Unique Performance for Inorganic Pigments. Enhancing The Performance of Your Products

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1 Unique Performance for Inorganic Pigments Enhancing The Performance of Your Products 1

2 SP- Pigments are surface treated with aluminosilicate (inci names: silica, alumina) to provide unique performance advantages for inorganic pigments: Surface Passivation Hydrophilicity Improved Dispersion 2

3 Surface Passivation - Yellow Iron Oxide Comparison of SP-Surface Passivated Treated Yellow Iron Oxide vs. Yellow Iron Oxide as a Function of Aging Time at 55 o C avobenzone Fe-chelation reaction was studied in the presence and in the absence of yellow oxide powders. The powders were dispersed in a solution containing 2.5% avobenzone in caprylictriglyceride (w/w). Samples were prepared by blending 7.5 g of solution, 0.4g powder and 0.06 g water. They were placed in an oven to age at 55 o C. treated treated 3 days 78 days 3

4 Hydrophilicity Yellow Iron Oxide & Titanium Dioxide SP-Surface Passivated treated powders are hydrophilic and disperse more readily in water than their non-treated counterparts The treated powders spontaneously disperse (no agitation) treated treated Spontaneous dispersion Spontaneous dispersion 4

5 Hydrophilicity - Red Iron Oxide The treated powders spontaneously disperse (no agitation) After shaking, the improved dispersion leads to a higher degree of light scattering with the same volume fraction of pigment (smaller particle size less agglomeration) treated treated Spontaneous dispersion After shaking 5

6 Improved Dispersion Black Iron Oxide The SP-Surface Passivated treated powders prefer to remain wetted and dispersed in water, whereas the nontreated powders plate-out over the substrate Water dispersion before shearing Water dispersion after shearing Treated 6

7 Improved Dispersion Black Iron Oxide The SP-Surface Passivated treated pigments do not agglomerate with carbomers allowing formulation of pigmented gels. Treated 7

8 Formulation Tinted Moisturizer Ingredient INCI Name % Water Phase A Deionized Water A Ultrez 10 Carbomer (Noveon) 0.25 B Butylene Glycol 4.00 B Methylparaben 0.20 C Tris Amino Tromethamine (Dow) 0.40 C Deionized Water 1.00 D Butylene Glycol 2.00 D Vanzan Xanthan Gum (Vanderbilt) 0.20 E Disodium EDTA 0.05 E Tween 60 Polysorbate-60 (Croda) 1.00 F Amphisol K Potassium Cetyl Phosphate (DSM) 2.00 Oil Phase G Dermol 2014 Octyldodecyl Myristate (Alzo) 9.00 G Escalol 557 Octinoxate (ISP) 4.00 G Parsol 1789 Avobenzone (DSM) 2.00 G Arlacel 60 Sorbitan Stearate (Croda) 1.00 G Alfol 16 Cetyl Alcohol (Sasol) 0.50 H Color Grind 2.00 I Glydant DMDM Hydantoin(Lonza) 0.18 I Deionized Water Color Grind: Dermol SP-4131 Iron Oxides, Silica, Alumina 0.70 SP-4206 Iron Oxides, Silica, Alumina 0.25 SP-4405 Iron Oxides, Silica, Alumina 0.05 Manufacturing Instructions: 1. Combine Part G. Heat to 75-80ºC with stirring. 2. Prepare color grind on a three roll mill. Add to Part G with stirring. 3. Sprinkle Ultrez 10 into water with slow homogenizer agitation. Heat to 55ºC. When dispersed, combine and add Part B. Combine and add Part C. Combine and add Part D. Add Part E ingredients in order. Turn off homogenizer. Add Part F. Heat to 75-80ºC with stirring for 15 minutes. Resume homogenizer agitation. 4. Add combined Parts GH to Parts A-F while homogenizing. Maintain temperature and agitation for 15 minutes. 5. Cool to 45ºC. Combine and add Part I. Cool to 30ºC. Drop batch. JCH

9 SP-4811 Titanium Dioxide SP-4206 Red Iron Oxide SP-4131 Yellow Iron Oxide SP-4405 Black Iron Oxide SP-4825 Micro Titanium Dioxide 9

10 The information contained in this document has been gathered from reference materials and /or Color Techniques Inc. test data and is to the best knowledge and belief of Color Techniques Inc., accurate and reliable. Such information is offered solely for your consideration, investigation and verification. It is not suggested or guaranteed that the hazard precautions or procedures described are the only ones which exist. Color Techniques Inc. makes no warranty, expressed or implied, with respect to the use of such information and assumes no responsibility therefore. Information on this safety data sheet is not intended to constitute a basis for product specification. 10