Wetting agents for improved compatibility in WATERBORNE COATINGs

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1 Wetting agents for improved compatibility in WATERBORNE COATINGs

2 Contents How to select the right wetting agent for a tinted coating system? Performance improved by the wetting agent Increased tinting strength Reduced rub-out effects Improved substrate wetting on metal and/or polyethylene Reduced water absorption Possible influences by the wetting agent Impact on storage stability Impact on gloss Impact on scrub resistance Impact on foaming Our product recommendation Wetting agents for acrylic lacquers Wetting agents for emulsion paints Product technical, safety and regulatory information

3 How to select the right wetting agent for a tinted coating system? Wetting agents are added to waterborne coatings to increase the wetting of the substrate, to improve the compatibility with pigments and other components, as well as, to reduce rub-out effects. At the same time wetting agents might have an influence on the coating s storage stability, gloss, scrub resistance and foaming behavior. Tinted paints are highly complex systems. It can be a technical challenge for the paint formulator to select the right wetting agent to develop a stable, high performing coating formulation, especially when considering that the product s sustainability aspects, such as low VOC / SVOC or ecolabel suitability, need to be taken into account. The industry can choose from a variety of wetting agent chemistries. As a key supplier to paint formulators, Clariant understands that it is important to a paint formulator to identify in a short time the most appropriate product which solves formulation problems with respect to incompatibility. Clariant has therefore evaluated its range of wetting agents for acrylic lacquers and emulsion paints according to the following set of parameters. Our objective is to deliver our customers the best application solution for a long-lasting and sustainable business. Influence on the coating formulation Performance boosted by wetting agents Performance parameter Acrylic lacquers Emulsion paints Tinting strength Rub-out Substrate wetting on metal and polyethylene Water absorption Possible influences of wetting agent Storage stability Impact on gloss Scrub resistance Foaming behavior

4 Performance improved by the wetting agent Increased tinting strength To achieve the full tinting strength potential of tinted coatings, the fillers and pigments must be well dispersed during formulation. A re-agglomeration of the particles should be avoided throughout the coating production, storage, application and drying. A low tinting strength in a coating can be caused by inefficient pigment-dispersion or re-agglomeration, as well as, pigment flocculation, which is also known as rub-out. Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard Tinting strength defined as 100% Tinting strength increased by up to 10% Tinting strength increased by more than 10% good performance excellent performance

5 Reduced rub-out effects A rub-out test is performed by rubbing the coating film with a finger while it is still moist but already starting to dry. In doing so the agglomerated pigments are being separated, which leads to an increased tinting strength at the rubbed spot. The bigger the difference in color intensity between the rubbed spot and the unrubbed area, the bigger the rub-out problem. Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard Strong rub-out effects Slight rub-out effects No rub-out good performance excellent performance

6 Improved substrate wetting on metal and/or polyethylene Substrate wetting enables uniform coating application. Good wetting is a prerequisite for optimal adhesion. Defects in the coating surface such as craters need to be minimized. Substrate wetting on metal Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard No adhesion of coating on metal substrate Good adhesion of coating on metal substrate Excellent adhesion of coating on metal substrate good performance excellent performance Substrate wetting on polyethylene Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard No adhesion of coating on polyethylene substrate Good adhesion of coating on polyethylene substrate Excellent adhesion of coating on polyethylene substrate good performance excellent performance

7 Reduced water absorption Surfactants have an influence on the film-forming properties of the coating formulation, which can lead to an increased resistance against water absorption. Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard High absorption of water into the coating film Moderate absorption of water into the coating film No absorption of water into the coating film good performance excellent performance

8 Possible influences by the wetting agent Impact on storage stability The use of wetting agent can have a negative influence on the paint stability. Paint formulators therefore try to select the additive with the lowest impact. To evaluate the paint stability a coating is stored at room temperature and at 50 C in the oven for 28 days. Paint stability refers to the interaction of the different ingredients at room temperature compared to the influence of heat storage through measurement of viscosity, sedimentation and syneresis. Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard Stable viscosity, no sedimentation or syneresis Moderate influence on viscosity, sedimentation and syneresis No or marginal influence on viscosity, sedimentation and syneresis moderate impact no impact Impact on gloss Coatings are classified or categorized by different gloss levels. There are high gloss, semi-gloss and matte paints available on the market. For a paint formulator it is important that the addition of a wetting agent to the formulation has little or no influence on the final gloss property. The difference of specular reflection of a coating surface can be measured with a gloss meter.

9 Impact on scrub resistance The use of a wetting agent can have a negative impact on the scrub resistance. Paint formulators, therefore, try to select the additive with the lowest influence. Standard procedures for determining the resistance of wall paints against abrasion by scrubbing are, for example, ASTM D 4213 or DIN EN ISO These standards describe the various testing methods for components and formulation systems used in waterborne interior wall and ceiling coatings. Coating without wetting agent Defined as standard Coating with wetting agent Comparison against defined standard: Scrub resistance defined as 100% Reducing film thickness moderately No change of film thickness or only marginal influence moderate impact no impact Impact on foaming Foam formation is caused by the entry of gas into the liquid formulation. This can happen during the production process when the coating is stirred or mixed. One possible source of foam is surfactants in the formulation. The foam behavior can be measured by determining the density of the liquid paint with a density meter. A higher density indicates less air is integrated in the paint formulation.

10 Our product recommendation Wetting agents for acrylic lacquers Clariant s wetting agents were evaluated against the described performance parameters in a glossy water-based acrylic lacquer that is VOC-free and resistant against blocking. The wetting agent was used as post additive in the following formulation (position 12). It also possible to use the wetting agent during the pre-mixing process step. POS Process step Product function Product description Product active content Product by weight percent 1 Solvent Water 15.00% 2 Pre-Mixing Binder Pure acrylate MFT 1 C; TG -10/50; particle size 0.10 µm 50% 15.00% 3 Dispersing agent Polyacrylate 45% 0.20% 4 Neutralization Ammonia 25% 0.30% 6 Defoamer Organic modified polysiloxane 25% 0.20% Grinding 6 Filler Titanium dioxide, rutile-type, coated with Al + Zr 100% 17.50% 7 Binder Pure acrylate MFT 1 C; TG -10/50; particle size 0.10 µm 50% 45.00% 8 Thickener Polyacrylate 30% 2.00% 9 Let-down Solvent Water 3.50% 10 Preservative Isothiazolinone MIT + BIT 2.5% 0.10% 11 Defoamer Organic modified polysiloxane 25% 0.20% 12 Post addition Wetting agent e.g. Genapol ED % 1.00%

11 Product recommendation Performance benefits Impact on formulation Product name Ionicity Active dosage in acrylic lacquer (PVC 20-50) Supply dosage in acrylic lacquer (PVC 20-50) Increased tinting strength Reduced rub-out Improved substrate wetting on metal Improved substrate wetting on polyethylene Reduced water absorbtion Reduced impact on storage stability Reduced impact on gloss Reduced impact on foaming Dispersogen MT 200 Nonionic 1.0% - 1.5% 1.0% - 1.5% Dispersogen PL 30 Nonionic 1.0% - 1.5% 1.0% - 1.5% Dispersogen AN 200 Anionic 1.2% - 1.5% 1.5% - 1.9% Dispersogen ECS Anionic 1.0% - 1.5% 3.3% - 5.0% Dispersogen LFS Anionic 1.0% - 1.5% 1.0% - 1.5% Emulsogen LCN 118 Nonionic 1.0% - 1.5% 1.3% % Emulsogen LCN 158 Nonionic 1.0% - 1.5% 1.3% % Emulsogen LCN 287 Nonionic 1.0% - 1.5% 1.4% - 2.1% Emulsogen TS 100 Nonionic 1.2% - 1.5% 1.2% - 1.5% Emulsogen TS 200 Nonionic 1.0% - 1.5% 1.0% - 1.5% Genapol ED 3060 Nonionic 1.0% - 1.5% 1.0% - 1.5% Genapol O 080 Nonionic 1.2% - 1.5% 1.2% - 1.5% Genapol O 100 Nonionic 1.0% - 1.5% 1.0% - 1.5% Legend excellent performance good performance no impact moderate impact

12 Wetting agents for emulsion paints Clariant s wetting agents were evaluated against the described performance parameters in a matte water-based emulsion paint for indoor and outdoor use, categorized under the scrub-resistance class 2 according to ISO The wetting agent was used as post additive in the following formulation (position 18). It also possible to use the wetting agent during the pre-mixing process step. POS Process step Product function Product description Product active content Product by weight percent 1 Solvent Water 22.00% 2 Thickener Cellulose 100% 0.30% 3 Pre-Mixing Neutralizing agent Caustic soda 10% 1.00% 4 Dispersing agent Polyacrylate 45% 0.40% 5 Defoamer Organic modified polysiloxane 25% 0.30% 6 Titanium dioxide, rutile-type, coated with Al + Zr 100% 10.00% 7 Talc d50 = 10µm 100% 8.00% 8 Kaolin clay d50 = 5µm 100% 3.00% 9 Grinding Filler Calcium carbonate PCC d50 = 1 µm 100% 5.00% 10 Calcium carbonate GCC d50 = 2µm 100% 8.00% 11 Calcium carbonate GCC d50= 5 µm 100% 10.00% 12 Calcium carbonate GCC d50= 10 µm 100% 5.00% 13 Binder Pure acrylate MFT 2 C; TG 13; particle size µm 53% 22.00% 14 Preservative Isothiazolinone MIT + BIT 2.5% 0.20% 15 Let-down Defoamer Organic modified polysiloxane 25% 0.30% 16 Thickener Acrylate 30% 2.50% 17 Solvent Water 1.25% 18 Post addition Wetting agent e.g. Emulsogen TS % 0.75%

13 Product recommendation Performance benefits Impact on formulation Product name Ionicity Active dosage in emulsion paints (PVC 40-80) Supply dosage in emulsion paints (PVC 40-80) Increased tinting strength Reduced rub-out Reduced impact on storage stability Reduced impact on scrub resistance Reducing impact on gloss Reduced impact on foaming Dispersogen AN 200 Anionic 0.5% - 1.5% 0.6% % Dispersogen ECS Anionic 0.5% - 1.0% 1.7% % Dispersogen MT 200 Nonionic 1.0% - 1.5% 1.0% - 1.5% Dispersogen PL 30 Nonionic 0.5% - 1.0% 0.5% - 1.0% Dispersogen LFS Anionic 1.0% - 1.5% 1.0% - 1.5% Emulsogen TS 200 Nonionic 1.0% - 1.5% 1.0% - 1.5% Emulsogen TS 100 Nonionic 0.5% - 1.0% 0.5% - 1.0% Genapol B Nonionic 1.0% - 1.5% 1.0% - 1.5% Genapol ED 3060 Nonionic 0.5% - 1.5% 0.5% - 1.5% Genapol O 080 Nonionic 0.5% - 1.0% 0.5% - 1.0% Genapol O 100 Nonionic 0.5% - 1.5% 0.5% - 1.5% Legend excellent performance good performance no impact moderate impact

14 Product technical, safety and regulatory information Technical data Environmental & safety properties Product name Ionicity Active content Appearance Ecolabel APEO-free 2 VOC SVOC Hazard suitability 1 Label 3 Ecotain Label Dispersogen AN 200 Anionic 80% Brownish, clear liquid < 0.1% < 7.0 % label free Dispersogen ECS Anionic 30% Yellowish, clear liquid < 0.1% < 3.0 % label free Dispersogen MT 200 Nonionic 100% Brownish liquid < 0.1% < 1.0 % label free Dispersogen PL 30 Nonionic 100% Viscous, cloudy liquid < 1.0% < 2.0 % label free Dispersogen LFS Anionic 100% Brownish, viscous liquid < 3.0% < 4.0 % label-free Emulsogen LCN 118 Nonionic 80% Clear liquid < 1.0% < 2.0% Emulsogen LCN 158 Nonionic 80% Clear liquid < 1.0% < 1.0% Emulsogen LCN 287 Nonionic 70% Clear liquid < 1.0% < 1.0% label free Emulsogen TS 100 Nonionic 100% Yellow turbid liquid, high viscous < 0.1% < 3.0% label free Emulsogen TS 200 Nonionic 100% Yellowish paste < 0.1% < 3.0 % label free Genapol B Nonionic 100% Brownish, viscous liquid < 1.0% < 0.8% label free Genapol ED 3060 Nonionic 100% Yellowish liquid < 1.0% < 1.0% label free Genapol O 080 Nonionic 100% Clear, viscous liquid < 0.2% < 3.0% Genapol O 100 Nonionic 100% White paste < 0.1% < 1.2% Legend 1 Product is suitable for paints and colorants that comply with the criteria of the European Ecoflower (2008/4453/EC; 2008/4452/EC), the German Blue Angel (RAL UZ 102:2010 and UZ 12a 11:2015), the Scandinavian Nordic Swan ( ) and the French NF Environment (NF130:2012). 2 Free of alkylphenol ethoxylates 3 Hazard label (GHS/CLP) is according to the Globally Harmonized System (GHS) of classification, labeling and packaging of chemical substances and mixtures. 4 EcoTain is Clariant s label for sustainability excellence products and solutions. It sets an ambitious benchmark and distinguishes itself by exceeding market standards while considering the overall benefits and impacts across the entire life cycle. Each product labeled as EcoTain goes through a systematic, in-depth screening process using 36 criteria in all three sustainability dimensions, i.e. social, environmental and economic.

15 regulatory information product name REACH (Status Clariant EU) AICS (Australia) DSL (Canada) ENCS (Japan) IECSC (China) KECI (Korea) NECI (Taiwan) NZIOC (New Zealand) PICCS (Philippines) TSCA (USA) Dispersogen AN Dispersogen ECS Dispersogen MT Dispersogen PL Dispersogen LFS Emulsogen TS Emulsogen TS Emulsogen LCN Emulsogen LCN Emulsogen LCN Genapol B Genapol ED Genapol O Genapol O Regulatory status as of

16 Clariant International Ltd BU Industrial & Consumer Specialties Rothausstrasse Muttenz Switzerland Sales & Marketing Phone: Application Development Phone: This information corresponds to the present state of our knowledge and is intended as a general description of our products and their possible applications. Clariant makes no warranties, express or implied, as to the information s accuracy, adequacy, sufficiency or freedom from defect and assumes no liability in connection with any use of this information. Any user of this product is responsible for determining the suitability of Clariant s products for its particular application. * Nothing included in this information waives any of Clariant s General Terms and Conditions of Sale, which control unless it agrees otherwise in writing. Any existing intellectual/industrial property rights must be observed. Due to possible changes in our products and applicable national and international regulations and laws, the status of our products could change. Material Safety Data Sheets providing safety precautions, that should be observed when handling or storing Clariant products, are available upon request and are provided in compliance with applicable law. You should obtain and review the applicable Material Safety Data Sheet information before handling any of these products. For additional information, please contact Clariant. Trademark of Clariant registered in numerous countries. * For sales to customers located within the United States and Canada the following applies in addition: NO EXPRESS OR IMPLIED WARRANTY IS MADE OF THE MERCHANTABILITY, SUITABILITY, FITNESS FOR A PARTICULAR PURPOSE OR OTHERWISE OF ANY PRODUCT OR SERVICE Clariant International AG, Rothausstrasse 61, 4132 Muttenz, Schweiz Product and service marks protected by Clariant

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