rb)-Dissolved 108 Selenium (Se)-Dissolved Silver (Ag)-Dissolved 104 Sodium (Na)-Dissolved 107 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved 108 Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 105 Tungsten (W)-Dissolved 104 Uranium (U)-Dissolved 105 Vanadium (V)-Dissolved 106 Zinc (Zn)-Dissolved 104

152 Workorder: L Report Date: 25-OCT-10 Page of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG LCS Zirconium (Zr)-Dissolved WG MB Aluminum (Al)-Dissolved < Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < 0.01 Cadmium (Cd)-Dissolved < Calcium (Ca)-Dissolved < 0.05 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < 0.01 Lead (Pb)-Dissolved < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved < 0.01 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < 0.1 Potassium (K)-Dissolved < Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved < Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved

153 Workorder: L Report Date: 25-OCT-10 Page 21 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG MB Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved < Zirconium (Zr)-Dissolved < Batch R14763 WG CCV Silicon (Si)-Dissolved Vanadium (V)-Dissolved 104 WG CVS Silicon (Si)-Dissolved 104 Vanadium (V)-Dissolved WG CVS Silicon (Si)-Dissolved Vanadium (V)-Dissolved MET-T-L-MS-WP Batch WG CCV Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total 95 Beryllium (Be)-Total 105 Bismuth (Bi)-Total Boron (B)-Total 107 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total 95 Copper (Cu)-Total Iron (Fe)-Total 93 Lead (Pb)-Total Lithium (Li)-Total 110

154 Workorder: L Report Date: 25-OCT-10 Page 22 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CCV Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total 94 Potassium (K)-Total Rubidium (Rb)-Total 95 Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 95 Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total 94 Uranium (U)-Total 92 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 94 WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total 106 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total

155 Workorder: L Report Date: 25-OCT-10 Page 23 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CVS Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 106 Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 94 Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total 95 Uranium (U)-Total 94 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 94 WG CVS Aluminum (Al)-Total 105 Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total 105 Bismuth (Bi)-Total 109

156 Workorder: L Report Date: 25-OCT-10 Page 24 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG CVS Boron (B)-Total 108 Cadmium (Cd)-Total 104 Calcium (Ca)-Total Cesium (Cs)-Total 110 Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 108 Magnesium (Mg)-Total Manganese (Mn)-Total 107 Molybdenum (Mo)-Total 104 Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total 107 Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 104 Tellurium (Te)-Total Thallium (Tl)-Total 105 Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total 108 Zinc (Zn)-Total Zirconium (Zr)-Total 105 WG DUP Aluminum (Al)-Total WG

157 Workorder: L Report Date: 25-OCT-10 Page 25 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG DUP Antimony (Sb)-Total WG Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total

158 Workorder: L Report Date: 25-OCT-10 Page 26 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG DUP Tungsten (W)-Total WG Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total

159 Workorder: L Report Date: 25-OCT-10 Page 27 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG DUP Strontium (Sr)-Total WG Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total G 27 Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG LCS Aluminum (Al)-Total 106 Antimony (Sb)-Total 105 Arsenic (As)-Total 104 Barium (Ba)-Total Beryllium (Be)-Total 107 Bismuth (Bi)-Total 109 Boron (B)-Total 114 Cadmium (Cd)-Total Calcium (Ca)-Total 105 Cesium (Cs)-Total 106 Chromium (Cr)-Total 105 Cobalt (Co)-Total 104 Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 108 Magnesium (Mg)-Total 105 Manganese (Mn)-Total 105 Molybdenum (Mo)-Total 104 Nickel (Ni)-Total Phosphorus (P)-Total 106

160 Workorder: L Report Date: 25-OCT-10 Page 28 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG LCS Potassium (K)-Total Rubidium (Rb)-Total 105 Selenium (Se)-Total Silicon (Si)-Total 115 Silver (Ag)-Total Sodium (Na)-Total 107 Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total 110 Thorium (Th)-Total Tin (Sn)-Total 104 Titanium (Ti)-Total 105 Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total 108 Zinc (Zn)-Total Zirconium (Zr)-Total WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total < Lead (Pb)-Total < Lithium (Li)-Total <

161 Workorder: L Report Date: 25-OCT-10 Page 29 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch WG MB Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total < Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total Sodium (Na)-Total < Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < Batch R14763 WG CCV Silicon (Si)-Total Vanadium (V)-Total 104 WG CVS Silicon (Si)-Total 104 Vanadium (V)-Total WG CVS Silicon (Si)-Total Vanadium (V)-Total N-TOTK-WP

162 Workorder: L Report Date: 25-OCT-10 Page 30 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff N-TOTK-WP Batch R WG CCV Total Kjeldahl Nitrogen WG CVS Total Kjeldahl Nitrogen WG DUP Total Kjeldahl Nitrogen L WG DUP Total Kjeldahl Nitrogen L WG DUP Total Kjeldahl Nitrogen L WG DUP Total Kjeldahl Nitrogen L WG LCS Total Kjeldahl Nitrogen WG LCS Total Kjeldahl Nitrogen WG MB Total Kjeldahl Nitrogen < WG MB Total Kjeldahl Nitrogen < WG MB Total Kjeldahl Nitrogen < WG MS Total Kjeldahl Nitrogen L MS-B - WG MS Total Kjeldahl Nitrogen L MS-B - WG MS Total Kjeldahl Nitrogen L MS-B - WG MS Total Kjeldahl Nitrogen L MS-B - NH3-COL-WP Batch R WG CCV Ammonia as N 105 WG Ammonia as N DUP L WG Ammonia as N LCS

163 Workorder: L Report Date: 25-OCT-10 Page 31 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff NH3-COL-WP Batch R WG MB Ammonia as N < 0.05 WG Ammonia as N MS L MS-B - P-TOTAL-WP Batch R WG CCV Phosphorus, Total WG CCV Phosphorus, Total 93 WG CVS Phosphorus, Total 108 WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total 109 WG DUP Phosphorus, Total L WG DUP Phosphorus, Total L WG MB Phosphorus, Total < 0.01 WG MS Phosphorus, Total L Batch R WG CCV Phosphorus, Total WG CCV Phosphorus, Total 94 WG CVS Phosphorus, Total WG CVS

164 Workorder: L Report Date: 25-OCT-10 Page 32 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff P-TOTAL-WP Batch R WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG DUP Phosphorus, Total L WG DUP Phosphorus, Total L WG MB Phosphorus, Total < 0.01 WG MS Phosphorus, Total L WG MS Phosphorus, Total L PH-WP Batch R WG CCV ph WG ph CVS - WG ph DUP L ph units WG ph DUP L ph units Batch R WG CCV ph WG ph CVS - WG ph DUP L ph units WG ph DUP L ph units SILICATE-COL-VA

165 Workorder: L Report Date: 25-OCT-10 Page 33 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff SILICATE-COL-VA Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG DUP Silicate (as SIO2) L WG DUP Silicate (as SIO2) L WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK SEP-10 WG CRM Silicate (as SIO2) VA-SIO2-CSPK SEP-10 WG DUP Silicate (as SIO2) L SEP-10 WG DUP Silicate (as SIO2) L SEP-10 WG MB Silicate (as SIO2) < 1 27-SEP-10 WG MB Silicate (as SIO2) < 1 27-SEP-10 SOLIDS-TDS-WP Batch R WG CVS Total Dissolved Solids WG DUP Total Dissolved Solids L WG MB

166 Workorder: L Report Date: 25-OCT-10 Page 34 of 36 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff SOLIDS-TDS-WP Batch R WG MB Total Dissolved Solids <5.0 5 SOLIDS-TOTSUS-WP Batch R WG CVS Total Suspended Solids WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L <5.0 <5.0 WG MB Total Suspended Solids <5.0 5 TURBIDITY-WP Batch R WG CCV Turbidity WG Turbidity CCV 104 WG Turbidity CVS WG Turbidity CVS WG Turbidity DUP L NTU WG Turbidity DUP L NTU WG Turbidity DUP L NTU WG Turbidity LCS

167 Workorder: L Report Date: 25-OCT-10 Page 35 of 36 Legend: Limit Confidence Interval (Laboratory Control Limits) DUP Duplicate RPD Relative Percent Difference Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description Duplicate results and limits are expressed in terms of absolute difference. MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. Relative Percent Difference Not Available due to result(s) being less than detection limit.

168 Workorder: L Report Date: 25-OCT-10 Page 36 of 36 Hold Time Exceedances: ALS Product Description Physical Tests Total Dissolved Solids Total Suspended Solids Turbidity ph Anions and Nutrients Anions scan (IC) Bromide Aggregate Organics Carbonaceous BOD Organic Parameters Chlorophyll-a & Pheophytin-a Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: Sample ID Sampling Date Date Processed Rec. HT Actual HT :00 16:00 16:00 16:00 13:00 10:00 10:00 16:00 13:00 10:00 10:00 16:00 13:00 10:00 10:00 16:00 16:00 07:56 07:56 10: 11:58 11:58 11:58 10:34 14:29 14:29 14:29 12:48 14:29 14:29 14:29 12:48 08:00 07: Units days days hours hours hours hours hours hours hours hours hours hours hours hours hours Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units). Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L were received on 12:00. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS. hours hours Qualifier EHT EHT EHTR EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR EHTL EHTR EHTR EHTR EHTL EHTR EHTR EHTR EHTR The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

169

170 ATTN: Clifton Samoiloff Commerce Drive Winnipeg MB R3P 0Y7 Phone: Date Received: Report Date: Version: 24-NOV-10 14: (MT) FINAL REV. 4 Certificate of Analysis Lab Work Order #: L Project P.O. #: NOT SUBMITTED ob Reference: Legal Site Desc: C of C Numbers: Comments: PLEASE NOTE: The order of samples reported is reversed from the order on the Chai of Custody. 19-NOV-10: 19-NOV-10: Revision1 24-NOV-10: THIS IS AN AMENDED REPORT Fraction -1 Rerun results are reported for Total Sodium and Total Strontium Robert S. Kitlar Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 1329 Niakwa Road East, Unit 12, Winnipeg, MB R2 3T4 Canada Phone: Fax: MANITOBA TECHNOLOGY CENTRE LTD. Part of the ALS Group A Campbell Brothers Limited Company

171 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 2 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC4-F10-WQ2 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True CLIENT 12:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total 1.1 < < 1.1 < <0.071 < <1 <5.0 < <5.0 < <0.50 < < < <0.50 < < < <0.0 < < < <0.00 < < DLA CU NTU 30-SEP NOV SEP-10 R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

172 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 3 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC4-F10-WQ2 Sampled By: Matrix: CLIENT 12:00 WATER Total Metals by ICP-MS Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved <0.030 < < <0.00 < < < < <0.00 < < <0.0 < < < NOV NOV-10 R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

173 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 4 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: UC4-F10-WQ2 CLIENT 12:00 WATER Dissolved Metals by ICP-MS Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < < < <2.0 <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units 01-OCT OCT OCT OCT OCT-10 R1475 R1475 R1475 R R R R R R L Sampled By: UC4-F10-WQ1 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True CLIENT 12:30 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Fluoride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total < < < < <0.071 < < < < < <0.50 < DLA CU NTU 30-SEP SEP-10 R R R R R R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

174 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 5 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC4-F10-WQ1 Sampled By: Matrix: CLIENT 12:30 WATER Total Metals by ICP-MS Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved < < < <0.00 < < < < < < R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

175 ALS LABORATORY GROUP ANALYTICAL REPORT L CONTD... PAGE 6 of 9 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L UC4-F10-WQ1 Sampled By: Matrix: CLIENT 12:30 WATER Dissolved Metals by ICP-MS Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < <0.00 < < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

176 QC Samples with Qualifiers & Comments: Reference Information L CONTD... PAGE 7 of 9 QC Type Description Parameter Qualifier Applies to Sample Number(s) Matrix Spike Matrix Spike Matrix Spike Total Kjeldahl Nitrogen Total Kjeldahl Nitrogen Ammonia as N MS-B MS-B MS-B L , -2 L , -2 L , -2 Sample Parameter Qualifier Key: Qualifier Description DLA MS-B Detection Limit Adjusted For required dilution Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. Test Method References: ALS Test Code Matrix Test Description Method Reference** ACIDITY-LOW-WP Acidity APHA Method 2310B ALK-TOT-WP Alkalinity APHA 23B Alkalinity of water is a measure of its acid neutralizing capacity. Alkalinity is imparted by bicarbonate, carbonate and hydroxide components of water. It is determined by titration with a standard solution of strong mineral acid to the successive HCO3- and H2CO3 endpoints indicated electrometrically. ANIONS5-IC-WP Anions scan (IC) EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". BR-IC-WP Bromide EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". C-DIS-ORG-WP Dissolved Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-ORG-WP Total Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. CHL/A,PHEO/A-ACET-WP Chlorophyll-a & Pheophytin-a APHA H, /750NM Chlorophyll-a is filtered from the sample, then extracted with 90 (v/v) acetone. Absorbance is measured spectrophotometrically at 664 nm and 750 nm. The extract is then acidified, converting chlorophyll-a to phaeophytin-a. Absorbance is determined again after acidification. The chlorophyll-a concentration is determined from the decrease in absorbance upon acidification. When a detection limit of 0.5 ug/l is required, the volume of sample filtered is doubled to 700mL. Samples with an OD664 before/od665 after acidification ratio (664b/665a) of 1.70 are considered to contain no pheophytin a and to be in excellent physiological condition. Solutions of pure pheophytin show no reduction in OD665 upon acidification and have a 664b/665a ratio of Thus, mixtures of chlorophyll a and pheophytin a have absorption peak ratios ranging between and 1.7. These ratios are based on the use of 90 acetone as solvent. COLOUR-TRUE-WP Colour, True APHA 4500 COLOR This analysis is carried out using procedures adapted from APHA 21 "Color". Colour (True Colour) is determined by filtering a sample through a 0.45 micron membrane filter followed by analysis of the filtrate using the platinum-cobalt colourimetric method. Colour is ph dependent. Unless otherwise

177 Reference Information L CONTD... PAGE 8 of 9 Test Method References: ALS Test Code Matrix Test Description Method Reference** indicated, reported colour results pertain to the ph of the sample as received to within +/- 1 ph unit. CONSULT-BOD-CBOD- WP Carbonaceous BOD APHA 5210 B-5 day Incub.-O2 electrode A sample of water is incubated for 5 days at degrees Celcius. Comparison of dissolved oxygen content at beginning and end of incubation provides a measure of Biochemical oxygen demand. If carbonaceous BOD is requested, TCMP is added to the sample to chemically inhibit nitrogenous oxygen demand. If soluble BOD is requested, the sample is filtered prior to analysis. EC-WP Conductivity APHA 2510B Conductivity of an aqueous solution refers to its ability to carry an electric current. Conductance of a solution is measured between two spatially fixed and chemically inert electrodes. ETL-HARDNESS-DIS-WP ETL-HARDNESS-TOT-WP HG-D-CVAF-WP Hardness Calculated Hardness Calculated Mercury Dissolved Calculated Calculated EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. HG-T-CVAF-WP Mercury Total EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. MET-D-L-MS-WP Dissolved Metals by ICP-MS U.S. EPA 0.8-DL Dissolved Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the Examination of and Wastewater method 3030B for filtration through a 0.45 um filter and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. MET-T-L-MS-WP Total Metals by ICP-MS U.S. EPA 0.8-TL Total Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the examination of and Wastewater Method 3030E and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. N-TOTK-WP Total Kjeldahl Nitrogen Quickchem method E Lachat Samples are digested with a sulphuric acid solution, cooled, diluted with water, and analyzed for ammonia. Total Kjeldahl nitrogen is the sum of freeammonia and organic nitrogen compounds which are converted to ammonium sulphate through this digestion process. Analysis is performed by Flow Injection Analysis (FIA). The ph of the digested sample is raised to a known, basic ph by neutralization with a concentrated buffer solution. This neutralization converts the ammonium cation to ammonia. The ammonia produced is heated with saliclyate and hypochlorite to produce blue colour which is proportional to the ammonia concentration. NH3-COL-WP Ammonia by colour APHA 4500 NH3 F Ammonia - Colourimeric using Salicylate-nitroprusside and hypochlorite, in an alkaline phosphate buffer. NO2+NO3-CALC-WP Nitrate+Nitrite CALCULATION P-TOTAL-WP Phosphorus, Total APHA, 18 P-T Samples are digested using a sulphuric acid-persulfate mixture to convert organic phosphorous to orthophosphate. The samples are analyzed by either the Flow Injection Analysis (FIA) or the Segmented Flow Analysis (SFA) method. The absorbance measured by the instrument is proportional to the concentration of orthophosphate in the sample, and is reported as phosphorous. PH-WP ph APHA 4500H

178 Reference Information L CONTD... PAGE 9 of 9 Test Method References: ALS Test Code Matrix Test Description Method Reference** ph of a sample is the determination of the activity of the hydrogen ions by potentiometric measurement using a standard hydrogen electrode and a reference electrode. SILICATE-COL-VA Silicate by Colourimetric analysis APHA 4500-SIO2 D. This analysis is carried out using procedures adapted from APHA Method 4500-SiO2 D. "Silica". Silicate (molybdate-reactive silica) is determined by the molybdosilicate-heteropoly blue colourimetric method. SOLIDS-TDS-WP Total Dissolved Solids APHA 2540 The residue remaining in a prepared casserole after passing the sample through a 1.2 um Whatman GF/C glass microfibre filter and drying at 180 degrees C. Samples may be dried at 105 degrees C if the client specifically requests this drying temperature. SOLIDS-TOTSUS-WP Total Suspended Solids APHA 2540 The residue retained by a prepared 1.5 um Whatman 934-AH glass microfibre filter dried at 105 degrees C. TURBIDITY-WP Turbidity APHA, 18, 2130B A strong light beam is sent through a transparent tube containing the sample. Light that is reflected at 90 degrees to the axis by suspended particles is detected by the photocell. The electrical response is proportional to the sample turbidity. ** ALS test methods may incorporate modifications from specified reference methods to improve performance. The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code WP VA Laboratory Location ALS LABORATORY GROUP - WINNIPEG, MANITOBA, CANADA ALS LABORATORY GROUP - VANCOUVER, BC, CANADA Chain of Custody Numbers: GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

179 Workorder: L Report Date: 24-NOV-10 Page 1 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ACIDITY-LOW-WP Batch R WG CVS Acidity (as CaCO3) WG DUP Acidity (as CaCO3) L ALK-TOT-WP Batch R WG CVS Alkalinity, Total (as CaCO3) WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < Batch R WG CVS Alkalinity, Total (as CaCO3) OCT-10 WG CVS Alkalinity, Total (as CaCO3) OCT-10 WG DUP Alkalinity, Total (as CaCO3) L OCT-10 Bicarbonate (HCO3) OCT-10 Carbonate (CO3) <0.60 < OCT-10 Hydroxide (OH) <0.40 < OCT-10 WG DUP Alkalinity, Total (as CaCO3) L OCT-10 Bicarbonate (HCO3) OCT-10 Carbonate (CO3) <0.60 < OCT-10 Hydroxide (OH) <0.40 < OCT-10 WG DUP L

180 Workorder: L Report Date: 24-NOV-10 Page 2 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff ALK-TOT-WP Batch R WG DUP Alkalinity, Total (as CaCO3) L OCT-10 Bicarbonate (HCO3) OCT-10 Carbonate (CO3) <0.60 < OCT-10 Hydroxide (OH) <0.40 < OCT-10 ANIONS5-IC-WP Batch R WG LCS Chloride Fluoride Nitrite-N Nitrate-N Sulfate WG Chloride MB < Fluoride < 0.1 Nitrite-N < 0.05 Nitrate-N < 0.05 Sulfate < BR-IC-WP Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 C-DIS-ORG-WP Batch R WG CCV Dissolved Organic Carbon SEP-10 WG CVS Dissolved Organic Carbon 29-SEP-10 WG DUP Dissolved Organic Carbon L SEP-10 WG MB Dissolved Organic Carbon < 1 29-SEP-10 C-TOT-ORG-WP

181 Workorder: L Report Date: 24-NOV-10 Page 3 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff C-TOT-ORG-WP Batch R WG CCV Total Organic Carbon 29-SEP-10 WG CVS Total Organic Carbon 29-SEP-10 WG DUP Total Organic Carbon L SEP-10 WG MB Total Organic Carbon < 1 29-SEP-10 CHL/A,PHEO/A-ACET-WP Batch R1475 WG CVS Chlorophyll a WG Chlorophyll a CVS COLOUR-TRUE-WP Batch R WG DUP Colour, True L <5.0 7 CU WG Colour, True LCS WG Colour, True MB <5.0 CU 5 CONSULT-BOD-CBOD-WP Batch R WG DUP BOD Carbonaceous L WG IRM BOD Carbonaceous 61-GG WG MB BOD Carbonaceous < 1 EC-WP Batch R WG CCV Conductivity WG Conductivity CVS WG DUP L

182 Workorder: L Report Date: 24-NOV-10 Page 4 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff EC-WP Batch R WG DUP Conductivity L umhos/cm WG Conductivity DUP L umhos/cm Batch R WG CCV Conductivity OCT-10 WG Conductivity CVS 04-OCT-10 WG Conductivity DUP L umhos/cm OCT-10 HG-D-CVAF-WP Batch R WG DUP L WG DUP L WG DUP L WG LCS WG MB WG MB WG MS L WG MS L

183 Workorder: L Report Date: 24-NOV-10 Page 5 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-D-CVAF-WP Batch R WG MS L Batch R WG DUP L WG DUP L WG LCS WG MB WG MB WG MS L WG MS L HG-T-CVAF-WP Batch R WG DUP L WG DUP L WG DUP L9332-4

184 Workorder: L Report Date: 24-NOV-10 Page 6 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff HG-T-CVAF-WP Batch R WG LCS WG MB WG MS L WG MS L WG MS L MET-D-L-MS-WP Batch WG CCV Aluminum (Al)-Dissolved 95 Antimony (Sb)-Dissolved 95 Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved 105 Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved 92 Chromium (Cr)-Dissolved 95 Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved

185 Workorder: L Report Date: 24-NOV-10 Page 7 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CCV Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved 94 Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved 95 Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 94 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved 104 Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved 104 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved

186 Workorder: L Report Date: 24-NOV-10 Page 8 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Copper (Cu)-Dissolved Iron (Fe)-Dissolved 104 Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved 94 Selenium (Se)-Dissolved Silicon (Si)-Dissolved 95 Silver (Ag)-Dissolved 95 Sodium (Na)-Dissolved Strontium (Sr)-Dissolved 95 Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved 91 WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved 106 Boron (B)-Dissolved 108

187 Workorder: L Report Date: 24-NOV-10 Page 9 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG CVS Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved 106 Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved 95 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 93 Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG DUP Aluminum (Al)-Dissolved WG Antimony (Sb)-Dissolved

188 Workorder: L Report Date: 24-NOV-10 Page 10 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Arsenic (As)-Dissolved WG Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved < < Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 26 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved

189 Workorder: L Report Date: 24-NOV-10 Page 11 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG DUP Uranium (U)-Dissolved WG Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG LCS Aluminum (Al)-Dissolved 108 Antimony (Sb)-Dissolved 111 Arsenic (As)-Dissolved 109 Barium (Ba)-Dissolved 109 Beryllium (Be)-Dissolved 116 Bismuth (Bi)-Dissolved 104 Boron (B)-Dissolved 111 Cadmium (Cd)-Dissolved 104 Calcium (Ca)-Dissolved 108 Cesium (Cs)-Dissolved 108 Chromium (Cr)-Dissolved 115 Cobalt (Co)-Dissolved 115 Copper (Cu)-Dissolved 109 Iron (Fe)-Dissolved 116 Lead (Pb)-Dissolved 106 Lithium (Li)-Dissolved 111 Magnesium (Mg)-Dissolved 109 Manganese (Mn)-Dissolved 105 Molybdenum (Mo)-Dissolved 109 Nickel (Ni)-Dissolved 105 Phosphorus (P)-Dissolved 111 Potassium (K)-Dissolved 109 Rubidium (Rb)-Dissolved 113 Selenium (Se)-Dissolved 107 Silicon (Si)-Dissolved 113 Silver (Ag)-Dissolved 104 Sodium (Na)-Dissolved 113 Strontium (Sr)-Dissolved 104 Tellurium (Te)-Dissolved 115

190 Workorder: L Report Date: 24-NOV-10 Page 12 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG LCS Tellurium (Te)-Dissolved 115 Thallium (Tl)-Dissolved 105 Thorium (Th)-Dissolved 106 Tin (Sn)-Dissolved 108 Titanium (Ti)-Dissolved 109 Tungsten (W)-Dissolved 107 Uranium (U)-Dissolved Vanadium (V)-Dissolved 111 Zinc (Zn)-Dissolved 109 Zirconium (Zr)-Dissolved 106 WG MB Aluminum (Al)-Dissolved < Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < 0.01 Cadmium (Cd)-Dissolved < Calcium (Ca)-Dissolved < 0.05 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < 0.01 Lead (Pb)-Dissolved < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved < 0.01 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < 0.1 Potassium (K)-Dissolved < Rubidium (Rb)-Dissolved

191 Workorder: L Report Date: 24-NOV-10 Page 13 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-D-L-MS-WP Batch WG MB Selenium (Se)-Dissolved Silicon (Si)-Dissolved < 0.05 Silver (Ag)-Dissolved Sodium (Na)-Dissolved < Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved < Zirconium (Zr)-Dissolved < MET-T-L-MS-WP Batch R WG CCV Aluminum (Al)-Total 94 Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total 95 Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total

192 Workorder: L Report Date: 24-NOV-10 Page 14 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CCV Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 95 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total 95 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total 92 Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total

193 Workorder: L Report Date: 24-NOV-10 Page 15 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CVS Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total 95 Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total 95 Tellurium (Te)-Total 95 Thallium (Tl)-Total Thorium (Th)-Total 95 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total 94 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 94 WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total 105

194 Workorder: L Report Date: 24-NOV-10 Page 16 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CVS Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total 104 Silver (Ag)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG DUP Aluminum (Al)-Total WG < < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total

195 Workorder: L Report Date: 24-NOV-10 Page 17 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG DUP Bismuth (Bi)-Total WG Boron (B)-Total Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG DUP Aluminum (Al)-Total WG

196 Workorder: L Report Date: 24-NOV-10 Page 18 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG DUP Antimony (Sb)-Total WG Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total <0.0 <0.0 Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total ,G Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total

197 Workorder: L Report Date: 24-NOV-10 Page 19 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG DUP Vanadium (V)-Total WG Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG LCS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total 104 Barium (Ba)-Total 108 Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total 105 Calcium (Ca)-Total Cesium (Cs)-Total 109 Chromium (Cr)-Total 105 Cobalt (Co)-Total 109 Copper (Cu)-Total 105 Iron (Fe)-Total 106 Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total 105 Molybdenum (Mo)-Total 107 Nickel (Ni)-Total 106 Phosphorus (P)-Total 106 Potassium (K)-Total Rubidium (Rb)-Total 109 Selenium (Se)-Total 104 Silicon (Si)-Total 107 Silver (Ag)-Total 105 Tellurium (Te)-Total 105 Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total

198 Workorder: L Report Date: 24-NOV-10 Page of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG LCS Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total 105 Vanadium (V)-Total 107 Zinc (Zn)-Total 106 Zirconium (Zr)-Total 105 WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total < Lead (Pb)-Total < Lithium (Li)-Total < Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total < Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total

199 Workorder: L Report Date: 24-NOV-10 Page 21 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG MB Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < Batch R WG CCV Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total 105 Beryllium (Be)-Total 95 Bismuth (Bi)-Total 107 Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total 105 Chromium (Cr)-Total Cobalt (Co)-Total 105 Copper (Cu)-Total 104 Iron (Fe)-Total 104 Lead (Pb)-Total 105 Lithium (Li)-Total Magnesium (Mg)-Total 105 Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total

200 Workorder: L Report Date: 24-NOV-10 Page 22 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CCV Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total 104 Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total 105 Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total 90 Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total 95 Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total

201 Workorder: L Report Date: 24-NOV-10 Page 23 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CVS Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total 104 Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 94 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total 95 Vanadium (V)-Total Zinc (Zn)-Total 94 Zirconium (Zr)-Total WG CVS Aluminum (Al)-Total Antimony (Sb)-Total 95 Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total

202 Workorder: L Report Date: 24-NOV-10 Page 24 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG CVS Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total 104 Silicon (Si)-Total Silver (Ag)-Total 95 Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total 93 Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total WG DUP Aluminum (Al)-Total WG < < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total

203 Workorder: L Report Date: 24-NOV-10 Page 25 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG DUP Boron (B)-Total WG < < Cadmium (Cd)-Total < < Calcium (Ca)-Total < < Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total <0.0 <0.0 Lead (Pb)-Total < < Lithium (Li)-Total <0.00 <0.00 Magnesium (Mg)-Total Manganese (Mn)-Total < < Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG DUP WG

204 Workorder: L Report Date: 24-NOV-10 Page 26 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total

205 Workorder: L Report Date: 24-NOV-10 Page 27 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG DUP Titanium (Ti)-Total WG G 27 Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG LCS Aluminum (Al)-Total 108 Antimony (Sb)-Total Arsenic (As)-Total 104 Barium (Ba)-Total 109 Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total 105 Cesium (Cs)-Total 111 Chromium (Cr)-Total 107 Cobalt (Co)-Total 111 Copper (Cu)-Total 106 Iron (Fe)-Total 110 Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total 106 Manganese (Mn)-Total 105 Molybdenum (Mo)-Total Nickel (Ni)-Total 106 Phosphorus (P)-Total 110 Potassium (K)-Total 105 Rubidium (Rb)-Total 107 Selenium (Se)-Total 105 Silicon (Si)-Total Silver (Ag)-Total

206 Workorder: L Report Date: 24-NOV-10 Page 28 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG LCS Sodium (Na)-Total 108 Strontium (Sr)-Total Tellurium (Te)-Total 106 Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total 105 Tungsten (W)-Total Uranium (U)-Total 105 Vanadium (V)-Total 108 Zinc (Zn)-Total 104 Zirconium (Zr)-Total WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total < Lead (Pb)-Total < Lithium (Li)-Total < Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total <0. 0.2

207 Workorder: L Report Date: 24-NOV-10 Page 29 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff MET-T-L-MS-WP Batch R WG MB Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total Sodium (Na)-Total < Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < N-TOTK-WP Batch R WG CCV Total Kjeldahl Nitrogen WG CVS Total Kjeldahl Nitrogen WG DUP Total Kjeldahl Nitrogen L WG DUP Total Kjeldahl Nitrogen L WG LCS Total Kjeldahl Nitrogen WG MB Total Kjeldahl Nitrogen < WG MB Total Kjeldahl Nitrogen < WG MS Total Kjeldahl Nitrogen L MS-B -

208 Workorder: L Report Date: 24-NOV-10 Page 30 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff N-TOTK-WP Batch R WG MS Total Kjeldahl Nitrogen L MS-B - NH3-COL-WP Batch R WG CCV Ammonia as N 105 WG Ammonia as N DUP L WG Ammonia as N LCS WG Ammonia as N MB < 0.05 WG Ammonia as N MS L MS-B - P-TOTAL-WP Batch R WG CCV Phosphorus, Total WG CCV Phosphorus, Total 93 WG CVS Phosphorus, Total 108 WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total 109 WG DUP Phosphorus, Total L WG DUP Phosphorus, Total L WG MB

209 Workorder: L Report Date: 24-NOV-10 Page 31 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff P-TOTAL-WP Batch R WG MB Phosphorus, Total < 0.01 WG MS Phosphorus, Total L PH-WP Batch R WG CCV ph WG ph CVS - WG ph DUP L ph units WG ph DUP L ph units SILICATE-COL-VA Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG DUP Silicate (as SIO2) L WG DUP Silicate (as SIO2) L WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 SOLIDS-TDS-WP

210 Workorder: L Report Date: 24-NOV-10 Page 32 of 34 Commerce Drive Winnipeg MB R3P 0Y7 Clifton Samoiloff SOLIDS-TDS-WP Batch R WG CVS Total Dissolved Solids WG DUP Total Dissolved Solids L WG MB Total Dissolved Solids <5.0 5 SOLIDS-TOTSUS-WP Batch R WG CVS Total Suspended Solids WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG MB Total Suspended Solids <5.0 5 TURBIDITY-WP Batch R WG CCV Turbidity WG Turbidity CCV 104 WG Turbidity CVS WG Turbidity CVS WG Turbidity DUP L NTU WG Turbidity DUP L NTU WG Turbidity DUP L NTU WG Turbidity LCS

211 Workorder: L Report Date: 24-NOV-10 Page 33 of 34 Legend: Limit Confidence Interval (Laboratory Control Limits) DUP Duplicate RPD Relative Percent Difference Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description Duplicate results and limits are expressed in terms of absolute difference. MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. Relative Percent Difference Not Available due to result(s) being less than detection limit.

212 Workorder: L Report Date: 24-NOV-10 Page 34 of 34 Hold Time Exceedances: ALS Product Description Physical Tests ph Anions and Nutrients Anions scan (IC) Bromide Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: Sample ID Sampling Date Date Processed Rec. HT Actual HT :00 12:30 12:00 12:30 12:00 12:30 11:58 11:58 14:29 14:29 14:29 14: Units hours hours hours hours hours hours Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units). Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L were received on 12:00. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS. Qualifier EHTR-FM EHTR-FM EHTR EHTR EHTR EHTR The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

213

214 Loginnum Acctnum Client Deptnum L W RECHECK ANALYSIS REPORT RC23591 Date: 19-NOV-10 13:52 Requestby Due Date Issued To CLIENT 19-NOV-10 GHILL CHILL 16-NOV-10 Recheck Comments Confirm sample ID / review data / reanalyze if possible. Nitrate-N rerun result < reported and NO2+NO3-CALC-WP recalculated to < meb-wp 17-Nov-10 Recheck Reason Quality control sample(s) failure (in-house or client QC) - field blank Action to Take Do whats necessary Issued By Date Initiated Samplenum L Prod ANIONS5-IC-WP Mat 1 Parm Syn Nitrate-N Result Units Measdate RCResult UCL RC RPD RCWork# RCMeasdate < NA 17-NOV-10 Initials T L MET-T-L-MS-WP 1 Sodium (Na)-Total <0.03 No Chart NA NA 17-NOV-10 DAG L MET-T-L-MS-WP 1 Strontium (Sr)-Total < No Chart NA NA 17-NOV-10 DAG L NO2+NO3-CALC-WP 1 Nitrate and Nitrite as N < NOV-10 Sample Comments: Analyst Comments:

215 ATTN: CLIFF SAMOILOFF COMMERCE DRIVE WINNIPEG MB R3P 0Y7 Phone: Date Received: Report Date: Version: -OCT-10 14:59 (MT) FINAL Certificate of Analysis Lab Work Order #: L9332 Project P.O. #: NOT SUBMITTED ob Reference: Legal Site Desc: C of C Numbers: Paul Nicolas Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 1329 Niakwa Road East, Unit 12, Winnipeg, MB R2 3T4 Canada Phone: Fax: MANITOBA TECHNOLOGY CENTRE LTD. Part of the ALS Group A Campbell Brothers Limited Company

216 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 2 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L WHC-F10-WQ2 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 11:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total < < < < < < < < < < <0.00 < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

217 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 3 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L WHC-F10-WQ2 Sampled By: Matrix: SK/MR 11:00 WATER Total Metals by ICP-MS Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved < < < < < < <0.00 < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

218 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 4 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: WHC-F10-WQ2 SK/MR 11:00 WATER Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: GRR-F10-WQ1 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 13:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total < < < < < < < < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

219 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 5 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L GRR-F10-WQ1 Sampled By: Matrix: SK/MR 13:00 WATER Total Metals by ICP-MS Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < <0.00 < < < < < < < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

220 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 6 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: GRR-F10-WQ1 SK/MR 13:00 WATER Dissolved Metals by ICP-MS Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: RDL-F10-WQ1 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 14:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen < < < < CU 25-SEP OCT-10 R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

221 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 7 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ1 Sampled By: Matrix: SK/MR 14:00 WATER Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved < < < < < <0.00 < < < NTU 18-OCT-10 R R R R R R R R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

222 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 8 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ1 SK/MR 14:00 WATER Dissolved Metals by ICP-MS Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < < < <0.00 < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R14763 R1475 R1475 R1475 R R R R R R L Sampled By: Matrix: RDL-F10-WQ2 SK/MR 16:00 WATER * Refer to Referenced Information for Qualifiers (if any) and Methodology.

223 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 9 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ2 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 16:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total < < < < < < < < <0.00 < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

224 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 10 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ2 Sampled By: Matrix: SK/MR 16:00 WATER Total Metals by ICP-MS Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved < < < < < < < < <0.00 < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

225 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 11 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ2 SK/MR 16:00 WATER Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: RDL-F10-WQ3 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 10:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total < < < < < < < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

226 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 12 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ3 Sampled By: Matrix: SK/MR 10:00 WATER Total Metals by ICP-MS Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < <0.00 < < < < < < < < < R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

227 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 13 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ3 SK/MR 10:00 WATER Dissolved Metals by ICP-MS Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: RDL-F10-WQ7 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 14:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen < < < < CU 25-SEP OCT-10 R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

228 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 14 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ7 Sampled By: Matrix: SK/MR 14:00 WATER Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved 14.4 < < < < < < <0.00 < < < NTU 15-OCT-10 R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

229 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 15 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ7 SK/MR 14:00 WATER Dissolved Metals by ICP-MS Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < < < <0.00 < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: Matrix: RDL-F10-WQ8 SK/MR 14:00 WATER * Refer to Referenced Information for Qualifiers (if any) and Methodology.

230 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 16 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ8 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 14:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total < < < < < < < < < < <0.00 < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

231 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 17 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ8 Sampled By: Matrix: SK/MR 14:00 WATER Total Metals by ICP-MS Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved < < < < < < <0.00 < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

232 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 18 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ8 SK/MR 14:00 WATER Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: RDL-F10-WQ9 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 14:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total < < < < < < < < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

233 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 19 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ9 Sampled By: Matrix: SK/MR 14:00 WATER Total Metals by ICP-MS Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < <0.00 < < < < < < R14763 R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

234 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ9 SK/MR 14:00 WATER Dissolved Metals by ICP-MS Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: RDL-F10-WQ4 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 10:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen < < < < CU 25-SEP OCT-10 R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

235 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 21 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ4 Sampled By: Matrix: SK/MR 10:00 WATER Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved < < < < <0.00 < < < < NTU 15-OCT-10 R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

236 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 22 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ4 SK/MR 10:00 WATER Dissolved Metals by ICP-MS Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < < < < <0.00 < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: Matrix: RDL-F10-WQ5 SK/MR 13:00 WATER * Refer to Referenced Information for Qualifiers (if any) and Methodology.

237 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 23 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ5 Sampled By: Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 13:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total < < < < < < < < < < < <0.00 < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

238 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 24 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ5 Sampled By: Matrix: SK/MR 13:00 WATER Total Metals by ICP-MS Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved < < < < < < <0.00 < R14763 R14763 R14763 R14763 * Refer to Referenced Information for Qualifiers (if any) and Methodology.

239 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 25 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L Sampled By: Matrix: RDL-F10-WQ5 SK/MR 13:00 WATER Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph < < <0.60 < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R L Sampled By: RDL-F10-WQ6 Matrix: WATER Miscellaneous Parameters Acidity (as CaCO3) Ammonia as N Bromide (Br) BOD Carbonaceous Colour, True SK/MR 11:00 Dissolved Organic Carbon Hardness (as CaCO3) Hardness (as CaCO3) Nitrate and Nitrite as N Phosphorus, Total Silicate (as SIO2) Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Total Suspended Solids Turbidity Anions scan (IC) Chloride Nitrite-N Nitrate-N Sulfate Total Metals by ICP-MS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total Cadmium (Cd)-Total Calcium (Ca)-Total < < < < < < < CU NTU 25-SEP OCT OCT-10 R R R R R R R R R R R R R R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

240 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 26 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ6 Sampled By: Matrix: SK/MR 11:00 WATER Total Metals by ICP-MS Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total Dissolved Metals by ICP-MS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved <0.00 < < < < < < < < < * Refer to Referenced Information for Qualifiers (if any) and Methodology.

241 ALS LABORATORY GROUP ANALYTICAL REPORT L9332 CONTD... PAGE 27 of 30 Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed Batch L RDL-F10-WQ6 Sampled By: Matrix: SK/MR 11:00 WATER Dissolved Metals by ICP-MS Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved Chlorophyll-a & Pheophytin-a Chlorophyll a Phaeophytin a ODb/ODa ph, Conductivity and Total Alkalinity Alkalinity Alkalinity, Total (as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Conductivity ph ph <0.00 < < ug/l ug/l ABS Ratio umhos/cm ph units R1475 R1475 R1475 R R R R R R * Refer to Referenced Information for Qualifiers (if any) and Methodology.

242 Reference Information L9332 CONTD... PAGE 28 of 30 QC Samples with Qualifiers & Comments: QC Type Description Parameter Matrix Spike Ammonia as N Qualifier MS-B Applies to Sample Number(s) L9332-1, -10, -11, -2, -3, -4, -5, -6, -7, -8, -9 Test Method References: ALS Test Code Matrix Test Description Method Reference** ACIDITY-LOW-WP Acidity APHA Method 2310B ALK-TOT-WP Alkalinity APHA 23B Alkalinity of water is a measure of its acid neutralizing capacity. Alkalinity is imparted by bicarbonate, carbonate and hydroxide components of water. It is determined by titration with a standard solution of strong mineral acid to the successive HCO3- and H2CO3 endpoints indicated electrometrically. ANIONS5-IC-WP Anions scan (IC) EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". BR-IC-WP Bromide EPA IC This analysis is carried out using procedures adapted from EPA Method "Determination of Inorganic Anions in Drinking by Ion Chromatography". C-DIS-ORG-WP Dissolved Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. C-TOT-ORG-WP Total Organic Carbon APHA 5310 B-INSTRUMENTAL-WP This method is applicable to the analysis of ground water, wastewater, and surface water samples. The form detected depends upon sample pretreatment: Unfiltered sample = TC, 0.45um filtered = TDC. Samples are injected into a combustion tube containing an oxidation catalyst. The carrier gas containing the combustion product from the combustion tube flows through an inorganic carbon reactor vessel and is then sent through a halogen scrubber into a sample cell set in a non-dispersive infrared gas analyzer (NDIR) where carbon dioxide is detected. For total inorganic carbon and dissolved inorganic carbon, the sample is injected into an IC reactor vessel where only the IC component is decomposed to become carbon dioxide. The peak area generated by the NDIR indicates the TC/TDC or TIC/DIC as applicable. The total organic carbon content of the sample is calculated by subtracting the TIC from the TC. TOC = TC-TIC, DOC = TDC-DIC, Particulate = Total - Dissolved. CHL/A,PHEO/A-ACET-WP Chlorophyll-a & Pheophytin-a APHA H, /750NM Chlorophyll-a is filtered from the sample, then extracted with 90 (v/v) acetone. Absorbance is measured spectrophotometrically at 664 nm and 750 nm. The extract is then acidified, converting chlorophyll-a to phaeophytin-a. Absorbance is determined again after acidification. The chlorophyll-a concentration is determined from the decrease in absorbance upon acidification. When a detection limit of 0.5 ug/l is required, the volume of sample filtered is doubled to 700mL. Samples with an OD664 before/od665 after acidification ratio (664b/665a) of 1.70 are considered to contain no pheophytin a and to be in excellent physiological condition. Solutions of pure pheophytin show no reduction in OD665 upon acidification and have a 664b/665a ratio of Thus, mixtures of chlorophyll a and pheophytin a have absorption peak ratios ranging between and 1.7. These ratios are based on the use of 90 acetone as solvent. COLOUR-TRUE-WP Colour, True APHA 4500 COLOR This analysis is carried out using procedures adapted from APHA 21 "Color". Colour (True Colour) is determined by filtering a sample through a 0.45 micron membrane filter followed by analysis of the filtrate using the platinum-cobalt colourimetric method. Colour is ph dependent. Unless otherwise indicated, reported colour results pertain to the ph of the sample as received to within +/- 1 ph unit. CONSULT-BOD-CBOD- WP Carbonaceous BOD APHA 5210 B-5 day Incub.-O2 electrode A sample of water is incubated for 5 days at degrees Celcius. Comparison of dissolved oxygen content at beginning and end of incubation provides a measure of Biochemical oxygen demand. If carbonaceous BOD is requested, TCMP is added to the sample to chemically inhibit nitrogenous oxygen demand. If soluble BOD is requested, the sample is filtered prior to analysis. EC-WP Conductivity APHA 2510B

243 Reference Information L9332 CONTD... PAGE 29 of 30 Test Method References: ALS Test Code Matrix Test Description Method Reference** Conductivity of an aqueous solution refers to its ability to carry an electric current. Conductance of a solution is measured between two spatially fixed and chemically inert electrodes. ETL-HARDNESS-DIS-WP ETL-HARDNESS-TOT-WP HG-D-CVAF-WP Hardness Calculated Hardness Calculated Mercury Dissolved Calculated Calculated EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. HG-T-CVAF-WP Mercury Total EPA245.7 V2.0 Mercury in filtered and unfiltered waters is oxidized with Bromine monochloride and analyzed by cold-vapour atomic fluorescence spectrometry. MET-D-L-MS-WP Dissolved Metals by ICP-MS U.S. EPA 0.8-DL Dissolved Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the Examination of and Wastewater method 3030B for filtration through a 0.45 um filter and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. MET-T-L-MS-WP Total Metals by ICP-MS U.S. EPA 0.8-TL Total Metals by ICP-MS: This analysis is carried out using sample preparation procedures adapted from Standard Methods for the examination of and Wastewater Method 3030E and analytical procedures adapted from U.S EPA Method 0.8 for analyis of metals by inductively coupled-mass spectrometery. N-TOTK-WP Total Kjeldahl Nitrogen Quickchem method E Lachat Samples are digested with a sulphuric acid solution, cooled, diluted with water, and analyzed for ammonia. Total Kjeldahl nitrogen is the sum of freeammonia and organic nitrogen compounds which are converted to ammonium sulphate through this digestion process. Analysis is performed by Flow Injection Analysis (FIA). The ph of the digested sample is raised to a known, basic ph by neutralization with a concentrated buffer solution. This neutralization converts the ammonium cation to ammonia. The ammonia produced is heated with saliclyate and hypochlorite to produce blue colour which is proportional to the ammonia concentration. NH3-COL-WP Ammonia by colour APHA 4500 NH3 F Ammonia - Colourimeric using Salicylate-nitroprusside and hypochlorite, in an alkaline phosphate buffer. NO2+NO3-CALC-WP Nitrate+Nitrite CALCULATION P-TOTAL-WP Phosphorus, Total APHA, 18 P-T Samples are digested using a sulphuric acid-persulfate mixture to convert organic phosphorous to orthophosphate. The samples are analyzed by either the Flow Injection Analysis (FIA) or the Segmented Flow Analysis (SFA) method. The absorbance measured by the instrument is proportional to the concentration of orthophosphate in the sample, and is reported as phosphorous. PH-WP ph APHA 4500H ph of a sample is the determination of the activity of the hydrogen ions by potentiometric measurement using a standard hydrogen electrode and a reference electrode. SILICATE-COL-VA Silicate by Colourimetric analysis APHA 4500-SIO2 D. This analysis is carried out using procedures adapted from APHA Method 4500-SiO2 D. "Silica". Silicate (molybdate-reactive silica) is determined by the molybdosilicate-heteropoly blue colourimetric method. SOLIDS-TDS-WP Total Dissolved Solids APHA 2540

244 Reference Information L9332 CONTD... PAGE 30 of 30 Test Method References: ALS Test Code Matrix Test Description Method Reference** The residue remaining in a prepared casserole after passing the sample through a 1.2 um Whatman GF/C glass microfibre filter and drying at 180 degrees C. Samples may be dried at 105 degrees C if the client specifically requests this drying temperature. SOLIDS-TOTSUS-WP Total Suspended Solids APHA 2540 The residue retained by a prepared 1.5 um Whatman 934-AH glass microfibre filter dried at 105 degrees C. TURBIDITY-WP Turbidity APHA, 18, 2130B A strong light beam is sent through a transparent tube containing the sample. Light that is reflected at 90 degrees to the axis by suspended particles is detected by the photocell. The electrical response is proportional to the sample turbidity. ** ALS test methods may incorporate modifications from specified reference methods to improve performance. The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code WP VA Laboratory Location ALS LABORATORY GROUP - WINNIPEG, MANITOBA, CANADA ALS LABORATORY GROUP - VANCOUVER, BC, CANADA Chain of Custody Numbers: GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

245 Workorder: L9332 Report Date: -OCT-10 Page 1 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF ACIDITY-LOW-WP Batch R WG CVS Acidity (as CaCO3) WG DUP Acidity (as CaCO3) L ALK-TOT-WP Batch R WG CVS Alkalinity, Total (as CaCO3) WG CVS Alkalinity, Total (as CaCO3) WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < WG DUP Alkalinity, Total (as CaCO3) L Bicarbonate (HCO3) Carbonate (CO3) <0.60 < Hydroxide (OH) <0.40 < ANIONS5-IC-WP Batch R WG LCS Chloride Nitrite-N Nitrate-N Sulfate WG Chloride MB < Nitrite-N < 0.05 Nitrate-N < 0.05

246 Workorder: L9332 Report Date: -OCT-10 Page 2 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF ANIONS5-IC-WP Batch R WG MB Sulfate < BR-IC-WP Batch R WG LCS Bromide (Br) WG Bromide (Br) MB < 0.1 C-DIS-ORG-WP Batch R WG CCV Dissolved Organic Carbon 02-OCT-10 WG CVS Dissolved Organic Carbon 01-OCT-10 Batch R WG CCV Dissolved Organic Carbon 19-OCT-10 WG CVS Dissolved Organic Carbon 18-OCT-10 WG MB Dissolved Organic Carbon < 1 18-OCT-10 C-TOT-ORG-WP Batch R WG CCV Total Organic Carbon 15-OCT-10 WG CVS Total Organic Carbon 15-OCT-10 WG DUP Total Organic Carbon L OCT-10 WG MB Total Organic Carbon < 1 15-OCT-10 Batch R WG CCV Total Organic Carbon 19-OCT-10 WG CVS Total Organic Carbon 18-OCT-10

247 Workorder: L9332 Report Date: -OCT-10 Page 3 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF C-TOT-ORG-WP Batch R WG DUP Total Organic Carbon L OCT-10 WG MB Total Organic Carbon < 1 18-OCT-10 CHL/A,PHEO/A-ACET-WP Batch R1475 WG CVS Chlorophyll a WG Chlorophyll a CVS COLOUR-TRUE-WP Batch R WG DUP Colour, True L CU 7.5 WG Colour, True LCS WG Colour, True MB <5.0 CU 5 CONSULT-BOD-CBOD-WP Batch R WG DUP BOD Carbonaceous L SEP-10 WG IRM BOD Carbonaceous 61-GG SEP-10 WG MB BOD Carbonaceous < 1 25-SEP-10 EC-WP Batch R WG CCV Conductivity WG Conductivity CVS WG Conductivity DUP L umhos/cm WG Conductivity DUP L umhos/cm HG-D-CVAF-WP

248 Workorder: L9332 Report Date: -OCT-10 Page 4 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF HG-D-CVAF-WP Batch R WG DUP L WG DUP L WG LCS WG MB WG MB WG MS L WG MS L HG-T-CVAF-WP Batch R WG DUP L WG DUP L WG DUP L WG LCS WG MB

249 Workorder: L9332 Report Date: -OCT-10 Page 5 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF HG-T-CVAF-WP Batch R WG MB WG MS L WG MS L WG MS L MET-D-L-MS-WP Batch WG CCV Aluminum (Al)-Dissolved 94 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved 95 Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved

250 Workorder: L9332 Report Date: -OCT-10 Page 6 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CCV Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 95 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 95 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG CVS Aluminum (Al)-Dissolved 92 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved

251 Workorder: L9332 Report Date: -OCT-10 Page 7 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CVS Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 95 Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved 95 Sodium (Na)-Dissolved 95 Strontium (Sr)-Dissolved 95 Tellurium (Te)-Dissolved 95 Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 95 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved 94 Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved 94 WG CVS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved 105 Cesium (Cs)-Dissolved

252 Workorder: L9332 Report Date: -OCT-10 Page 8 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG CVS Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved 104 Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved Zirconium (Zr)-Dissolved WG DUP Aluminum (Al)-Dissolved WG <0.00 <0.00 Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved

253 Workorder: L9332 Report Date: -OCT-10 Page 9 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG DUP Beryllium (Be)-Dissolved WG Bismuth (Bi)-Dissolved Boron (B)-Dissolved Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < < Lead (Pb)-Dissolved < < Lithium (Li)-Dissolved Magnesium (Mg)-Dissolved Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < < Potassium (K)-Dissolved Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved Silver (Ag)-Dissolved Sodium (Na)-Dissolved Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved 26 Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved <0.00 <0.00

254 Workorder: L9332 Report Date: -OCT-10 Page 10 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG DUP Zinc (Zn)-Dissolved WG <0.00 <0.00 Zirconium (Zr)-Dissolved < < WG LCS Aluminum (Al)-Dissolved Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved 106 Beryllium (Be)-Dissolved 108 Bismuth (Bi)-Dissolved Boron (B)-Dissolved 104 Cadmium (Cd)-Dissolved Calcium (Ca)-Dissolved Cesium (Cs)-Dissolved 108 Chromium (Cr)-Dissolved 106 Cobalt (Co)-Dissolved 106 Copper (Cu)-Dissolved Iron (Fe)-Dissolved Lead (Pb)-Dissolved Lithium (Li)-Dissolved 104 Magnesium (Mg)-Dissolved 105 Manganese (Mn)-Dissolved 106 Molybdenum (Mo)-Dissolved 105 Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved 109 Potassium (K)-Dissolved Rubidium (Rb)-Dissolved 108 Selenium (Se)-Dissolved Silicon (Si)-Dissolved 108 Silver (Ag)-Dissolved 104 Sodium (Na)-Dissolved 107 Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved 108 Thallium (Tl)-Dissolved Thorium (Th)-Dissolved

255 Workorder: L9332 Report Date: -OCT-10 Page 11 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG LCS Tin (Sn)-Dissolved Titanium (Ti)-Dissolved 105 Tungsten (W)-Dissolved 104 Uranium (U)-Dissolved 105 Vanadium (V)-Dissolved 106 Zinc (Zn)-Dissolved 104 Zirconium (Zr)-Dissolved WG MB Aluminum (Al)-Dissolved < Antimony (Sb)-Dissolved Arsenic (As)-Dissolved Barium (Ba)-Dissolved Beryllium (Be)-Dissolved Bismuth (Bi)-Dissolved Boron (B)-Dissolved < 0.01 Cadmium (Cd)-Dissolved < Calcium (Ca)-Dissolved < 0.05 Cesium (Cs)-Dissolved Chromium (Cr)-Dissolved Cobalt (Co)-Dissolved Copper (Cu)-Dissolved Iron (Fe)-Dissolved < 0.01 Lead (Pb)-Dissolved < Lithium (Li)-Dissolved < Magnesium (Mg)-Dissolved < 0.01 Manganese (Mn)-Dissolved Molybdenum (Mo)-Dissolved Nickel (Ni)-Dissolved Phosphorus (P)-Dissolved < 0.1 Potassium (K)-Dissolved < Rubidium (Rb)-Dissolved Selenium (Se)-Dissolved Silicon (Si)-Dissolved < 0.05 Silver (Ag)-Dissolved

256 Workorder: L9332 Report Date: -OCT-10 Page 12 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-D-L-MS-WP Batch WG MB Sodium (Na)-Dissolved < Strontium (Sr)-Dissolved Tellurium (Te)-Dissolved Thallium (Tl)-Dissolved Thorium (Th)-Dissolved Tin (Sn)-Dissolved Titanium (Ti)-Dissolved Tungsten (W)-Dissolved Uranium (U)-Dissolved Vanadium (V)-Dissolved Zinc (Zn)-Dissolved < Zirconium (Zr)-Dissolved < Batch R14763 WG CCV Cadmium (Cd)-Dissolved Copper (Cu)-Dissolved 104 Silicon (Si)-Dissolved Tin (Sn)-Dissolved Vanadium (V)-Dissolved 104 WG CVS Cadmium (Cd)-Dissolved Copper (Cu)-Dissolved Silicon (Si)-Dissolved 104 Tin (Sn)-Dissolved Vanadium (V)-Dissolved WG CVS Cadmium (Cd)-Dissolved Copper (Cu)-Dissolved Silicon (Si)-Dissolved Tin (Sn)-Dissolved Vanadium (V)-Dissolved MET-T-L-MS-WP

257 Workorder: L9332 Report Date: -OCT-10 Page 13 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CCV Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total 95 Beryllium (Be)-Total 105 Bismuth (Bi)-Total Boron (B)-Total 107 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total 95 Copper (Cu)-Total Iron (Fe)-Total 93 Lead (Pb)-Total Lithium (Li)-Total 110 Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total 94 Potassium (K)-Total Rubidium (Rb)-Total 95 Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 95 Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total

258 Workorder: L9332 Report Date: -OCT-10 Page 14 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CCV Tungsten (W)-Total 94 Uranium (U)-Total 92 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 94 WG CVS Aluminum (Al)-Total Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total 106 Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 106 Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 94

259 Workorder: L9332 Report Date: -OCT-10 Page 15 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CVS Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total 95 Uranium (U)-Total 94 Vanadium (V)-Total Zinc (Zn)-Total Zirconium (Zr)-Total 94 WG CVS Aluminum (Al)-Total 105 Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total 105 Bismuth (Bi)-Total 109 Boron (B)-Total 108 Cadmium (Cd)-Total 104 Calcium (Ca)-Total Cesium (Cs)-Total 110 Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 108 Magnesium (Mg)-Total Manganese (Mn)-Total 107 Molybdenum (Mo)-Total 104 Nickel (Ni)-Total Phosphorus (P)-Total Potassium (K)-Total Rubidium (Rb)-Total 107

260 Workorder: L9332 Report Date: -OCT-10 Page 16 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG CVS Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total 104 Tellurium (Te)-Total Thallium (Tl)-Total 105 Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total 108 Zinc (Zn)-Total Zirconium (Zr)-Total 105 WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total Magnesium (Mg)-Total

261 Workorder: L9332 Report Date: -OCT-10 Page 17 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Manganese (Mn)-Total WG Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG DUP Aluminum (Al)-Total WG Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < < Cadmium (Cd)-Total < < Calcium (Ca)-Total Cesium (Cs)-Total Chromium (Cr)-Total

262 Workorder: L9332 Report Date: -OCT-10 Page 18 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG DUP Cobalt (Co)-Total WG Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total < < Lithium (Li)-Total Magnesium (Mg)-Total Manganese (Mn)-Total Molybdenum (Mo)-Total Nickel (Ni)-Total <0.00 <0.00 Phosphorus (P)-Total <0. <0. Potassium (K)-Total Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total Silver (Ag)-Total Sodium (Na)-Total Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total 26 Tin (Sn)-Total Titanium (Ti)-Total G 27 Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < < Zirconium (Zr)-Total < < WG LCS Aluminum (Al)-Total 106 Antimony (Sb)-Total 105 Arsenic (As)-Total 104 Barium (Ba)-Total Beryllium (Be)-Total 107

263 Workorder: L9332 Report Date: -OCT-10 Page 19 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG LCS Bismuth (Bi)-Total 109 Boron (B)-Total 114 Cadmium (Cd)-Total Calcium (Ca)-Total 105 Cesium (Cs)-Total 106 Chromium (Cr)-Total 105 Cobalt (Co)-Total 104 Copper (Cu)-Total Iron (Fe)-Total Lead (Pb)-Total Lithium (Li)-Total 108 Magnesium (Mg)-Total 105 Manganese (Mn)-Total 105 Molybdenum (Mo)-Total 104 Nickel (Ni)-Total Phosphorus (P)-Total 106 Potassium (K)-Total Rubidium (Rb)-Total 105 Selenium (Se)-Total Silicon (Si)-Total 115 Silver (Ag)-Total Sodium (Na)-Total 107 Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total 110 Thorium (Th)-Total Tin (Sn)-Total 104 Titanium (Ti)-Total 105 Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total 108 Zinc (Zn)-Total Zirconium (Zr)-Total WG MB

264 Workorder: L9332 Report Date: -OCT-10 Page of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG MB Aluminum (Al)-Total < Antimony (Sb)-Total Arsenic (As)-Total Barium (Ba)-Total Beryllium (Be)-Total Bismuth (Bi)-Total Boron (B)-Total < 0.01 Cadmium (Cd)-Total < Calcium (Ca)-Total < 0.1 Cesium (Cs)-Total Chromium (Cr)-Total Cobalt (Co)-Total Copper (Cu)-Total Iron (Fe)-Total < Lead (Pb)-Total < Lithium (Li)-Total < Magnesium (Mg)-Total < 0.01 Manganese (Mn)-Total < Molybdenum (Mo)-Total Nickel (Ni)-Total < Phosphorus (P)-Total < Potassium (K)-Total < Rubidium (Rb)-Total Selenium (Se)-Total Silicon (Si)-Total < 0.05 Silver (Ag)-Total Sodium (Na)-Total < Strontium (Sr)-Total Tellurium (Te)-Total Thallium (Tl)-Total Thorium (Th)-Total Tin (Sn)-Total Titanium (Ti)-Total

265 Workorder: L9332 Report Date: -OCT-10 Page 21 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF MET-T-L-MS-WP Batch WG MB Tungsten (W)-Total Uranium (U)-Total Vanadium (V)-Total Zinc (Zn)-Total < Zirconium (Zr)-Total < Batch R14763 WG CCV Cadmium (Cd)-Total Copper (Cu)-Total 104 Silicon (Si)-Total Tin (Sn)-Total Vanadium (V)-Total 104 WG CVS Cadmium (Cd)-Total Copper (Cu)-Total Silicon (Si)-Total 104 Tin (Sn)-Total Vanadium (V)-Total WG CVS Cadmium (Cd)-Total Copper (Cu)-Total Silicon (Si)-Total Tin (Sn)-Total Vanadium (V)-Total N-TOTK-WP Batch R WG CCV Total Kjeldahl Nitrogen WG CVS Total Kjeldahl Nitrogen WG DUP Total Kjeldahl Nitrogen L WG LCS Total Kjeldahl Nitrogen WG MB

266 Workorder: L9332 Report Date: -OCT-10 Page 22 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF N-TOTK-WP Batch R WG MB Total Kjeldahl Nitrogen < WG MB Total Kjeldahl Nitrogen < WG MS Total Kjeldahl Nitrogen L WG MS Total Kjeldahl Nitrogen L NH3-COL-WP Batch R WG CCV Ammonia as N 105 WG Ammonia as N DUP L WG Ammonia as N LCS WG Ammonia as N MB < 0.05 WG Ammonia as N MS L MS-B - P-TOTAL-WP Batch R WG CCV Phosphorus, Total WG CCV Phosphorus, Total 93 WG CVS Phosphorus, Total 108 WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total WG CVS Phosphorus, Total 109

267 Workorder: L9332 Report Date: -OCT-10 Page 23 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF P-TOTAL-WP Batch R WG DUP Phosphorus, Total L WG DUP Phosphorus, Total L WG MB Phosphorus, Total < 0.01 WG MS Phosphorus, Total L PH-WP Batch R WG CCV ph WG ph CVS - WG ph DUP L ph units WG ph DUP L ph units SILICATE-COL-VA Batch R WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG CRM Silicate (as SIO2) VA-SIO2-CSPK WG DUP Silicate (as SIO2) L WG DUP Silicate (as SIO2) L WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1 WG MB Silicate (as SIO2) < 1

268 Workorder: L9332 Report Date: -OCT-10 Page 24 of 27 COMMERCE DRIVE WINNIPEG MB R3P 0Y7 CLIFF SAMOILOFF SOLIDS-TDS-WP Batch R WG CVS Total Dissolved Solids WG DUP Total Dissolved Solids L WG MB Total Dissolved Solids <5.0 5 SOLIDS-TOTSUS-WP Batch R WG CVS Total Suspended Solids WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG DUP Total Suspended Solids L WG MB Total Suspended Solids <5.0 5 TURBIDITY-WP Batch R WG CCV Turbidity 105 WG Turbidity CCV 104 WG Turbidity CVS WG Turbidity CVS WG Turbidity DUP L NTU WG Turbidity LCS

269 Workorder: L9332 Report Date: -OCT-10 Page 25 of 27 Legend: Limit Confidence Interval (Laboratory Control Limits) DUP Duplicate RPD Relative Percent Difference Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description Duplicate results and limits are expressed in terms of absolute difference. MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. Relative Percent Difference Not Available due to result(s) being less than detection limit.

270 Workorder: L9332 Report Date: -OCT-10 Page 26 of 27 Hold Time Exceedances: ALS Product Description Physical Tests Turbidity ph Anions and Nutrients Anions scan (IC) Bromide Organic / Inorganic Carbon Dissolved Organic Carbon Total Organic Carbon Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: Sample ID Sampling Date Date Processed Rec. HT Actual HT :00 10:00 11:00 13:00 14:00 16:00 10:00 14:00 14:00 14:00 10:00 13:00 11:00 11:00 13:00 10:00 10:00 11:00 11:00 13:00 10:00 10:00 11:00 11:00 14:00 16:00 14:00 14:00 11:00 14:00 16:00 14:00 14:00 10:50 10:50 11:42 11:42 11:42 11:42 11:42 11:42 11:42 11:42 11:42 11:42 11:42 14:29 14:29 14:29 11:50 11:50 14:29 14:29 14:29 11:50 11:50 18-OCT-10 22:00 18-OCT-10 22:44 18-OCT-10 23:35 19-OCT-10 00:19 19-OCT-10 01:04 18-OCT-10 21:46 18-OCT-10 22:30 18-OCT-10 23:14 18-OCT-10 23:50 19-OCT-10 00: Units hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours hours Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units). Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L9332 were received on 09:10. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government days days days days days days days days days days Qualifier EHTL EHTL EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTR-FM EHTL EHTL EHTL EHTL EHTL EHTL EHTL EHTL EHTL EHTL EHT EHT EHT EHT EHT EHT EHT EHT EHT EHT

271 Workorder: L9332 Report Date: -OCT-10 Page 27 of 27 requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS. The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

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