July 1, 2014 LELAP Lab ID # AI No Accreditation Year FY 2015 Renewal due FY 2016

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1 July 1, 2014 LELAP Lab ID # AI No Accreditation Year FY 2015 Renewal due FY 2016 Mr. Jake Fahlenkamp 1600 W Tacoma Broken Arrow, Oklahoma Re: Scope of Accreditation Dear Mr. Fahlenkamp: The Louisiana Department of Environmental Quality s laboratory accreditation program, in accordance with Louisiana Administrative Code, Title 33, Part I, Subpart 3, Laboratory Accreditation, accredits this laboratory for Fiscal Year This accreditation does not constitute an endorsement of the suitability of the listed methods for any specific purpose. The laboratory is accredited for the method as identified on the application for accreditation; if the method is partially identified on the application for accreditation, the laboratory is accredited for the versions listed on the current application or referenced in the laboratory standard operating procedure. National Environmental Laboratory Accreditation Program (NELAP) accreditation is granted only for those methods/analytes for which NELAP is indicated as the type of accreditation. STATE is indicated as the type of accreditation for those methods/analytes for which accreditation by the Louisiana Environmental Laboratory Accreditation Program (LELAP) is granted. Accreditation is dependent on the laboratory s successful ongoing compliance with regulations as outlined in the Louisiana Administrative Code, Title 33, Part I, Subpart 3, Laboratory Accreditation, and with the standards adopted by the NELAP Accreditation Council. The accreditation certificate is the property of the State of Louisiana. Should your accreditation be suspended or revoked, your laboratory must return the certificate of accreditation to the department and delete any electronic copies until your accreditation status is restored. LAC 33:I.5313.A and/or NELAC require that the laboratory report include all relevant information. Therefore, the certificate number shall be placed in the upper right corner of all laboratory reports. If the test report includes results of any test for which the laboratory is not accredited, the unaccredited results must be clearly identified as such. Post Office Box 4313 Baton Rouge, Louisiana Phone Fax

2 Mr. Jake Fahlenkamp July 1, 2014 Page 2 of 2 We request that you examine the scope of accreditation attachment for accuracy and completeness. If you find that an analyte for which you expected to be accredited is not listed, please examine your records to ensure that: 1. You have met the requirements for successful participation in proficiency test studies as outlined in LAC 33:I.4711 and in the NELAC Standard In the case of accreditation by recognition, the requested analyte must be listed for the requested method and matrix on both the certificate issued by the Primary Accreditation Body and on the Louisiana application form. If after reviewing this information, the scope and/or certificate are inaccurate, please notify us immediately. If you have any questions, please contact your assigned assessor Elizabeth West, Environmental Scientist at (318) Sincerely, Lourdes Iturralde Administrator Notifications and Accreditations Section OES, Public Participation & Permit Support Services Division LI:PB:ew

3 STATE OF LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY Is hereby granting a Louisiana Environmental Laboratory Accreditation to 1600 W Tacoma Broken Arrow, Oklahoma Agency Interest No According to the Louisiana Administrative Code, Title 33, Part I, Subpart 3, LABORATORY ACCREDITATION, the State of Louisiana formally recognizes that this laboratory is technically competent to perform the environmental analyses listed on the scope of accreditation detailed in the attachment. The laboratory agrees to perform all analyses listed on this scope of accreditation according to the Part I, Subpart 3 requirements and acknowledges that continued accreditation is dependent on successful ongoing compliance with the applicable requirements of Part I. Please contact the Department of Environmental Quality, Louisiana Environmental Laboratory Accreditation Program (LELAP) to verify the laboratory s scope of accreditation and accreditation status. Accreditation by the State of Louisiana is not an endorsement or a guarantee of validity of the data generated by the laboratory. To be accredited initially and maintain accreditation, the laboratory agrees to participate in two single-blind, single-concentration PT studies, where available, per year for each field of testing for which it seeks accreditation or maintains accreditation as required in LAC 33:I Certificate Number: Lourdes Iturralde, Administrator Expiration Date: June 30, 2015 Notifications and Accreditations Section Issued On: July 1, 2014 Public Participation & Permit Support Services Division

4 STATE OF LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY AI Number: Issue Date: July 1, 2014 Expiration Date: June 30, W Tacoma, Broken Arrow, Oklahoma Certificate Number: Nitrogen Monoxide EPA CTM State LA Nitrogen dioxide EPA CTM State LA Oxides of nitrogen EPA CTM State LA Carbon dioxide EPA State LA Oxides of nitrogen EPA State LA Oxygen EPA State LA Sampling EPA State LA Sulfur dioxide EPA State LA Verification of Gas Dilution EPA State LA Systems for Field Instrument Calibration Stack gas velocity, volume flow rate EPA 2B 1272 State LA Stack gas velocity, volume flow rate EPA 2D 1274 State LA in small stacks/ducts Landfill gas production flow rate EPA 2E 1275 State LA Stack gas velocity, volume flow rate EPA 2E 1275 State LA Stack gas velocity, volume flow rate EPA 2F 1276 State LA Stack gas velocity, volume flow rate EPA 2G 1277 State LA Stack gas velocity, volume flow rate EPA 2H 1278 State LA NO2 to NO Conversion Efficiency EPA ALT State LA Fugitive Emission Frequency EPA State LA Visible emissions from coke oven EPA State LA batteries Sampling EPA Method State LA Carbon monoxide CEMS Performance Specification 4B 2371 State LA Oxygen CEMS Performance Specification 4B 2371 State LA Sampling CEMS Performance Specification 4B 2371 State LA Formaldehyde ASTM D State LA Mercury CEMS Performance Specification State LA PEMS Certification CEMS Performance Specification State LA Sampling EPA CTM State LA Sulfuric acid mist, sulfur dioxide EPA CTM State LA Hydrogen sulfide EPA State LA Sampling EPA State LA Oxides of nitrogen CEMS Performance Specification State LA Sampling CEMS Performance Specification State LA Sulfur dioxide CEMS Performance Specification State LA Carbon dioxide CEMS Performance Specification State LA Oxygen CEMS Performance Specification State LA Sampling CEMS Performance Specification State LA Carbon monoxide CEMS Performance Specification State LA Sampling CEMS Performance Specification State LA Calibration Drift and Relative CEMS Performance Specification State LA Accuracy Tests Sampling CEMS Performance Specification State LA Stack gas velocity, volume flow rate CEMS Performance Specification State LA Ammonia as N EPA CTM State LA Carbon monoxide EPA CTM State LA Oxides of nitrogen EPA CTM State LA Oxygen EPA CTM State LA Traverse Points EPA Method State LA Page 1 of 4

5 Carbon monoxide EPA Method State LA Sampling EPA Method State LA Ethane EPA State LA Methane EPA State LA Total Gaseous Organic EPA State LA Compounds Oxides of nitrogen EPA Method State LA Particulates EPA Method State LA Particulates, SO2, NOx, sulfur EPA Method State LA removal efficiency Sampling EPA Method State LA Carbon monoxide CEMS Performance Specification 4A State LA Sampling CEMS Performance Specification 4A State LA Traverse Points EPA Method 1A State LA Stack gas velocity, volume flow rate EPA Method State LA Sampling EPA Method State LA Gaseous Organic Compound EPA Method 25A State LA Emissions Total Gaseous Organic EPA Method 25A State LA Compounds Carbon dioxide EPA Method 3A State LA Oxygen EPA Method 3A State LA Sampling EPA Method 3A State LA Sampling EPA TO State LA ,1,1-Trichloroethane EPA State LA Extractive FTIR Specifications EPA State LA Formaldehyde EPA State LA Organic and Inorganic Emissions EPA State LA by FTIR Sampling EPA State LA Formaldehyde EPA State LA Sampling EPA State LA Sampling EPA 12 (FAA) State LA Sampling EPA 13A State LA Particulates EPA State LA Sampling EPA State LA Particulates EPA 201A State LA Particulates <10 um EPA 201A State LA Sampling EPA 201A State LA Condensible Particulate Matter EPA State LA Fine particulates <2.5 um EPA State LA Particulates EPA State LA Sampling EPA State LA Chloride EPA State LA Chlorine EPA State LA Fluoride EPA State LA Hydrochloric acid (Hydrogen EPA State LA chloride (gas only)) Hydrogen fluoride (Hydrofluoric EPA State LA acid) Hydrogen halides and halogens EPA State LA Sampling EPA State LA Bromide EPA 26A State LA Chloride EPA 26A State LA Chlorine EPA 26A State LA Hydrochloric acid (Hydrogen EPA 26A State LA AI Number: Issue Date: July 1, 2014 Certificate Number: Expiration Date: June 30, 2015 Page 2 of 4

6 chloride (gas only)) Hydrogen Bromide (HBr) EPA 26A State LA Hydrogen fluoride (Hydrofluoric EPA 26A State LA acid) Hydrogen halides and halogens EPA 26A State LA Sampling EPA 26A State LA Mercury EPA Method 29 (CVAA) State LA Sampling EPA Method 29 (CVAA) State LA Arsenic EPA Method 29 (GFAA) State LA Beryllium EPA Method 29 (GFAA) State LA Cadmium EPA Method 29 (GFAA) State LA Sampling EPA Method 29 (GFAA) State LA Selenium EPA Method 29 (GFAA) State LA Antimony EPA Method 29 (ICP) State LA Arsenic EPA Method 29 (ICP) State LA Barium EPA Method 29 (ICP) State LA Beryllium EPA Method 29 (ICP) State LA Cadmium EPA Method 29 (ICP) State LA Chromium EPA Method 29 (ICP) State LA Cobalt EPA Method 29 (ICP) State LA Copper EPA Method 29 (ICP) State LA Lead EPA Method 29 (ICP) State LA Manganese EPA Method 29 (ICP) State LA Nickel EPA Method 29 (ICP) State LA Sampling EPA Method 29 (ICP) State LA Selenium EPA Method 29 (ICP) State LA Silver EPA Method 29 (ICP) State LA Thallium EPA Method 29 (ICP) State LA Total Phosphorus EPA Method 29 (ICP) State LA Zinc EPA Method 29 (ICP) State LA Antimony EPA Method 29 (ICP-MS) State LA Arsenic EPA Method 29 (ICP-MS) State LA Barium EPA Method 29 (ICP-MS) State LA Beryllium EPA Method 29 (ICP-MS) State LA Cadmium EPA Method 29 (ICP-MS) State LA Chromium EPA Method 29 (ICP-MS) State LA Cobalt EPA Method 29 (ICP-MS) State LA Copper EPA Method 29 (ICP-MS) State LA Lead EPA Method 29 (ICP-MS) State LA Manganese EPA Method 29 (ICP-MS) State LA Nickel EPA Method 29 (ICP-MS) State LA Sampling EPA Method 29 (ICP-MS) State LA Selenium EPA Method 29 (ICP-MS) State LA Silver EPA Method 29 (ICP-MS) State LA Thallium EPA Method 29 (ICP-MS) State LA Total Phosphorus EPA Method 29 (ICP-MS) State LA Zinc EPA Method 29 (ICP-MS) State LA Stack gas velocity, volume flow rate EPA Method 2A State LA in small stacks/ducts Stack gas velocity, volume flow rate EPA Method 2C State LA in small stacks/ducts Carbon dioxide, oxygen, dry EPA Method State LA molecular weight Sampling EPA 30B State LA Moisture content EPA Method State LA Particulates EPA State LA AI Number: Issue Date: July 1, 2014 Certificate Number: Expiration Date: June 30, 2015 Page 3 of 4

7 Sampling EPA State LA Sampling EPA 5A State LA Particulates EPA 5B State LA Sampling EPA 5B State LA Sampling EPA 5D State LA Particulates EPA 5E State LA Sampling EPA 5E State LA Non-sulfate particulates EPA 5F State LA Sampling EPA 5F State LA Sampling EPA 5G State LA Sampling EPA 5H State LA Sampling EPA 5I State LA Sampling EPA State LA Sampling EPA Method 6C State LA Sulfur dioxide EPA Method 6C State LA Oxides of nitrogen EPA Method 7E State LA Sampling EPA Method 7E State LA Sampling EPA State LA Sulfuric acid mist, sulfur dioxide EPA State LA Opacity EPA Method State LA Carbon monoxide ASTM D State LA Oxides of nitrogen ASTM D State LA Oxygen ASTM D State LA Mercury ASTM D State LA Sampling ASTM D State LA Sulfur dioxide NCASI 8A State LA Sulfuric acid mist NCASI 8A State LA Non Potable Water Bromide EPA 300.1, Rev State LA Chloride EPA 300.1, Rev State LA Sulfate EPA 300.1, Rev State LA Ammonia as N EPA State LA Ammonium ASTM D State LA Solid Chemical Materials Bromide EPA 300.1, Rev State LA Chloride EPA 300.1, Rev State LA Sulfate EPA 300.1, Rev State LA Biological Tissue NONE NONE NONE NONE NONE AI Number: Issue Date: July 1, 2014 Certificate Number: Expiration Date: June 30, 2015 Page 4 of 4