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Available online at www.sciencedirect.com ScienceDirect Procedia Engineering 81 (2014 ) 1731 1736 11th International Conference on Technology of Plasticity, ICTP 2014, 19-24 October 2014, Nagoya Congress Center, Nagoya, Japan Hot stamping parts with tailored properties by local resistance heating Weikang Liang, Liang Wang, Yong Liu, Yilin Wang, Yisheng Zhang* State Key Laboratory of Material Processing and Die & Mould Technology, Huazhong University of Science and Technology Wuhan 430074, China Abstract Hot stamping parts, such as B-pillar, crash beams and bumpers, with the tailored mechanical properties, fulfil the requirements of anti-collision properties of the vehicle. In this work, a resistance heating system was developed in terms of Joule s Law. Local resistance heating was proposed to achieve the tailored mechanical properties of hot stamping parts by adjusting temperature distribution of the heated blank. The results indicated that the tailored temperature distribution of the blank was realized and the temperature field of the blank could be divided into three regions: high temperature, transition and unheated region. The Vickers hardness of high temperature region varied from 470 HV10 to 500 HV10. While for transition region, it ranged from 160 HV10 to 470 HV10, and that of the unheated region was 160±5 HV10. It demonstrated that the blank with tailed properties was obtained. 2014 The Authors.Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license Selection (http://creativecommons.org/licenses/by-nc-nd/3.0/). and peer-review under responsibility of Nagoya University and Toyohashi University of Technology. Selection and peer-review under responsibility of the Department of Materials Science and Engineering, Nagoya University Keywords: Hot stamping; Tailored properties; Local resistance heating; Tailored temperature distribution 1. Introduction With the requirements of weight reduction and safety improvement, hot stamping parts of ultra-high strength steel have been widely used in the automotive industry [1]. In the traditional hot stamping forming process, the ultra-high strength steel is heated up to the austenitization temperature in a heating furnace, then formed and * Corresponding author. Zhang Yisheng, Professor; Tel: +86-027-87544457; FAX: +86-027-87547935. E-mail address:zhangys@mail.hust.edu.cn 1877-7058 2014 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/3.0/). Selection and peer-review under responsibility of the Department of Materials Science and Engineering, Nagoya University doi:10.1016/j.proeng.2014.10.222

1732 Weikang Liang et al. / Procedia Engineering 81 ( 2014 ) 1731 1736 quenched after being transferred into a die during the dwell stage [2]. Hot stamping parts with high strength and low ductility are not suitable for the safety of automobile [3]. However, hot stamping parts owning tailored properties (different regions of the parts own different mechanical properties) fulfill the safety requirements of automobile parts. In the existed literature, tailored welded blanks, tailored rolling blanks, die with different thermal conductivity or different temperature, blank of different initial temperature, different contact area and subsequent heat treatment were proposed to achieve tailored properties. Many scholars have carried out a series of studies on how to realize the tailored mechanical properties of the hot stamping parts. A B-pillar with tailored properties was obtained by the tailored welded blank, without affecting the crush performance requirements of roof and side [4]. Microstructure evolution and mechanical properties of hot stamping parts were adjusted through controlling the cooling rate of the blank using local heating of the tool [5]. The heat transfer of blank was dominated by means of applying the special equipment varied the heat transfer coefficient from 7W/mK to 66 W/mK [6]. The tailored mechanical properties of hot stamping parts were realized by slotting die locally [7]. The tailoring tempering process was achieved through a heated and a cooled zone of a plate tool [8]. A laboratory-scale hot-formed B-pillar was manufactured through controlling the cooling rate of the blank locally during the hot forming process using a segmented die with local heating and cooling zones [9]. The influence of air gap on the hardness and strength distribution was discussed using two different ultra-high strength steels[ 10]. In this work, strategy of local resistance heating was proposed to achieve the tailored mechanical properties by adjusting the temperature distribution of the blank. The quality of sheared edges has improved in punching process of ultra-high strength steel sheets by means of resistance heating [11]. Punching process using the local resistance heating of shearing zone was developed to cut the ultra-high strength steel sheets [12]. Punching process of a small hole in a die-quenched steel sheet having high strength using local resistance heating of a shearing zone was developed to decrease the punching load[13]. The tailored die quenching process of steel parts having a strength distribution using bypass resistance heating in hot stamping was developed [14]. The variations of temperature rising rate, uniform temperature region and energy efficiency were studied [15]. However, effects of the local resistance heating on the performance of the parts were worth further studied. This work also focuses on influence of the local resistance heating on the mechanical properties of a rectangular blank experimentally. Nomenclature Q I R t c w h m Joule s heat current of resistance heating resistance of the blank time of the electrifying electric resistivity of the blank specific heat of the blank density of the blank width of the blank thickness of the blank quality of the blank temperature increment of the blank temperature rising rate of the blank 2. Experimental 2.1. Materials An ultra-high strength boron steel having a thickness of 1.8 mm was used. Chemical compositions and thermalmechanical properties of the steel is shown in Table 1 and Table 2, respectively. The density () of ultra-high strength boron steel is 7830 kg/m 3.

Weikang Liang et al. / Procedia Engineering 81 ( 2014 ) 1731 1736 1733 Table 1. Chemical compositions of ultra-high strength boron steel [wt. %]. Chemical elements C Si Mn P S Cr Ni Mo Ti B Contents 0.23 0.17 0.95 0.01 0.002 0.24 1.50 0.21 0.023 0.0019 Table 2. Thermal-mechanical properties of ultra-high strength boron steel. Temperature [K] 293 373 473 573 673 773 873 973 1073 1173 1273 C T [J/kg K] 444 487 520 544 561 573 581 586 590 596 603 T [10e- 0.18 0.261 0.38 0.489 0.586 0.672 0.741 0.806 0.86 0.92 1.16 2.2. Resistance heating system A resistance heating system was designed in terms of Joule s Law (Fig. 1). The actual temperature of the blank was measured and responded by a non-contact temperature sensor. The distribution of real-time temperature field and steady temperature field in the blank was recorded by an infrared thermography (FLIR A320). The firing angle of the silicon controlled rectifier and the single-phase transformer original side voltage were regulated by the programmable logic controller. Fig.1. Resistance heating system. 2.3. Temperature calculation model of resistance heating Resistance heating is a process that Joule s heat is generated by the current being transferred to the blank. The temperature increment of the blank is calculated from the adiabatic approximation:, (1), (2) where Q is Joule s heat, I is the current of resistance heating, R is the resistance of the blank, t is the time of the electrifying, is the electric resistivity of the blank, c is the specific heat of the blank, is the density of the blank, w is the width of the blank, h is the thickness of the blank, m is the quality of blank and is the temperature increment of the blank. The temperature rising rate of the blank () is calculated from the adiabatic approximation: =. (3)

1734 Weikang Liang et al. / Procedia Engineering 81 ( 2014 ) 1731 1736 2.4. Experiments design The experiments of ultra-high strength boron steel of rectangular blanks (374 100 1.8 mm 3 ) were implemented on the local resistance heating system and a 2000 kn CNC servo press. The modelling of movable local resistance heating device on die was shown in Fig. 2. The movable electrode moved down driving by cylinder, then the blank was compressed by the movable electrode and electrode. The contact pressure between electrodes and the blank was provided by the cylinder. An AC power was supplied by a single-phase transformer. The power and the voltage of the transformer was 20 kw and 10 V, respectively. The environment temperature of the experiment was 20 C. The real-time temperature of the blank was controlled by PID (Proportion, Integration, and Differentiation) regulators of the S7-200 PLC (programmable logic controller) during heating and soaking stage. 3. Results and discussions Fig. 2. Modeling of movable local resistance heating device on die. 3.1. Variations of temperature rising rate The temperature rising rate of the blank by local resistance heating was shown in Fig. 3. Heating the blank from 20 C to 950 C required only 15 s and the average temperature rising rate reached 62 C/s. The control strategy of the PID regulator of the S7-200 PLC realized rapid heating during the heating stage. The temperature was stable during the soaking stage (35s). Fig. 3. Temperature rising rate of blank.

Weikang Liang et al. / Procedia Engineering 81 ( 2014 ) 1731 1736 1735 3.2. Temperature distribution of blank The steady temperature field in the blank was shown in Fig. 4, which could be divided into three regions in longitude direction, i.e. high temperature, transition and unheated region. The temperature of the blank in the middle region, namely high temperature region, was uniform. While the regions in the blank close to the copper electrodes and in contact with the copper electrodes (unlabelled in images in Fig. 4) were called transition region. The temperature of this region was lower than that of high temperature region, owing to the lost energy by conduction through the copper electrodes. The region in the blank out of the copper electrodes, unlabelled in images in Fig. 4, was called unheated region. As explained in Fig.5, mean temperature of the rectangular regions (Fig.4) in the blank was utilized to characterize the steady temperature field. It indicated that the temperature in high temperature region varied from 920 C to 970 C and the length of this region was about 200 mm. While the temperature of transition region changed from 100 C to 920 C and the length of this region was about 144 mm. The temperature of unheated region ranged from 40 C to 100 C and the length of this region was about 30 mm. The results showed that the tailored temperature distribution of the blank was realized through local resistance heating. Transition region High temperature region Rectangular Fig. 4. Steady temperature field of blank. Fig. 5. Mean temperature distribution of blank for images in Fig. 4. 3.3. Hardness tests results The hardness was tested under 430 SVD Vickers of Wolpert Wilson Instruments after the oxide of the hot stamping specimens being cleaned. Fig. 6. Distribution of Vickers hardness.

1736 Weikang Liang et al. / Procedia Engineering 81 ( 2014 ) 1731 1736 The hardness data of the blanks represented an average measurement of three through-width measurements. The hardness distribution of the blanks in the high temperature region, transition region and unheated region was illustrated in Fig. 6. The high temperature region had a hardness varied from 470 HV10 to 500 HV10, which indicated that a full martensite microstructure was obtained in this region. While the hardness of the transition region changed from 160 HV10 to 470 HV10, which showed that a mixed microstructure was obtained. The hardness of the unheated region was 160 ± 5 HV10. These results demonstrated that the hot stamping blank with tailored properties was realized by means of the local resistance heating. 4. Conclusions (1) The average temperature rising rate of the resistance heating reached 62 C/s. (2) The tailored temperature distribution of the blank was realized, and the temperature field of the blank could be divided into high temperature, transition and unheated regions. (3) Hardness of the high temperature region with a length of 200 mm varied from 470 HV10 to 500 HV10. While for transition region with a length of 144 mm, it changed from 160 HV10 to 470 HV10, and that of the unheated region with a length of 30 mm was 160±5 HV10. (4) Tailored mechanical properties of the hot stamping blank were achieved through the local resistance heating. Acknowledgements This research work is financially supported by the National Natural Science Foundation of China (Grant No. 51275185) and National Basic Research Program of China ( 973 Program) (Grant No. 2010CB630802-3). References [1] Wang Chao, Zhang YiSheng, Tian XiaoWei, Zhu Bin, Li Jian, 2012. Thermal contact conductance estimation and experimental validation in hot stamping process. SCIENCECHINA-TECHNOLOGICAL, JUL, 55(7), 1852-1857. [2] Karbasian, H., A.E. Tekkaya, 2010. A review on hot stamping. Journal of Materials Processing Technology, 210(15), 2103-2118. [3] ZhuBin, Zhang YiSheng, Li Jian; Wang Chao, H,Ye, Z-C, 2011. Simulation research of hot stamping and phase transition of automotive high strength steel. Materials Research Innovations, 15, 426-430. [4] Pan F., Zhu P., Zhang Y., 2010. Metamodel-based lightweight design of B-pillar with TWB structurevia support vector regression. Computers & Structures, 88(1-2), 36-44. [5] Merklein M., Svec T., 2013. Hot stamping: manufacturing functional optimized components. Production Engineering, 7(2-3), 141-151. [6] Casas B, Latre D, Rodriguez N, et al20081st International Conference on Hot Sheet Metal Forming of High-Performance Steel, Kassel, Germany,. [7] K. Mori, Okuda Y, 2010. Tailor die quenching in hot stamping for producing ultra-high strength steel formed parts having strength distribution. CIRP Annals-Manufacturing Technology, 59, 291-294. [8] Svec. T., Grüner. M., Merklein. M., 2011. FE-simulation of the heat transfer by defined cooling conditions during the hot stamping process. Key Engineering Materials, 473, 699-706. [9] George. R., A. Bardelcik, M.J. Worswick, 2012. Hot forming of boron steels using heated and cooled tooling for tailored properties. Journal of Materials Processing Technology, 212, 2386-2399. [10] Wang Zijian, Xu Ya, He Wenting, Zhang Yisheng, 2013. Hot Stamping of Two Different High Strength Steel with Tailored Properties. Advanced Materials Research,395-396, 909-913. [11] K. Mori, S. Saito, S. Maki, 2008. Warm and hot punching of ultra high strength steel sheet. CIRP Annals Manufacturing Technology, 57 (1), 321 324. [12] K. Mori, T. Maeno, S. Fuzisaka, 2012. Punching of ultra-high strength steel sheets using local resistance heating of shearing zone. Journal of Materials Processing Technology, 212, 534-540. [13] K. Mori, T. Maeno, Y. Maruo, 2012. Punching of small hole of die-quenched steel sheets using local resistance heating. CIRP Annals- Manufacturing Technology, 61, 255-258. [14] K. Mori, T. Maeno, K. Mongkolkaji, 2013. Tailored die quenching of steel parts having strength distribution using bypass resistance heating in hot stamping. Journal of Materials Processing Technology, 213,508-514. [15] Liang Weikang, Zhou Minglin, Liu Huiqiang, Zhang Yisheng, 2014. Experimental study on conduction heating of ultra-high strength boron steel. Advanced Materials Research, 898, 185-188.