Madhya Pradesh Waste Management Project Laboratory, Plot No. 104, Industrial Area No. II, Pithampur, Dhar, Madhya Pradesh

Transcription

1 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 1 of 8 CHEMICAL TESTING I. POLLUTION AND ENVIRONMENT 1. Waste Water (Effluent & Sewage) ph APHA 22nd Edition, 2012; 4500 H+ B (Electrometric Temperature 2550 B ( & Field Methods) Conductivity 2510 B ( Total Solids 2540 B (Total Solids Dried at O C) Total Dissolved Solids 2540 C (Total Dissolve Solids Total Suspended Solids Dried at 180 O C) 2540 D (Total Suspended Solids Dried at O C) Fixed Solids 2540 E(Fixed & Volatile Solids ignited at 550 O C) Volatile Solids 2540 E(Fixed & Volatile Solids ignited at 550 O C) Chlorides as Cl Cl - B & C (Argentometric Residual Chlorine as Cl 4500 Cl B (Idometric Method I) Dissolved Oxygen 4500 O C (Azide Modification) o C -50 o C 2 µmho/cm µmho/cm 1 mg/l mg/l 1 mg/l -100 mg/l 1 mg/l -12 mg/l

2 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 2 of 8 Oil & Grease 5520 B,(Liquid Liquid, Partition Gravimetric Chemical Oxygen Demand Biological Oxygen Demand (5 Days at 20 o C) 5220 B (Open Reflux 5210 B, 4500-O. C ( 5- Day BOD Test & Azide Modification) IS : 3025 : Part 44 3 Days at 27 O C Cadmium Cd 3111 (Direct Air Acetylene Flame Total Chromium as Cr Flame Iron as Fe Flame Lead as Pb Flame Manganese as Mn 3111 B (Direct Air Acetylene Flame Nickel as Ni Flame Zinc as Zn Flame Copper as Cu 3111 B(Direct Air Acetylene Flame 5 mg/l mg/l 5 mg/l mg/l 0.10 mg/l mg/l 1.0 mg/l -100 mg/l 0.5 mg/l -100 mg/l 1.0 mg/l -100mg/L 0.1mg/L -100mg/L 0.5 mg/l -100 mg/l 0.1 mg/l -100mg/L 0.5 mg/l -100 mg/l

3 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 3 of 8 2. Waste (Hazardous) ph USEPA 1998 SW-846; 9045 C (Solid & Waste ph) Bulk Density APHA 2710 F (Specific Gravity) Calorific Value IS:1350 Part II 1970 (Bomb Calorimeter) Moisture content IS 326 (Part 21) :2001 (KF Titration) Loss on drying at 105 o C 2540 (Total Solid Dried at Loss on ignition at 550 o C o C) 2540 (Fixed & Volatile Solids Ignited at 550 o C) Paint Filter Liquid Test USEPA 1998, SW-846; 9095 A (Paint Filter Liquid Test) Reactive Cyanide as HCN Total Cyanide as CN - USEPA 1998, SW-846; 9014 (Titrimetric & Manual Spectrophotometric Determinative Method for Cyanide) USEPA 1998, SW-846; 9010B, 9014 (Distillation Titrimetric & manual Spectrophotometric Determinative method for Cyanide) Total Sulfide as S -2 USEPA 1998, SW-846; 9215 (Potentiometric determination of sulphide in aqueous samples and distillates with ion-selective electrode) Reactive Sulfide as H 2 S USEPA 1998, SW-846; 9034 (Titrimetric Procedure For Acid-Soluble And Acid Insoluble Sulfides) gm/cc - 3 gm/cc 500 cal/gm - 10,000 cal/gm 0.1%-100% 5%- 80% 5%- 100% Pass/ Fail 1 mg/kg mg/kg 10 mg/kg -500 mg/kg 10 mg/kg -50 mg/kg 10 mg/kg mg/kg

4 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 4 of 8 Water soluble halides USEPA 1998, SW-846; 9253 (as Cl - ) (Titrimetric, Silver Nitrate) Metals by Digestion Cadmium as Cd USEPA 1998, SW-846; 7130 Copper as Cu USEPA 1998, SW-846; 7210 Total Chromium as Cr USEPA 1998, SW-846; 7190 Iron as Fe USEPA 1998, SW-846; 7380 Lead as Pb USEPA 1998, SW-846; 7420 Manganese as Mn USEPA 1998, SW-846; 7460 Nickel as Ni USEPA 1998, SW-846; 7520 Zinc as Zn USEPA 1998, SW-846; 7950 Metals by TCLP Cadmium as Cd USEPA 1998, SW-846; 7130 Total Chromium as Cr USEPA 1998, SW-846; mg/kg mg/kg 5 mg/kg -200 mg/kg 5 mg/kg mg/kg 5 mg/kg -500 mg/kg 5 mg/kg -1000mg/Kg 10 mg/kg - 500mg/Kg 5 mg/kg mg/kg 5 mg/kg -50 mg/kg 5 mg/kg -100 mg/kg 0.1 mg/l - 10 mg/l 0.1 mg/l - 20 mg/l

5 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 5 of 8 Hexavalent Chromium as Cr Cr B (Colorimetric Iron as Fe USEPA 1998, SW-846; 7380 Lead as Pb USEPA 1998, SW-846; 7420 Manganese as Mn USEPA 1998, SW-846; 7460 Nickel as Ni USEPA 1998, SW-846; 7520 Copper as Cu USEPA 1998, SW-846; 7210 Zinc as Zn USEPA 1998, SW-846; mg/l -10 mg/l 0.1 mg/l - 50 mg/l 0.1 mg/l - 50mg/L 0.1 mg/l - 20 mg/l 0.5 mg/l -20 mg/l 0.5 mg/l -20 mg/l 0.5 mg/l - 50 mg/l II. WATER 1. Surface & Ground Water ph 4500 H + B (Electrometric Temperature 2550 B ( & Field Methods) Conductivity 2510 B( Acidity as CaCO B (Titration Alkalinity as CaCO B (Titration C -50 C 2 µmhos/cm µmhos/cm

6 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 6 of 8 Total Solids 2540 B (Total Solids Dried at O C) Total Dissolved Solids 2540 C (Total Dissolve Solids Dried at Total Suspended Solids 180 O C) 2540 D (Total Suspended Solids Dried at O C) Fixed Solids 2540 E(Fixed & Volatile Solids ignited at 550 O C) Volatile Solids 2540 E(Fixed & Volatile Solids ignited at 550 C) Chlorides as Cl Cl - B & C (Argentometric Residual Chlorine as 4500 Cl Cl B (Idometric Method I) Total Hardness as 2340 CaCO 3 C (EDTA Titrimetric Dissolved Oxygen 4500 O C (Azide Modification) Oil & Grease 5520 B,(Liquid Liquid, Partition Gravimetric Chemical Oxygen Demand Biological Oxygen Demand (5 Days at 20 o C) 3 Days at 27 O C 5220 B(Open Reflux 5210 B, 4500-O. C( 5- Day BOD Test & Azide Modification) IS : 3025 : Part mg/l mg/l 1.0 mg/l -10 mg/l 5 mg/l mg/l 2 mg/l -12 mg/l 10 mg/l - 50 mg/l 5 mg/l -500 mg/l 5 mg/l mg/l

7 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 7 of 8 Calcium as Ca 3500 Ca B (EDTA Titrimetric Sodium as Na 3500 Na B (Flame Emission Photometric Magnesium as Mg 3500-Mg B (Calculation Potassium as K 3500 K B (Flame Emission Photometric Cadmium Cd 3111 (Direct Air Acetylene Flame Total Chromium as Cr Flame Iron as Fe Flame Lead as Pb Flame Manganese as Mn Flame Nickel as Ni Flame Zinc as Zn Flame Copper as Cu Flame 10 mg/l -100mg/L 5 mg/l mg/l 10 mg/l -1000mg/L 5 mg/l mg/l 0.10 mg/l mg/l 1.0 mg/l - 10 mg/l 0.5 mg/l -50 mg/l 1.0 mg/l -10mg/L 0.10 mg/l -10 mg/l 0.5 mg/l -10 mg/l 0.1 mg/l - 10 mg/l 0.5 mg/l -10 mg/l

8 Madhya Pradesh Waste Management Project, Certificate Number TC-5022 (in lieu of T-2449) Page 8 of 8 III. ATMOSPHERIC POLLUTION 1. Ambient Air Sulphur Dioxide IS 5182 (Part II) 4 µg/m µg/m 3 Oxides of Nitrogen IS 5182 (Part VI) 10 µg/m µg/m 3 PM 10 IS 5182 (Part 23) 10 µg/m µg/m 3 Ammonia as Nitrogen LAB SOP No.60 5 µg/m µg/m 3 Lead IS 5182(Part 22) 0.1 µg/m 3-10 µg/m3