For More Cost- Effective Production: Manufacturing Processes Based on Cavity Pressure

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For More Cost- Effective Production: Manufacturing Processes Based on Cavity Pressure Composites Process transparency and quality assurance in the production of fiber-reinforced composite structural elements.

Thor Jorgen Udvang/Shutterstock.com Lightweight Construction: Efficiency Combined with Quality Ever-growing industry requirements emphasizing energy and r esource conservation have led to an increasing demand for lightweight designs that meet mobility needs in all sectors. Fiber-reinforced composites offer the ideal solution thanks to their high specific strength and rigidity. Composite materials feature significantly lightweight components with highly robust construction. On account of these assets, composites are used in systems and machines that set demanding technical requirements for efficiency and durability. Benefits at a Glance: Extremely lightweight components Shorter cycle times Low tolerances Class A surfaces are possible on both sides Defined wall thicknesses Process reliability and quality assurance thanks to cavity pressure monitoring The aerospace industry has been using composite parts for a long time. Now, the automotive sector is also using more of these materials to keep up with the trend towards enhanced efficiency and optimized use of resources. The changeover to 2

renewables calls for more widespread use of CO 2 -independent energy sources, such as wind turbines all of these developments are steadily boosting demand for composite structural elements. Automated manufacturing processes for composite parts are continuously developed and optimized to meet these demands. Resin transfer molding (RTM) and wet molding are just two examples of processes that harbor vast potential for highly automated production. With the mold cavity pressure sensor, you can virtually take a look inside the mold so you can: Find the ideal settings for a reproducible process Drastically reduce set-up times Detect defects in the preform or cavity Detect defects in the finished part online Control components such as the resin pump or press With a range of sensors and systems specifically tailored to these requirements, Kistler delivers individual solutions to optimize and automate manufacturing processes, including the related quality assurance activities. 3

Image Source: Dow Automotive Systems The Composite Process: State-of-the-Art Series Production Mass-produced composite parts must be increasingly lightweight yet robust. Production has to be based on stable processes that are always reproducible in order to ensure that dimensional and optical requirements for these parts are met. Until recently, fiber-reinforced parts were manufactured using complex manual methods, but these have largely been replaced by highly automated processes. Automated processes guarantee maximum productivity and high volumes with consistent quality. Injection processes (such as the RTM process) or depositing processes with pre-impregnated fiber fabrics (wet molding) are preferred. Based on a closed two-part mold, both processes deliver consistent part dimensions in addition to high-quality optical surfaces. 4

The RTM process 1 Manufacturing the preform Fiber mats or fabrics are stacked in a defined sequence and fiber orientation. The package is molded into the required shape using a dedicated mold. The binding powder added during stacking melts due to the heat impact and fixes the mats or fabrics in the correct shape. The resulting preform has the shape and contour of the injection form, with dimensional stability for easy handling. Evacuation 2 Injection The preform is placed into the mold. The cavity is evacuated after the mold is closed. This prevents air inclusions in the final product. The resin/hardener mixture is injected into the cavity at a defined pressure, while the preform is impregnated with resin. Curing of the resin starts once the cavity is filled. The part is demolded when it has been cured sufficiently. Wet molding Hardener Resin Hardener Resin Hardener Resin Hardener Resin Hardener Resin Dry fiber mats or fabrics are impregnated with the resin/hardener mixture. The impregnated fiber mats are placed into the mold. The time factor is relevant here because the reaction has already started. This is why robots are often used to perform this step. The resin continues to disperse as the mold closes, and the entire cavity is filled after complete closure. After curing, the mold opens and the part can be demolded. 5

Using Cavity Pressure Measurement for Optimal Results Much like other filling processes (e.g. injection molding), the pressure curve is a key factor in process optimization and production monitoring. Characteristic process phases such as evacuation, filling and curing can easily be identified from the pressure curve so process parameters can be easily identified to make production more cost-effective. The pressure signal can also be used as a control variable for individual process steps, allowing for online process control. Anomalies in the pressure curve show whether defects can be expected in the final part and if so, which ones. The pressure signal is also captured and recorded to allow traceability of individual process steps. For these reasons, the pressure curve is an essential tool for quality assurance. Using the Pressure Curve to Identify Defects: Vacuum is too weak or intermittent: Causes: Faulty mold sealing Vacuum pump failure Consequence: Air bubbles and imperfections in the part Irregularities in the injection phase: Causes: Dislocation of the preform Preform defect/incorrect orientation of a layer Consequence: Incorrect fiber content Dry spots 6

3 Pressure 4 Pressure 0 1 2 Time 0 Time 1 2 3 4 Reference Pressure Curve: RTM 1. Cavity evacuation begins after the mold is closed. The level and consistency of the vacuum are critical to prevent air inclusions in the part. 2. As soon as the resin reaches the sensor position, there is a linear increase in cavity pressure. This reflects the continuous increase in flow resistance that the resin must overcome while the preform is impregnated. 3. When the cavity is completely filled, any possible overflows and risers can be closed and the resin pump can be switched off. The pressure now settles at the maximum level, equivalent to the pressure set on the resin pump. 4. The resin volume shrinks during the reaction, causing a continuous pressure drop until it reaches atmospheric pressure levels. Causes and Consequences of Deviations 1. A vacuum that is too weak or intermittent suggests that the mold sealing function is inadequate. This leaves a high residual air volume in the mold, which can cause air inclusions in the finished part. The pressure curve shows whether evacuation of the mold is insufficient. Injection can be stopped at the outset before a low-quality part is produced. 2. The gradient of the pressure signal during the injection phase depends on the permeability of the preform. Therefore, deviations from the normal pressure gradient may indicate differences in the preform composition or in the orientation of individual layers, or foreign objects in the mold. 3. Major pressure variations during the injection phase indicate dislocation of the preform, or of individual layers. An increase in pressure therefore serves as a reference for the preform's quality. 4. A falling pressure curve during the reaction phase indicates that the volume is starting to decrease, and curing of the resin system is beginning. Much like the injection phase, the gelation speed can be deduced from the timing and gradient of the decrease. This makes it possible to determine the time still needed for sufficient curing of the part, allowing the optimal time for demolding to be calculated. Monitoring Composite Processes with Kistler Use our animation to experience convincing, first-class Kistler solutions the sure way to achieve 100 % quality in your production: /Composites 7

Sensors, Connection Technology and Analysis Systems Sensors Precise, reproducible pressure measurements can only be obtained with reliable sensors that measure accurately. Kistler offers the right solution for all molded part geometries and all installation conditions. Kistler sensors have virtually unlimited service lifetimes; they deliver highly linear measuring results and operate independently of temperature. They offer high-resolution measurement of the smallest pressure variations at up to 200 bar, and/or temperature changes of up to 275 C. Kistler also offers a wide variety of temperature sensors for specific customer solutions. ComoNeo ComoNeo is Kistler's process monitoring system for cavity pressure-based optimization, control, monitoring and documentation of injection molding, with separation of good and bad parts. The system is suitable for every application and it cuts quality costs because faulty parts are detected automatically. ComoNeo is compact, meets industry standards and is easily configurable. It features a process-oriented operating philosophy and integrates flexibly into various production environments. The system has up to 32 inputs for piezoelectric cavity pressure sensors, up to 16 inputs for temperature measurements and four analog voltage inputs for machine signals (screw drive, machine pressure, etc). 6157B Measuring & connecting 9247A 9211B 9211 Monitoring & regulation 2869B + Monitor 8 6157B9247A 2869B + Monitor 2869B 2869B

1B Charge Amplifiers Kistler's product range also includes charge amplifiers specially adapted to the composite process. Charge amplifiers convert the sensor signal into an analog 0-10 V signal. This signal can then be visualized and processed with a suitable data acquisition system. Charge amplifiers for use with composites offer special amplification ranges that optimally support relatively low pressures. Regulation The pressure signal is fed back to the individual production system components, so active process control is also possible. For example, the resin pump's feeding pressure can be controlled. Without pump control, there is a risk that the mold halves could be pressed open by the feeding pressure after the cavity is completely filled. This feature prevents incorrect part dimensions and damage to the mold. Software The basic ComoNeo package can be expanded with the K istler ComoDataCenter. All ComoNeo devices can be linked in the ComoDataCenter. Live and historical data views are available. 2205 2205 1708 2205 1708 1708 Documentation & analysis Laptop 1200A49 1200A49 1457A1 1457A1 1995A Regulation & control Laptop 1995A Laptop 1200A49 1457A1 1995A 9

Front diameter 9 mm 9 mm Measurands (p: pressure; T: temperature) p p+t Technical Data Type 6161A 4001A Installation sketch M12x1 16 + 0 Sensors 6 24 6 24 M12 ø9 M12 ø9 6 adjust 0,4 60 11 H7 +0,018 0 0,015 9H7 20 12 h Measuring range Temperature mv/k 10 Pressure bar 1 200 1 2, 5, 10 or 50 Sensitivity 18,5 pc/bar 0,2 V/bar Operating temperature Mold temperature C 40... 200 20... 275 Applications + Characteristics Accessories Automotive (fast curing resins) HP RTM SMC Wetmolding Minimum overall height mm 35 90 Aerospace (slow curing resins) LP RTM Resin infusion Data sheet: see 6161A (003-053) 4001A (003-248) Unlimited measuring time Temperature compensated Pressure signal for processes with changing temperatur conditions 10

Sales Center Tech Center Production Center Worldwide Presence for Our Customers As well as to sensors and systems for quality assurance in high-quality injection molding applications, Kistler offers a wide range of services. These include expert advice on our solutions, professional support and calibration services, as well as speedy deliveries of spare parts worldwide. To enhance its technical support, Kistler establishes Tech Centers worldwide to deliver the specialized service that processors and their customers expect in order to achieve zero-defect production. 11

960-184e-02.17 2017, Kistler Group Kistler Group Eulachstrasse 22 8408 Winterthur Switzerland Tel. +41 52 224 11 11 The Kistler Group includes Kistler Holding AG and all its subsidiaries in Europe, Asia, the Americas and Australia. Find your local contact at