Participating Schedule for 2018/19

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1 Participating Schedule for /19 Water Chemical Analysis Sample Name Analytes Enrolment Date Sample Dispatch Period Quarter 1 of Sample 3A: Mineral Constituents in potable water ph, Electrical Conductivity, Dissolved 180 C, Turbidity, Colour, Nitrate, Nitrite, Fluoride, Sulphate, Chloride, Ammonia, Sodium, Potassium, Calcium, Magnesium and Alkalinity (TA) Sample 3B: Colour Colour Sample 3D: Mercury Mercury Sample 4A: Trihalomethane Bromoform, Bromodichloromethane, Bibromochloromethane and Chloroform Sample 1F: Cyanide Weak Acid Dissociable (WAD) Cyanide, and Free Cyanide March Sample 1G: Chromium VI (Hexavalent) Chromium VI (Hexavalent) March Sample 4E: Diesel Organics Diesel Range organics (DRO) in water March Sample 4F: Oil and Grease Oil and Grease March Page 1 of 15

2 Participating Schedule for /19 Quarter 2 of Sample 1A: Metals in water Antimony (Sb), Aluminium (Al), Arsenic, Barium (Ba), Beryllium (Be), Boron (B),Cadmium (Cd),Chromium (Cr), Cobalt (Co), Copper (Cu), Iron (Fe),Lead (Pb),,Manganese (Mn), Molybdenum (Mo), Nickel (Ni), Selenium (Se), Silicon (Si), Strontium (Sr),Thorium (Th) Vanadium (V), Zinc (Zn), Silver (Ag) and Zirconium (Zr) March Sample 1B: Gold Gold (Au) March Sample 1C: Lithium Lithium March Sample 1D: Uranium Uranium March 03 rd to 6 th April 03 rd to 6 th April 03 rd to 6 th April 03 rd to 6 th April Sample 1E: Silica Free (reactive & dissolved) Silica, Colloidal Silica (Calculation) and Silica March 03 rd to 6 th April Sample 2H: Settleable Solid Settleable Solid (SS) March 03 rd to 6 th April Sample 1H: Metals in Waste Water Arsenic, Boron (B), Cadmium (Cd), Chromium, Copper (Cu), Iron (Fe),Lead (Pb),Manganese (Mn), Selenium (Se), Thallium (Tl), Tellurium (Te), Mercury (Hg) and its compound April 4 th May Sample 1I: Tin and Titanium Tin and Titanium April 4 th May Sample 2A: Nutrients in Water Nitrogen, Nitrate, Ammonia, Orthophosphate, Oxygen Absorbed, Chemical Oxygen Demand, Dissolved Organic Carbon, Organic Carbon, Biochemical Oxygen Demand (5 days), Methylene Blue Active Substances and Non-Ionic Surfactants April 30 rd April to 4 th May Sample 2B: Phosphate and TKN Phosphate and Kjeldahl Nitrogen (TKN) April 4 th May Page 2 of 15

3 Participating Schedule for /19 Sample 2C: Nitrite Nitrite April Sample 2D: TSS,TDS and TS Suspended Solids, Dissolved Solids and Solids April 4 th May 4 th May Sample 3A: Mineral Constituents in ground water ph, Electrical Conductivity, Dissolved 180 C, Turbidity, Colour, Nitrate, Nitrite, Fluoride, Sulphate, Chloride, Ammonia, Sodium, Potassium, Calcium, Magnesium and Alkalinity (TA) April 04 th May Sample 3B: Colour Colour April Sample 3C: Chromium Chromium April Sample 3D: Mercury Mercury April Sample 3E: Acidity Acidity April Sample 4A: Trihalomethane Bromoform, Bromodichloromethane, Bibromochloromethane and Chloroform April Sample 1F: Cyanide Weak Acid Dissociable (WAD) Cyanide, and Free Cyanide May Sample 1G: Chromium VI (Hexavalent) Chromium VI (Hexavalent) May 4 th May 04 th May 04 th May 04 th May 04 th May June June Sample 2E: Poly Aromatic Acenaphthene, Acenaphthylene, Anthracene, Benz(a)anthracene, th Benz(a)pyrene,Benzo(b)flouranthene, Benzo(k)flouranthene, 04 to 08 th Benzo(b/k)flouranthene(sum), Benzo(ghi)perylene, Chrysene, May June Page 3 of 15

4 Participating Schedule for /19 (PAH) Sample 2F: Sludge Dibenz(ah)anthraces, Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene, PAH % total 105 C (TS), % Volatile solids 550 C (VSS) (Volatiles Suspended Solid), Volatile Fatty Acids (VFA), Volatile Suspended Solids/ Solids (Calculated), Paste PH May June Sample 2G: Volatile Organic Compounds Acetone, Acetonitrile, Acrolein, Acrylonitrile, Benzene, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, 2-Butanone (MEK), n-butylbenzene, sec- Butylbenzene, tert-butylbenzene, tert-butyl methyl ether (MTBE), Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethylvinylether, Chloroform, Chloromethane, 2-Chlorotoluene, 4-Chlorotoluene, 1,2- Dibromo-3-chloropropane (DBCP), 1,2-Dibromoethane (EDB), Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4- Dichlorobenzene, Dichlorodifluoromethane (Freon 12), 1,1- Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethylene, cis-1,2- Dichloroethylene, trans-1,2-dichloroethylene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis- 1,3-Dichloropropylene, trans-1,3-dichloropropylene, Ethylbenzene, Hexachlorobutadiene, Hexachloroethane, 2-Hexanone, Isopropylbenzene, 4-Isopropyltoluene, Methylene chloride, 4-Methyl- 2-pentanone (MIBK), Naphthalene, Nitrobenzene, n-propylbenzene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethylene, Toluene, 1,2,3-Trichlorobenzene, 1,2,4- Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2 Trichloroethane, Trichloroethylene, Trichlorofluoromethane, 1,2,3-Trichloropropane (TCP), 1,2,4-Trimethylbenzene, 1,3,5-Trimethylbenzene, Vinyl acetate, Vinyl chloride, m-xylene, m&p-xylene, o-xylene, p-xylene, Xylenes, total May June Sample 4B: Phenols Benzoic acid, 4-Chloro-3-methylphenol, 2-Chlorophenol, 2,4- Dichlorophenol, 2,6-Dichlorophenol, 2,4-Dimethylphenol, 4,6-Dinitro- 2-methylphenol, 2,4-Dinitrophenol, 2-Methylphenol, 4-Methylphenol, 2-Nitrophenol, 4-Nitrophenol, Pentachlorophenol, Phenol, 2,3,4,6- Tetrachlorophenol, 2,4,5-Trichlorophenol and 2,4,6-Trichlorophenol May June Sample 4C : th TPH (C10-C40), TPH Aliphatic>C10-C12, TPH Aliphatic>C12-C16, 04 to 08 th TPH Aliphatic C16-C21, TPH Aliphatic>C21-C35, TPH Aliphatic>C35-C40, May June Page 4 of 15

5 Participating Schedule for /19 Petroleum (TPH) Sample 4D: BTEX compounds TPH Aromatic>EC10-EC12, TPH Aromatic>EC12-EC16, TPH Aromatic>EC16-EC21, TPH Aromatic>EC21-EC35, TPH Aromatic>EC35- EC40 Benzene, tert-butyl methyl ether (MTBE),Ethylbenzene, Toluene, m- Xylene, m&p-xylene, o-xylene, p-xylene, Xylenes, total June Sample 4E: Diesel Organics Diesel Range organics (DRO) in water May Sample 4F: Oil and Grease Oil and Grease May June June Quarter 3 of Sample 1A: Metals in water Antimony (Sb), Aluminium (Al), Arsenic, Barium (Ba), Beryllium (Be), Boron (B),Cadmium (Cd),Chromium (Cr), Cobalt (Co), Copper (Cu), Iron (Fe),Lead (Pb),,Manganese (Mn), Molybdenum (Mo), Nickel (Ni), Selenium (Se), Silicon (Si), Strontium (Sr),Thorium (Th) Vanadium (V), Zinc (Zn), Silver (Ag) and Zirconium (Zr) June Sample 1B: Gold Gold (Au) June Sample 1C: Lithium Lithium June Sample 1D: Uranium Uranium June 02 nd to 06 th July 02 nd to 06 th July 02 nd to 06 th July 02 nd to 06 th July Sample 1E: Silica Free (reactive & dissolved) Silica, Colloidal Silica (Calculation) and Silica June 02 nd to 06 th July Sample 2H: Settleable Solid Settleable Solid (SS) June Sample 1H: Heavy Metals in Waste Water Arsenic, Boron (B), Cadmium (Cd), Chromium, Copper (Cu), Iron (Fe),Lead (Pb),Manganese (Mn), Selenium (Se), Thallium (Tl), Tellurium (Te), Mercury (Hg) and its compound July 02 nd to 06 th July Page 5 of 15

6 Participating Schedule for /19 Sample 1I: Tin and Titanium Tin and Titanium July Sample 2A: Nutrients in Water Nitrogen, Nitrate, Ammonia, Orthophosphate, Oxygen Absorbed, Chemical Oxygen Demand, Dissolved Organic Carbon, Organic Carbon, Biochemical Oxygen Demand (5 days), Methylene Blue Active Substances and Non-Ionic Surfactants July Sample 2B: Phosphate and TKN Phosphate and Kjeldahl Nitrogen (TKN) July Sample 2C: Nitrite Nitrite July Sample 2D: TSS,TDS and TS Suspended Solids, Dissolved Solids and Solids July Synthetic Sample 3A: Mineral Constituents in water ph, Electrical Conductivity, Dissolved 180 C, Turbidity, Colour, Nitrate, Nitrite, Fluoride, Sulphate, Chloride, Ammonia, Sodium, Potassium, Calcium, Magnesium and Alkalinity (TA) July Sample 3B: Colour Colour July Sample 3C: Chromium Chromium July Sample 3D: Mercury Mercury July Sample 3E: Acidity Acidity July Sample 4A: Bromoform, Bromodichloromethane, Bibromochloromethane and July Page 6 of 15

7 Participating Schedule for /19 Trihalomethane Chloroform Sample 1F: Cyanide Weak Acid Dissociable (WAD) Cyanide, and Free Cyanide Sample 1G: Chromium VI (Hexavalent) Chromium VI (Hexavalent) Sample 2E: Poly Aromatic (PAH) Sample 2F: Sludge Acenaphthene, Acenaphthylene, Anthracene, Benz(a)anthracene, Benz(a)pyrene,Benzo(b)flouranthene, Benzo(k)flouranthene, Benzo(b/k)flouranthene(sum), Benzo(ghi)perylene, Chrysene, Dibenz(ah)anthraces, Fluoranthene, Fluorene, Indeno(1,2,3- cd)pyrene, Naphthalene, Phenanthrene, Pyrene, PAH % total 105 C (TS), % Volatile solids 550 C (VSS) (Volatiles Suspended Solid), Volatile Fatty Acids (VFA), Volatile Suspended Solids/ Solids (Calculated), Paste PH Sample 2G: Volatile Organic Compounds: Volatiles Organic Compounds Acetone, Acetonitrile, Acrolein, Acrylonitrile, Benzene, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, 2-Butanone (MEK), n-butylbenzene, sec-butylbenzene, tert-butylbenzene, tert-butyl methyl ether (MTBE), Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethylvinylether, Chloroform, Chloromethane, 2-Chlorotoluene, 4-Chlorotoluene, 1,2- Dibromo-3-chloropropane (DBCP), 1,2-Dibromoethane (EDB), Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4- Dichlorobenzene, Dichlorodifluoromethane (Freon 12), 1,1- Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethylene, cis-1,2- Dichloroethylene, trans-1,2-dichloroethylene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis- 1,3-Dichloropropylene, trans-1,3-dichloropropylene, Ethylbenzene, Hexachlorobutadiene, Hexachloroethane, 2- Hexanone, Isopropylbenzene, 4-Isopropyltoluene, Methylene chloride, 4-Methyl-2-pentanone (MIBK), Naphthalene, Nitrobenzene, n-propylbenzene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2- Tetrachloroethane, Tetrachloroethylene, Toluene, 1,2,3- Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2 Trichloroethane, Trichloroethylene, Trichlorofluoromethane, Page 7 of 15

8 Participating Schedule for /19 1,2,3-Trichloropropane (TCP), 1,2,4-Trimethylbenzene, 1,3,5- Trimethylbenzene, Vinyl acetate, Vinyl chloride, m-xylene, m&p- Xylene, o-xylene, p-xylene, Xylenes, total Sample 4B: Phenols Sample 4C : Petroleum (TPH) Sample 4D: BTEX compounds Benzoic acid, 4-Chloro-3-methylphenol, 2-Chlorophenol, 2,4- Dichlorophenol, 2,6-Dichlorophenol, 2,4-Dimethylphenol, 4,6- Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2-Methylphenol, 4- Methylphenol, 2-Nitrophenol, 4-Nitrophenol, Pentachlorophenol, Phenol, 2,3,4,6-Tetrachlorophenol, 2,4,5-Trichlorophenol and 2,4,6- Trichlorophenol TPH (C10-C40), TPH Aliphatic>C10-C12, TPH Aliphatic>C12-C16, TPH Aliphatic C16-C21, TPH Aliphatic>C21-C35, TPH Aliphatic>C35- C40, TPH Aromatic>EC10-EC12, TPH Aromatic>EC12-EC16, TPH Aromatic>EC16-EC21, TPH Aromatic>EC21-EC35, TPH Aromatic>EC35-EC40 Benzene, tert-butyl methyl ether (MTBE),Ethylbenzene, Toluene, m- Xylene, m&p-xylene, o-xylene, p-xylene, Xylenes, total Sample 4E: Diesel Organics Diesel Range organics (DRO) in water Sample 4F: Oil and Grease Oil and Grease Quarter 4 of Sample 1A: Metals in water Antimony (Sb), Aluminium (Al), Arsenic, Barium (Ba), Beryllium (Be), Boron (B),Cadmium (Cd),Chromium (Cr), Cobalt (Co), Copper (Cu), Iron (Fe),Lead (Pb),,Manganese (Mn), Molybdenum (Mo), Nickel (Ni), Selenium (Se), Silicon (Si), Strontium (Sr),Thorium (Th) Vanadium (V), Zinc (Zn), Silver (Ag) and Zirconium (Zr) September 01 th to 05 th Oct Sample 1B: Gold Gold (Au) September 01 th to 05 th Oct Sample 1C: Lithium Lithium September 01 th to 05 th Oct Page 8 of 15

9 Participating Schedule for /19 Sample 1D: Uranium Uranium September 01 th to 05 th Oct Sample 1E: Silica Free (reactive & dissolved) Silica, Colloidal Silica (Calculation) and Silica September 01 th to 05 th Oct Sample 2H: Settleable Solid Settleable Solid (SS) September 01 th to 05 th Oct Sample 1H: Heavy Metals in Waste Water Arsenic, Boron (B), Cadmium (Cd), Chromium, Copper (Cu), Iron (Fe),Lead (Pb),Manganese (Mn), Selenium (Se), Thallium (Tl), Tellurium (Te), Mercury (Hg) and its compound Sample 1I: Tin and Titanium Tin and Titanium Sample 2A: Nutrients in Water Nitrogen, Nitrate, Ammonia, Orthophosphate, Oxygen Absorbed, Chemical Oxygen Demand, Dissolved Organic Carbon, Organic Carbon, Biochemical Oxygen Demand (5 days), Methylene Blue Active Substances and Non-Ionic Surfactants Sample 2B: Phosphate and TKN Phosphate and Kjeldahl Nitrogen (TKN) Sample 2C: Nitrite Nitrite Sample 2D: TSS,TDS and TS Suspended Solids, Dissolved Solids and Solids Sample 3A: Mineral Constituents in potable water ph, Electrical Conductivity, Dissolved 180 C, Turbidity, Colour, Nitrate, Nitrite, Fluoride, Sulphate, Chloride, Ammonia, Sodium, Potassium, Calcium, Magnesium and Alkalinity (TA) Sample 3B: Colour Colour Page 9 of 15

10 Participating Schedule for /19 Sample 3C: Chromium Chromium Sample 3D: Mercury Mercury Sample 3E: Acidity Acidity Sample 4A: Trihalomethane Bromoform, Bromodichloromethane, Bibromochloromethane and Chloroform Sample 1F: Cyanide Weak Acid Dissociable (WAD) Cyanide, and Free Cyanide Sample 1G: Chromium VI (Hexavalent) Chromium VI (Hexavalent) Sample 2E: Poly Aromatic (PAH) Sample 2F: Sludge Acenaphthene, Acenaphthylene, Anthracene, Benz(a)anthracene, Benz(a)pyrene,Benzo(b)flouranthene, Benzo(k)flouranthene, Benzo(b/k)flouranthene(sum), Benzo(ghi)perylene, Chrysene, Dibenz(ah)anthraces, Fluoranthene, Fluorene, Indeno(1,2,3- cd)pyrene, Naphthalene, Phenanthrene, Pyrene, PAH % total 105 C (TS), % Volatile solids 550 C (VSS) (Volatiles Suspended Solid), Volatile Fatty Acids (VFA), Volatile Suspended Solids/ Solids (Calculated), Paste PH Sample 2G: Volatile Organic Compounds Acetone, Acetonitrile, Acrolein, Acrylonitrile, Benzene, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, 2-Butanone (MEK), n-butylbenzene, sec-butylbenzene, tert-butylbenzene, tert-butyl methyl ether (MTBE), Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethylvinylether, Chloroform, Chloromethane, 2-Chlorotoluene, 4-Chlorotoluene, 1,2- Dibromo-3-chloropropane (DBCP), 1,2-Dibromoethane (EDB), Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4- Dichlorobenzene, Dichlorodifluoromethane (Freon 12), 1,1- Page 10 of 15

11 Participating Schedule for /19 Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethylene, cis-1,2- Dichloroethylene, trans-1,2-dichloroethylene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis- 1,3-Dichloropropylene, trans-1,3-dichloropropylene, Ethylbenzene, Hexachlorobutadiene, Hexachloroethane, 2- Hexanone, Isopropylbenzene, 4-Isopropyltoluene, Methylene chloride, 4-Methyl-2-pentanone (MIBK), Naphthalene, Nitrobenzene, n-propylbenzene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2- Tetrachloroethane, Tetrachloroethylene, Toluene, 1,2,3- Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2 Trichloroethane, Trichloroethylene, Trichlorofluoromethane, 1,2,3-Trichloropropane (TCP), 1,2,4-Trimethylbenzene, 1,3,5- Trimethylbenzene, Vinyl acetate, Vinyl chloride, m-xylene, m&p- Xylene, o-xylene, p-xylene, Xylenes, total Sample 4B: Phenols Sample 4C : Petroleum (TPH) Sample 4D: BTEX compounds Benzoic acid, 4-Chloro-3-methylphenol, 2-Chlorophenol, 2,4- Dichlorophenol, 2,6-Dichlorophenol, 2,4-Dimethylphenol, 4,6- Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2-Methylphenol, 4- Methylphenol, 2-Nitrophenol, 4-Nitrophenol, Pentachlorophenol, Phenol, 2,3,4,6-Tetrachlorophenol, 2,4,5-Trichlorophenol and 2,4,6- Trichlorophenol TPH (C10-C40), TPH Aliphatic>C10-C12, TPH Aliphatic>C12-C16, TPH Aliphatic C16-C21, TPH Aliphatic>C21-C35, TPH Aliphatic>C35- C40, TPH Aromatic>EC10-EC12, TPH Aromatic>EC12-EC16, TPH Aromatic>EC16-EC21, TPH Aromatic>EC21-EC35, TPH Aromatic>EC35-EC40 Benzene, tert-butyl methyl ether (MTBE),Ethylbenzene, Toluene, m- Xylene, m&p-xylene, o-xylene, p-xylene, Xylenes, total Sample 4E: Diesel Organics Diesel Range organics (DRO) in water Sample 4F: Oil and Grease Oil and Grease Quarter 1 of Page 11 of 15

12 Participating Schedule for /19 Sample 1A: Metals in water Antimony (Sb), Aluminium (Al), Arsenic, Barium (Ba), Beryllium (Be), Boron (B),Cadmium (Cd),Chromium (Cr), Cobalt (Co), Copper (Cu), Iron (Fe),Lead (Pb),,Manganese (Mn), Molybdenum (Mo), Nickel (Ni), Selenium (Se), Silicon (Si), Strontium (Sr),Thorium (Th) Vanadium (V), Zinc (Zn), Silver (Ag) and Zirconium (Zr) December 07 th to 11 th Jan Sample 1B: Gold Gold (Au) December 07 th to 11 th Jan Sample 1C: Lithium Lithium December 07 th to 11 th Jan Sample 1D: Uranium Uranium December 07 th to 11 th Jan Sample 1E: Silica Free (reactive & dissolved) Silica, Colloidal Silica (Calculation) and Silica December 07 th to 11 th Jan Sample 2H: Settleable Solid Settleable Solid (SS) December 07 th to 11 th Jan Sample 1H: Heavy Metals in Waste Water Arsenic, Boron (B), Cadmium (Cd), Chromium (Cr), Copper (Cu), Iron (Fe),Lead (Pb),Manganese (Mn), Selenium (Se), Thallium (Tl), Tellurium (Te), Mercury (Hg) and its compound Sample 1I: Tin and Titanium Tin and Titanium Sample 2A: Nutrients in Water Nitrogen, Nitrate, Ammonia, Orthophosphate, Oxygen Absorbed, Chemical Oxygen Demand, Dissolved Organic Carbon, Organic Carbon, Biochemical Oxygen Demand (5 days), Methylene Blue Active Substances and Non-Ionic Surfactants Sample 2A: Nutrients in Water Phosphate and Kjeldahl Nitrogen (TKN) Sample 2B: Phosphate and Nitrite Page 12 of 15

13 Participating Schedule for /19 TKN Sample 2D: TSS,TDS and TS Suspended Solids, Dissolved Solids and Solids Sample 3A: Mineral Constituents in ground water ph, Electrical Conductivity, Dissolved 180 C, Turbidity, Colour, Nitrate, Nitrite, Fluoride, Sulphate, Chloride, Ammonia, Sodium, Potassium, Calcium, Magnesium and Alkalinity (TA) Sample 3B: Colour Colour Sample 3C: Chromium Chromium Sample 3D: Mercury Mercury Sample 3E: Acidity Acidity Sample 4A: Trihalomethane Bromoform, Bromodichloromethane, Bibromochloromethane and Chloroform Sample 1F: Cyanide Weak Acid Dissociable (WAD) Cyanide, and Free Cyanide Sample 1G: Chromium VI (Hexavalent) Chromium VI (Hexavalent) Sample 2E: Poly Aromatic (PAH) Acenaphthene, Acenaphthylene, Anthracene, Benz(a)anthracene, Benz(a)pyrene,Benzo(b)flouranthene, Benzo(k)flouranthene, Benzo(b/k)flouranthene(sum), Benzo(ghi)perylene, Chrysene, Dibenz(ah)anthraces, Fluoranthene, Fluorene, Indeno(1,2,3- cd)pyrene, Naphthalene, Phenanthrene, Pyrene, PAH Sample 2F: % total 105 C (TS), % Volatile solids 550 C (VSS) Page 13 of 15

14 Participating Schedule for /19 Sludge (Volatiles Suspended Solid), Volatile Fatty Acids (VFA), Volatile Suspended Solids/ Solids (Calculated), Paste PH Sample 2G: Volatile Organic Compounds Acetone, Acetonitrile, Acrolein, Acrylonitrile, Benzene, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, 2-Butanone (MEK), n-butylbenzene, sec-butylbenzene, tert-butylbenzene, tert-butyl methyl ether (MTBE), Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethylvinylether, Chloroform, Chloromethane, 2-Chlorotoluene, 4-Chlorotoluene, 1,2- Dibromo-3-chloropropane (DBCP), 1,2-Dibromoethane (EDB), Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4- Dichlorobenzene, Dichlorodifluoromethane (Freon 12), 1,1- Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethylene, cis-1,2- Dichloroethylene, trans-1,2-dichloroethylene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis- 1,3-Dichloropropylene, trans-1,3-dichloropropylene, Ethylbenzene, Hexachlorobutadiene, Hexachloroethane, 2- Hexanone, Isopropylbenzene, 4-Isopropyltoluene, Methylene chloride, 4-Methyl-2-pentanone (MIBK), Naphthalene, Nitrobenzene, n-propylbenzene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2- Tetrachloroethane, Tetrachloroethylene, Toluene, 1,2,3- Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2 Trichloroethane, Trichloroethylene, Trichlorofluoromethane, 1,2,3-Trichloropropane (TCP), 1,2,4-Trimethylbenzene, 1,3,5- Trimethylbenzene, Vinyl acetate, Vinyl chloride, m-xylene, m&p- Xylene, o-xylene, p-xylene, Xylenes, total Sample 4B: Phenols Sample 4C : Petroleum (TPH) Benzoic acid, 4-Chloro-3-methylphenol, 2-Chlorophenol, 2,4- Dichlorophenol, 2,6-Dichlorophenol, 2,4-Dimethylphenol, 4,6- Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2-Methylphenol, 4- Methylphenol, 2-Nitrophenol, 4-Nitrophenol, Pentachlorophenol, Phenol, 2,3,4,6-Tetrachlorophenol, 2,4,5-Trichlorophenol and 2,4,6- Trichlorophenol TPH (C10-C40), TPH Aliphatic>C10-C12, TPH Aliphatic>C12-C16, TPH Aliphatic C16-C21, TPH Aliphatic>C21-C35, TPH Aliphatic>C35- C40, TPH Aromatic>EC10-EC12, TPH Aromatic>EC12-EC16, TPH Aromatic>EC16-EC21, TPH Aromatic>EC21-EC35, TPH Aromatic>EC35-EC40 Page 14 of 15

15 Participating Schedule for /19 Sample 4D: BTEX compounds Benzene, tert-butyl methyl ether (MTBE),Ethylbenzene, Toluene, m- Xylene, m&p-xylene, o-xylene, p-xylene, Xylenes, total Sample 4E: Diesel Organics Diesel Range organics (DRO) in water Sample 4F: Oil and Grease Oil and Grease PT Deputy Coordinator: N Mutileni Signature Date: 11/12/17 (Compiler) PT Coordinator: MD Mawela (Pr Tech (Eng) Signature Date: 11/12/17 (Approver) Page 15 of 15