Author: Kerry J. Libbert Mechanical Engineer. Performing Activity: Naval Surface Warfare Center Code 4045 Crane, Indiana Date.

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1 AD-A Ill ilili ill i radi II HI II DODPOPHMIUSA/DODINADTR92108 REVISION A PERFORMANCE ORIENTED PACKAGING TESTING OF MK 635 MOD 0 SHIPPING AND STORAGE CONTAINER FOR PACKING GROUP II SOLID HAZARDOUS MATERIALS Author: Kerry J. Libbert Mechanical Engineer Performing Activity: Code 4045 Crane, Indiana Date August 1993 FINAL DTIC ELECTE S¼. SEP20190 j S DISTRIBUTION UNLIMITED Sponsoring Organization: Code 4024 Crane, Indiana S9 06 _ z n nnn

2 Prepared by: R. F. Sanders Reviewed by: Approved by: I,,00 e.5c 5ygor

3 Form Approved OMB No Public reporting burden of this collection of information is estimated to average 1 hour per response, including the time for reviewing instructions., searching existing data sources, gathering and maintaining the data needed, and completing and reviewing the collection of information. Send comments regarding this burden estimate or any other aspect of this collection of information, including suggestions for reducing this burden, to Washington Headquarters Services, Directorate for Information Operations and Reports, 1215 Jefferson Davis Highway, Suite 1204, Arlington. VA , and to the Office of Management and Budget, Paperwork Reduction Project ( ), Washington, DC AGENCY USE ONLY (Leave blank) 2. REPORT DATE 3. REPORT TYPE AND DATES COVERED August 1993 POP Test, Revision A 4. TITLE AND SUBTITLE 5. FUNDING NUMBERS Performance Oriented Packaging Testing of MK 635 Mod 0 Shipping and Storage Container for Packing Group II Solid Hazardous Materials 6. AUTHOR(S) Kerry J. Libbert 7. PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) 8. PERFORMING ORGANIZATION REPORT NUMBER Plastics and Packaging Applications Branch (Code 4045) DODPOPHM/USA/DOD/NADTR Highway 361 Revision A Crane IN SPONSORING/MONITORING AGENCY NAME(S) AND ODDRESS(ES) 10. SPONSORING/MONITORING AGENCY REPORT NUMBER Countermeasures Branch (Code 4027) Same as above 300 Highway 361 Crane IN SUPPLEMENTARY NOTES N/A 12a. DISTRIBUTION/AVAILABILITY STATEMENT 12b. DISTRIBUTION CODE 13. ABSTRACT (Maximum 200 words) Qualification tests were performed to determine whether the in-service MK 635 Mod 0 Shipping and Storage Container could be utilized to contain properly dunnaged solid type hazardous materials weighing up to a gross weight of 32 kg (70.5 pounds). The tests were conducted in accordance with Performance Oriented Packaging (POP) requirements specified by the Code of Federal Regulations, Title 49 CFR, Parts 107 through 178. The MK 635 has conformed to the POP performance requirements; i.e., the container successfully retained its contents throughout the specified tests. 14. SUBJECT TERMS 15. NUMBER OF PAGES 6 POP Test of MK 635 Mod 0 Shipping and Storage 16. PRICE CODE Container 17. 9ECURITY CLASSIFICATION OF 18. SECURITY CLASSIFICA- 19. SECURITY CLASSIFICA- 20. LIMITATION TEPORT 1ON OF THIS PAGE TION OF ABSTRACT OF ABSTRACT UNCLASSIFIED UL UL UL W NP Standard Form 298 (Rev 2-89) Prawribed by AN&I Sid ,

4 INTRODUCTION This Performance Oriented Packaging (POP) test was performed to ascertain whether the MK 635 Mod 0 Shipping and Storage Container meets the Packing Group II requirements specified by the Code of Federal Regulations, Title 49 CFR, Parts 107 through 178, dated 31 December The objectives were to evaluate the adequacy of the container in protecting the hazardous materials. The MK635 Mod 0 Shipping and Storage Container is a steel drum with a removeable lid. Each container lid was secured with a V-retainer and a lead seal during the testing. TESTS PERFORMED 1. Drop Test This test was performed in accordance with Title 49 CFR, Part 178, Subpart M, Sec Six containers were used during the test series, one for each drop. Three drops were conducted at each orientation listed below from a height of 1.2 meters: a. 450 from vertical on V-retainer closure b. Horizontal on container seam (closure of V-retainer positioned 1800 from seam) The tests were performed at ambient temperature ( F). The contents of the container should be retained within its packaging and exhibit no damage liable to affect safety during transport. 2. Stacking Test This test was performed in accordance with Title 49 CFR, Part 178, Subpart M, Sec Three different containers were used, each with a stack weight of 1000 pounds. This represents the weight imposed on the bottom container of a tenfoot stack of like containers weighing 70.5 pounds each. The test was performed for 24 hours. After the allowed time, the weight was removed and the container examined. Any leakage, deterioration, or distortion which could adversely affect transport or reduce its strength or cause instability in stacks of packages is cause for rejection. 3. Base Level Vibration Test One sample container was loaded with live Flexible Linear Shaped Charges and closed as for shipment. The container was subjected to standard transportation vibration testing for a period of six hours. The test was performed for two hours in each of the three principal axes. T~' t

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6 PASS/FAIL (UN CRITERIA) The criteria for passing the drop test is outlined in Title 49 CFR, Part 178, Subpart M, Sec (f): A package is considered to successfully pass the drop tests if for each sample tested, the entire contents are retained by an inner packaging (e.g. a plastic bag) even if the closure on the top head of the drum is no longer sift proof. 2. Stacking Test The criteria for passing the stacking test is outlined in Title 49 CFR, Part 178, Subpart M, Sec : No test sample may show any deterioration which could adversely affect transportation safety or any distortion likely to reduce its strength, cause instability in stacks of packages, or cause damage to inner packagings likely to reduce safety in transportation. 3. Vibration Test The criteria for passing the Vibration Test is outlined Title 49 CFR, Part 178, Subpart M, Sec : Immediately following the period of vibration, each package must be removed from the platform, turned on its side and observed for any evidence of leakage. A packaging passes the vibration test if there is no rupture or leakage from any of the packages. No test sample should show any deterioration which could adversely affect transportation safety or any distortion liable to reduce packaging strength. TEST RESULTS A@@osston XTIS GRA&IFor 1. Drop Test DTIC TAB Unannounced C] Satisfactory. 3ustifrcation 2. Stacking Test D, D0 tributian/ Satisfactory. Availability Codes 3. est Vbraton 3. estmat Vbraion ~stavail and/or Special. Satisfactory. DISCUSSION DTIC QUALITY INSECTUD a - 1. Drop Test After each drop the container was inspected for any damage which would be cause for rejection. The containers were slightly damaged during the tests, but all V-retainers and lead seals remained fastened securely.

7 2. Stacking Test Three containers were individually tested. Each container was visibly inspected after the 24-hour period was over. There was no leakage, distortion, or deterioration to the container as a result of this test. The containers are shown in figure Vibration Test Immediately following the vibration test, each container was removed from the platform, turned on its side and observed for any evidence of leakage. There was no evidence of leakage of contents. REFERENCE MATERIAL Code of Federal Regulations Title 49 CFR, Parts DISTRIBUTION LIST Commander Crane Division Code 4045 ane Code 4024 Crane, IN Commanding Officer Naval Weapons Station Earle Code 50 and Code Colts Neck, NJ Defense Technical Information Center (2 copies) ATTN: DTIC/FDAC (Virginia Guidi) Bldg. 5, Cameron Station Alexandria, VA Commander U.S. Army Armament, Research, Development and Engineering Center SMCAR-ESK Rock Island, IL Defense General Supply Center DDRV-TMPA (Dave Gay) Richmond, VA

8 DATA SHEET CONTAINER: POP MARKING: MK635 Shipping and ( l 1A2/Y32/S/** Storage Container ) USA/DOD/NAD Type: 1A2 UN Code: See Table I Drawing Number: Material: Steel Gross Weight: Dimensions: 32.0 kg 1.31 m L x.20 m DIA (70.5 pounds) (51.56" L x 8.0" DIA) Closure (Method/type): Screw-on cap Tare Weight: 4.6 kg (10.1 pounds) Additional Description: Lid secured with V-retainer and lead seal (MS ) during tests. Alternate container nomenclature "CONTAINER, SHIPPING AND STORAGE, FOR NATO SEA GNAT", Drawing PRODUCTS: See Table I Proper Shipping Name: United Nations Number: See Table II See Table I United Nations Packing Group: II Physical State: Solid Amount Per Container: See Table I Net Weight: Varies TEST PRODUCT: Name: Sand Physical State: Solid Size: N/A Quantity: N/A Dunnage: None Gross Weight: 32.0 kg (70.5 lbs.)

9 TABLE I NALC/ NSN ITEM PACKING HAZ. UN # PER GROSS DODIC DRAWING CL. NO. CNTR. WT. 3W MK216-0 RF CTG C W MK216-1 RF CTG W a-0290 MK186-0/E CTG J W MK229-0 PRAC. CTG S W MK229-0 PRAC. CTG S W MK CTG W MK CTG S W MK214-0 RF CTG S W MK214-1 RF CTG EW MK CRG G EW MK CTG G EW MK CTG S EW MK CTG. * S EW MK CTG S ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG I.ID ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D ML GR/FT FLEX CHG D N/A ** CRG G N/A EX CRG. * 1.3J * ALTERNATE PACKING DRAWING ** NATO NUMBER *** PACKING SKETCH (53711) 90-D-1536 TABLE II UN NO. PROPER SHIPPING NAME 0010 AMMUNITION, INCENDIARY 0054 CARTRIDGES, SIGNAL 0171 AMMUNITION, INCENDIARY 0173 RELEASE DEVICES, EXPLOSIVE 0386 ROCKET MOTORS 0247 AMMUNITION, INCENDIARY 0288 CHARGES, SHAPED, FLEXIBLE, LINEAR