Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK
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1 ccredited to Laboratory locations: Schedule of ccreditation United Kingdom ccreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK Petroservice House Macklin venue illingham TS23 4Y Issue No: 020 Issue date: 25 pril 2017 Contact: Mr ndrew Smith Tel: +44 (0) Fax: +44 (0) andrew.smith@sgs.com Website: below s covered by the organisation and their relevant activities details ctivity code ddress Petroservice House Macklin venue illingham TS23 4Y Local contact ndrew Smith Fuels, Oils and Lubricants ddress Environmental Laboratory Unit 2 Macklin venue illingham TS23 4Y Local contact ndrew Smith Environmental Samples, Fuels, Oils and Lubricant, iofuels ssessment Manager: DC1 Page 1 of 10
2 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 DETIL OF CCREDITTION PETROLEUM ND PETROLEUM PRODUCTS Chemical and Physical Tests Flexible scope enabling new versions of existing accredited standard test methods to be introduced in accordance with documented SGS UK corporate procedure R- Gen-1QP143 ppearance STM E2680 Visual inspection Colour (Pt/Co) STM D5386 Density/Specific gravity IP 365 STM D4052 Distillation at atmospheric pressure Flash Point Nitrogen STM D86 STM D93 Pensky Martens Closed Cup (PMCC) STM D5762 Chemiluminescence Organic halogens as chlorine IP 510 by Microcoulometric Refractive index STM D1218 Water content STM E203 by Karl Fisher Crude Oil Sulphur content STM D2622 by WD-XRF ROMTIC HYDROCRONS Total sulphur STM D7183 by UV Fluorescence IO-ETHNOL ppearance IP 573, EN Copper content Higher alcohols, methanol and volatile impurities IP 556, EN by Graphite Furnace IP 571, EN by Gas ssessment Manager: DC1 Page 2 of 10
3 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 IO-ETHNOL (cont d) Chemical and Physical Tests (cont d) Flexible scope enabling new versions of existing accredited standard test methods to be introduced in accordance with documented SGS UK corporate procedure R- Gen-1QP143 (cont d) Inorganic chloride content Involatile material EN by Ion chromatography EC/2870/2000 method II by evaporation on steam bath Involatile material IP 576, EN Gravimetric Phosphorus EN 15487, IP 555 Spectrometric Sulphur EN 15486, IP 554 y UVF Total acidity EN 15491, IP 538 Colour titration Water content (% m/m) EN 15489, IP 539 by coulometric Karl Fisher ITUMEN Penetration IP 49 Softening point IP 58 LPG (Propane, butane, isobutane) Hydrocarbon composition IP 405 Gas Hydrocarbon composition STM D2163 Gas Mercury STM D6350 (Modified) tomic Fluorescence Spectroscopy ssessment Manager: DC1 Page 3 of 10
4 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 LIQUID PETROLEUM HYDROCRONS Total mercury UOP 938 Mercury nalyser tomic Fluorescence Trace nitrogen STM D4629 Chemiluminescence LIGHT HYDROCRON, DIESEL, ENGINE OIL, SPRK IGNITION Cetane Number STM D613 Individual components in spark ignition engine fuels STM D6733 by Gas Motor Octane Number (MON) STM D (Historical) Research Octane Number (RON) STM D (Historical) Total sulphur STM D5453 UV Fluorescence NPHTHS Detailed analysis of petroleum naphthas STM D5134 by Gas NTURL GS Composition to C 10 (as per table 1 of method) Calorific value, density, relative density and Wobbe index from the composition of gaseous fuels Mercury Mono-ethylene Glycol (MEG) content STM D1945 Gas ISO 6976 calculation based on GC data STM D6350 tomic Fluorescence Spectroscopy R-ILENV-TP020 Thermal desorption of sampling tubes and Gas ssessment Manager: DC1 Page 4 of 10
5 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 REFINERY GS Chemical Tests Composition (as per section 1 S EN of method) Mol % Hydrogen 0.01 to Oxygen/rgon 0.01 to 21.0 Nitrogen 0.01 to 78.1 Carbon Monoxide 0.01 to 5.0 Carbon Dioxide 0.01 to 25.0 Dihydrogen Sulphide 0.01 to 1.0 Methane 0.01 to Ethane 0.01 to Ethene 0.01 to Ethyne 0.01 to 1.0 Propane 0.01 to 7.0 Propene 0.01 to Propyne 0.01 to 3.0 Propadiene 0.01 to 1.0 Isobutane 0.01 to 6.0 n-utane 0.01 to 4.0 trans-2-utene 0.01 to utene 0.01 to Methylpropene 0.01 to 2.0 Cis-2-utene 0.01 to 2.4 1,3-utadiene 0.01 to 3.0 Isopentane 0.01 to 1.0 n-pentane 0.01 to 1.0 C to 9.0 Flexible scope to allow the analyte range to be changed by following in house procedure R.il- 1QP007 SOILS Determination of Extractable Petroleum Hydrocarbons (EPH) C 10 to C 36 Documented In-House Method R-ILENVI-TP015 Using GC-FID and meeting the requirements of the Environment gency MCERTS Performance Standard chemical testing of soil ssessment Manager: DC1 Page 5 of 10
6 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 TRDE EFFLUENTS Chemical Tests Documented In-House Methods: mmonia as Nitrogen Chloride Chemical Oxygen Demand (COD) iochemical Oxygen Demand (OD) Metals: luminium, ntimony, rsenic, arium, erylium, Cadmium, Chromium, Cobalt, Copper, Lead, Manganese, Mercury, Molybdenum, Nickel, Selenium, Thallium, Thorium, Uranium, Vanadium and Zinc Semi-Volatile Organic Compounds (SVOC): Phenol is (2-chloroethyl) ether 2-chloro phenol enzyl alcohol 2-methyl phenol is (2-chloro isopropyl) ether 3 & 4 methyl phenol n-nitroso-di-n-propylamine Nitrobenzene Isophorone 2-nitrophenol 2,4-dimethyl phenol is (2-chloro ethoxy) methane 2,4-dichlorophenol 4-chloro-3-methyl phenol 2,4,6-trichlorophenol 2,4,5-trichlorophenol 2-nitro aniline Dimethyl phthalate R-ILENVI-TP010 by quakem Discrete nalyser R-ILENVI-TP009 by quakem Discrete nalyser R-ILENVI-TP011 by quakem Discrete nalyser R-ILENVI-TP012 R-ILENVI-TP004 by ICP-MS RILENVI-TP001 based on USEP Method 8270 by GC/MS ssessment Manager: DC1 Page 6 of 10
7 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 TRDE EFFLUENT (cont d) Chemical Tests (cont d) Semi-Volatile Organic Compounds (SVOC): (cont d) cenaphthylene cenaphthene Dibenzofuran 2,3,5,6-tetrachlorophenol 2,3,4,6-tetrachlorophenol Diethylphthalate 4-chlorophenyl phenyl ether Fluorene Diphenylamine zobenzene 4-bromo-phenyl ether Hexachlorobenzene Phenanthrene nthracene Carbazole Dibutyl phthalate Fluoranthene Pyrene enzyl butyl phthalate enz(a)anthracene Chrysene Di-n-octyl phthalate enzo(b)fluoranthene enzo(k)fluoranthene enzo(a)pyrene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene enzo(g,h,i)perylene RILENVI-TP001 based on USEP Method 8270 by GC/MS (cont d) Volatile Organic Compounds RILENVI-TP002 based on (VOC): USEP Method 8260c Di ethyl ether by Headspace GC/MS 1,1-dichloroethene Methyl iodide 1,1,2-trichloroethane llyl chloride CS2 t-1,2-dichloroethene 1,1-dichloroethane Chloroprene cis-1,2-dichloroethene romochloromethane Trichloromethane ssessment Manager: DC1 Page 7 of 10
8 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 TRDE EFFLUENT (cont d) Chemical Tests (cont d) Volatile Organic Compounds RILENVI-TP002 based on (VOC) (cont d): USEP Method 8260c 2,2-dichloropropane by Headspace GC/MS Tetrahydrofuran (cont d) 1,2-dichloroethane 1,1,1-trichloroethane 1,1-dichloroprop-1-ene CCl4 enzene Dibromomethane 1,2-dichloropropane Trichloroethylene romodichloromethane cis-1,3-dichloropropene trans-1,3-dichloropropene 1,1,2-trichloroethane Toluene 1,3-dichloropropane Dibromochloromethane 1,2-dibromoethane Tetrachloroethylene 1,1,1,2-tetrachloroethane Chlorobenzene Ethyl benzene Meta & Para Xylenes Tribromomethane cis-1,4-dichlorobutene Styrene 1,1,2,2-tetrachloroethane Ortho Xylene trans-1,4-dichlorobutene 1,2,3-trichloropropane iso-propyl benzene romobenzene n-propyl benzene 2-Chlorotoluene 4-Chlorotoluene 1,3,5-Trimethyl benzene Pentachloroethane Tert-butyl benzene 1,2,4-trimethyl benzene Sec-butyl benzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 4-iso-propyltoluene 1,2-Dichlorobenzene ssessment Manager: DC1 Page 8 of 10
9 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 TRDE EFFLUENT (cont d) Chemical Tests (cont d) Volatile Organic Compounds RILENVI-TP002 based on (VOC) (cont d): USEP Method 8260c by Headspace GC/MS utyl benzene (cont d) 1,2-Dibromo-3-chloro propane 1,2,4-trichlorobenzene Naphthalene Hexachlorobutadiene 1,2,3-Trichloro benzene WTERS Chemical Tests Ground water and saline water Determination of Extractable Petroleum Hydrocarbons (EPH) C 10 to C 36 R-ILENVI-TP015 Using GC-FID Ground water, trade effluent, land and prepared leachate, surface water and process water ph RILENVI-TP017 based on STM D1293 Conductivity RILENVI-TP018 based on STM D1125 Ground water, trade effluent and surface water Suspended Solids RILENVI-TP019 based on S EN 872:2005 IOFUELS Flexible scope enabling new versions of existing accredited standard test methods to be introduced in accordance with documented SGS UK corporate procedure R- Gen-1QP143 Solid biofuels Total Moisture S EN ISO using nalysis Moisture sh S EN ISO using S EN ISO using ssessment Manager: DC1 Page 9 of 10
10 Schedule of ccreditation United Kingdom ccreditation Service ccredited to Issue No: 020 Issue date: 24 pril 2017 Solid biofuels (cont d) Carbon, Hydrogen, Nitrogen S EN ISO using Combustion nalyser Calorific value Sulphur and Chlorine S EN ISO using omb Calorimetry S EN ISO using Ion Solid recovered fuels Total Moisture S EN using nalysis Moisture sh Carbon, Hydrogen, Nitrogen Calorific value Sulphur, Fluorine, romine and Chlorine iomass Content S EN using S EN using S EN using Combustion nalyser S EN using omb Calorimetry S EN using Ion S EN using Selective Dissolution Method END ssessment Manager: DC1 Page 10 of 10
Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK
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