9848 ABERDEEN ROAD COLDSTREAM, BC V1B2K9 (250) 550-3741 SOIL ANALYSIS REVIEWED BY: Andrew Garrard, B.Sc., General Manager DATE REPORTED: Mar 09, 2016 PAGES (INCLUDING COVER): 12 VERSION*: 1 Should you require any information regarding this analysis please contact your client services representative at (778) 452-4000 *NOTES VERSION 1: Sample receipt temperature 1 C. All samples will be disposed of within 30 days following analysis. Please contact the lab if you require additional sample storage time. Laboratories (V1) Page 1 of 12 Member of: Association of Professional Engineers, Geologists and Geophysicists of Alberta (APEGGA) Western Enviro-Agricultural Laboratory Association (WEALA) Environmental Services Association of Alberta (ESAA) AGAT Laboratories is accredited to ISO/IEC 17025 by the Canadian Association for Laboratory Accreditation Inc. (CALA) and/or Standards Council of Canada (SCC) for specific tests listed on the scope of accreditation. AGAT Laboratories (Mississauga) is also accredited by the Canadian Association for Laboratory Accreditation Inc. (CALA) for specific drinking water tests. Accreditations are location and parameter specific. A complete listing of parameters for each location is available from www.cala.ca and/or www.scc.ca. The tests in this report may not necessarily be included in the scope of accreditation. All reportable information as specified by ISO 17025:2005 is available from AGAT Laboratories upon request
DATE RECEIVED: 2016-03-01 Parameter Unit SAMPLE DESCRIPTION: SAMPLE TYPE: DATE SAMPLED: G / S RDL Aluminum µg/g 10 Arsenic µg/g 0.1 Cadmium µg/g 0.01 Chromium µg/g 1 Cobalt µg/g 0.1 Copper µg/g 0.2 Lead µg/g 0.1 Mercury µg/g 0.01 Molybdenum µg/g 0.2 Nickel µg/g 0.5 Phosphorus µg/g 5 Selenium µg/g 0.1 Zinc µg/g 1 ph 1:2 ph units 0.1 Comments: RDL - Reported Detection Limit; G / S - Guideline / Standard 7414333-7414335 Results are based on the dry weight of the sample #1 Compost Certificate of Analysis British Columbia Metals Schedule 4 and 5 #2 Compost 2/29/2016 2/29/2016 7414333 7414335 32000 14400 4.0 3.7 0.42 0.43 20 19 5.5 5.1 36.3 34.3 16.3 20.6 0.05 0.05 1.6 1.1 16.3 13.3 1450 1790 0.9 0.7 100 100 8.3 8.6 DATE REPORTED: 2016-03-03 CERTIFICATE OF ANALYSIS (V1) Certified By: Page 2 of 12
DATE RECEIVED: 2016-03-01 C:N Ratio Parameter Unit SAMPLE DESCRIPTION: SAMPLE TYPE: DATE SAMPLED: G / S RDL Nitrogen - Total % 0.02 Organic Carbon-Total % 0.02 Comments: RDL - Reported Detection Limit; G / S - Guideline / Standard #1 Compost Certificate of Analysis #2 Compost 2/29/2016 2/29/2016 7414333 7414335 15.4 14.1 1.01 1.08 15.6 15.2 C:N Ratio DATE REPORTED: 2016-03-04 CERTIFICATE OF ANALYSIS (V1) Certified By: Page 3 of 12
DATE RECEIVED: 2016-03-01 Parameter Unit SAMPLE DESCRIPTION: SAMPLE TYPE: DATE SAMPLED: G / S RDL Available Ammonium (NH4 - N) mg/kg 1 Organic Matter by Loss on Ignition % 0.3 Comments: RDL - Reported Detection Limit; G / S - Guideline / Standard 7414333-7414335 * Analysis performed at AGAT Laboratories Calgary. #1 Compost Certificate of Analysis #2 Compost 2/29/2016 2/29/2016 7414333 7414335 13 8 31.5 31.4 Analysis - Organic Matter (LOI) / Ammonium DATE REPORTED: 2016-03-09 CERTIFICATE OF ANALYSIS (V1) Certified By: Page 4 of 12
DATE RECEIVED: 2016-03-01 Parameter Unit SAMPLE DESCRIPTION: SAMPLE TYPE: DATE SAMPLED: G / S RDL Total Organic Carbon % 0.15 Fraction Organic Carbon in 0.0015 Comments: RDL - Reported Detection Limit; G / S - Guideline / Standard 7414333-7414335 * Analysis performed at AGAT Laboratories Calgary. #1 Compost Certificate of Analysis #2 Compost 2/29/2016 2/29/2016 7414333 7414335 13.5 16.5 0.135 0.165 Analysis - Total Organic Carbon (W-B Wet Oxidation) DATE REPORTED: 2016-03-08 CERTIFICATE OF ANALYSIS (V1) Certified By: Page 5 of 12
DATE RECEIVED: 2016-03-01 Parameter Unit SAMPLE DESCRIPTION: SAMPLE TYPE: DATE SAMPLED: G / S RDL ph (Saturated Paste) ph units 0.1 Electrical Conductivity (Saturated Paste) ms/cm 0.01 Saturation Percentage % Comments: RDL - Reported Detection Limit; G / S - Guideline / Standard #1 Compost Certificate of Analysis ph, Electrical Conductivity - Saturate Paste #2 Compost 2/29/2016 2/29/2016 7414333 7414335 8.0 8.2 1.32 1.20 112 104 DATE REPORTED: 2016-03-04 CERTIFICATE OF ANALYSIS (V1) Certified By: Page 6 of 12
Quality Assurance Analysis RPT Date: DUPLICATE REFERENCE MATERIAL METHOD BLANK SPIKE MATRIX SPIKE PARAMETER Batch Sample Id Dup #1 Dup #2 RPD Method Blank Measured Value Acceptable Limits Lower Upper Acceptable Limits Recovery Lower Upper Acceptable Limits Recovery Lower Upper British Columbia Metals Schedule 4 and 5 Aluminum 7416186 12000 12300 2.7% < 10 110% 70% 130% 99% 90% 110% Arsenic 7416186 2.9 2.9 2.0% < 0.1 70% 70% 130% 100% 90% 110% Cadmium 7416186 0.06 0.05 11.1% < 0.01 83% 70% 130% 99% 90% 110% Chromium 7416186 20 21 4.3% < 1 110% 70% 130% 106% 90% 110% Cobalt 7416186 8.6 10.0 15.4% < 0.1 109% 70% 130% 103% 90% 110% Copper 7416186 33.6 34.3 2.2% < 0.2 103% 70% 130% 105% 90% 110% Lead 7416186 2.5 2.6 3.3% < 0.1 96% 70% 130% 98% 90% 110% Mercury 7416186 0.03 0.03 0.0% < 0.01 116% 70% 130% 91% 90% 110% Molybdenum 7416186 0.3 0.3 0.0% < 0.2 102% 70% 130% 102% 90% 110% Nickel 7416186 17.7 18.1 2.2% < 0.5 112% 70% 130% 106% 90% 110% Phosphorus 7416186 468 455 2.8% < 5 105% 70% 130% 94% 85% 115% Selenium 7416186 0.3 0.2 0.0% < 0.1 96% 90% 110% Zinc 7416186 38 37 3.2% < 1 108% 70% 130% 109% 90% 110% ph 1:2 7416186 9.2 9.2 0.0% < 0.1 100% 90% 110% 100% 95% 105% Comments: RPDs are calculated using raw analytical data and not the rounded duplicate values reported. ph, Electrical Conductivity - Saturate Paste ph (Saturated Paste) 7414333 20151 6.81 6.81 0.3% < 0.1 96% 80% 120% Electrical Conductivity (Saturated 7414333 20151 2.97 2.99 0.7% < 0.01 94% 80% 120% Paste) Saturation Percentage 7414333 20151 31.7 31.9 0.6% < 100% 80% 120% C:N Ratio Nitrogen - Total 7414333 7414333 1.01 1.02 0.4% < 0.02 98% 80% 120% Analysis - Total Organic Carbon (W-B Wet Oxidation) Total Organic Carbon 7417646 7417646 0.75 0.88 16.0% < 0.15 93% 80% 120% 91% 80% 120% Comments: If Matrix spike value is NA, the spiked analyte concentration was lower than that of the matrix contribution. If the RPD value is NA, the results of the duplicates are under 5X the RDL and will not be calculated. Analysis - Organic Matter (LOI) / Ammonium Available Ammonium (NH4 - N) 7414333 7414333 13 13 0.0% < 1 92% 80% 120% 100% 80% 120% 103% 80% 120% Organic Matter by Loss on Ignition 424 3.5 3.6 2.8% < 0.3 NA 80% 120% NA 80% 120% Certified By: QUALITY ASSURANCE REPORT (V1) Page 7 of 12 AGAT Laboratories is accredited to ISO/IEC 17025 by the Canadian Association for Laboratory Accreditation Inc. (CALA) and/or Standards Council of Canada (SCC) for specific tests listed on the scope of accreditation. AGAT Laboratories (Mississauga) is also accredited by the Canadian Association for Laboratory Accreditation Inc. (CALA) for specific drinking water tests. Accreditations are location and parameter specific. A complete listing of parameters for each location is available from www.cala.ca and/or www.scc.ca. The tests in this report may not necessarily be included in the scope of accreditation.
Analysis Aluminum Arsenic Cadmium Chromium Cobalt Copper Lead Mercury Molybdenum Nickel Phosphorus Selenium Zinc ph 1:2 PARAMETER MET-181-6106, MET-181-6106, INOR-181-6031 Method Summary AGAT S.O.P EPA 6010C EPA 6010C BC MOE Lab Manual B (ph, Electrometric, ) LITERATURE REFERENCE ANALYTICAL TECHNIQUE ICP/OES ICP/OES PH METER C:N Ratio Nitrogen - Total INOR-181-6027 Modified from ASTM E1019-11 COMBUSTION Available Ammonium (NH4 - N) SOIL 0630, INST 0420 SM 4500-NH3 G DISCRETE ANALYZER Organic Matter by Loss on Ignition SOIL 470 McKeague 3.81 COMBUSTION Total Organic Carbon SOIL 0480; SOIL 0110; SOIL NELSON 1996; SHEPPARD 2007 0120 SPECTROPHOTOMETER ph (Saturated Paste) LAB-181-4022 BC MOE Lab Manual Section B PH METER Electrical Conductivity (Saturated Paste) LAB-181-4022 BC MOE Lab Manual Section B CONDUCTIVITY METER Saturation Percentage LAB-181-4022 BC MOE Lab Manual Section B GRAVIMETRIC METHOD SUMMARY (V1) Page 8 of 12
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