Appendix D - Geotechnical Report

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1 Appendix D - Geotechnical Report

29 CHUNG AND VANDER DOELEN ATTN: ERIC CHUNG 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 Date Received: Report Date: Version: 18-AUG AUG-15 :35 (MT) FINAL Client Phone: Certificate of Analysis Lab Work Order #: L Project P.O. #: G15100 Job Reference: G15100 C of C Numbers: , Legal Site Desc: Mary-Lynn Pires Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.] ADDRESS: 60 Northland Road, Unit 1, Waterloo, ON N2V 2B8 Canada Phone: Fax: ALS CANADA LTD Part of the ALS Group A Campbell Brothers Limited Company

30 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 2 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH1-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Leachable Anions & Nutrients ms/cm ph units Chloride Anions and Nutrients Sulphate Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent <5.0 < < mg/kg SAR mg/l mg/l mg/l 25-AUG L Sampled By: Matrix: BH1-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Moisture Polycyclic Aromatic Hydrocarbons Acenaphthene ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

31 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 3 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH1-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Polycyclic Aromatic Hydrocarbons Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d Polychlorinated Biphenyls Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Total PCBs Surrogate: d-terphenyl <0.042 <0.030 < <0.010 <0.010 <0.010 <0.010 < AUG AUG AUG AUG AUG AUG L Sampled By: Matrix: BH2-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine) ms/cm ph units SAR mg/l mg/l mg/l

32 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 4 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH2-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Metals Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent 6.5 < < < L Sampled By: Matrix: BH2-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Moisture Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene 6.73 <0.042 <0.030 < ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

33 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 5 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH2-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Polycyclic Aromatic Hydrocarbons Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d Polychlorinated Biphenyls Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Total PCBs Surrogate: d-terphenyl <0.010 <0.010 <0.010 <0.010 < AUG AUG AUG AUG AUG AUG L Sampled By: Matrix: BH3-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals < < ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine) ms/cm ph units SAR mg/l mg/l mg/l

34 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 6 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH3-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Speciated Metals Chromium, Hexavalent < L Sampled By: Matrix: BH3-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Moisture Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d Polychlorinated Biphenyls Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Total PCBs Surrogate: d-terphenyl 3.15 <0.042 <0.030 < <0.010 <0.010 <0.010 <0.010 < AUG AUG AUG AUG AUG AUG L Sampled By: Matrix: BH4-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides ms/cm ph units ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

35 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 7 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH4-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent <5.0 < < SAR mg/l mg/l mg/l L Sampled By: Matrix: BH5-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals ms/cm ph units SAR mg/l mg/l mg/l ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

36 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L BH5-1 Sampled By: D. FONDEVILLA on 21-JUL-15 Matrix: SOIL L CONTD... Page 8 of AUG-15 :35 (MT) Guideline Limits #1 #2 Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d < <0.042 <0.030 < ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

37 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 9 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH6-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent < < < ms/cm ph units SAR mg/l mg/l mg/l L Sampled By: Matrix: BH7-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Leachable Anions & Nutrients Chloride Anions and Nutrients Sulphate < ms/cm ph units mg/kg 25-AUG ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

38 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 10 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH7-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent < < SAR mg/l mg/l mg/l L Sampled By: Matrix: BH8-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals ms/cm ph units SAR mg/l mg/l mg/l ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

39 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 11 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH8-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent < < < L Sampled By: Matrix: BH8-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Moisture Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene 12.3 <0.042 <0.030 < ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

40 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 12 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH8-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Polycyclic Aromatic Hydrocarbons Naphthalene Phenanthrene Pyrene Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d L Sampled By: Matrix: BH9-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Leachable Anions & Nutrients Chloride Anions and Nutrients Sulphate Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) <20 < < < ms/cm ph units mg/kg SAR mg/l mg/l mg/l 25-AUG ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

41 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 13 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH9-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Speciated Metals Chromium, Hexavalent < L Sampled By: Matrix: BH9-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Moisture Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d Polychlorinated Biphenyls Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Total PCBs Surrogate: d-terphenyl 5.68 <0.042 <0.030 < <0.010 <0.010 <0.010 <0.010 < AUG AUG AUG AUG AUG AUG L Sampled By: Matrix: BH10-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests ph Saturated Paste Extractables SAR Calcium (Ca) ph units SAR mg/l ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

42 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH10-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Saturated Paste Extractables Magnesium (Mg) Sodium (Na) mg/l mg/l L Sampled By: Matrix: BH11-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent < < < ms/cm ph units SAR mg/l mg/l mg/l L Sampled By: Matrix: BH12-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

43 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L CONTD... Page 15 of AUG-15 :35 (MT) Guideline Limits L Sampled By: Matrix: BH12-1 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Conductivity Moisture ph Cyanides Cyanide, Weak Acid Diss Saturated Paste Extractables SAR Calcium (Ca) Magnesium (Mg) Sodium (Na) Metals Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Boron (B), Hot Water Ext. Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) Speciated Metals Chromium, Hexavalent < < < ms/cm ph units SAR mg/l mg/l mg/l L Sampled By: Matrix: BH12-2 D. FONDEVILLA on 21-JUL-15 SOIL #1 #2 Physical Tests Moisture Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

44 ANALYTICAL GUIDELINE REPORT G15100 Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed L BH12-2 Sampled By: D. FONDEVILLA on 21-JUL-15 Matrix: SOIL L CONTD... Page 16 of AUG-15 :35 (MT) Guideline Limits #1 #2 Polycyclic Aromatic Hydrocarbons Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1+2-Methylnaphthalenes 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate: 2-Fluorobiphenyl Surrogate: p-terphenyl d <0.042 <0.030 < ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine) #1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

45 G15100 Reference Information L CONTD... Page 17 of AUG-15 :35 (MT) Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference*** B-HWS-R511-WT Soil Boron-HWE-O.Reg 153/04 (July 2011) HW EXTR, EPA 6010B A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CL-R511-WT Soil Chloride-O.Reg 153/04 (July EPA ) 5 grams of dried soil is mixed with 10 grams of distilled water for a minimum of 30 minutes. The extract is filtered and analyzed by ion chromatography. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CN-WAD-R511-WT Soil Cyanide (WAD)-O.Reg 153/04 MOE 3015/APHA 4500CN I-WAD (July 2011) The sample is extracted with a strong base for 16 hours, and then filtered. The filtrate is then distilled where the cyanide is converted to cyanogen chloride by reacting with chloramine-t, the cyanogen chloride then reacts with a combination of barbituric acid and isonicotinic acid to form a highly colored complex. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CR-CR6-IC-WT Soil Hexavalent Chromium in Soil SW A/7199 This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). EC-R511-WT Soil Conductivity-O.Reg 153/04 (July 2011) MOEE E3138 A representative subsample is tumbled with de-ionized (DI) water. The ratio of water to soil is 2:1 v/w. After tumbling the sample is then analyzed by a conductivity meter. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). HG CVAA-WT Soil Mercury in Soil by CVAAS EPA 200.2/1631E (mod) Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). MET CCMS-WT Soil Metals in Soil by CRC ICPMS EPA 200.2/6020A (mod) Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CRC ICPMS. Method Limitation: This method is not a total digestion technique. It is a very strong acid digestion that is intended to dissolve those metals that may be environmentally available. This method does not dissolve all silicate materials and may result in a partial extraction. depending on the sample matrix, for some metals, including, but not limited to Al, Ba, Be, Cr, Sr, Ti, Tl, and V. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Soil ABN-Calculated Parameters SW MOISTURE-WT PAH-511-WT Soil Soil Moisture PAH-O.Reg 153/04 (July 2011) Gravimetric: Oven Dried SW /8270 A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported).

46 G15100 Reference Information L CONTD... Page 18 of AUG-15 :35 (MT) PCB-511-WT Soil PCB-O.Reg 153/04 (July 2011) SW /8082 An aliquot of a solid sample is extracted with a solvent, extract is cleaned up and analyzed on the GC/MS. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). PH-R511-WT Soil ph-o.reg 153/04 (July 2011) MOEE E3137A A minimum 10g portion of the sample is extracted with 20mL of 0.01M calcium chloride solution by shaking for at least 30 minutes. The aqueous layer is separated from the soil and then analyzed using a ph meter and electrode. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). SAR-R511-WT Soil SAR-O.Reg 153/04 (July 2011) SW C A dried, disaggregated solid sample is extracted with deionized water, the aqueous extract is separated from the solid, acidified and then analyzed using a ICP/OES. Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). SO4-WT Soil Sulphate EPA *** ALS test methods may incorporate modifications from specified reference methods to improve performance. Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/l - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation. Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review. Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information.

47 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 1 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed B-HWS-R511-WT Soil Batch R WG DUP Boron (B), Hot Water Ext. L WG IRM Boron (B), Hot Water Ext. SALINITY_SOIL WG MB Boron (B), Hot Water Ext. < 0.1 WG MS Boron (B), Hot Water Ext. L N/A MS-B - CL-R511-WT Soil Batch R WG DUP Chloride L AUG-15 WG Chloride LCS AUG-15 WG Chloride MB < AUG-15 WG Chloride MS L AUG-15 CN-WAD-R511-WT Soil Batch R WG DUP Cyanide, Weak Acid Diss L RPD-NA N/A 35 WG LCS Cyanide, Weak Acid Diss WG MB Cyanide, Weak Acid Diss 0.05 WG MS Cyanide, Weak Acid Diss L CR-CR6-IC-WT Soil Batch R WG CRM Chromium, Hexavalent WT-SQC WG DUP Chromium, Hexavalent L <0.20 <0.20 RPD-NA N/A 35 WG LCS Chromium, Hexavalent WG MB

48 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 2 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed CR-CR6-IC-WT Soil Batch R WG MB Chromium, Hexavalent < EC-R511-WT Soil Batch R WG DUP Conductivity WG ms/cm WG Conductivity LCS WG Conductivity LCS WG Conductivity MB < ms/cm HG CVAA-WT Soil Batch R WG CRM Mercury (Hg) WT-CANMET-TILL WG Mercury (Hg) DUP WG < < RPD-NA N/A 40 WG Mercury (Hg) LCS WG Mercury (Hg) MB < mg/kg Batch R WG CRM Mercury (Hg) WT-CANMET-TILL WG Mercury (Hg) DUP WG WG Mercury (Hg) LCS WG Mercury (Hg) MB < mg/kg MET CCMS-WT Soil Batch R WG CRM Antimony (Sb) WT-CANMET-TILL Arsenic (As) 109.8

49 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 3 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed MET CCMS-WT Soil Batch R WG CRM Barium (Ba) WT-CANMET-TILL Beryllium (Be) Cadmium (Cd) 97.2 Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) 91.9 Molybdenum (Mo) Nickel (Ni) Selenium (Se) 89.3 Silver (Ag) 96.8 Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) WG Antimony (Sb) DUP WG < RPD-NA N/A 30 Arsenic (As) Barium (Ba) Beryllium (Be) < RPD-NA N/A 30 Boron (B) <5.0 <5.0 RPD-NA N/A 30 Cadmium (Cd) RPD-NA N/A 30 Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Molybdenum (Mo) 0.43 J Nickel (Ni) Selenium (Se) <0.20 RPD-NA N/A 30 Silver (Ag) <0.20 < RPD-NA N/A 40 Thallium (Tl) RPD-NA N/A 30 Uranium (U) Vanadium (V)

50 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 4 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed MET CCMS-WT Soil Batch R WG DUP Zinc (Zn) WG WG Antimony (Sb) LCS Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) WG Antimony (Sb) MB < mg/kg 0.1 Arsenic (As) < mg/kg 0.1 Barium (Ba) mg/kg 0.5 Beryllium (Be) < mg/kg 0.1 Boron (B) <5.0 mg/kg 5 Cadmium (Cd) <0.020 mg/kg 0.02 Chromium (Cr) mg/kg 0.5 Cobalt (Co) < mg/kg 0.1 Copper (Cu) mg/kg 0.5 Lead (Pb) mg/kg 0.5 Molybdenum (Mo) < mg/kg 0.1 Nickel (Ni) mg/kg 0.5 Selenium (Se) <0.20 mg/kg 0.2

51 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 5 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed MET CCMS-WT Soil Batch R WG MB Silver (Ag) < mg/kg 0.1 Thallium (Tl) mg/kg 0.05 Uranium (U) mg/kg 0.05 Vanadium (V) <0.20 mg/kg 0.2 Zinc (Zn) <2.0 mg/kg 2 Batch R WG CRM Antimony (Sb) WT-CANMET-TILL Arsenic (As) Barium (Ba) 99.7 Beryllium (Be) 87.2 Cadmium (Cd) 92.8 Chromium (Cr) Cobalt (Co) 10 Copper (Cu) 97.0 Lead (Pb) 92.8 Molybdenum (Mo) 97.5 Nickel (Ni) Selenium (Se) 89.7 Silver (Ag) 96.1 Thallium (Tl) 95.1 Uranium (U) Vanadium (V) Zinc (Zn) 97.5 WG Antimony (Sb) DUP WG < RPD-NA N/A 30 Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu)

52 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 6 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed MET CCMS-WT Soil Batch R WG DUP Lead (Pb) WG Molybdenum (Mo) Nickel (Ni) Selenium (Se) <0.20 RPD-NA N/A 30 Silver (Ag) <0.20 < RPD-NA N/A 40 Thallium (Tl) RPD-NA N/A 30 Uranium (U) Vanadium (V) Zinc (Zn) WG Antimony (Sb) LCS Arsenic (As) Barium (Ba) Beryllium (Be) Boron (B) Cadmium (Cd) Chromium (Cr) Cobalt (Co) Copper (Cu) Lead (Pb) Molybdenum (Mo) Nickel (Ni) Selenium (Se) Silver (Ag) Thallium (Tl) Uranium (U) Vanadium (V) Zinc (Zn) WG Antimony (Sb) MB < mg/kg 0.1 Arsenic (As) < mg/kg 0.1 Barium (Ba) mg/kg 0.5 Beryllium (Be) < mg/kg 0.1 Boron (B) <5.0 mg/kg 5

53 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 7 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed MET CCMS-WT Soil Batch R WG MB Cadmium (Cd) <0.020 mg/kg 0.02 Chromium (Cr) mg/kg 0.5 Cobalt (Co) < mg/kg 0.1 Copper (Cu) mg/kg 0.5 Lead (Pb) mg/kg 0.5 Molybdenum (Mo) < mg/kg 0.1 Nickel (Ni) mg/kg 0.5 Selenium (Se) <0.20 mg/kg 0.2 Silver (Ag) < mg/kg 0.1 Thallium (Tl) mg/kg 0.05 Uranium (U) mg/kg 0.05 Vanadium (V) <0.20 mg/kg 0.2 Zinc (Zn) <2.0 mg/kg 2 MOISTURE-WT Soil Batch R WG DUP Moisture L WG Moisture LCS WG Moisture MB < 0.1 PAH-511-WT Soil Batch R WG DUP 1-Methylnaphthalene WG <0.030 <0.030 RPD-NA N/A 40 2-Methylnaphthalene <0.030 <0.030 RPD-NA N/A 40 Acenaphthene RPD-NA N/A 40 Acenaphthylene RPD-NA N/A 40 Anthracene RPD-NA N/A 40 Benzo(a)anthracene RPD-NA N/A 40 Benzo(a)pyrene RPD-NA N/A 40 Benzo(b)fluoranthene RPD-NA N/A 40 Benzo(g,h,i)perylene RPD-NA N/A 40 Benzo(k)fluoranthene RPD-NA N/A 40

54 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 8 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed PAH-511-WT Soil Batch R WG DUP Chrysene WG RPD-NA N/A 40 Dibenzo(ah)anthracene RPD-NA N/A 40 Fluoranthene RPD-NA N/A 40 Fluorene RPD-NA N/A 40 Indeno(1,2,3-cd)pyrene RPD-NA N/A 40 Naphthalene RPD-NA N/A 40 Phenanthrene RPD-NA N/A 40 Pyrene RPD-NA N/A 40 WG IRM 1-Methylnaphthalene ALS PAH1 RM Methylnaphthalene Acenaphthene 69.9 Acenaphthylene Anthracene 67.3 Benzo(a)anthracene Benzo(a)pyrene 92.9 Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene 76.7 Chrysene Dibenzo(ah)anthracene Fluoranthene Fluorene 71.2 Indeno(1,2,3-cd)pyrene 94.3 Naphthalene 96.0 Phenanthrene Pyrene WG LCS 1-Methylnaphthalene Methylnaphthalene 89.0 Acenaphthene 90.9 Acenaphthylene 91.1 Anthracene 91.3 Benzo(a)anthracene 89.0

55 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 9 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed PAH-511-WT Soil Batch R WG LCS Benzo(a)pyrene 92.4 Benzo(b)fluoranthene 88.5 Benzo(g,h,i)perylene 77.5 Benzo(k)fluoranthene 89.2 Chrysene 93.7 Dibenzo(ah)anthracene 80.8 Fluoranthene 89.7 Fluorene 91.9 Indeno(1,2,3-cd)pyrene 79.1 Naphthalene 89.7 Phenanthrene 89.6 Pyrene 95.4 WG MB 1-Methylnaphthalene < Methylnaphthalene < Acenaphthene 0.05 Acenaphthylene 0.05 Anthracene 0.05 Benzo(a)anthracene 0.05 Benzo(a)pyrene 0.05 Benzo(b)fluoranthene 0.05 Benzo(g,h,i)perylene 0.05 Benzo(k)fluoranthene 0.05 Chrysene 0.05 Dibenzo(ah)anthracene 0.05 Fluoranthene 0.05 Fluorene 0.05 Indeno(1,2,3-cd)pyrene 0.05 Naphthalene 0.05 Phenanthrene 0.05 Pyrene 0.05 Surrogate: 2-Fluorobiphenyl 89.5 Surrogate: p-terphenyl d 88.0 PCB-511-WT Soil

56 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 10 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed PCB-511-WT Soil Batch R WG DUP Aroclor 1242 WG <0.010 <0.010 RPD-NA N/A AUG-15 Aroclor 1248 <0.010 <0.010 RPD-NA N/A AUG-15 Aroclor 1254 <0.010 <0.010 RPD-NA N/A AUG-15 Aroclor 1260 <0.010 <0.010 RPD-NA N/A AUG-15 WG Aroclor 1242 LCS AUG-15 Aroclor AUG-15 Aroclor AUG-15 Aroclor AUG-15 WG Aroclor 1242 MB < AUG-15 Aroclor 1248 < AUG-15 Aroclor 1254 < AUG-15 Aroclor 1260 < AUG-15 Surrogate: d-terphenyl AUG-15 WG Aroclor 1242 MS WG AUG-15 Aroclor AUG-15 Aroclor AUG-15 PH-R511-WT Soil Batch R WG DUP ph L J ph units WG ph LCS 7.03 ph units SAR-R511-WT Soil Batch R WG DUP Calcium (Ca) WG mg/l Sodium (Na) mg/l Magnesium (Mg) mg/l WG Calcium (Ca) IRM WT SAR Sodium (Na) 99.5 Magnesium (Mg) 96.1

57 Quality Control Report Workorder: L Report Date: 25-AUG-15 Page 11 of Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Test Matrix Reference Result Qualifier Units RPD Limit Analyzed SAR-R511-WT Soil Batch R WG MB Calcium (Ca) mg/l 1 Sodium (Na) mg/l 1 Magnesium (Mg) mg/l 1 SO4-WT Soil Batch R WG CRM Sulphate AN-CRM-WT WG Sulphate DUP L <20 RPD-NA mg/kg N/A 30 WG Sulphate LCS WG Sulphate MB <20 mg/kg 20

58 Workorder: L Quality Control Report Report Date: 25-AUG-15 Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Page 12 of Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate Sample Parameter Qualifier Definitions: Qualifier Description J MS-B RPD-NA Duplicate results and limits are expressed in terms of absolute difference. Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. Relative Percent Difference Not Available due to result(s) being less than detection limit.

59 Workorder: L Quality Control Report Report Date: 25-AUG-15 Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Page 13 of Hold Time Exceedances: ALS Product Description Physical Tests Moisture Leachable Anions & Nutrients Cyanide (WAD)-O.Reg 153/04 (July 2011) Polycyclic Aromatic Hydrocarbons Sample ID Sampling Date Date Processed Rec. HT Actual HT Chloride-O.Reg 153/04 (July 2011) Cyanides PAH-O.Reg 153/04 (July 2011) Legend & Qualifier Definitions: EHTR-FM: EHTR: EHTL: EHT: Rec. HT: JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL-15 16:17 16:18 16:19 16:20 16:21 16:22 16:23 16:24 16:25 16:26 16:27 16:28 16:29 16:30 16:31 16:32 16:33 25-AUG-15 01:34 25-AUG-15 01:35 25-AUG-15 01:36 18-AUG-15 19:43 18-AUG-15 19:44 18-AUG-15 19:45 18-AUG-15 19:46 18-AUG-15 19:47 18-AUG-15 19:48 18-AUG-15 19:49 18-AUG-15 19:50 18-AUG-15 19:51 18-AUG-15 19:52 18-AUG-15 19:53 18-AUG-15 16:18 18-AUG-15 16:19 18-AUG-15 16:20 18-AUG-15 16:21 18-AUG-15 16:22 18-AUG-15 16:23 18-AUG-15 16:24 Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended. Exceeded ALS recommended hold time prior to sample receipt. Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry. Exceeded ALS recommended hold time prior to analysis. ALS recommended hold time (see units) Units days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days days Qualifier EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHT EHT EHT EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR EHTR

60 Workorder: L Quality Control Report Report Date: 25-AUG-15 Client: Contact: CHUNG AND VANDER DOELEN 311 VICTORIA ST. N. KITCHENER ON N2H 5E1 ERIC CHUNG Page of Notes*: Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes. Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt is used for calculation purposes. Samples for L were received on 18-AUG-15 12:00. ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS. The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against predetermined data quality objectives to provide confidence in the accuracy of associated test results. Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.