TITLE 252. DEPARTMENT OF ENVIRONMENTAL QUALITY CHAPTER 305. LABORATORY SERVICES. 252: Purpose :

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1 Codification through the 2008 legislative session. Section 1-11; Appendices A & B: Board adoption - February 29, 2008 Gubernatorial approval - April 23, 2008 Legislative approval and final adoption - May 2, 2008 Effective date - July 11, 2008 TITLE 252. DEPARTMENT OF ENVIRONMENTAL QUALITY CHAPTER 305. LABORATORY SERVICES Subchapter Section 252: Purpose : Appendix A. Samples Submitted by Government Entities Appendix B. Samples Submitted by Private Citizens 1

2 Subchapter 1. Purpose Section 252: Purpose 252: Basis and authority 252: Applicability 252: Terms 252: Severability 252: Definitions 252: Laboratory services 252: Quality assurance/quality control 252: Governmental sample analyses [REVOKED] 252: Private citizen sample analyses [REVOKED] 252: Required fees and other pricing Appendix A. Appendix B. Samples Submitted by Government Entities Samples Submitted by Private Citizens 252: Purpose The rules in this Chapter implement the Oklahoma Environmental Quality Code (27: et seq.) and provide procedures and fees for laboratory services offered by the State Environmental Laboratory of the Department of Environmental Quality. 252: Basis and authority OAC 252:305 was promulgated and adopted pursuant to the Oklahoma Environmental Quality Code, O.S.Supp. 1993, Sections and : Applicability This Chapter applies to Department of Environmental Quality's State Environmental Laboratory and the analytical services it provides. 252: Terms Terms used in this Chapter shall have the meanings given to them in OAC 252: or the Oklahoma Environmental Quality Code. Any technical term not defined thereby shall be defined by: (1) its generally accepted scientific meaning, or (2) its standard dictionary meaning. 252: Severability The provisions of this Chapter are severable, and if any part or provision hereof shall be held void, the decision of the court in so holding shall not affect or impair any of the remaining parts or provisions of this Chapter. 252: Definitions The following words or terms, when used in this Chapter, shall have the following meaning, unless the context clearly indicates otherwise. "Department" means the Oklahoma Department of Environmental Quality. "State Environmental Laboratory" means the environmental laboratory under the jurisdiction of, and operated by, the Department of Environmental Quality. 252: Laboratory services (a) Types. The types of services available from the State Environmental Laboratory include analyses relating to asbestos, gas chromatography/ mass spectrometry, general chemistry, metals 2

3 chemistry, microbiology, organic chemistry and radiochemistry. (b) For department. The State Environmental Laboratory shall provide such services and perform laboratory analyses as is necessary to implement and enforce the programs and functions under the jurisdiction of the Department. Analytical services available to the Department include, but are not limited to, the analysis of samples for the purpose of: (1) assisting with studies and investigations of pollution or suspected pollution; (2) providing factual data to support any order, permit, function or program of the Department; (3) providing accurate information on water and wastewater; and (4) evaluating compliance data from treatment systems, disposal systems, discharges, and other facilities, sites and activities. (c) For others. In addition to supporting the work of the Department, the State Environmental Laboratory shall provide analytical services upon request to individuals (private citizens requesting assistance in evaluating their individual water wells or suspected pollution of their property) according to 252: , cities, towns, counties, state institutions and other state and federal agencies according to 252: [See 27A: ] (d) Exceptions. The State Environmental Laboratory shall not provide analytical services to entities required to perform monitoring in response to permits or rules of the Department or other state environmental agency permits or rules except that analytical services will be provided to public water supply systems. 252: Quality assurance/quality control The State Environmental Laboratory shall maintain a written quality assurance plan and implement it into a quality assurance/quality control (QA/QC) program to ensure that all routinely generated data are scientifically valid and defensible and are of known and acceptable precision and accuracy. 252: Governmental sample analyses [REVOKED] 252: Private citizen sample analyses [REVOKED] 252: Required fees and other pricing (a) Fees. Fees established for samples submitted by governmental entities are listed in Appendix A. Fees established for samples submitted by private citizens are listed in Appendix B. (b) Discount. The State Environmental Lab may discount certain analytical work for customers who provide a large volume of prescheduled samples. Discounts will be determined by the Director of Customer Services taking into account cost savings to the agency. (c) Other analysis. The State Environmental lab will consider performing other types of analyses upon special request. The fees for these tests will be based upon method development costs, actual analytical costs and a $2.00 per sample charge for processing of invoices and payments. (d) Supply and consumables charges. Unless otherwise specified by the Director of Customer Services, the analytical fees reflected in these rules include sample containers, sample digestion/extraction and any other consumables necessary to perform the requested analytical work. (e) Other charges. The State Environmental Lab will consider accommodating extraordinary requests with respect to data handling, quality assurance, sample handling or reporting. The fees for these extraordinary requests will be based upon administrative costs, actual personnel costs and any associated development costs. (f) Annual Fee Adjustment. To assist in meeting rising costs to the DEQ of the environmental services associated with the laboratory services program, the fees set out in this Section and Appendices A and B shall be automatically adjusted on July 1st every year to correspond to the percentage, if any, by which the Consumer Price Index (CPI) for the most recent calendar year exceeds the CPI for the previous calendar year. The DEQ may round the adjusted fees up to the nearest dollar. The DEQ may waive collection of an automatic increase in a given year if it determines other revenues, including appropriated state general revenue funds, have increased sufficiently to make the funds generated by the automatic adjustment unnecessary in that year. A 3

4 waiver does not affect future automatic adjustments. (1) Any automatic fee adjustment under this subsection may be averted or eliminated, or the adjustment percentage may be modified, by rule promulgated pursuant to the Oklahoma Administrative Procedures Act. The rulemaking process may be initiated in any manner provided by law, including a petition for rulemaking pursuant to 75 O.S. 305 and OAC 252:4-5-3 by any person affected by the automatic fee adjustment. (2) If the United States Department of Labor ceases to publish the CPI or revises the methodology or base years, no further automatic fee adjustments shall occur until a new automatic fee adjustment rule is promulgated pursuant to the Oklahoma Administrative Procedures Act. (3) For purposes of this subsection, Consumer Price Index or CPI means the Consumer Price Index - All Urban Consumers (U.S. All Items, Current Series, =100, CUUR0000SA0) published by the United States Department of Labor. The CPI for a calendar year is the figure denoted by the Department of Labor as the Annual index figure for that calendar year. 4

5 Appendix A. Samples Submitted by Government Entities METHOD ANALYTE MATRIX FEE GAS CHROMATOGRAPHY/MASS SPECTRA EPA VOLATILE ORGANICS IN DRINKING WATER-VOC LIQUID $ EPA VOLATILE ORGANICS IN DRINKING WATER-THM LIQUID $ EPA 8260M VOLATILE ORGANICS SOLID $ EPA 8260M VOLATILE ORGANICS LIQUID $ EPA 8270M SEMIVOLATILE ORGANICS SOLID $ EPA 8270M SEMIVOLATILE ORGANICS LIQUID $ GENERAL CHEMISTRY SM 2320 ALKALINITY, BICARBONATE LIQUID $16.00 SM 2320 ALKALINITY, CARBONATE LIQUID $16.00 EPA ALKALINITY, TOTAL LIQUID $16.00 EPA BROMATE LIQUID $64.00 EPA BROMIDE LIQUID $32.00 SM 5310 C CARBON, TOTAL DISSOLVED LIQUID $48.00 SM 5910 B CARBON, TOTAL DISSOLVED W/UV-254 (SUVA) LIQUID $69.00 SM 5310 C CARBON, TOTAL ORGANIC LIQUID $42.00 SM H2 CHLOROPHYLL A / PHEOPHYTIN EXTRACT $10.00 SM H2 CHLOROPHYLL A / PHEOPHYTIN, (FILTER & EXTRACTION ONLY) LIQUID $23.00 SM HM CHLOROPHYLL A IN PERIPHYTIN (ETHANOL) EXTRACT $13.00 EPA CHLORATE LIQUID $64.00 EPA CHLORIDE LIQUID $21.00 EPA M CHLORIDE SOLID $30.00 SM 4500 Cl CHLORINE, TOTAL LIQUID $8.00 SM 4500 Cl CHLORINE, TOTAL RESIDUAL LIQUID $8.00 EPA CHLORITE LIQUID $64.00 EPA COLOR, APPARENT LIQUID $11.00 EPA COLOR, TRUE LIQUID $14.00 EPA CYANIDE LIQUID $64.00 EPA M CYANIDE SOLID $64.00 SM 5210 B DEMAND, BIOCHEMICAL OXYGEN-5 DAY LIQUID $42.00 SM 5210 B DEMAND, BIOCHEMICAL OXYGEN-20 DAY LIQUID $60.00 EPA DEMAND, CARBONACEOUS BIOCHEMICAL OXYGEN-5 DAY LIQUID $42.00 EPA DEMAND, CARBONACEOUS BIOCHEMICAL OXYGEN-20 DAY LIQUID $60.00 EPA DEMAND, OXYGEN CHEMICAL LIQUID $33.00 EPA M DEMAND, OXYGEN CHEMICAL SOLID $38.00 FILTRATION CENTRIFICATION (SAMPLE PREPARATION) LIQUID $8.00 EPA FLUORIDE LIQUID $24.00 SM 4500 FC FLUORIDE by ISE/FIA LIQUID $23.00 EPA HARDNESS, CALCIUM LIQUID $16.00 EPA HARDNESS, TOTAL LIQUID $16.00 EPA NITROGEN, AMMONIA LIQUID $24.00 EPA NITROGEN, AMMONIA SOLID $27.00 EPA NITROGEN, KJELDAHL LIQUID $27.00 EPA NITROGEN, KJELDAHL SOLID $

6 EPA NITROGEN, NITRATE LIQUID $24.00 EPA NITROGEN, NITRATE/NITRITE LIQUID $24.00 EPA NITROGEN, NITRITE LIQUID $24.00 CALCULATE D NITROGEN, ORGANIC LIQUID $5.00 CALCULATE D NITROGEN, TOTAL LIQUID $5.00 EPA 1664 OIL & GREASE LIQUID $64.00 EPA 1664 M OIL & GREASE SOLID $80.00 SM4500 O OXYGEN, DISSOLVED LIQUID $8.00 EPA ph LIQUID $11.00 EPA 9045 ph SOLID $11.00 EPA PHOSPHORUS, ORTHO LIQUID $16.00 EPA PHOSPHORUS, TOTAL LIQUID $31.00 MEHLICH 3 PHOSPHORUS, TOTAL EXTRACTABLE SOLID $46.00 SM 2540 F SOLIDS, SETTLEABLE LIQUID $13.00 SM 2540 D SOLIDS, TOTAL SUSPENDED LIQUID $31.00 EPA SOLIDS, TOTAL LIQUID $25.00 SM 2540 C SOLIDS, TOTAL DISSOLVED LIQUID $31.00 EPA SOLIDS, TOTAL VOLATILE LIQUID $32.00 EPA SOLIDS, VOLATILE SUSPENDED LIQUID $32.00 EPA SPECIFIC CONDUCTANCE LIQUID $11.00 EPA SULFATE LIQUID $16.00 EPA TURBIDITY LIQUID $16.00 METALS EPA ALUMINUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 ALUMINUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA ALUMINUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 ALUMINUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA ANTIMONY, TOTAL BY ICP LIQUID $21.00 EPA 6010 ANTIMONY, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA ANTIMONY, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 ANTIMONY, TOTAL BY ICP (Digestion: EPA 3051) SOLID $21.00 EPA 6200 ANTIMONY, TOTAL BY XRF SOLID $12.00 EPA ARSENIC, TOTAL BY ICP LIQUID $21.00 EPA 6010 ARSENIC, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA ARSENIC, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 ARSENIC, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6020 ARSENIC, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6010 ARSENIC, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 ARSENIC, TOTAL BY XRF SOLID $12.00 EPA ARSENIC, TOTAL BY ICP-MS FISH $80.00 EPA BARIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 BARIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA BARIUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 BARIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6010 BARIUM, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6020 BARIUM, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 BARIUM, TOTAL BY XRF SOLID $12.00 EPA BERYLLIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 BERYLLIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA BERYLLIUM, TOTAL BY ICP-MS LIQUID $

7 EPA 6010 BERYLLIUM, TOTAL BY ICP SOLID $21.00 EPA 6010 BORON, TOTAL (Digestion: EPA 3051) LIQUID $27.00 EPA 6010 BORON, TOTAL (Digestion: EPA 3051) SOLID $27.00 EPA CADMIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 CADMIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA CADMIUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 CADMIUM, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6010 CADMIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 CADMIUM, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 CADMIUM, TOTAL BY XRF SOLID $12.00 EPA CADMIUM, TOTAL BY ICP-MS FISH $80.00 EPA CALCIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 CALCIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA 6010 CALCIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $21.00 EPA 6200 CALCIUM, TOTAL BY XRF SOLID $21.00 EPA CHROMIUM, TOTAL BY ICP (Digestion: EPA 3050) LIQUID $21.00 EPA 6010 CHROMIUM, TOATAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA CHROMIUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 CHROMIUM, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6010 CHROMIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 CHROMIUM, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 CHROMIUM, TOTAL BY XRF SOLID $12.00 EPA COLBALT, TOTAL BY ICP LIQUID $21.00 EPA 6010 COBALT, TOTAL BY ICP LIQUID $27.00 EPA COBALT, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 COBALT, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 COBALT, TOTAL BY XRF SOLID $12.00 EPA COPPER, TOTAL BY ICP LIQUID $21.00 EPA 6010 COPPER, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA COPPER, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 COPPER, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 COPPER, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 COPPER, TOTAL BY XRF SOLID $12.00 EPA IRON, TOTAL BY ICP LIQUID $21.00 EPA 6010 IRON, TOTAL BY ICP SOLID $21.00 EPA 6200 IRON, TOTAL BY XRF SOLID $12.00 EPA LEAD, TOTAL BY ICP LIQUID $21.00 EPA 6010 LEAD, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA LEAD, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 LEAD, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6010 LEAD, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 LEAD, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 LEAD, TOTAL BY XRF SOLID $12.00 EPA LEAD, TOTAL BY ICP-MS FISH $80.00 EPA MAGNESIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 MAGNESIUM, TOATL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA 6010 MAGNESIUM, TOTAL BY ICP SOLID $21.00 EPA MANGANESE, TOTAL BY ICP LIQUID $21.00 EPA 6010 MANGANESE, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA MANGANESE, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 MANGANESE, TOTAL BY ICP (Digestion: EPA 3050) SOLID $

8 EPA 6010 MANGANESE, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 MANGANESE, TOTAL BY XRF SOLID $12.00 EPA 245.1/7470 MERCURY, TOTAL LIQUID $69.00 EPA 7470/7471 MERCURY, TOTAL SOLID $84.00 EPA 6200 MERCURY BY XRF SOLID $12.00 EPA MERCURY, TOTAL FISH $84.00 EPA 7473 MERCURY, TOTAL (DIRECT ANALYSIS) FISH $42.00 EPA MOLYBDENUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 MOLYBDNUM BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA MOLYBDENUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 MOLYBDENUM, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6010 MOLYBDENUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 MOLYDNENUM, TOTAL BY XRF SOLID $12.00 EPA NICKEL, TOTAL BY ICP LIQUID $21.00 EPA 6010 NICKEL, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA NICKEL, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 NICKEL, TOTAL BY ICP (Digestion: EPA 3050) SOLID $21.00 EPA 6010 NICKEL, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 NICKEL, TOTAL BY XRF SOLID $12.00 EPA POTASSIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 POTASSIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA 6010 POTASSIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 POTASSIUM, TOTAL BY XRF SOLID $12.00 EPA SELENIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 SELENIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA SELENIUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 SELENIUM, TOTAL BY ICP SOLID $21.00 EPA 6010 SELENIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 SELENIUM, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 SELENIUM, TOTAL BY XRF SOLID $12.00 EPA SILVER, TOTAL BY ICP LIQUID $21.00 EPA 6010 SILVER, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA SILVER, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 SILVER, TOTAL BY ICP SOLID $21.00 EPA 6010 SILVER, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 SILVER, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 SILVER, TOTAL BY XRF SOLID $12.00 EPA SODIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 SODIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA 6010 SODIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA THALLIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 THALLIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA THALLIUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 THALLIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 THALLIUM, TOTAL BY XRF SOLID $12.00 EPA TIN, TOTAL BY ICP LIQUID $21.00 EPA 6010 TIN, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 TIN, TOTAL BY XRF SOLID $12.00 EPA 1311 TOXIC CHARACTERISTIC LEACHING PROCEDURE (TCLP) (METALS ONLY) $ EPA URANIUM, TOTAL BY ICP-MS LIQUID $

9 EPA 6200 URANIUM, TOTAL BY XRF SOLID $12.00 EPA VANADIUM, TOTAL BY ICP LIQUID $21.00 EPA 6010 VANADIUM, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA VANADIUM, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 VANADIUM, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6200 VANADIUM, TOTAL BY XRF SOLID $12.00 EPA ZINC, TOTAL BY ICP LIQUID $21.00 EPA 6010 ZINC, TOTAL BY ICP (Digestion: EPA 3051) LIQUID $27.00 EPA ZINC, TOTAL BY ICP-MS LIQUID $21.00 EPA 6010 ZINC, TOTAL BY ICP SOLID $21.00 EPA 6010 ZINC, TOTAL BY ICP (Digestion: EPA 3051) SOLID $27.00 EPA 6020 ZINC, TOTAL BY ICP-MS (Digestion: EPA 3050) SOLID $21.00 EPA 6200 ZINC, TOTAL BY XRF SOLID $12.00 EPA ZINC, TOTAL BY ICP-MS FISH $80.00 CLP 05.3 SOLIDS, PERCENT SOLID $21.00 M ICROBIOLOGY SM 9223 COLIFORM, TOTAL & E. COLI, MOST PROBABLE NUMBER (MPN)/QUANTI-TRAY LIQUID $21.00 SM 9223 COLIFORM, TOTAL AND E. COLI, PRESENCE/ABSENCE (PA) LIQUID $21.00 SM 9222B TOTAL & FECAL COLIFORMS (MF) (W/ECHERCHIA COLI BROTH CONFIMRATION) LIQUID $25.00 SM 9260 ENTERIC PATHOGEN (SALMONELLA, SHIGELLA, ETC.) (QUALITATIVE) LIQUID $80.00 SM 9230C FECAL STREPTOCOCCI-MF LIQUID $21.00 SM 9222D FECAL COLIFORM-MF LIQUID $21.00 EPA 1600 ENTEROCOCCI SCREEN (BY SPECIAL REQUEST) LIQUID $28.00 EPA 1600 ENTEROCOCCI CONFIRM (BY SPECIAL REQUEST) LIQUID $69.00 ASTM D6503 ENTEROCOCCI SCREEN LIQUID $27.00 HACH IRON AND SULFUR BACTRIA (P/A) LIQUID $37.00 SM 9215B STANDARD PLATE COUNT (HETEROTROHIC PLATE COUNT) LIQUID $32.00 SWTR SIM PLATE COUNT (HPC) LIQUID $27.00 SM 8050B MICROTOX LIQUID $ ORGANIC CHEM ISTRY EPA ETHYLENE DIBROMIDE (EDB) IN DRINKING WATER LIQUID $ EPA 547 GLYPHOSATE IN DRINKING WATER LIQUID $ EPA HALOACETIC ACIDS/DALAPON IN WATER LIQUID $ EPA 608 PCB IN WASTEWATER LIQUID $ EPA 8082 PCB IN SEDIMENT SOLID $ EPA 507 NITROGEN-PHOSPHOROUS PESTICIDES IN DRINKING WATER LIQUID $ EPA 614 NITROGEN-PHOSPHOROUS PESTICIDES IN WASTEWATERS LIQUID $ EPA 8141 NITROGEN-PHOSPHORUS PESTICIDES IN SOLIDS & WASTES SOLIDS $ EPA 508 CHLORINATED PESTICIDES IN DRINKING WATER LIQUID $ EPA 608 ORGANOCHLORINATED PESTICIDES IN WASTEWATER LIQUID $ EPA 8081 CHLORINATED PESTICIDES IN SEDIMENT SOLID $ EPA HERBICIDES IN DRINKING WATER & WASTEWATER LIQUID $ EPA 8151 HERBICIDES IN WATER, WASTE LIQUID SOLID $ SEL SOP 125 PERCENT MOISTURE IN SEDIMENT SOLID $21.00 FDA 303E4C1 FISH TISSUE SAMPLE (FILET) PREPARATION ONLY FISH $

10 FDA 303E4C1 FDA 303E4C1 FISH TISSUE SAMPLE (WHOLE EVISCERATED) PREPARATION ONLY FISH TISSUE SAMPLE (WHOLE UNEVISCERATED) PREPARATION ONLY FISH $ FISH $ DEQ PESTICIDE SCAN IN FISH FISH $ EPA 1020 FLASH POINT LIQUID $27.00 TX 1005 M OK 8020/8015 TOTAL PETROLEUM HYDROCARBONS (TPH) GASOLINE RANGE ORGANIC CONSTITUENTS INCLUDING BTEX (OKLA-GRO) LIQUID SOLID $74.00 LIQUID $74.00 DEQ POLYCHLORINATE BIPHENYL (PCB) IN OIL LIQUID $ RADIOCHEM ISTRY EPA GROSS ALPHA/BETA LIQUID $90.00 EPA GROSS ALPHA LIQUID $80.00 EPA GROSS BETA LIQUID $80.00 DEQ1 GROSS ALPHA/BETA IN SWIPE $53.00 EPA RADIUM 226 LIQUID $69.00 EPA RADIUM 228 LIQUID $ EPA URANIUM LIQUID $27.00 EPA 520/ RADON AIR AIR $

11 Appendix B. Samples Submitted by Private Citizens METHOD ANALYTE MATRIX FEE PRIVATE CITIZEN SAM PLES SM 9223 COLIFORM, TOTAL AND E COLI, PRESENCE/ABSENCE (PA) ROUTINE CHEMICAL (INCLUDES ALKALINITY, CHLORIDE, NITRATE/NITRITE, SPECIFIC CONDUCTANCE, ph, SULFATE, TOTAL DISSOLVED SOLIDS, TOTAL HARNDESS LIQUID $21.00 LIQUID $ EPA LEAD LIQUID $21.00 EPA FLUORIDE LIQUID $24.00 EPA NITRATE/NITRITE LIQUID $24.00 EPA CHLORIDE LIQUID $21.00 EPA 507 NITROGEN-PHOSPHORUS PESTICIDE IN DRINKING WATER LIQUID $ EPA 508 CHLORINATED PESTICIDE IN DRINKING WATER LIQUID $ EPA 520/ RADON CANISTERS AIR $