SUMMARY OF RESEARCH DATA USING META-LAX TECHNOLOGY

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RESEARCH SUMMARY SUMMARY OF RESEARCH DATA USING META-LAX TECHNOLOGY 1. U.S. DEPARTMENT OF ENERGY, 1989 "There is evidence that the Meta-Lax system is performing comparable to the thermal stress relief process on A36 carbon steel." "The 4140 plates not sub-resonant [sub-harmonic] vibrated during welding were cracking at the weld crater at the end of each pass made. This did not occur when sub-resonant [sub-harmonic] vibrating. This could be very significant when welding high strength materials where there are weld starts and stops in the middle of a weld assembly." Test plates, A36 (or 4140), being Meta-Lax Weld Conditioned (i.e. Meta-Lax DURING welding). Test plates were restrained for up to 30 days. Table 1. Weld Joint Strength 30 Days After Welding, A36 Material. PSI MPa Untreated: 45,000 310 Heat-Treat Stress Relieved 63,000 434 Preheated 69,000 476 Meta-Lax Stress Relief 89,200 615 86,500 596 Meta-Lax Stress Relieved weldments were 98% stronger than untreated and 41% stronger than heat treat stress relieved weldments. Meta-Lax Weld Conditioned weldments were 92% stronger than untreated and 25% stronger than preheated weldments. 1300 North Campbell Road, Royal Oak, Michigan, U.S.A. 48067 (800) Meta-Lax (248) 582.0900 FAX (248) 582.0901 Copyright Bonal Technologies, Inc. 1998 is a registered trademark of Bonal Technologies, Inc. Form Number 30700

2. LMSC / RICHARD SKINNER, P.E., 1987 & 1993 "The findings demonstrate that the frequency [for vibration stress relief] is always in a subharmonic range." This mathematical study verifies what Bonal refers to as Meta-Lax Principle #1. Peak Amplitude SUB-har -harmonic zone Harmonic zone Frequency Figure 1. Meta-Lax Principle #1: The optimum frequency for stress relieving when using vibrational energy must correspond to the SUB-harmonic portion of the harmonic curve. Mr. Skinner mathematically verified that the sub-harmonic frequency was the optimum frequency for vibrational stress relief on the following materials (as examples): 1018 hot rolled steel 1020 hot rolled steel 5083 aluminum 6061-T6 aluminum 7075-T6 aluminum 6A1-4V titanium 3. UNIVERSITY OF CALIFORNIA - BERKELEY / WONG & JOHNSON, 1987 "The findings regarding the shift in natural frequency as a result of residual stress may provide a method for examining the effectiveness of stress relieving processes." This mathematical study verifies in two ways what Bonal refers to as Meta-Lax Principle #2. First, the natural [harmonic] frequency of a part, which has residual stress, is in an unnatural location. Second, the "shifting" phenomenon that occurs as the stress level is reduced can be used to "examine the effectiveness of the stress relief process." FREQUENCY (HZ) STRESS RELIEF by Bonal Technologies, Inc. 0 10 20 30 40 50 60 70 80 90 100 110 120 130 A M P L I T U D E DATE July, 16 CUSTOMER ADDRESS M-L Fabricators Detroit, MI OPERATOR Dave JOB NO. 41575 PART NO. 5274-2 WEIGHT 7,500 lbs. MATERIAL 1020 HRS PART NAME Column Weldment SIZE 19 x 42 x 170 FORCE INDUCER 2 AT ECC % 60 TIME SETTINGS 1st READOUT COLOR NOTE: Meta-Lax is complete, for that force inducer location, FIRST SCAN SECOND SCAN THIRD SCAN 2nd READOUT COLOR when harmonic peaks have stabilized, i.e. when frequencies M-L S.R. TIME M-L S.R. TIME M-L S.R. TIME repeat. 3rd READOUT COLOR FREQ. MIN. FREQ. MIN. FREQ. MIN. Meta-Lax is the registered trademark of FORM NO. 10480 59 25 54 10 BONAL TECHNOLOGIES, INC., Southfield, Michigan, U.S.A. Figure 2. Meta-Lax Principle #2: The harmonic curve of a thermally stressed workpiece will shift and eventually stabilize in a new frequency location as the workpiece becomes stress relieved. 2 Copyright Bonal Technologies, Inc. 1998

4. GRUMMAN AEROSPACE, 1988 Table 2. Strength Summary from 6061-T6 test plates. Heat Treat Stress Relief Yield Strength 71,000 psi 60,000 psi Ultimate Strength 80,000 psi 72,000 psi Meta-Lax Weld Conditioned plates were 11-18% higher strength than heat treated plates. of 6061-T6 test plates. 6061-T6 test plates after welding. Photomicrograph of Meta-Lax stress relief during & after welding. Normal weld metal following standard thermal stress relief. Table 3. Distortion Summary of 6061-T6 Fixtures After Saw Cut. (-5) Heat Treat Stress Relief (-7) Distortion 0.161 inches 0.524 inches Meta-Lax Weld Conditioned fixtures had 69% less distortion than heat treat stress relieved fixtures. MLWC TSR of aluminum fixtures. Side-by-side comparison after saw cut. Copyright Bonal Technologies, Inc. 1998 3

GRUMMAN AEROSPACE - Continued Table 4. Distortion Summary for 6061-T6 Wing Supports After Machining. Distortion Meta-Lax Stress Relief Heat Treat Stress Relief Normal 0.002 inches 0.003 inches 0.029 inches Meta-Lax Stress Relieved supports had 50% less distortion than heat treat stress relief. Meta-Lax Stress Relieved supports had 97% less distortion than untreated. Two 6061-T6 wing supports at inspection station. Table 5. Distortion Summary After Welding 10-foot diameter A36 disks. Normal Distortion 0.375 inches 5.5 inches Meta-Lax Weld Conditioned disk had 93% less distortion. of 10 foot diameter A36 disk. 10 foot diameter disk after welding. 4 Copyright Bonal Technologies, Inc. 1998

5. WATERVLIET ARSENAL/ALFRED UNIVERSITY, 1994 "We interpret these data to show that [Meta-Lax] treatment has completely eliminated the rejects due to distortion apparently caused by residual stresses. Evaluation of available data shows that, without [Meta-Lax], 12 of 18 barrels were rejected due to distortion." The barrels, 120mm mortars, were of 4135 forged steel. Meta-Lax reduced scrap rate from 67% to 0%. Nine mortar barrels being Meta-Lax Stress Relieved simultaneously. 6. CHARLES BRONSON, (Metallurgist Marathon LeTourneau) 1974 "In evaluating all of the tests that we have made so far the evidence indicates that vibrating while welding [using Meta-Lax] and also after welding definitely results in less residual locked-in stresses that could be detrimental to the endurance of the welded structure while in service." Table 6. Distortion Summary of N-20 Test Plates. Normal Welding Distortion 0.031 inch 0.375 inch Meta-Lax Weld Conditioned plates had 92% less distortion. Table 7. Cracking Summary of N-30 Plates Welded to 4820 Shaft. Crack Length Normal Welding 0.1875 inches 11.750 inches Meta-Lax Weld Conditioned plates had 98% less cracking. Copyright Bonal Technologies, Inc. 1998 5

CHARLES BRONSON - Continued Table 8. Charpy Impact Value Summary from N-20 Plates. Charpy Impact Value (-50 o F) Normal Welding 6.4 ft.-lbs. 3.6 ft.-lbs. Meta-Lax Weld Conditioned plates had 77% higher impact value. 7. BONAL CORPORATION, 1984 "Using Meta-Lax stress relief during welding on two different setups resulted in grain refinement of the weld metal from both setups compared to the untreated weld." Setup #1: Meta-Lax Weld Conditioning. Setup #2: Meta-Lax Weld Conditioning. Normal Weld Metal. 8. BONAL TECHNOLOGIES, 1996 Table 9. Distortion Summary on Plates after Heat Treating. 3 Each 1/2 x 3 x 48 inch - A36 Material Distortion AFTER Heat Treating Meta-Lax Treated Plates Before Heat Treating 0.0089 inch average Untreated Plates 0.023 inch average Meta-Lax Stress Relieved plates had 69% less distortion than untreated plates. Six A36 test plates after grinding. 6 Copyright Bonal Technologies, Inc. 1998

BONAL TECHNOLOGIES - Continued Table 10. Distortion Summary on Bars after Flame Hardening. 1.5 x 1.5 x 60 inches - 1045 Material Distortion After Flame Hardening Meta-Lax Treated Bars Before Flame Hardening Untreated Bars 0.0110 inch average 0.0155 inch average Meta-Lax Stress Relieved bars had 29% less distortion after flame hardening than untreated bars. 9. WAYNE STATE UNIVERSITY, 1982 Table 11. Ductility Summary of 1020 Plates. As Welded 5.4% Meta-Lax Weld Conditioned Heat Treat Stress Relieved Ductility Value 22.0% 28.0% Base Metal 32.0% Meta-Lax Weld Conditioned plates were 307% more ductile than untreated plates. Meta-Lax Weld Conditioned plates were 79% as high as the heat treat Stress Relieved plates yet without using any heat. 10. OAK RIDGE NATIONAL LAB, 1993 "On the basis of these residual stress measurements no degradation of mechanical properties from vibratory [Meta-Lax] treatment during welding is expected." Normal Copyright Bonal Technologies, Inc. 1998 7

11. OHIO STATE UNIVERSITY, 1986 "Refinement occurred in the cupronickel alloy when vibrational waves were applied. The greatest refinement was obtained when 40% of the resonant peak frequency was induced to the base material during welding." Top section of cupronickel, welded at 5 i.p.m. without vibration. Top section of cupronickel, welded at 5 i.p.m. with vibration 40% of resonant peak. 12. SHOU UNIVERSITY, CHINA, 1998 "Residual stress in weld samples subject to [sub-harmonic] vibration is significantly reduced relative to samples either subjected to resonant vibration or not subjected to any vibration." PSI 87,000 72,500 58,000 MPa 600 500 400 No Vibration At Resonant Peak At 5Hz LESS than Peak At 10Hz LESS than Peak Stress 43,500 29,000 14,500 300 200 100 0 0.5 1 1.5 2 2.5 3 (cm) 0.2.39.59.79.98 1.18 (inch) Distance Figure 3. Residual stress distribution of weldments. 8 Copyright Bonal Technologies, Inc. 1998