EQUIPMENT PARTICLE ANALYSIS

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1 Sample ID: TAM-ST Sample Date: Equip. Desc.: Storage Tank Received Date: 7/20/2000 Reservoir Cap.: 3000 Gal.(s) L(s) Prev. Sample: #REF! UKN Machine Time: Not Prov Hrs. First Sample: Lube Time: Not Prov Hrs. Recommendation(s): FILTER LUBRICANT to remove excessive levels of lubricant degradation, in the form of tramp oil (petroleum based product). Discussion of Test Results: The equipment particle concentration (EPC) of 88,764 is much higher than expected for a fluid of this type. Analytical results show the presence of excessive concentration of lubricant degradation in the form of tramp oil (petroleum based product). Lubricant degradation in the form of tramp oil (petroleum based product) not only clogs return ports, valves and filters but will also contribute to the over all poor performance of rotating equipment. Additional the presence of petroleum reduce the fire retardant capabilities of this fluid. Note that this was the FIRST sample tested from this equipment. QUANTITATIVE TESTING: NAS-1638 Particle Count ISO-4406 Cleanliness Rating ASTM-D Viscosity at 40 C > ,000 10,000 1, ISO 4406 Code Small Large Centastokes (cst) % Spec..-10% QUALITATIVE TESTING: Ferrous Wear: Nonferrous Metals: Contaminants: Rating Max. Rating Max. Rating Max. Classification um Classification um Classification um Rubbing 15 Rubbing Lube Degradtion N/A Severe Sliding Severe Sliding Sand/Dirt N/A Cutting Cutting Fibers Rolling Cont. (Brg.) Rolling Cont.(Brg.) Spheres Spheres Spheres Plastic/Ceramic Black Oxides (Fe 3 O 4 ) N/A Oxides Particle Count Misc. Data Red Oxides (Fe 2 O 3 ) Other ,568 PLP: 41.9% Corrosive (FeO) ,757 ISO Scale 23/22 Other Composition(s) Copper White Babbitt ,274 Visc. cst: SUS 100F ph: 9.44 EPC: 88,764 Alk. Resv. N/A 1952 PdM Analyst: NBR 1.1

2 Sample ID: TAM-ST Sample Date: Equip. Desc.: Storage Tank Received Date: 7/20/2000 Reservoir Cap.: 3000 Gal.(s) L(s) Prev. Sample: #REF! UKN Machine Time: Not ProvHrs. First Sample: Lube Time: Not ProvHrs. IMAGE 1 IMAGE 2 Shown in this image are examples of the high concentration of Lubricant Degradation (tramp oil). Note that this image was taken under low magnification to show the extent of the problem. This image was left blank. Light: White Reflected & Green Transmitted Light: 100X 95 µm 00X 0 µm 1952 PdM Analyst: NBR 1.2

3 Sample ID: TAM-PRCY Sample Date: Equip. Desc.: Pump Room Central System Received Date: 7/20/2000 Reservoir Cap.: 1200 Gal.(s) 4542 L(s) Prev. Sample: #REF! UKN Machine Time: Not Prov Hrs. First Sample: Lube Time: Not Prov Hrs. Recommendation(s): CHECK AIR FILTERS & BREATHER ELEMENTS, where present, to ensure proper working condition. FILTER LUBRICANT to remove excessive levels of lubricant degradation and outside contaminants. Discussion of Test Results: The equipment particle concentration (EPC) of 84,720 is much higher than expected for this type of equipment. Analytical results show the presence of excessive concentration of lubricant degradation in both forms of tramp oil (petroleum based product) and varnish & lacquer. Test results also show the presence eof natural fiber material. This natural fiber material appears to be composed of cellulose (paper) media. Damaged air filter or breather elements are permitting the entry of outside (sand & dirt) contamination into this system. Lubricant degradation in the form of tramp oil (petroleum based product) not only clogs return ports, valves and filters but will also contribute to the over all poor performance of rotating equipment. Additional the presence of petroleum reduce the fire retardant capabilities of this fluid. Note that this was the FIRST sample tested from this equipment. QUANTITATIVE TESTING: NAS-1638 Particle Count ISO-4406 Cleanliness Rating ASTM-D Viscosity at 40 C > ,000 10,000 1, ISO 4406 Code Small Large Centastokes (cst) % Spec..-10% QUALITATIVE TESTING: Ferrous Wear: Nonferrous Metals: Contaminants: Rating Max. Rating Max. Rating Max. Classification um Classification um Classification um Rubbing 15 Rubbing Lube Degradtion N/A Severe Sliding Severe Sliding Sand/Dirt N/A Cutting Cutting Fibers N/A Rolling Cont. (Brg.) Rolling Cont.(Brg.) Spheres Spheres Spheres Plastic/Ceramic Black Oxides (Fe 3 O 4 ) N/A Oxides Particle Count Misc. Data Red Oxides (Fe 2 O 3 ) Other ,663 PLP: 37.8% Corrosive (FeO) ,832 ISO Scale 23/22 Other Composition(s) Copper White Babbitt ,123 Visc. cst: SUS 100F ph: 9.15 EPC: 84,720 Alk. Resv. N/A 1953 PdM Analyst: NBR 2.3

4 Sample ID: TAM-PRCY Sample Date: Equip. Desc.: Pump Room Central System Received Date: 7/20/2000 Reservoir Cap.: 1200 Gal.(s) 4542 L(s) Prev. Sample: #REF! UKN Machine Time: Not ProvHrs. First Sample: Lube Time: Not ProvHrs. IMAGE 1 IMAGE 2 Shown in this image is an example of the natuiral fiber material (cellulose). This image displays examples of the outside sand & dirt contamination with rings of tram oil surrounding the debris. Light: White Reflected & Green Transmitted Light: White Reflected & Green Transmitted 200X 75 µm 100X 90 µm 1953 PdM Analyst: NBR 2.4

5 Sample ID: TAM-PS Sample Date: Equip. Desc.: Pusher System Received Date: 7/20/2000 Reservoir Cap.: 600 Gal.(s) 2271 L(s) Prev. Sample: #REF! UKN Machine Time: Not Prov Hrs. First Sample: Lube Time: Not Prov Hrs. Recommendation(s): FILTER LUBRICANT to remove excessive levels of lubricant degradation and Metal Oxides. Then continue regular operation. Sample this equipment at a routine time interval. Discussion of Test Results: The equipment particle concentration (EPC) of 20,030 is much higher than expected for this type of equipment. Analytical results show the presence of excessive concentration of lubricant degradation in both forms of tramp oil (petroleum based product) and varnish & lacquer. Testing also show the presence of Black Metal Oxides (Fe 3 O 4 ). Black Oxides form as the result of heat due to friction from improper or inadequate lubrication during the formation of the particles. Lubricant degradation in the form of tramp oil (petroleum based product) not only clogs return ports, valves and filters but will also contribute to the over all poor performance of this equipment. Additional the presence of petroleum reduce the fire retardant capabilities of this fluid. Note that this was the FIRST sample tested from this equipment. QUANTITATIVE TESTING: NAS-1638 Particle Count ISO-4406 Cleanliness Rating ASTM-D Viscosity at 40 C > ,000 10,000 1, ISO 4406 Code Small Large Centastokes (cst) % Spec..-10% QUALITATIVE TESTING: Ferrous Wear: Nonferrous Metals: Contaminants: Rating Max. Rating Max. Rating Max. Classification um Classification um Classification um Rubbing 15 Rubbing Lube Degradtion N/A Severe Sliding Severe Sliding Sand/Dirt N/A Cutting Cutting Fibers Rolling Cont. (Brg.) Rolling Cont.(Brg.) Spheres Spheres Spheres Plastic/Ceramic Black Oxides (Fe 3 O 4 ) N/A Oxides Particle Count Misc. Data Red Oxides (Fe 2 O 3 ) Other ,003 PLP: 10.1% Corrosive (FeO) ,512 ISO Scale 21/18 Other Composition(s) Copper White Babbitt Visc. cst: SUS 100F ph: 9.09 EPC: 20,030 Alk. Resv. N/A 1954 PdM Analyst: NBR 3.5

6 Sample ID: TAM-PS Sample Date: Equip. Desc.: Pusher System Received Date: 7/20/2000 Reservoir Cap.: 600 Gal.(s) 2271 L(s) Prev. Sample: #REF! UKN Machine Time: Not ProvHrs. First Sample: Lube Time: Not ProvHrs. IMAGE 1 IMAGE 2 Shown in this image are examples of the Black Metal Oxides seen in this equipment. This image displays examples of the Black Metal Oxides and Varnish & Lacquer contamination. Light: White Reflected & Green Transmitted Light: White Reflected & Green Transmitted 500X 35 µm 500X 30 µm 1954 PdM Analyst: NBR 3.6

7 Sample ID: TAM-SS Sample Date: Equip. Desc.: Straightener System Received Date: 7/20/2000 Reservoir Cap.: Ukn Gal.(s) ##### L(s) Prev. Sample: #REF! UKN Machine Time: Not Prov Hrs. First Sample: Lube Time: Not Prov Hrs. Recommendation(s): CHANGE OIL FILTER. FILTER LUBRICANT to remove excessive levels of lubricant degradation and outside contaminants. Then continue regular operation. Sample this equipment at a routine time interval. Discussion of Test Results: The equipment particle concentration (EPC) of 17,879 is much higher than expected for this type of equipment. Analytical results show the presence of excessive concentration of lubricant degradation in both forms of tramp oil (petroleum based product) and varnish & lacquer. Additionally test results show the presence of Black Metal Oxides (Fe 3 O 4 ) and outside contaminants (sand & dirt). Many of these contaminants are much greater than 10 micrometer (um) indicating the oil filter is in by-pass. Lubricant degradation in the form of tramp oil (petroleum based product) not only clogs return ports, valves and filters but will also contribute to the over all poor performance of this equipment. Additional the presence of petroleum reduce the fire retardant capabilities of this fluid. Note that this was the FIRST sample tested from this equipment. QUANTITATIVE TESTING: NAS-1638 Particle Count ISO-4406 Cleanliness Rating ASTM-D Viscosity at 40 C > ,000 10,000 1, ISO 4406 Code Small Large Centastokes (cst) % Spec..-10% QUALITATIVE TESTING: Ferrous Wear: Nonferrous Metals: Contaminants: Rating Max. Rating Max. Rating Max. Classification um Classification um Classification um Rubbing 15 Rubbing Lube Degradtion N/A Severe Sliding Severe Sliding Sand/Dirt N/A Cutting Cutting Fibers Rolling Cont. (Brg.) Rolling Cont.(Brg.) Spheres Spheres Spheres Plastic/Ceramic Black Oxides (Fe 3 O 4 ) N/A Oxides Particle Count Misc. Data Red Oxides (Fe 2 O 3 ) Other ,467 PLP: 13.5% Corrosive (FeO) ,994 ISO Scale 21/18 Other Composition(s) Copper White Babbitt Visc. cst: SUS 100F ph: 9.05 EPC: 17,879 Alk. Resv. N/A 1954 PdM Analyst: NBR 4.7

8 Sample ID: TAM-SS Sample Date: Equip. Desc.: Straightener System Received Date: 7/20/2000 Reservoir Cap.: Ukn Gal.(s) ##### L(s) Prev. Sample: #REF! UKN Machine Time: Not ProvHrs. First Sample: Lube Time: Not ProvHrs. IMAGE 1 IMAGE 2 Shown in this image are examples of the Black Metal Oxides, Outside contaminants and Tramp Oil contamination seen in this equipment. Note the size of these oxides particles are in excess of 250um conglomerate. This image was left blank. Light: White Reflected & Green Transmitted Light: 100X 95 µm 00X 0 µm 1954 PdM Analyst: NBR 4.8

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