SCOPE OF ACCREDITATION TO ISO/IEC 17025:2005

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1 SCOPE OF ACCREDITATION TO ISO/IEC 17025:2005 VALE CANADA LTD. COPPER CLIFF ANALYTICAL SERVICES 18 Rink Street Copper Cliff, Ontario P0M 1N0 Canada Mr. Claude Serre Phone: CHEMICAL Valid To: September 30, 2018 Certificate Number: In recognition of the successful completion of the A2LA evaluation process, accreditation is granted to this laboratory to perform the following tests on these materials/matrices: copper electrolytes, EW copper cathodes, copper anodes, nickel, nickel alloys and salts, nickel oxides (FRM, FEN, FEW, FMW, FRW), cobalt and cobalt oxide, copper and nickel concentrates and mattes (MRF, MEF, MK, MY, BM), plant intermediates, auto-catalysts, environmental waters and effluents, liquid sulfur dioxide, sulfuric acid and oleum, occupational exposure monitoring samples (CS 2 in air, inhalable and respirable dust, oil mist, respirable combustible dust, α-quartz, elements and H 2 SO 4 on filters, nickel speciation, non-dietary arsenic and nickel in urine). Description Colorimetry: Determination of Fe in H 2 SO 4 Determination of NOx in H 2 SO 4 Determination of Percent Transmittance in H 2 SO 4 SP-011 SP-013 SP-016 Electrochemical Methods: Determination of Ammonia Nitrogen in Waters and Effluents Determination of ph in Waters and Effluents Determination of Conductivity in Waters and Effluents ENV-001 ENV-009 ENV-010 Fire Assay: Fire Assay Preparation of Solid Samples for Platinum, Gold, Palladium, Rhodium, and Silver PM-160 (A2LA Cert. No ) Revised 07/28/2017 Page 1 of 4

2 Description Electroplating: Determination of Cu and Ni in Process / Customer Materials by Acid Dissolution / Electro-deposition Determination of Cu in Refinery Samples by Acid Dissolution / Electro-deposition Determination of Ni in Refinery Samples by Acid Dissolution / Electro-deposition GL-161 NR-001 NR-002 Flame Atomic Absorption Spectrometry (FAAS): Determination of Cu, Ni, Co and Fe in Refinery Samples by FAAS Determination of Fe in Nickel Powders and Pellets by La Collection / FAAS NR-009 NR-052 Graphite Furnace Atomic Absorption Spectrometry (GF-AAS): Determination of Se and Te in Electrolyte Solutions by GF-AAS Determination of As, Se and Te in EW Copper Cathodes by GF-AAS Determination of Nickel in Urine by PE-AA600 GF-AAS EW-005 EW-014 NR-026 Gas Chromatography Mass Spectrometry (GC-MS): Determination of CS 2 on 3M Organic Vapor Monitors by Extraction / GC-MS OEMP-110 Gravimetry: Determination of Baghouse Dust by Gravimetric Analysis Determination of Total Suspended Solids by Gravimetry Determination of Total Dissolved Solids in Water and Effluent by Gravimetry Determination of Specific Gravity in E/W Slurries by Gravimetry Determination of Oil Mist on Personal Monitoring Membranes by Gravimetry Determination of Inhalable and Respirable Dust by Gravimetry ENV-025 ENV-002 ENV-015 EW-009 OEMP-106 OEMP-107 Ion Chromatography (IC): Determination of Cl -, F -, NO 2 -, NO 3 -, PO 4 3-, and SO 4 2- in Water by IC ENV-008 Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES): Determination of Ag, Al, As, B, Ba, Be, Bi, Ca, Cd, Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, P, Pb, S, Sb, Se, Si, Sn, Te, Ti, V, Zn, and Zr in Waters by ICP-OES Determination of Total Hardness (CaCO 3 ) in Waters and Effluents by ICP-OES Determination of Ca, Co, K and Na in Ni Products by ICP-OES Determination of Al 2 O 3, As, Ba, Bi, CaO, Cd, Co, CrO 3, Cu, Fe, K, Li, MgO, Mn, Mo, Ni, P, Pb, S, Sb, Se, Si, SiO 2, Sn, TiO 2, V, and Zn in Various Samples by Sodium Peroxide Fusion / ICP-OES (TSPG) ENV-003 ENV-012 FP-007 GL-001 (A2LA Cert. No ) Revised 07/28/2017 Page 2 of 4

3 Description Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) (cont d): Determination of As, CaO, Co, Cu, Ni, Fe, S, Cr, MgO, SiO 2 and Pb in Mills Samples by Sodium Peroxide Fusion / ICP-OES (Mills Task) Determination of Cu, Co and Ni in Process / Customer Materials by Acid Dissolution / ICP-OES (PMET) Determination of Elements and Sulphuric Acid Mist on Filters by ICP-OES (Ag, Al, As, Ba, Be, Bi, Ca, Cd, Co, Cr, Cu, Fe, Mg, Mn, Na, Ni, P, Pb, Pd, Pt, Rh, S, Sb, Se, Sn, Te, Ti, V, Zn) Chemical Speciation of Ni Phases in Industrial Dust by Sequential Leaching / ICP- OES (Soluble, Sulfidic, Metallic, Oxidic) The Dissolution and ICP Analysis of Lead Prills from Fire Assay for Pt, Pd, Rh, Au, and Ag. Inductively Coupled Plasma-Mass Spectrometry (ICP-MS): Determination of Trace Elements in Waters and Effluents by ICP-MS (Al, Cr, Mn, As, Se, Mo, Ag, Cd, Hg, Tl, Pb) Determination of Trace Elements in Ni, Co, their Oxides and Salts by Y Collection / ICP-MS (Be, B, Al, Si, P, Ti, V, Cr, Fe, Mn, Ga, As, Se, Mo, In, Sn, Sb, Te, Pb, Bi) Determination of Trace Elements in Ni, Co, their oxides and Salts by ICP-MS (Na, Mg, Cu, Zn, Ag, Cd, Ba, Hg, Tl, Ni) Determination of Ge, Hf, Nb, Re, Ta, Th, U, W and Zr in Ni Products by ICP-MS Determination of Ni, Co, Zn, and Ag in EW Cu Cathodes by ICP-MS Determination of Trace Elements (Fe, As, Se, Sn, Sb, Te, Pb, Bi) in Cu Cathodes by Y Collection / ICP-MS Determination of Precious Metals and Trace Elements in Cu Anodes by ICP-MS (V, Cr, Fe, Mn, Co, Ni, Zn, As, Se, Ru, Rh, Pd, Ag, Cd, Sn, Sb, Te, Ba, Ir, Pt, Au, Pb, Bi) Determination of Trace Impurities in Ni Oxide by Pressure Dissolution / ICP-MS (Mg, Al, P, Ca, Ti, V, Cr, Mn, Fe, Zn, As, Se, Cd, Sn, Sb, Te, Tl, Pb, Bi) Determination of Ag, Au, Ir, Pd, Pt, Rh and Ru in Ni Oxide and Other Products by Pressure Dissolution / ICP-MS Determination of Non-dietary As in Urine by Extraction / ICP-MS (Sum of As3, As5, Monomethylarsenic Acid, Dimethylarsenic Acid) Leco Combustion: Determination of C and S in Metal-bearing Ores and Other Samples by LECO CS-400 (High) Determination of C and S in Metal-bearing Ores and Other Samples by LECO CS-844 (Low) Determination of O 2 in Nickel Powders and Pellets by LECO RO-416DR GL-109 GL-162 OEMP-104 OEMP-105 PM-161 ENV-005 FP-001 FP-003 FP-006 FP-011 FP-014 FP-021 FP-023 FP-024 OEMP-103 NR-003 NR-004 NR-006 Titration: Determination of Alkalinity as CaCO 3 by Titration Determination of Acidity by Titration Determination of Permanganate Oxidizable Matter (POM) in H 2 SO 4 ENV-006 ENV-007 SP-014 (A2LA Cert. No ) Revised 07/28/2017 Page 3 of 4

4 Description Titration (cont d): Determination of SO 2 in H 2 SO 4 by I 2 Titration SP-015 X-ray Diffraction (XRD): Determination of Respirable -Quartz on Silver Membrane OEMP-101 X-ray Fluorescence Spectrometry (XRF): General Procedure for Metallurgical Sample Analyses by XRF Determination of Cu, Ni, Co, Fe, Pb, As, Ca, Zn, Cr 2 O 3 and SiO2 in FBR Products by XRF Determination of Ni, Pb, Fe and As in Anode Copper by XRF Determination of Cu, Ni, Co, Fe, Pb, As, Ca, Zn, Cr 2 O 3, and Si in Monthly Samples by XRF Analyses of Furnace Matte and Slag Samples by XRF XRF-001 XRF-006 XRF-007 XRF-008 XRF-009 (A2LA Cert. No ) Revised 07/28/2017 Page 4 of 4

5 Accredited Laboratory A2LA has accredited VALE CANADA LTD. COPPER CLIFF ANALYTICAL SERVICES Copper Cliff, Ontario, Canada for technical competence in the field of Chemical Testing This laboratory is accredited in accordance with the recognized International Standard ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISO-ILAC-IAF Communiqué dated 8 January 2009). Presented this 22 nd day of September, President and CEO For the Accreditation Council Certificate Number Valid to September 30, 2018 Revised July 27, 2017 For the tests to which this accreditation applies, please refer to the laboratory s Chemical Scope of Accreditation.

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