Anatek Labs, Inc - Spokane Spokane, WA

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1 Anatek Labs, Inc - Spokane Spokane, WA has complied with provisions set forth in Chapter WAC and is hereby recognized by the Department of Ecology as an ACCREDITED LABORATORY for the analytical parameters listed on the accompanying Scope of Accreditation. This certificate is effective November 16, 2017 and shall expire November 15, Witnessed under my hand on November 22, 2017 Rebecca Wood Acting Lab Accreditation Unit Supervisor Laboratory ID C585

2 WASHINGTON STATE DEPARTMENT OF ECOLOGY ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM SCOPE OF ACCREDITATION Anatek Labs, Inc - Spokane Spokane, WA is accredited for the analytes listed below using the methods indicated. Full accreditation is granted unless stated otherwise in a note. EPA is the U.S. Environmental Protection Agency. SM is "Standard Methods for the Examination of Water and Wastewater." SM refers to EPA approved method versions. ASTM is the American Society for Testing and Materials. USGS is the U.S. Geological Survey. AOAC is the Association of Official Analytical Chemists. Other references are described in notes. Drinking Water Turbidity EPA 180.1_2_1993 Chloride Fluoride Nitrate Nitrate + Nitrite Nitrite Sulfate Cyanide, Total EPA 335.4_1_1993 Total Organic Carbon EPA 415.3_2005 Color SM 2120 B-2011 Alkalinity SM 2320 B-2011 Hardness (calc.) SM 2340 B-2011 Hardness, Total (as CaCO3) SM 2340 C-2011 Specific Conductance SM 2510 B-2011 Solids, Total Dissolved SM 2540 C-2011 Cyanide, Total SM 4500-CN E-2011 ph SM 4500-H+ B-2011 Orthophosphate SM 4500-P F-2011 Total Organic Carbon SM 5310 C-2011 Aluminum Antimony Arsenic Page 1 of 11

3 Barium Beryllium Cadmium Chromium Copper Lead Manganese Mercury Nickel Selenium Silver Thallium Total Uranium Zinc 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dichlorobenzene 1,2-Dichloroethane (Ethylene dichloride) 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (Methyl ethyl ketone, MEK) 2-Chlorotoluene 2-Hexanone Page 2 of 11

4 4-Chlorotoluene 4-Isopropyltoluene (p-cymene) 4-Methyl-2-pentanone (MIBK) Acetone Acrolein (Propenal) Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane (Ethyl chloride) Chloroform cis-1,2-dichloroethylene cis-1,3-dichloropropene Dibromomethane Dichlorodifluoromethane (Freon-12) Dichloromethane (DCM, Methylene chloride) Ethylbenzene Hexachlorobutadiene Isopropylbenzene Methyl bromide (Bromomethane) Methyl chloride (Chloromethane) Methyl tert-butyl ether (MTBE) m-xylene Naphthalene n-butylbenzene n-propylbenzene o-xylene p-xylene sec-butylbenzene Styrene Page 3 of 11

5 tert-butylbenzene Tetrachloroethylene (Perchloroethylene) Toluene Total Trihalomethanes trans-1,2-dichloroethylene trans-1,3-dichloropropylene trans-1,4-dichloro-2-butene Trichloroethene (Trichloroethylene) Trichlorofluoromethane (Freon 11) Vinyl chloride Xylene (total) Gross Alpha EPA Gross Beta EPA Radium-226 EPA Heterotrophic Bacteria Heterotrophic Bacteria Total & Fecal Coli - detect Simplate SM 9215 B (PCA) SM 9221 B (LTB) + E1 (EC) Fecal coliform-count SM 9222 D (mfc) Total Coli/Ecoli - count Total Coli/Ecoli - detect Non-Potable Water Turbidity Chloride Fluoride Nitrate Nitrate + Nitrite Nitrite Sulfate Cyanide, Total Chemical Oxygen Demand (COD) Total Organic Carbon Total Organic Halides (TOX) SM 9223 B (Colilert QTray) SM 9223 B Colilert EPA 180.1_2_1993 EPA 335.4_1_1993 EPA 410.4_2_1993 EPA 415.3_2005 EPA 9020B_2_1994 Alkalinity SM 2320 B-2011 Hardness, Total (as CaCO3) SM 2340 C Page 4 of 11

6 Specific Conductance SM 2510 B-2011 Solids, Total Dissolved SM 2540 C-2011 Solids, Total Suspended SM 2540 D-2011 Solids, Total, Fixed and Volatile SM 2540 E Cyanide, Total SM 4500-CN E-2011 ph SM 4500-H+ B-2011 Ammonia SM 4500-NH3 H-2011 Nitrate + Nitrite SM 4500-NO3 F-2011 Nitrogen, Total Kjeldahl SM 4500-Norg C-2011 Orthophosphate SM 4500-P G-2011 Phosphorus, Total SM 4500-P H-2011 Biochemical Oxygen Demand (BOD) SM 5210 B-2011 Dissolved Organic Carbon SM 5310 C-2011 Total Organic Carbon SM 5310 C-2011 Aluminum 1 Antimony 1 Arsenic 1 Barium 1 Beryllium 1 Cadmium 1 Calcium Chromium 1 Cobalt 1 Copper 1 Iron Lead 1 Magnesium Manganese 1 Molybdenum 1 Nickel 1 Potassium Selenium 1 Silver 1 Sodium Thallium 1 Total Uranium 1 Page 5 of 11

7 Vanadium 1 Zinc 1 1,1,1,2-Tetrachloroethane EPA 624 1,1,1-Trichloroethane EPA 624 1,1,2,2-Tetrachloroethane EPA 624 1,1,2-Trichloroethane EPA 624 1,1-Dichloroethane EPA 624 1,1-Dichloroethylene EPA 624 1,2,3-Trichlorobenzene EPA 624 1,2,4-Trichlorobenzene EPA 624 1,2-Dibromoethane (EDB, Ethylene dibromide) EPA 624 1,2-Dichlorobenzene EPA 624 1,2-Dichloroethane (Ethylene dichloride) EPA 624 1,2-Dichloropropane EPA 624 1,3-Dichlorobenzene EPA 624 1,4-Dichlorobenzene EPA Butanone (Methyl ethyl ketone, MEK) EPA Chloroethyl vinyl ether EPA Isopropyltoluene (p-cymene) EPA 624 Acetone EPA 624 Acrolein (Propenal) EPA 624 Acrylonitrile EPA 624 Benzene EPA 624 Bromodichloromethane EPA 624 Bromoform EPA 624 Carbon tetrachloride EPA 624 Chlorobenzene EPA 624 Chlorodibromomethane EPA 624 Chloroethane (Ethyl chloride) EPA 624 Chloroform EPA 624 cis-1,3-dichloropropene EPA 624 Dibromochloropropane EPA 624 Dichlorodifluoromethane (Freon-12) EPA 624 Dichloromethane (DCM, Methylene chloride) EPA 624 Ethylbenzene EPA 624 Methyl bromide (Bromomethane) EPA 624 Page 6 of 11

8 Methyl chloride (Chloromethane) EPA 624 Methyl tert-butyl ether (MTBE) EPA 624 Methylene chloride (Dichloromethane) EPA 624 Naphthalene EPA 624 Styrene EPA 624 Tetrachloroethylene (Perchloroethylene) EPA 624 Toluene EPA 624 trans-1,2-dichloroethylene EPA 624 trans-1,3-dichloropropylene EPA 624 Trichloroethene (Trichloroethylene) EPA 624 Trichlorofluoromethane (Freon 11) EPA 624 Vinyl chloride EPA 624 Heterotrophic Bacteria Heterotrophic Bacteria Total Coli/Ecoli - count Fecal coliform-count Simplate SM 9215 B (PCA) SM 9221 B (LTB) + F (EC Mug) + C SM 9221 E2 (A1) + C MPN Fecal coliform-count SM 9222 D (mfc) Salmonella SM 9260 D 4 Solid and Chemical Materials Chloride Fluoride Nitrate Nitrite Sulfate Cyanide, Total EPA 335.4_1_ Total Organic Halides (TOX) EPA 9020B_2_1994 Extractable Organic Halides EPA ph EPA 9045D_2002 Chloride EPA 9076 Cyanide, Total SM 4500-CN E Ammonia SM 4500-NH3 H-2011 Nitrate + Nitrite SM 4500-NO3 F-2011 Nitrogen, Total Kjeldahl SM 4500-Norg C-2011 Orthophosphate SM 4500-P F-2011 Page 7 of 11

9 Aluminum EPA 6020A_(2/07) 1 Antimony EPA 6020A_(2/07) 1 Arsenic EPA 6020A_(2/07) 1 Barium EPA 6020A_(2/07) 1 Beryllium EPA 6020A_(2/07) 1 Boron EPA 6020A_(2/07) Cadmium EPA 6020A_(2/07) 1 Calcium EPA 6020A_(2/07) 1 Chromium EPA 6020A_(2/07) 1 Cobalt EPA 6020A_(2/07) 1,2 Copper EPA 6020A_(2/07) 1 Iron EPA 6020A_(2/07) Lead EPA 6020A_(2/07) 1 Magnesium EPA 6020A_(2/07) 1 Manganese EPA 6020A_(2/07) 1 Mercury EPA 6020A_(2/07) 1 Molybdenum EPA 6020A_(2/07) 1 Nickel EPA 6020A_(2/07) 1 Potassium EPA 6020A_(2/07) 1 Selenium EPA 6020A_(2/07) 1 Silver EPA 6020A_(2/07) 1 Sodium EPA 6020A_(2/07) 1 Strontium EPA 6020A_(2/07) Thallium EPA 6020A_(2/07) 1 Tin EPA 6020A_(2/07) Titanium EPA 6020A_(2/07) Total Uranium EPA 6020A_(2/07) 1 Vanadium EPA 6020A_(2/07) 1 Zinc EPA 6020A_(2/07) 1 Benzene EPA 8021B_2_(12/96) Ethylbenzene EPA 8021B_2_(12/96) m+p-xylene EPA 8021B_2_(12/96) o-xylene EPA 8021B_2_(12/96) Toluene EPA 8021B_2_(12/96) Xylene (total) EPA 8021B_2_(12/96) Aroclor-1016 (PCB-1016) Page 8 of 11

10 Aroclor-1221 (PCB-1221) Aroclor-1232 (PCB-1232) Aroclor-1242 (PCB-1242) Aroclor-1248 (PCB-1248) Aroclor-1254 (PCB-1254) Aroclor-1260 (PCB-1260) Diesel range organics (DRO) Gasoline range organics (GRO) 1,1,1,2-Tetrachloroethane 1,1,1-Trichloro-2,2,2-trifluoroethane 1,1,1-Trichloro-2-propanone 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichlorofluoroethane 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,3-Trimethylbenzene 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-chloropropane (DBCP) 1,2-Dibromoethane (EDB, Ethylene dibromide) 1,2-Dichlorobenzene 1,2-Dichloroethane (Ethylene dichloride) 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,3-Dichloropropene 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (Methyl ethyl ketone, MEK) WDOE NWTPH- Dx_(1997) WDOE NWTPH- Gx_(1997) Page 9 of 11

11 2-Chloroethyl vinyl ether 2-Chlorotoluene 2-Hexanone 2-Hexene 4-Bromofluorobenzene 4-Chlorotoluene 4-Isopropyltoluene (p-cymene) 4-Methyl-2-pentanone (MIBK) Acetone Acrolein (Propenal) Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoethane (Ethyl Bromide) Bromoethene Bromoform Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane (Ethyl chloride) Chloroform cis & trans-1,2-dichloroethene cis-1,2-dichloroethylene cis-1,3-dichloropropene Dibromomethane Ethylbenzene Hexachlorobutadiene Iodomethane (Methyl iodide) Isopropylbenzene m+p-xylene Methyl bromide (Bromomethane) Methyl chloride (Chloromethane) Methyl tert-butyl ether (MTBE) Page 10 of 11

12 Methylene chloride (Dichloromethane) m-xylene Naphthalene n-butylbenzene n-propylbenzene o-xylene p-xylene sec-butylbenzene Styrene tert-butylbenzene Tetrachloroethylene (Perchloroethylene) Toluene trans-1,2-dichloroethylene trans-1,3-dichloropropylene trans-1,4-dichloro-2-butene Trichloroethene (Trichloroethylene) Trichlorofluoromethane (Freon 11) Vinyl acetate Vinyl chloride Xylene (total) Fecal coliform-count EPA 1680 (MTF) - 04/10 Salmonella EPA 1682 (MSRV) - 07/06 Fecal coliform-count SM 9221 E2 (A1) + C MPN Accredited Parameter Note Detail 1) Accreditation based in part on recognition of Florida NELAP accreditation. 2) Provisional accreditation pending acceptable PT completion.(3) Accreditation is for Fixed Dissolved Solids only. (4) Method no longer approved for compliance testing. 11/22/2017 Authentication Signature Rebecca Wood, Acting Lab Accreditation Unit Supervisor Date Page 11 of 11